CN108135798A - It is a kind of to improve color make-up composition for turning viscous and preparation method thereof - Google Patents
It is a kind of to improve color make-up composition for turning viscous and preparation method thereof Download PDFInfo
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- CN108135798A CN108135798A CN201680056650.5A CN201680056650A CN108135798A CN 108135798 A CN108135798 A CN 108135798A CN 201680056650 A CN201680056650 A CN 201680056650A CN 108135798 A CN108135798 A CN 108135798A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
The present invention relates to a kind of color make-up compositions for improving and turning viscous and preparation method thereof.Specifically, the present invention provide it is a kind of comprising silicate class film forming agent, silsesquioxane alkanes film forming agent, plate powder and spherical powder without wax color make-up composition.In addition, the present invention provides the preparation method without wax color make-up composition, this method includes：A) the step of silicate class film forming agent, silsesquioxane alkanes film forming agent, plate powder and spherical powder being mixed；And the step of hydrocarbon ils is to form the composition of paste formulation b) is added in into the mixture.The color make-up composition of the present invention, which not only improves, to be turned viscous, improves persistence, but also moisturizing sense and smear do not reduce compared with traditional composition, and preparation method has technologic convenience, has the characteristics that improve production efficiency.
Description
Technical field
This application claims the priority based on the South Korea patent application the 10-2015-0137380th on the 30th of September in 2015
Interests, meanwhile, the full content as part of this specification disclosed in the South Korea patent application document is included in this theory
In bright book.
A kind of can be prepared the present invention relates to oil without using wax and high-content, improvement turns the color make-up composition glued and its a system
Preparation Method.
Background technology
Traditional color make-up composition is in process of production usually very common using wax as neccessary composition such as lipstick
's.Wax is added to the appropriate hardness and shape that color make-up dosage form is used to form in color make-up composition, usually with high-melting-point, and
And it is used with the oil and pigment combination of high-content.However, mentioned component cannot be very on lip or skin surface due to its property
It is dry well, therefore moisture state is kept when in use, and easily turns to adhere on cup or clothes, daily life is caused very
Big inconvenience.In addition, remaining in skin surface without turning viscous part, pass through at any time also due to skin and external rings
Border influences and is wiped free of, therefore dressing is unable to last very long.
Therefore, the user of color make-up product needs the trouble in face of correcting and smearing again cosmetics for several times daily, and
Therefore user largely uses color make-up composition by restraint of liberty.In order to solve these problems, exploitation is needed to improve
The color make-up composition of form.
As the scheme to solve the above problems, it is thought that the main reason for dosage form of traditional color make-up composition occurs and turns and glue is
The oil of wax and high-content, therefore, it is considered that the use for limiting these materials is most effective.However, preparing agent without using waxed
In the case of, there are various technology restrictions, are such as difficult to be formed the paste (paste) of debita spissitudo or are difficult to be formed in hardening
Preparation with appropriate hardness etc..On the other hand, it has attempted to using the film forming agent in mascara preparations maintain lasting effects
And anti-rotation stop is glued, however, different from eyebrow, lip or skin are largely moved and have many wrinkles, therefore when being smeared
Generating hardening and cracking or smear reduces and generates uncomfortable use feeling, exists and is not suitable for commercialized problem.
Therefore, in order to overcome the technology restriction, various researchs have been carried out to color make-up composition.In addition, in color make-up
In the manufacturing process of composition, if containing wax, must have high temperature process condition to melt wax, and need repeatedly fusing wax
Process, there are problems that production efficiency reduction, make it more quick and simple so as to propose to need to improve process.
[existing technical literature]
[patent document]
(patent document 1) is for lip Cosmetics or matte cosmetic compositions (the Korean Patent No. 10- of lip treatment
No. 1060881).
Invention content
Traditional color make-up composition is in process of production usually very common using wax as neccessary composition such as lipstick
's.Wax is added to the appropriate hardness and shape that color make-up dosage form is used to form in color make-up composition, usually with high-melting-point, and
And it is used with the oil and pigment combination of high-content.However, mentioned component cannot be very on lip or skin surface due to its property
It is dry well, therefore moisture state is kept when in use, and easily turns to adhere on cup or clothes, daily life is caused very
Big inconvenience.In addition, remaining in skin surface without turning viscous part, pass through at any time also due to skin and external rings
Border influences and is wiped free of, therefore dressing is unable to last very long.
Therefore, the user of color make-up product needs the trouble in face of correcting and smearing again cosmetics for several times daily, and
Therefore user largely uses color make-up composition by restraint of liberty.In order to solve these problems, exploitation is needed to improve
The color make-up composition of form.
As the scheme to solve the above problems, it is thought that the main reason for dosage form of traditional color make-up composition occurs and turns and glue is
The oil of wax and high-content, therefore, it is considered that the use for limiting these materials is most effective.However, preparing agent without using waxed
In the case of, there are various technology restrictions, are such as difficult to be formed the paste (paste) of debita spissitudo or are difficult to be formed in hardening
Preparation with appropriate hardness etc..On the other hand, it has attempted to using the film forming agent in mascara preparations maintain lasting effects
And anti-rotation stop is glued, however, different from eyebrow, lip or skin are largely moved and have many wrinkles, therefore when being smeared
Generating hardening and cracking or smear reduces and generates uncomfortable use feeling, exists and is not suitable for commercialized problem.
Therefore, in order to overcome the technology restriction, various researchs have been carried out to color make-up composition.In addition, in color make-up
In the manufacturing process of composition, if containing wax, must have high temperature process condition to melt wax, and need repeatedly fusing wax
Process, there are problems that production efficiency reduction, make it more quick and simple so as to propose to need to improve process.
[existing technical literature]
[patent document]
(patent document 1) is for lip Cosmetics or matte cosmetic compositions (the Korean Patent No. 10- of lip treatment
No. 1060881).
In order to realize the purpose, the present invention provides one kind to include esters of silicon acis (silicate) class film forming agent, sesquialter silicon
The color make-up composition of oxygen alkane (silsesquioxane) class film forming agent, plate powder and spherical powder.
At this point, the color make-up composition can further include silication compound of polysaccharide as film forming agent.
At this point, the silication compound of polysaccharide can be trimethyl silicane alkoxy silicyl carbamyl amylopectin
(trimethylsiloxysilylcarbamoyl pullulan)。
At this point, the silicate class film forming agent can be selected from trimethyl silicane alkoxy esters of silicon acis
(trimethylsiloxysilicate), phenylpropyl dimethyl-silicon alkoxy esters of silicon acis
(phenylpropyldimethylsiloxysilicate), trimethyl silicane alkoxy esters of silicon acis/dimethyl silicone polymer crosslinking
Polymer (trimethylsiloxysilicate/dimethicone crosspolymer) and dimethyl silicone polymer/ethylene
Base trimethyl silicane alkoxy esters of silicon acis cross-linked polymer (dimethicone/vinyltrimethylsiloxysilicate
Crosspolymer) at least one of group of combination.
At this point, the silsesquioxane alkanes film forming agent can be selected from polyphenylsilsesquioxane
(polyphenylsilsesquioxane), poly- propylsilsesquioxane (polypropylsilsesquioxane) and poly- diformazan
In the group of radical siloxane/silsesquioxane copolymer (dimethicone/silsesquioxane copolymer) combination extremely
Few one kind.
At this point, the silicate class film forming agent can be trimethyl silicane alkoxy esters of silicon acis
(trimethylsiloxysilicate), and silsesquioxane alkanes film forming agent can be poly- propylsilsesquioxane
(polypropylsilsesquioxane)。
At this point, the spherical powder can be selected from silica, polymethyl methacrylate (PMMA), polyurethane
(PU), at least one of group of poly methyl silsesquioxane (PMSQ) and nylon combination.
At this point, the plate powder can be at least one in the group that talcum, boron nitride, mica and sericite combine
Kind.
At this point, the weight ratio of the silicate class film forming agent and silsesquioxane alkanes film forming agent can be 3:1~3:3.
At this point, the total weight based on composition, the silicate class film forming agent and silsesquioxane alkanes film forming agent always contain
Amount can be 10 to 40 weight %.
The weight ratio of the spherical powder and plate powder can be 2：1~2：2.
At this point, the total content of the total weight based on composition, the spherical powder and plate powder can be 30 to 95 weights
Measure %.
At this point, the total weight based on composition, the content of oil contained in the color make-up composition can be no more than 40 weights
Measure %.
In addition, the present invention provides a kind of preparation method of color make-up composition, this method includes：
A) silicate class film forming agent, silsesquioxane alkanes film forming agent, plate powder and spherical powder are mixed
(mixing) the step of；With
B) hydrocarbon ils (hydrocarbon) is added in into the mixture to form the composition of paste (paste) dosage form
Step.
At this point, the step a) can include：
A-1 the step of) spherical powder and plate powder are mixed；With
A-2) by the mixed of silicate class film forming agent and silsesquioxane alkanes film forming agent and the spherical powder and plate powder
Close the step of object is mixed.
At this point, in step b), moisturizer and functional polymer can be further added.
At this point, the color make-up composition can be prepared at 15~30 DEG C.
The effect of invention：
By using the Technical Solving, color make-up composition for improved of the invention turns viscous and improves persistence,
And compared with traditional composition, moisturizing sense and smear do not reduce.
In addition, according to the Technical Solving, fusing is omitted due to preparing the process of color make-up composition of the present invention
The process of wax, so technique can carry out at room temperature, and the process time also shortens to 10~20 minutes, so as to improve system
Convenience and production efficiency when standby simultaneously reduce cost.
Description of the drawings
Fig. 1 is after the composition of (a) embodiment 1 and (b) comparative example 2 is applied to dermatine respectively, for confirming paper
The image for turning viscous degree on towel；
Fig. 2 is when the composition of (a) embodiment 1 and (b) comparative example 2 being applied directly to lip respectively, for confirming paper
The image for turning viscous degree on cup；
Fig. 3 is persistent image for confirming the composition of (a) embodiment 1 and (b) comparative example 1.
Specific embodiment
The present invention provides one kind to include silicate class film forming agent, silsesquioxane alkanes film forming agent, plate powder and spherical shape
The color make-up composition of powder.
In addition, the present invention provides a kind of preparation method of color make-up composition, this method includes：
A) step for mixing silicate class film forming agent, silsesquioxane alkanes film forming agent, plate powder and spherical powder
Suddenly；With
B) the step of hydrocarbon ils is to form the composition of paste formulation is added in into the mixture.
The color make-up composition of the present invention, can be preferably as colour containing a small amount of oily " no wax (Wax-free) " preparation
Color make-up composition is used more preferably as lip (lip) portion color make-up composition." the no wax (Wax-free) " used in this specification
Refer to the preparation of the not content of wax.Exemplary dosage form such as lip adornment dosage form etc. must contain wax and a large amount of oil in traditional color make-up, with this phase
Instead, color make-up composition of the invention can be by being used in mixed way film forming agent and powder, and is only made without wax and with a small amount of oil
It is standby.Therefore, color make-up composition of the invention efficiently reduces after smearing turns viscous and improves persistent effect.
In addition, the color make-up composition of the present invention by using film forming agent persistent with improving in the composition
Effect." persistence " refers to the environmental stimulus such as the sebum secreted in itself due to skin or sweat or temperature or humidity, system
Agent stability time to time change in itself and the phenomenon that smearing state is deteriorated, this is different from the concept of " turning viscous ", turn it is viscous and
The stability of preparation in itself is unrelated, refers to when being applied in external physical contact, such as when skin is contacted with another object, change
Cosmetic compositions are turned to adhere to the phenomenon that object or smearing state variation.
In the present specification, color make-up composition of the invention is mainly around lipstick, lip gloss, lip-stick, lip gloss, liner etc.
Lip Cosmetics product illustrates, however, the present invention is not limited thereto, can be using freedom and flexibility as the group for being applicable in the present composition
Into any type of State of cosmetics use with effect.
Present disclosure is described in detail below.In the description below, in order to help to understand that the present invention provides most
Representative example, but the interest field of the present invention is without being limited thereto, it is thus understood that and the present invention includes and the description below equalization
All authority range.
<Color make-up composition>
Film forming agent
The color make-up composition of the present invention includes silicate class film forming agent and silsesquioxane alkanes film forming agent as composition
One component, with provide for anti-rotation stop glue without wax color make-up composition.The film forming agent when with following powder combinations in use,
It can most effectively improve and turn viscous and raising persistence.
The silicate class film forming agent can be selected from trimethyl silicane alkoxy esters of silicon acis, phenylpropyl dimethyl-silicon alkoxy
Esters of silicon acis, trimethyl silicane alkoxy esters of silicon acis/Dimethicone Crosspolymer and dimethyl silicone polymer/vinyl three
At least one of group of methyl-monosilane oxygroup esters of silicon acis cross-linked polymer combination.
The silsesquioxane alkanes film forming agent can be selected from polyphenylsilsesquioxane, poly- propylsilsesquioxane and gather
At least one of group of dimethyl siloxane/silsesquioxane copolymer combination.
The silicate class and silsesquioxane alkanes film forming agent can more broadly be attributed to silicon class film forming agent, include silicon class MQ trees
Fat and there can be various M/Q ratios.The product of the silicon resinoid includes the MQ1600 (front threes of Dow Corning companies
Base silane oxygroup esters of silicon acis), TMS-803 (trimethyl silicane alkoxy esters of silicon acis), the KF-7312K of Wacker-Belsil companies
(the phenylpropyl dimethylsilanes of Silshine 151 of (trimethyl silicane alkoxy esters of silicon acis and dimethyl silicone polymer), GE companies
Oxygroup esters of silicon acis) and MQ1640 etc..
As the preferred embodiment of the present invention, trimethyl silicane alkoxy esters of silicon acis can be used as the silicic acid
Esters film forming agent can use poly- propylsilsesquioxane as the silsesquioxane alkanes film forming agent.
Two kinds of film forming agents of the present invention are characterized in that together comprising use.If this is because using only any one
The film forming agent of type then can cause the use of color make-up composition to feel under the weather.For example, using only trimethyl silicane alkoxy
In the case of the silicate class film forming agent such as esters of silicon acis, dosage form surface is hardened as repairing nail body, leads to the problem of flexibility reduction.
Therefore, there is appropriate rigidity and flexibility to be formed by being used together silicate class film forming agent and silsesquioxane alkanes film forming agent
Dosage form.
Meanwhile other than described two film forming agents, color make-up composition can also further include silication compound of polysaccharide
Film forming agent as the present invention.As silication compound of polysaccharide, it is preferable to use by trimethylsiloxy silicyl
Isocyanates reacts the substance to be formed with compound of polysaccharide.The example of compound of polysaccharide can include cellulose, Arabic gum, sea
Alginic acid, carrageenan, xanthans, pulullan polysaccharide etc..
The silication compound of polysaccharide can further comprise by using pulullan polysaccharide (pullulan) as polysaccharide
The trimethyl silicane alkoxy silicyl carbamyl amylopectin for closing object reaction and being formed.The trimethyl silicane alkoxy first silicon
The product of alkyl carbamoyl amylopectin can include TSPL 30-D5 (the trimethyl silicane alkoxy first of Shin Etsu companies
Silylamido formyl amylopectin and cyclopentasiloxane) and TSPL 30-ID (trimethyl silicane alkoxy silicyl amino first
Acyl amylopectin and Permethyl 99A).
Weight based on all compositions, the total content that may include film forming agent in the compositions of the present invention is preferably 10~
40 weight %.If its content is less than 10 weight %, the degree that forms a film unobvious, so as to which the present invention anti-rotation stop to be provided is glued
It is reduced with persistent effect is improved, if its content is more than 40 weight %, dosage form becomes too hard, and use feeling can reduce.
In addition, silsesquioxane alkanes film forming agent and the weight ratio of silicate class film forming agent are preferably 3 in film forming agent：1~3：
3, more preferably 3：2.But its range is it is not necessary to be confined to the range, but can be according to color make-up product type, mesh
And effect to be provided and change.
Powder
In the color make-up composition of the present invention, while use spherical powder and plate powder.
The spherical powder can be organic dust, and can it is preferable to use selected from silica, polymethylacrylic acid
Methyl esters (PMMA), polyurethane (PU), poly methyl silsesquioxane (PMSQ) and nylon combination at least one of group.
The plate powder can be inorganic powder, and can it is preferable to use selected from talcum, boron nitride, mica and thin,tough silk cloud
At least one of group of mother's combination, more preferably using mica.
If using only the spherical powder in the material, powder may occur when in use and disperse, if be used only
Plate powder, then the main body transposition reduction of composition cause smear to be deteriorated.Therefore, when by spherical powder and plate powder one
Rise in use, ghe layer can smoothly be detached from and mildly be smeared, and can be closely adhere on skin without
It disperses.
The total content of total weight based on composition, spherical powder of the invention and plate powder is preferably 30~80 weights
Measure %.If its content is less than 30 weight %, it is difficult to form paste (paste) phase, if its content is more than 80 weight %,
It is likely to form preparation really up to the mark.
In addition, the weight ratio of spherical powder and plate powder is preferably 2：1~2：2 range, preferred weight ratio are
6：5.But weight ratio is not limited to the range, can according to the type of color make-up product, purposes and effect degree to be provided and
Variation.
As described above, the color make-up composition of the present invention comprising film forming agent and powder is characterized in that, without using wax and with
The prior art, which is compared, generally contains lesser amount of oil.At this point, the content of oil can influence glossiness, it is therefore desirable to be glued with anti-rotation stop
Effects equalizer consider, adjust oil content, the oil that composition is made to contain appropriate amount.Oil content of the prior art must reach
70~80%, in contrast, the oil content in color make-up composition of the invention is not limited to extra high level and can be certainly
By selecting.40 weight % are preferably more than for improving the oil content for turning viscous, this is equivalent to half of the prior art, more preferably
No more than 20 weight %.
In addition, the color make-up composition of the present invention can further include functional material such as moisturizer and polymer.
<Preparation method>
In addition, the present invention provides the preparation method of color make-up composition, this method includes：
A) step for mixing silicate class film forming agent, silsesquioxane alkanes film forming agent, plate powder and spherical powder
Suddenly；With
B) the step of hydrocarbon ils is to form the composition of paste formulation is added in into the mixture.
At this time, it is preferable that the step a) can include：
A-1 the step of) spherical powder and plate powder are mixed；With
A-2) by the mixed of silicate class film forming agent and silsesquioxane alkanes film forming agent and the spherical powder and plate powder
Close the step of object is mixed.
Composition grain is ultimately formed according to above-mentioned preparation method color make-up composition, i.e., on powder film forming agent and hydrocarbon ils according to
Secondary formation coating.This structure glues aspect more effectively in use feeling and anti-rotation stop.For example, color make-up composition is applied to lip
It after portion etc., will not feel tight, and will not turn viscous after the preparation drying smeared.
Meanwhile the film forming agent and the mixture of powder prepared by the step (a) of the present invention forms diluted paste formulations, is
In addition the dilute strength of control preparation simultaneously adds various functions, in the step (b) addition hydrocarbon ils, can further add
Other oil, moisturizer and functional polymer.
The preparation method of color make-up composition of the present invention is characterized in that, is carried out in the range of 15~30 DEG C of room temperature, chief engineer
About 10~20 minutes skill time.
In order to produce the traditional color make-up composition for including wax, it is necessary to which fusing has 90 DEG C or more high-melting-point under the high temperature conditions
Wax, the process for melting wax also needs to 3 to 4 iterative process, and dissolves by heating process and usually require about 1 hour or longer
Process time.In contrast, the present invention can reduce the complicated processes in technique, improve convenience and machinability, and
Cost is reduced, so as to improve whole production efficiency.
Pair evaluation example related with the effect of the present invention and experimental example 1~4 illustrate below.In an experiment, using tool
There is the color make-up composition of the ingredient of example 1 below, comparative example 1 and comparative example 2.But following experimental example is only with the present invention's
The experimental example related with effect is formed, interest field of the invention and effect are without being limited thereto.
<Embodiment 1 and comparative example 1>
Table 1
The color make-up composition of embodiment 1 and comparative example 1 is prepared according to the content of the ingredient shown in upper table 1 and combination.It is real
The color make-up composition that example 1 is the present invention is applied, comparative example 1 is the color make-up for not including film forming agent compared with the color make-up composition of the present invention
Composition.
<Comparative example 2>
Table 2
The color make-up composition of comparative example 2 is prepared according to the content of the ingredient shown in upper table 2 and combination.The coloured silk of comparative example 2
Composition for cosmetics belongs to traditional color make-up composition using wax.
<Preparation example>
1) powder raw material and pigment are mixed and added into mixer, then mixed 1 minute.
2) film forming agent and silicon is added in the mixed raw material of step 1) and mixed 1 minute.
3) mixture of step 2) is transferred in kneader, and adds in hydrocarbon ils, moisturizer and polymer, then with 2 ranks
Section mixing 15 minutes.
<Evaluate example>
In the evaluation example, that evaluates the embodiment 1, comparative example 1 and comparative example 2 turns viscosity, persistence and smear.
The sensory evaluation organized by 30 members is evaluated, and 1~5 point (1 is be evaluated as according to the outstanding degree of projects：Very not
It is~5 points good：It is very good).The total score of each project is shown with average value.
As a result it is shown in the following table 3.
Table 3
| Project | Embodiment 1 | Comparative example 1 | Comparative example 2 |
| Do not turn viscous | 4.3 | 2.0 | 1.0 |
| Persistence | 4.1 | 2.7 | 2.3 |
| Smear | 3.9 | 3.6 | 4.0 |
With reference to upper table 3 as can be seen that embodiment 1 is compared with the traditional composition of comparative example 2, do not turn viscous, persistence obtains
To improvement, and smear is maintained at equivalent horizontal.Additionally it is possible to determine by the composition of embodiment 1 with not including film forming agent
The composition of comparative example 1 when being compared, the composition of embodiment 1 does not turn viscous and a persistence is improved.
In following experimental example, the several experimental examples related with the Analyses Methods for Sensory Evaluation Results have been shown in particular.
<Experimental example 1>Turn viscous experiment 1
Comparing embodiment 1 and comparative example 2 confirm the difference for turning viscous characteristic.
As experimental method, each composition of embodiment 1 and comparative example 2 is applied to dermatine three times by rolling
On, it is then covered with paper handkerchief, is suppressed 1 minute with paperweight, then compare the degree for turning to adhere to paper handkerchief.The result of experimental example 1 such as Fig. 1
It is shown.
With reference to Fig. 1 it has been confirmed that the conventional formulation containing wax comparative example 2 (under) in the case of, the composition that smears
Significantly turn to adhere on paper handkerchief, and embodiment 1 (on) in the case of, in contrast, do not turn viscous.
<Experimental example 2>Turn viscous experiment 2
By the method different from the experimental example 1, the difference of embodiment 1 and the viscous characteristic of 2 turns of comparative example is confirmed.
As experimental method, the composition of embodiment 1 and comparative example 2 is applied to lip, and after 30 minutes respectively
When drinking the water in dixie cup, more each composition turns to adhere to the degree on dixie cup.The results are shown in Figure 2 for experimental example 2.
With reference to Fig. 2 it has been confirmed that in the case of embodiment 1 (left side), do not occur to turn viscous, and in comparative example 2 (right side)
In the case of, the composition for being applied to lip significantly has occurred and turns viscous.
<Experimental example 3>Durability experiment
Persistent degree of composition is influenced in order to study the presence or absence of film forming agent, uses the embodiment 1 and ratio
Composition compared with example 1 carries out endurance life test.
As experimental method, the composition of embodiment 1 and comparative example 1 is applied on dermatine respectively, it then will be complete
Portion's dermatine immerses caprylic/capric triglyceride (caprylic/capric triglyceride) and water with 1:4 ratio systems
(assuming that similar to skin condition) and (shaking) is vibrated in standby solution 20 minutes.The results are shown in Figure 3.
With reference to Fig. 3 it has been confirmed that in the case of embodiment 1 (left side), composition keeps initial smearing state and does not almost have
It is wiped free of, but in the case of comparative example 1 (right side), there are many places to come off the part to bleach.
In addition, in order to confirm color make-up composition according to the present invention, compared with traditional color make-up composition comprising wax whether
With the suitable degree of drying used, following experiments are carried out using the composition of embodiment 1 and comparative example 2.The experiment is for example following
Experimental example 4 shown in.
<Experimental example 4>Drying experiment
Measure the degree of skin surface moisture evaporation
In order to measure the degree of the moisture evaporation of skin surface, it is thus identified that after carrying out skin contact to 10 subjects
The average value of measurement.As a result it is as shown in table 4 below.
Table 4
| Embodiment 1 | Comparative example 2 | |
| After just smearing | 40 | 43 |
| After smearing 2 hours | 30 | 33 |
| After smearing 5 hours | 24 | 27 |
It is according to the present invention with reference to table 4 it has been confirmed that compared with as the comparative example 2 of traditional color make-up composition of the content of wax
Color make-up composition embodiment 1 without special difference, has the aridity of similarity degree in actual use.Thus, it will be seen that with
Conventional formulation is compared, and color make-up composition according to the present invention does not cause special drawing or dry.
To dry sensory evaluation
The sensory evaluation is carried out by the Appraisal Mission of 10 member compositions, and each project is be evaluated as 1~5 according to outstanding degree
Divide (1：Hardly feel~5：It is very serious).As a result, the average value of embodiment 1 is 2.4, the average value of comparative example 2 is
2.1, therefore the two is be evaluated as being not significantly different in actual use, has similar aridity.
The comprehensive evaluation example and Examples 1 to 4 it is all as a result, it has been confirmed that color make-up composition according to the present invention
Be free from the preparation of wax, at the same be also improve turn a viscous, excellent durability, smear and moisturizing sense be not compared with traditional composition
The color make-up composition of reduction.
Claims (17)
1. a kind of color make-up combination comprising silicate class film forming agent, silsesquioxane alkanes film forming agent, plate powder and spherical powder
Object.
2. according to the entitlement requests color make-up composition of the 1st, it is characterized in that, the color make-up composition further includes silication
Compound of polysaccharide is as film forming agent.
3. according to the entitlement requests color make-up composition of the 2nd, it is characterized in that, the silication compound of polysaccharide is trimethyl silicane
Alkoxysilyl carbamyl amylopectin.
4. according to the entitlement requests color make-up composition of the 1st, it is characterized in that, the silicate class film forming agent is selected from front three
Base silane oxygroup esters of silicon acis, phenylpropyl dimethyl-silicon alkoxy esters of silicon acis, trimethyl silicane alkoxy esters of silicon acis/polydimethylsiloxanes
In the group of alkane cross-linked polymer and dimethyl silicone polymer/vinyl trimethylsilane oxygroup esters of silicon acis cross-linked polymer combination
It is at least one.
5. according to the entitlement requests color make-up composition of the 1st, it is characterized in that, the silsesquioxane alkanes film forming agent is to be selected from
In the group of polyphenylsilsesquioxane, poly- propylsilsesquioxane and dimethyl silicone polymer/silsesquioxane copolymer combination
At least one.
6. according to the entitlement requests color make-up composition of the 1st, it is characterized in that, the silicate class film forming agent is trimethyl silicane
Trimethylsiloxysilicate, silsesquioxane alkanes film forming agent are poly- propylsilsesquioxanes.
7. according to the entitlement requests color make-up composition of the 1st, it is characterized in that, the spherical powder be selected from silica,
Polymethyl methacrylate, polyurethane, poly methyl silsesquioxane and nylon combination at least one of group.
8. according to the entitlement requests color make-up composition of the 1st, it is characterized in that, the plate powder is selected from talcum, nitridation
At least one of group of boron, mica and sericite combination.
9. according to the entitlement requests color make-up composition of the 1st, it is characterized in that, the silicate class film forming agent and silsesquioxane
The weight ratio of alkanes film forming agent is 3:1~3:3.
10. according to the entitlement requests color make-up composition of the 1st, it is characterized in that, the total weight based on composition, the silicic acid
The total content of esters film forming agent and silsesquioxane alkanes film forming agent is 10 to 40 weight %.
11. according to the entitlement requests color make-up composition of the 1st, it is characterized in that, the weight of the spherical powder and plate powder
It is 2 to measure ratio:1~2:2.
12. according to the entitlement requests color make-up composition of the 1st, it is characterized in that, the total weight based on composition, the spherical shape
The total content of powder and plate powder is 30 to 95 weight %.
13. according to the entitlement requests color make-up composition of the 1st, it is characterized in that, the total weight based on composition, the color make-up
The oil content contained in composition is no more than 40 weight %.
14. a kind of preparation method of color make-up composition, the method includes：
A) the step of silicate class film forming agent, silsesquioxane alkanes film forming agent, plate powder and spherical powder being mixed；With
B) the step of hydrocarbon ils is to form the composition of paste formulation is added in into the mixture.
15. according to the preparation method of the entitlement requests color make-up composition of the 14th, it is characterized in that, the step a) includes,
A-1 the step of) spherical powder and plate powder are mixed；With
A-2) by silicate class film forming agent and silsesquioxane alkanes film forming agent and the spherical powder and the mixture of plate powder
The step of being mixed.
16. according to the preparation method of the entitlement requests color make-up composition of the 14th, it is characterized in that, in the step b),
Further add moisturizer and functional polymer.
17. according to the preparation method of the color make-up composition of the entitlement requests any one of the 14th to the 16th, feature
For the color make-up composition is prepared at 15~30 DEG C.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR10-2015-0137380 | 2015-09-30 | ||
| KR1020150137380A KR102453363B1 (en) | 2015-09-30 | 2015-09-30 | Cosmetic composition having improved performance of transfer-resistant, and processing method thereof |
| PCT/KR2016/010418 WO2017057862A1 (en) | 2015-09-30 | 2016-09-19 | Makeup composition having reduced transfer, and preparation method therefor |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN108135798A true CN108135798A (en) | 2018-06-08 |
| CN108135798B CN108135798B (en) | 2021-10-26 |
Family
ID=58427345
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201680056650.5A Active CN108135798B (en) | 2015-09-30 | 2016-09-19 | Color cosmetic composition for improving transfer viscosity and preparation method thereof |
Country Status (5)
| Country | Link |
|---|---|
| KR (1) | KR102453363B1 (en) |
| CN (1) | CN108135798B (en) |
| HK (1) | HK1254685A1 (en) |
| SG (1) | SG11201802191XA (en) |
| WO (1) | WO2017057862A1 (en) |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112888715A (en) * | 2018-10-18 | 2021-06-01 | 东亚合成株式会社 | Silsesquioxane derivative composition and use thereof |
| CN113143786A (en) * | 2020-12-26 | 2021-07-23 | 广州集妍化妆品科技有限公司 | Velvet matte texture lip glaze and preparation method thereof |
| CN114469782A (en) * | 2021-12-31 | 2022-05-13 | 浙江百姿化妆品股份有限公司 | Novel eye shadow and preparation process thereof |
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| KR102394641B1 (en) * | 2017-07-24 | 2022-05-09 | (주)아모레퍼시픽 | Make-up cosmetic composition |
| KR102033510B1 (en) * | 2017-12-28 | 2019-11-08 | 한국콜마주식회사 | Eye Make-Up Cosmetic Composition |
| KR102086315B1 (en) * | 2018-06-26 | 2020-03-09 | 코스맥스 주식회사 | Wax-free typed cosmetic composition for eye makeup |
| WO2020118403A1 (en) * | 2018-12-12 | 2020-06-18 | Botica Comercial Farmacêutica Ltda. | Cosmetic composition for lip makeup |
| KR102153538B1 (en) * | 2018-12-14 | 2020-09-08 | 주식회사 엘지생활건강 | Lip Cosmetic Composition for Improving Gross and Color Transfer |
| US20210386654A1 (en) * | 2018-12-27 | 2021-12-16 | L'oreal | Anhydrous composition for caring for and/or making up keratin materials |
| KR20210038006A (en) | 2019-09-30 | 2021-04-07 | (주)아모레퍼시픽 | Lip cosmetic composition |
| KR102472578B1 (en) * | 2020-05-06 | 2022-11-30 | 코스맥스 주식회사 | Lip cosmetic composition comprising copolymerized silicone polymer, hydrocarbon-based oil and silicone powder |
| KR102417956B1 (en) * | 2020-06-05 | 2022-07-07 | 한국콜마주식회사 | Lip cosmetic composition |
| KR102459288B1 (en) * | 2020-07-02 | 2022-10-26 | 주식회사 코스메카코리아 | Gel thickener-free oil-dispersion typed cosmetic composition for eye makeup |
| KR102518286B1 (en) | 2020-10-28 | 2023-04-05 | 코스맥스 주식회사 | Cosmetic composition for manufacturing stick typed lip balm and stick typed lip balm having an enhanced usability and functionality manufactured by the same |
| KR102441385B1 (en) * | 2021-04-09 | 2022-09-07 | (주)아모레퍼시픽 | Method for evaluating lip product ability for preventing from being stained |
| KR102319499B1 (en) * | 2021-05-13 | 2021-11-05 | 한국콜마주식회사 | Oil-dispersed type cosmetic composition of wax-free having improved performance of transfer resistant |
| CN114224747B (en) * | 2021-11-24 | 2023-04-11 | 上海蔻沣生物科技有限公司 | Modified powder, preparation method thereof and cosmetic containing modified powder |
| KR102539387B1 (en) * | 2021-12-06 | 2023-06-07 | (주)나우코스 | Water-in-oil emulsion cosmetic composition for lips with excellent gloss, moisturizing and sliding feeling |
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2016
- 2016-09-19 CN CN201680056650.5A patent/CN108135798B/en active Active
- 2016-09-19 SG SG11201802191XA patent/SG11201802191XA/en unknown
- 2016-09-19 WO PCT/KR2016/010418 patent/WO2017057862A1/en active Application Filing
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2018
- 2018-10-25 HK HK18113666.6A patent/HK1254685A1/en unknown
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| CN113143786A (en) * | 2020-12-26 | 2021-07-23 | 广州集妍化妆品科技有限公司 | Velvet matte texture lip glaze and preparation method thereof |
| CN114469782A (en) * | 2021-12-31 | 2022-05-13 | 浙江百姿化妆品股份有限公司 | Novel eye shadow and preparation process thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| KR102453363B1 (en) | 2022-10-07 |
| WO2017057862A1 (en) | 2017-04-06 |
| HK1254685A1 (en) | 2019-07-26 |
| SG11201802191XA (en) | 2018-04-27 |
| KR20170038265A (en) | 2017-04-07 |
| CN108135798B (en) | 2021-10-26 |
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