CN108124866A - Grape flower wing steinernema sex attractant and its preparation method and application - Google Patents
Grape flower wing steinernema sex attractant and its preparation method and application Download PDFInfo
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- CN108124866A CN108124866A CN201611077313.2A CN201611077313A CN108124866A CN 108124866 A CN108124866 A CN 108124866A CN 201611077313 A CN201611077313 A CN 201611077313A CN 108124866 A CN108124866 A CN 108124866A
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- Prior art keywords
- flower wing
- grape flower
- sex attractant
- wing steinernema
- steinernema
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- 235000009754 Vitis X bourquina Nutrition 0.000 title claims abstract description 83
- 235000012333 Vitis X labruscana Nutrition 0.000 title claims abstract description 83
- 235000014787 Vitis vinifera Nutrition 0.000 title claims abstract description 83
- 241001480238 Steinernema Species 0.000 title claims abstract description 74
- 239000000877 Sex Attractant Substances 0.000 title claims abstract description 55
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 240000006365 Vitis vinifera Species 0.000 title description 63
- -1 carbon diene Chemical class 0.000 claims abstract description 26
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 16
- 241000238631 Hexapoda Species 0.000 claims abstract description 15
- 241000607479 Yersinia pestis Species 0.000 claims abstract description 14
- 235000019439 ethyl acetate Nutrition 0.000 claims abstract description 9
- 238000012544 monitoring process Methods 0.000 claims abstract description 6
- 230000001629 suppression Effects 0.000 claims abstract description 6
- 206010061217 Infestation Diseases 0.000 claims abstract description 4
- 241000219095 Vitis Species 0.000 claims abstract 20
- 239000004698 Polyethylene Substances 0.000 claims description 10
- 229920000573 polyethylene Polymers 0.000 claims description 10
- 239000002904 solvent Substances 0.000 claims description 10
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 9
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 claims description 8
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 claims description 6
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims description 6
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 claims description 4
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 4
- 238000007789 sealing Methods 0.000 claims description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 2
- 235000019483 Peanut oil Nutrition 0.000 claims description 2
- 235000019486 Sunflower oil Nutrition 0.000 claims description 2
- 229950005499 carbon tetrachloride Drugs 0.000 claims description 2
- 239000012188 paraffin wax Substances 0.000 claims description 2
- 239000000312 peanut oil Substances 0.000 claims description 2
- 239000002600 sunflower oil Substances 0.000 claims description 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 claims description 2
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 claims 3
- 150000001993 dienes Chemical class 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 4
- 239000002552 dosage form Substances 0.000 abstract description 3
- 230000002045 lasting effect Effects 0.000 abstract description 3
- 231100000252 nontoxic Toxicity 0.000 abstract description 3
- 230000003000 nontoxic effect Effects 0.000 abstract description 3
- 241001465754 Metazoa Species 0.000 abstract description 2
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 abstract 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- 239000003016 pheromone Substances 0.000 description 5
- 238000012360 testing method Methods 0.000 description 4
- 235000013399 edible fruits Nutrition 0.000 description 3
- 150000002148 esters Chemical class 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 2
- ZHNUHDYFZUAESO-UHFFFAOYSA-N Formamide Chemical compound NC=O ZHNUHDYFZUAESO-UHFFFAOYSA-N 0.000 description 2
- 241000255777 Lepidoptera Species 0.000 description 2
- 241000255901 Tortricidae Species 0.000 description 2
- 244000078534 Vaccinium myrtillus Species 0.000 description 2
- 235000021028 berry Nutrition 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000003337 fertilizer Substances 0.000 description 2
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 description 2
- 229920000053 polysorbate 80 Polymers 0.000 description 2
- 230000002265 prevention Effects 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- UPLPHRJJTCUQAY-WIRWPRASSA-N 2,3-thioepoxy madol Chemical compound C([C@@H]1CC2)[C@@H]3S[C@@H]3C[C@]1(C)[C@@H]1[C@@H]2[C@@H]2CC[C@](C)(O)[C@@]2(C)CC1 UPLPHRJJTCUQAY-WIRWPRASSA-N 0.000 description 1
- 241001465180 Botrytis Species 0.000 description 1
- 241000167854 Bourreria succulenta Species 0.000 description 1
- 235000011511 Diospyros Nutrition 0.000 description 1
- 244000236655 Diospyros kaki Species 0.000 description 1
- 241001261102 Lobesia Species 0.000 description 1
- 241001261104 Lobesia botrana Species 0.000 description 1
- 240000007817 Olea europaea Species 0.000 description 1
- 235000006029 Prunus persica var nucipersica Nutrition 0.000 description 1
- 244000017714 Prunus persica var. nucipersica Species 0.000 description 1
- 244000294611 Punica granatum Species 0.000 description 1
- 235000014360 Punica granatum Nutrition 0.000 description 1
- 235000017848 Rubus fruticosus Nutrition 0.000 description 1
- 235000003095 Vaccinium corymbosum Nutrition 0.000 description 1
- 235000017537 Vaccinium myrtillus Nutrition 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000007605 air drying Methods 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 235000021029 blackberry Nutrition 0.000 description 1
- 235000021014 blueberries Nutrition 0.000 description 1
- 235000019693 cherries Nutrition 0.000 description 1
- 229940125797 compound 12 Drugs 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 235000021038 drupes Nutrition 0.000 description 1
- 150000002168 ethanoic acid esters Chemical class 0.000 description 1
- 230000009545 invasion Effects 0.000 description 1
- 230000001418 larval effect Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000035800 maturation Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/02—Saturated carboxylic acids or thio analogues thereof; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01G—HORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
- A01G13/00—Protecting plants
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Environmental Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Dentistry (AREA)
- Engineering & Computer Science (AREA)
- Plant Pathology (AREA)
- Pest Control & Pesticides (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Agronomy & Crop Science (AREA)
- Toxicology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Catching Or Destruction (AREA)
Abstract
The present invention relates to insect sex pheromone preparing technical field, more particularly to grape flower wing steinernema sex attractant and its preparation method and application.A kind of grape flower wing steinernema sex attractant disclosed by the invention, including 1 alcohol acetic ester (E7, Z9 12 of (E, Z) 7,90 two carbon diene:) and (Z) 9 dodecylene acetic acid esters (Z9 12 Ac:Ac).Grape flower wing steinernema sex attractant provided by the invention prepares simple, and dosage form is various, using simple, has very strong trapping capability, stability is good；Specificity is strong, does not generate resistance, and natural enemy is not injured, nontoxic to people and animals, environmental-friendly；Lasting period is long, and control effect can maintain more than 30d.The grape flower wing steinernema sex attractant can be applied to pest quarantine, Insect infestation monitoring, mass trapping and the Insect pest suppression of grape flower wing steinernema, be of great significance for comprehensive treatment grape flower wing steinernema.
Description
Technical field
The present invention relates to insect sex pheromone preparing technical field, more particularly to grape flower wing steinernema sex attractant and
Preparation method and application.
Background technology
Grape flower wing steinernema Lobesia botrana (Denis et Schiffermuller), belong to Lepidoptera
(Lepidoptera), Tortricidae (Tortricidae), flower wing steinernema category (Lobesia) are a kind of a variety of warps of serious harm
It helps the worldwide pest of plant flowers and fruit, includes that our country is listed as important inward plant quarantine to have in world many countries
Evil insect.Grape flower wing steinernema is mainly with the flower and berry of larval feeding grape, if ripe grape cluster meets with moth worm and attacks
It hits, berry can infect Botrytis disease and further rot.In addition to grape, the volume moth also endanger olive, blackberry, blueberry, cherry, nectarine,
Persimmon and pomegranate etc..The grape flower wing steinernema source place of production is Italy, has reached all Europe, Africa the north and western, Asia
The Middle East and the Far East Area and Some Areas of USA.2009 to 2014 grape flower wing steinernema wreaking havoc in California, USA
The local grape for being worth about 5,700,000,000 dollars and drupe crop is caused to be on the hazard, almost so that the grape outlet in the U.S. therefore and in
It is disconnected.With the increase of international fruit trade, the risk that grape flower wing steinernema invades China further increases, thus strengthen into
While the quarantine dynamics of border grape, strengthen the basic research to it, to cope with grape flower wing steinernema to China's grape industry
Challenge.
Using insect pheromone prevention harmful organism skill is controlled as a kind of harmful organism environmentally friendly, that specificity is strong
Art, fast-developing at home and abroad in recent years, there are many pheromone products of pest at home to be widely applied.Due to letter
The presence of the plain polymorphism of breath, i.e., there may be differences for the pheromones component and ratio of the insect of the same race of different geotypes, may lead
Application effect is not good enough at home for the grape flower wing steinernema pheromone product of cause foreign applications maturation.It is therefore desirable to fruit into
The pheromones component and ratio for the grape flower wing steinernema that mouth state and its surrounding countries occur are studied, and are grape flower wing rouleau
Synthetical prevention after the quarantine and invasion of moth provides technical support.
Invention content
In view of this, it is an object of the present invention to provide a kind of grape flower wing steinernema sex attractant, for grape
Pest quarantine, Insect infestation monitoring, mass trapping and the Insect pest suppression of flower wing steinernema, reach comprehensive treatment grape flower wing steinernema
Purpose.
The present invention also aims to provide the preparation method of above-mentioned grape flower wing steinernema sex attractant.
The present invention also aims to provide the application process of above-mentioned grape flower wing steinernema sex attractant.
A kind of grape flower wing steinernema sex attractant, including (E, Z) -7,9- 12 carbon diene -1- alcohol acetic esters (E7, Z9-
12:) and (Z) -9- dodecylene acetic acid esters (Z9-12 Ac:Ac).
The quality percentage of 12 carbon diene -1- alcohol acetic esters of (E, Z) -7,9- in the grape flower wing steinernema sex attractant
It is 20-95% than content.
A kind of preparation method of grape flower wing steinernema sex attractant, by (E, Z) -7,12 carbon diene -1- alcohol acetic acid of 9-
It after ester and the mixing of (Z) -9- dodecylenes acetic acid esters, is dissolved, is instilled in anti-mouth Rubber end using easy volatile solvent, treat that solvent volatilizees
It is dry to obtain grape flower wing steinernema sex attractant lure.
The easy volatile solvent is dichloromethane, one kind in chloroform, tetrachloromethane, n-hexane, pentane.
A kind of preparation method of grape flower wing steinernema sex attractant, by (E, Z) -7,12 carbon diene -1- alcohol acetic acid of 9-
After ester and the mixing of (Z) -9- dodecylenes acetic acid esters, dissolved, added in polyethylene bottle using difficult solvent flashing, obtained after sealing
Grape flower wing steinernema sex attractant lure.
The hardly possible solvent flashing is atoleine, chlorinated paraffin, peanut oil, sunflower oil, dimethyl sulfoxide (DMSO), N, N- diformazans
One kind in base formamide.
The application process of above-mentioned grape flower wing steinernema sex attractant will secure grape flower wing steinernema sex attractant
Trapper hangs on generation or the region of grape flower wing steinernema may occur, for the quarantine of grape flower wing steinernema pest, worm
Feelings monitoring, mass trapping and Insect pest suppression.
The trapper is lured for insect-sticking plate trapper, ship type trapper, triangle trapper, Doliform trapper and basin shape
Catch one kind in device.
Compared with prior art, the present invention has the advantages that：Grape flower wing steinernema provided by the invention draws
Lure can be applied to pest quarantine, Insect infestation monitoring, mass trapping and the Insect pest suppression of grape flower wing steinernema, for comprehensive treatment
Grape flower wing steinernema is of great significance.The grape flower wing steinernema sex attractant is prepared simply, and dosage form is various, uses letter
Single, condition is feasible, has very strong trapping capability, and stability is good；Specificity is strong, does not generate resistance, and natural enemy is not injured, right
People and animals are nontoxic, environmental-friendly；Resistance is strong, is not afraid of wind, rainforest and solarization；Lasting period is long, control effect can maintain 30d with
On.
Specific embodiment
The specific embodiment of the present invention is described in detail below, it is to be understood that protection scope of the present invention is not
It is restricted by specific implementation.
The preparation of 1 grape flower wing steinernema sex attractant of embodiment (anti-mouth rubber lure)
Different grape flower wing steinernema sex attractant (anti-mouth rubber lure) formulas is as shown in table 1.By (E, Z) -7,9-
12 carbon diene -1- alcohol acetic esters (E7, Z9-12:) and (Z) -9- dodecylene acetic acid esters (Z9-12 Ac:Ac) by different proportion
Mixing (total amount is 1000 μ g), after 500 μ L n-hexane dissolutions, instills in the anti-mouth Rubber end of 500 μ L, Portugal is obtained after air-drying
Grape wing steinernema sex attractant lure.
The different grape flower wing steinernema sex attractant of table 1 (anti-mouth rubber lure) is formulated
The preparation of 2 grape flower wing steinernema sex attractant (polyethylene bottle lure) of embodiment
Different grape flower wing steinernema sex attractant (polyethylene bottle lure) formulas is as shown in table 2.By (E, Z) -7,9-
12 carbon diene -1- alcohol acetic esters (E7, Z9-12:) and (Z) -9- dodecylene acetic acid esters (Z9-12 Ac:Ac) by different proportion
Mixing (total amount is 1000 μ g), after being dissolved with 500 μ L chlorinated paraffins, adds in the polyethylene bottle of 1000 μ L, is obtained after sealing
Grape flower wing steinernema sex attractant lure.
Different grape flower wing steinernema sex attractant (polyethylene bottle lure) formula of table 2
3 grape flower wing steinernema sex attractant of embodiment (anti-mouth rubber lure) field trial
Selection grape variety, growing way, fertilizer and water management are consistent, and area is tested in 10 mu or more of vineyard in flakes
Field is uniformly arranged 8 insect-sticking plate trappers containing grape flower wing steinernema sex attractant (anti-mouth rubber lure) in embodiment 1
(trapper is purchased in Zhangzhou Enjoy Science ＆ Technology Development Co., Ltd.), while sex attractant control (SP) and blank control are set
(CK), wherein sex attractant control (SP) is compound { the 12 carbon diene -1- alcohol of (E, Z) -7,9- containing following mass ratio
Acetic acid esters (E7, Z9-12:Ac), 12 carbon diene -1- alcohol (E7, Z9-12 of (E, Z) -7,9-:) and (Z) -9- dodecylene second OH
Acid esters (Z9-12:Ac it is) 100:5:1) } the insect-sticking plate trapper of the anti-mouth rubber lure of the 1000 μ g of content prepared；Blank pair
It is the insect-sticking plate trapper without lure according to (CK).
Three repetitions of each processing setting, random alignment.The grape flower wing steinernema quantity traped is investigated every three days, together
Shi Genghuan insect-sticking plates are persistently investigated 30 days.Result of the test is as shown in table 3.
3 grape flower wing steinernema sex attractant of table (anti-mouth rubber lure) field test results
The experimental results showed that lure prepared in accordance with the present invention has grape flower wing steinernema certain trapping ability,
The middle lure prepared according to formula 1-7 is best to grape flower wing steinernema trapping capability, is significantly better than sex attractant control (SP).
Embodiment 4 grape flower wing steinernema sex attractant (polyethylene bottle lure) field trial
Selection grape variety, growing way, fertilizer and water management are consistent, and area is tested in 10 mu or more of vineyard in flakes
Field is uniformly arranged 8 Doliform trappers containing grape flower wing steinernema sex attractant (polyethylene bottle lure) in embodiment 2
(trapper is purchased in Beijing Pherobio Technology Co., Ltd.), while sex attractant control (SP) and blank are set
Compare (CK), wherein sex attractant control (SP) be containing following mass ratio compound 12 carbon diene of (E, Z) -7,9- -
1- alcohol acetic esters (E7, Z9-12:Ac), 12 carbon diene -1- alcohol (E7, Z9-12 of (E, Z) -7,9-:) and 12 carbon of (Z) -9- OH
Alkene acetic acid esters (Z9-12:Ac it is) 100:5:1) } the Doliform trapper of the polyethylene bottle lure of the 1000 μ g of content prepared；Blank
It is the Doliform trapper without lure to compare (CK).
Three repetitions of each processing setting, random alignment.The water containing 1% Tween 80 is added in all Doliform trappers
Solution 200mL prevents the grape flower wing steinernema traped from escaping.The grape flower wing steinernema number traped is investigated every three days
Amount is both the Tween 80 aqueous solution replaced in trapper, persistently investigates 30 days.Result of the test is as shown in table 4.
Table 4 grape flower wing steinernema sex attractant (polyethylene bottle lure) field test results
The experimental results showed that lure prepared in accordance with the present invention has grape flower wing steinernema certain trapping ability,
The middle lure prepared according to formula 2-7 is best to grape flower wing steinernema trapping capability, is significantly better than sex attractant control (SP).
It can be seen that sex attractant disclosed by the invention can accurately be used for the pest quarantine of grape flower wing steinernema, worm
Feelings monitoring, mass trapping and Insect pest suppression.The grape flower wing steinernema sex attractant prepares simple, and dosage form is various, using simple,
Condition is feasible, has very strong trapping capability, and stability is good；Specificity is strong, does not generate resistance, natural enemy is not injured, to people
Raise it is nontoxic, it is environmental-friendly；Resistance is strong, is not afraid of wind, rainforest and solarization；Lasting period is long, and control effect can maintain more than 30d.
Disclosed above is only several specific embodiments of the present invention, and still, the present invention is not limited to this, any ability
What the technical staff in domain can think variation should all fall into protection scope of the present invention.
Claims (8)
1. a kind of grape flower wing steinernema sex attractant, it is characterised in that including 12 carbon diene -1- alcohol acetic acid of (E, Z) -7,9-
Ester and (Z) -9- dodecylene acetic acid esters.
2. the grape flower wing steinernema sex attractant according to claim 1, which is characterized in that the grape flower wing
The mass percentage content of 12 carbon diene -1- alcohol acetic esters of (E, Z) -7,9- is 20-95% in steinernema sex attractant.
3. a kind of preparation method of grape flower wing steinernema sex attractant, which is characterized in that by (E, Z) -7,12 carbon diene of 9- -
After 1- alcohol acetic esters and the mixing of (Z) -9- dodecylenes acetic acid esters, dissolved using easy volatile solvent, instill in anti-mouth Rubber end, treat
Solvent volatilization is dry to obtain grape flower wing steinernema sex attractant lure.
4. the preparation method of the grape flower wing steinernema sex attractant according to claim 3, which is characterized in that institute
Easy volatile solvent is stated as one kind in dichloromethane, chloroform, tetrachloromethane, n-hexane, pentane.
5. a kind of preparation method of grape flower wing steinernema sex attractant lure, which is characterized in that by (E, Z) -7,12 carbon of 9-
After diene -1- alcohol acetic esters and the mixing of (Z) -9- dodecylenes acetic acid esters, dissolved using difficult solvent flashing, add in polyethylene bottle
In, obtain grape flower wing steinernema sex attractant lure after sealing.
6. the preparation method of the grape flower wing steinernema sex attractant according to claim 5, which is characterized in that institute
Difficult solvent flashing is stated as in atoleine, chlorinated paraffin, peanut oil, sunflower oil, dimethyl sulfoxide (DMSO), N,N-dimethylformamide
One kind.
7. the application process of the grape flower wing steinernema sex attractant according to claim 3 or claim 5, feature exist
In the trapper for securing grape flower wing steinernema sex attractant is hung on generation or grape flower wing steinernema may occur
Region, for the quarantine of grape flower wing steinernema pest, Insect infestation monitoring, mass trapping and Insect pest suppression.
8. the application process of grape flower wing steinernema sex attractant according to claim 7, which is characterized in that described lures
Device is caught as one kind in insect-sticking plate trapper, ship type trapper, triangle trapper, Doliform trapper and basin shape trapper.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611077313.2A CN108124866B (en) | 2016-11-30 | 2016-11-30 | Sex attractant for cabbage caterpillar and preparation method and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611077313.2A CN108124866B (en) | 2016-11-30 | 2016-11-30 | Sex attractant for cabbage caterpillar and preparation method and application thereof |
Publications (2)
| Publication Number | Publication Date |
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| CN108124866A true CN108124866A (en) | 2018-06-08 |
| CN108124866B CN108124866B (en) | 2020-10-09 |
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| CN201611077313.2A Expired - Fee Related CN108124866B (en) | 2016-11-30 | 2016-11-30 | Sex attractant for cabbage caterpillar and preparation method and application thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109452278A (en) * | 2018-11-26 | 2019-03-12 | 中国农业科学院植物保护研究所 | It is a kind of for preventing and treating the sex pheromone analog of grape flower wing steinernema |
| CN109548785A (en) * | 2018-11-26 | 2019-04-02 | 中国农业科学院植物保护研究所 | Grape flower wing steinernema lure composition and its application and lure |
| CN114732012A (en) * | 2022-04-11 | 2022-07-12 | 河南爱树科技发展有限公司 | Long-acting compound attractant for grape flower-fin diamond back moth and grape penetrating fin moth and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102812873A (en) * | 2011-06-09 | 2012-12-12 | 信越化学工业株式会社 | Mating disruption method using acetate-containing mating disruptant |
| EP2944194B1 (en) * | 2014-05-15 | 2017-01-25 | Peter Witasek | Method for implementing mating disruption |
-
2016
- 2016-11-30 CN CN201611077313.2A patent/CN108124866B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102812873A (en) * | 2011-06-09 | 2012-12-12 | 信越化学工业株式会社 | Mating disruption method using acetate-containing mating disruptant |
| EP2944194B1 (en) * | 2014-05-15 | 2017-01-25 | Peter Witasek | Method for implementing mating disruption |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109452278A (en) * | 2018-11-26 | 2019-03-12 | 中国农业科学院植物保护研究所 | It is a kind of for preventing and treating the sex pheromone analog of grape flower wing steinernema |
| CN109548785A (en) * | 2018-11-26 | 2019-04-02 | 中国农业科学院植物保护研究所 | Grape flower wing steinernema lure composition and its application and lure |
| CN114732012A (en) * | 2022-04-11 | 2022-07-12 | 河南爱树科技发展有限公司 | Long-acting compound attractant for grape flower-fin diamond back moth and grape penetrating fin moth and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN108124866B (en) | 2020-10-09 |
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