CN108112998A - A kind of passion fruit shell extract and preparation method thereof - Google Patents

A kind of passion fruit shell extract and preparation method thereof Download PDF

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Publication number
CN108112998A
CN108112998A CN201810180398.XA CN201810180398A CN108112998A CN 108112998 A CN108112998 A CN 108112998A CN 201810180398 A CN201810180398 A CN 201810180398A CN 108112998 A CN108112998 A CN 108112998A
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CN
China
Prior art keywords
passion fruit
fruit shell
shell extract
extractor
filtered fluid
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Pending
Application number
CN201810180398.XA
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Chinese (zh)
Inventor
李爱萍
郑开斌
徐晓俞
李程勋
陈昱璇
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CROP Research Institute of Fujian Academy of Agricultural Sciences
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CROP Research Institute of Fujian Academy of Agricultural Sciences
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Priority to CN201810180398.XA priority Critical patent/CN108112998A/en
Publication of CN108112998A publication Critical patent/CN108112998A/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/105Plant extracts, their artificial duplicates or their derivatives
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/10Natural spices, flavouring agents or condiments; Extracts thereof
    • A23L27/12Natural spices, flavouring agents or condiments; Extracts thereof from fruit, e.g. essential oils
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L3/00Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
    • A23L3/40Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by drying or kilning; Subsequent reconstitution
    • A23L3/46Spray-drying
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Polymers & Plastics (AREA)
  • Nutrition Science (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Health & Medical Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Botany (AREA)
  • Mycology (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Preparation Of Fruits And Vegetables (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses a kind of passion fruit shell extracts and preparation method thereof, the described method comprises the following steps:Passion fruit shell is cleaned and is placed in extractor, add in solvent and is heated to the temperature in extractor as 40 80 DEG C, when cohobation 38 is small;Then solution and the filtering in extractor are collected, obtains filtered fluid;Filtered fluid is concentrated into the 10 30% of filtered fluid volume, obtains concentrate;Then concentrate is subjected to vacuum spray drying, obtains passion fruit shell extract.The method of the present invention can save passion fruit fragrance from damage to greatest extent, and the passion fruit shell extract of making can directly take orally, and can also brew into beverage and take or be supplied to food processing enterprises to be used as flavouring or trophic function raw material.

Description

A kind of passion fruit shell extract and preparation method thereof
Technical field
The present invention relates to food processing fields, and in particular to a kind of passion fruit shell extract and preparation method thereof.
Background technology
Passion fruit, is the herbaceous species plant of Passifloraceae Passiflora, and fruit flesh many juice has the U.S. of " king of fruit juice " Reputation, can eat raw, may be made as the tasty beverage of fragrance, may further be used to addition in Other Drinks to improve the quality of beverage, make Into jelly etc..Seed extracts oil, can edible and soapmaking, liquefaction paint etc..Passion fruit fruit flesh generally only accounts for the full fruit weight of passion fruit 1/3rd, shell accounts for 2/3rds of weight.At present, shell is except being used to extract pectin, medical components or processing fruit on a small quantity Outside dried meat, partly as feed conversion, the flavor component of shell is not utilized well.It is made using passion fruit shell as raw material Pulvis, electuary have no appearance, and the passion fruit shell extract containing passion fruit flavor component will have very wide in food, field of beverage Wealthy development prospect.
High temperature fragrance is met in process due to passion fruit to destroy, using fruit flesh as the Passion Fruit Juice of raw material in order to protect Hold fragrance, the quick-frozen method of stoste can only be used to obtain, and using passion fruit, shell as raw material other converted products, if than Dried meat etc. all makes passion fruit fragrance lose totally because of the application of high temperature.Meanwhile the application of passion fruit shell at present, except small part It is still largely that burning slatterns for making preserved fruit, extraction pectin and part for processing outside feed, therefore passion fruit shell Application value is great.
The content of the invention
In view of the above-mentioned deficiencies in the prior art, it is an object of the present invention to provide a kind of passion fruit shell extract and its making side Method, this method can save passion fruit fragrance from damage to greatest extent, make the passion fruit shell extract of making can directly take orally, and also can Brewing into beverage takes or is supplied to food processing enterprises to be used as flavouring or trophic function raw material.
To achieve the above object, the present invention adopts the following technical scheme that:
A kind of production method of passion fruit shell extract, comprises the following steps:
1)The passion fruit shell clear water rinsed clean of fruit flesh will be dug up;
2)Passion fruit shell is placed in extractor, adds in solvent, is then heated to the temperature in extractor as 40-80 DEG C, reflux When distillation 3-8 is small;
3)The solution in extractor and filtering are collected, obtains filtered fluid;
4)Above-mentioned filtered fluid is concentrated into the 10-30% of filtered fluid volume, obtains concentrate;
5)Above-mentioned concentrate is subjected to vacuum spray drying, obtains passion fruit shell extract.
Step 2)In, the mass ratio of the passion fruit shell and solvent is 1: 1-10.
Step 2)In, the solvent is pure water or mountain spring water.
Step 2)In, the heating is heated using electrical heating or vapor.
Step 3)In, the filtering is using 200-300 mesh sieve net filtrations.
Step 4)In, the concentration is concentrated using mvr, and thickening temperature is 40-80 DEG C.
Step 5)In, the vacuum spray drying temperature is 40-80 DEG C.
In passion fruit shell extraction process, if too little solvent, solvent can not flood shell, cause the active ingredient of part shell It can not dissolve out, and too little solvent easily leads to solvent and is evaporated;If solvent is too many, distillate concentration is low, increases to the concentration in rear road Workload, and increase energy consumption;Therefore, it is 1: 1-10 that the present invention, which controls the mass ratio of fragrant fruit shell and solvent,.
Extraction process, if temperature is too low, distillation time extends, and energy consumption is big;If temperature is too high, extracting solution fragrance component is broken Bad, quality reduces.Therefore, the Extracting temperature in extractor of the present invention is controlled at 40-80 DEG C.
Extraction process, if extraction time is too short, extraction is insufficient;If extraction time is too long, volatile aroma, loss it is serious and And energy consumption increases.Therefore, when cohobation time 3-8 of the present invention is small.
The extracting solution selection 200-300 mesh screens of the present invention are filtered, if mesh size is too big, small impurity removal effect It is bad;If mesh size is too small, difficulty in filtration can be increased and reduce the rate of filtration, improve energy consumption.
Extracting solution after filtering carries out mvr concentrations, and 40-80 DEG C of thickening temperature, evaporation capacity reaches 70%-90%.It is dense using mvr Contracting can make thickening temperature control within 40-80 DEG C, in order to avoid temperature is too high to cause volatile aroma, reduce quality.Evaporation capacity control The 10-30% that filtered fluid in 70%-90%, i.e., is concentrated into filtered fluid volume is made, convenient for the vacuum spray drying in rear road.
The invention has the advantages that:
1st, increase Business Economic Benefit, reduce shell waste and pollution on the environment.The shell weight of passion fruit accounts for fruit weight 65% or so, per mu yield passion fruit yield just has 1000 kilograms of shell per acre by 1500 kilograms of calculations.Processing preserved fruit, feed etc. are pressed 50% meter of shell usage amount then still has 500 kilograms or so of shell waste per acre.This discarded shell is fragrant for extracting hundred Shell extract, the yield of extract is in terms of 2%-3%, and passion fruit shell extract is in terms of 300 yuan of per kilogram price(With reference to FLOS CHRYSANTHEMI ALBA from Haizhou of China 300 yuan/kilogram of jasmine tea), then it is the economic benefit that enterprise increases more than 3000 yuan per acre.
2nd, passion fruit product market is enriched.Solid beverage is gradually subject to market to welcome in recent years, and passion fruit shell extract can To be fabricated to electuary, it is convenient for carrying, and can be voluntarily allocated according to the taste of oneself.
3rd, as flavouring or trophic function raw material, food processing enterprises are supplied to.Passion fruit shell extract can be supplied to The food enterprises such as cake making, jelly, candy, the fumet of the food as passion fruit taste.In addition, passion fruit extract Active ingredient have clearing away the lungheat and moisturizing, ataralgesia and blood stop dysentery, treatment cough, dry throat, constipation, insomnia, dysmenorrhoea, pass Section pain, dysentery and other effects can utilize passion fruit shell extract to make functional food, and for different demands, crowd eats.
Description of the drawings
Fig. 1 is the ion flow graph of the GC-M detections of passion fruit shell extract prepared by embodiment 1.
Specific embodiment
A kind of production method of passion fruit shell extract, comprises the following steps:
1)The passion fruit shell clear water rinsed clean of fruit flesh will be dug up;
2)Passion fruit shell is placed in extractor, add in solvent, the solvent be pure water or mountain spring water, the passion fruit shell Mass ratio with solvent is 1: 1-10, and then electrical heating or vapor are heated to the temperature in extractor as 40-80 DEG C, and reflux is steamed Evaporate 3-8 it is small when;
3)It collects the solution in extractor and uses 200-300 mesh sieve net filtrations, obtain filtered fluid;
4)Above-mentioned filtered fluid is subjected to mvr concentrations, thickening temperature is 40-80 DEG C, is concentrated into the 10-30% of filtered fluid volume, obtains Concentrate;
5)Above-mentioned concentrate under the conditions of 40-80 DEG C is subjected to vacuum spray drying, obtains passion fruit shell extract.
Embodiment 1
A kind of production method of passion fruit shell extract, comprises the following steps:
1)The passion fruit shell clear water rinsed clean of fruit flesh will be dug up;
2)Passion fruit shell being placed in extractor, addition pure water, the mass ratio of the passion fruit shell and pure water is 1: 5, Then the temperature in electrical heating to extractor is 60 DEG C, when cohobation 5..5 is small;
3)It collects the solution in extractor and uses 250 mesh sieve net filtrations, obtain filtered fluid;
4)Above-mentioned filtered fluid is subjected to mvr concentrations, thickening temperature is 60 DEG C, is concentrated into the 20% of filtered fluid volume, is concentrated Liquid;
5)Above-mentioned concentrate under the conditions of 60 DEG C is subjected to vacuum spray drying, obtains passion fruit shell extract.
Using GC-MS detection techniques, passion fruit shell extract manufactured in the present embodiment is detected, GC-M testing results As shown in Figure 1, the fragrance component remained in extract has more than 20 kinds, wherein mainly having:(Z)-blatter alcohol, just oneself Alcohol, n-octyl alcohol, linalool, pine needle oleyl alcohol, gaultherolin, cineole etc..
Embodiment 2
A kind of production method of passion fruit shell extract, comprises the following steps:
1)The passion fruit shell clear water rinsed clean of fruit flesh will be dug up;
2)Passion fruit shell being placed in extractor, addition mountain spring water, the mass ratio of the passion fruit shell and mountain spring water is 1: 10, Then vapor is heated to the temperature in extractor as 40 DEG C, when cohobation 8 is small;
3)It collects the solution in extractor and uses 200 mesh sieve net filtrations, obtain filtered fluid;
4)Above-mentioned filtered fluid is subjected to mvr concentrations, thickening temperature is 40 DEG C, is concentrated into the 30% of filtered fluid volume, is concentrated Liquid;
5)Above-mentioned concentrate under the conditions of 40 DEG C is subjected to vacuum spray drying, obtains passion fruit shell extract.
Embodiment 3
A kind of production method of passion fruit shell extract, comprises the following steps:
1)The passion fruit shell clear water rinsed clean of fruit flesh will be dug up;
2)Passion fruit shell is placed in extractor, adds pure water, the mass ratio of the passion fruit shell and pure water is 1: 1, so The temperature in electrical heating to extractor is 80 DEG C afterwards, when cohobation 3 is small;
3)It collects the solution in extractor and uses 300 mesh sieve net filtrations, obtain filtered fluid;
4)Above-mentioned filtered fluid is subjected to mvr concentrations, thickening temperature is 80 DEG C, is concentrated into the 10% of filtered fluid volume, is concentrated Liquid;
5)Above-mentioned concentrate under the conditions of 80 DEG C is subjected to vacuum spray drying, obtains passion fruit shell extract.

Claims (8)

1. a kind of production method of passion fruit shell extract, it is characterised in that:It comprises the following steps:
1)Passion fruit shell is eluted with water;
2)Passion fruit shell is placed in extractor, adds in solvent, is then heated to the temperature in extractor as 40-80 DEG C, reflux When distillation 3-8 is small;
3)The solution in extractor and filtering are collected, obtains filtered fluid;
4)Above-mentioned filtered fluid is concentrated into the 10-30% of filtered fluid volume, obtains concentrate;
5)Above-mentioned concentrate is subjected to vacuum spray drying, obtains passion fruit shell extract.
2. a kind of production method of passion fruit shell extract according to claim 1, it is characterised in that:Step 2)In, institute The mass ratio for stating passion fruit shell and solvent is 1: 1-10.
3. a kind of production method of passion fruit shell extract according to claim 1, it is characterised in that:Step 2)In, institute Solvent is stated as pure water or mountain spring water.
4. a kind of production method of passion fruit shell extract according to claim 1, it is characterised in that:Step 2)In, institute Heating is stated to heat using electrical heating or vapor.
5. a kind of production method of passion fruit shell extract according to claim 1, it is characterised in that:Step 3)In, institute It is using 200-300 mesh sieve net filtrations to state filtering.
6. a kind of production method of passion fruit shell extract according to claim 1, it is characterised in that:Step 4)In, institute Stating concentration is concentrated using mvr, and thickening temperature is 40-80 DEG C.
7. a kind of passion fruit shell extract production method according to claim 1, it is characterised in that:Step 5)In, it is described Vacuum spray drying temperature is 40-80 DEG C.
8. the passion fruit shell extract obtained according to any production methods of claim 1-7.
CN201810180398.XA 2018-03-05 2018-03-05 A kind of passion fruit shell extract and preparation method thereof Pending CN108112998A (en)

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Application Number Priority Date Filing Date Title
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111513214A (en) * 2020-04-08 2020-08-11 臻富(福建)果汁食品有限公司 Production process of passion fruit juice beverage
CN113180146A (en) * 2021-04-30 2021-07-30 武汉轻工大学 Preparation method of passion fruit shell extracting solution and livestock and poultry breeding method

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104305055A (en) * 2014-11-06 2015-01-28 广西大学 Full-utilization comprehensive processing process for improving value of passion fruit peels
US20150181917A1 (en) * 2014-01-02 2015-07-02 Alice Chang Plant powder, plant bag, and dried plant; plant including herb, tea, root, flower, flower bud, pollen, stem, stem shoot, leaf, bulb, cereal grain, nut, seed, bean, fruit, fruit skin, vegetable, and vegetable skin
CN107628944A (en) * 2017-11-02 2018-01-26 厦门福美科技有限公司 The method and system of low-ester pectin and calcium citrate is extracted from passion fruit shell

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20150181917A1 (en) * 2014-01-02 2015-07-02 Alice Chang Plant powder, plant bag, and dried plant; plant including herb, tea, root, flower, flower bud, pollen, stem, stem shoot, leaf, bulb, cereal grain, nut, seed, bean, fruit, fruit skin, vegetable, and vegetable skin
CN104305055A (en) * 2014-11-06 2015-01-28 广西大学 Full-utilization comprehensive processing process for improving value of passion fruit peels
CN107628944A (en) * 2017-11-02 2018-01-26 厦门福美科技有限公司 The method and system of low-ester pectin and calcium citrate is extracted from passion fruit shell

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111513214A (en) * 2020-04-08 2020-08-11 臻富(福建)果汁食品有限公司 Production process of passion fruit juice beverage
CN113180146A (en) * 2021-04-30 2021-07-30 武汉轻工大学 Preparation method of passion fruit shell extracting solution and livestock and poultry breeding method

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Application publication date: 20180605

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