CN108101365A - Double-deck reaction glaze of solution cavity and preparation method thereof - Google Patents
Double-deck reaction glaze of solution cavity and preparation method thereof Download PDFInfo
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- CN108101365A CN108101365A CN201711263853.4A CN201711263853A CN108101365A CN 108101365 A CN108101365 A CN 108101365A CN 201711263853 A CN201711263853 A CN 201711263853A CN 108101365 A CN108101365 A CN 108101365A
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Classifications
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/89—Coating or impregnation for obtaining at least two superposed coatings having different compositions
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Structural Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Curing Cements, Concrete, And Artificial Stone (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses double-deck reaction glaze of a kind of solution cavity and preparation method thereof, glaze used in the double-deck reaction glaze of solution cavity includes ground-coat enamel material and glaze material, and the component and each component mass parts of the ground-coat enamel material are as follows:35 parts~38 parts of potassium feldspar;3 parts~6 parts of talcum;26 parts~30 parts of Jiepai clay;17 parts~23 parts of quartz;4 parts~6 parts of zinc oxide;The component and each component mass parts of the glaze material are as follows:30 parts~35 parts of potassium feldspar;3 parts~6 parts of zinc oxide;10 parts~15 parts of albite;8 parts~12 parts of calcite;15 parts~18 parts of quartz;3 parts~4 parts of Guizhou clay;7 parts~10 parts of dolomite;Wherein, solution cavity particle is added in ground-coat enamel material;The component and each component mass parts of solution cavity particle are as follows:35 parts~40 parts of potassium feldspar;6 parts~8 parts of zinc oxide;12 parts~14 parts of wollastonite;14 parts~16 parts of dolomite;8 parts~10 parts of vanadic anhydride;10 parts~16 parts of borax.Solution cavity effect can be presented in the glaze paint of the present invention, very beautiful.
Description
Technical field
The present invention relates to double-deck reaction glaze of a kind of solution cavity and preparation method thereof.
Background technology
At present, there is not solution cavity effect in the glaze paint of the double-deck reaction glaze of the prior art, and aesthetics is inadequate.
The content of the invention
The technical problems to be solved by the invention are the defects of overcoming the prior art, provide a kind of solution cavity double-deck reaction glaze,
Solution cavity effect can be presented in its glaze paint, very beautiful.
In order to solve the above technical problems, the technical scheme is that:The double-deck reaction glaze of a kind of solution cavity, used in it
Glaze includes ground-coat enamel material and glaze material, and the component and each component mass parts of the ground-coat enamel material are as follows:35 parts~38 parts of potassium feldspar;It is sliding
3 parts~6 parts of stone;26 parts~30 parts of Jiepai clay;17 parts~23 parts of quartz;4 parts~6 parts of zinc oxide;The component of the glaze material and
Each component mass parts are as follows:30 parts~35 parts of potassium feldspar;3 parts~6 parts of zinc oxide;10 parts~15 parts of albite;8 parts of calcite~
12 parts;15 parts~18 parts of quartz;3 parts~4 parts of Guizhou clay;7 parts~10 parts of dolomite;Wherein, solution cavity particle is added in ground-coat enamel material;
The component and each component mass parts of solution cavity particle are as follows:35 parts~40 parts of potassium feldspar;6 parts~8 parts of zinc oxide;12 parts of wollastonite~
14 parts;14 parts~16 parts of dolomite;8 parts~10 parts of vanadic anhydride;10 parts~16 parts of borax.
The present invention also provides a kind of preparation method of the double-deck reaction glaze of solution cavity, the step of method, is as follows:
A) ground-coat enamel material is stocked up according to each component and each component mass parts;
B) according to 1.6 ︰ 0.6 of mass ratio=1 ︰ of ground-coat enamel material ︰ ball ︰ water, when wet ball grinding 12~14 is small, the ground-coat enamel after ball milling
After expecting 200 mesh sieves, 53~54 Baume concentration are modulated into, add in the solution cavity particle of 10g/ kg of water glaze, then clean green body is taken to soak
Panchromatic ground-coat enamel material or half color ground-coat enamel;
C) glaze material is stocked up according to each component and each component mass parts:
D) according to 1.6 ︰ 0.6 of mass ratio=1 ︰ of overglaze material ︰ ball ︰ water, when wet ball grinding 12~14 is small, the overglaze after ball milling
After expecting 200 mesh sieves, 52~54 Baume concentration are modulated into, clean green body is taken to soak panchromatic glaze material;
E) green body for having soaked glaze material is put into roller kilns to be fired in 1200 DEG C of oxidizing atmospheres.
After employing above-mentioned technical proposal, the present invention is by the test to vanadic anhydride strong flux, and to borax high fever
The test of mistake in the collocation substances such as solvent and clay, has createed solution cavity particle next, by adding in the solution cavity in ground-coat enamel
Grain so that the reaction that overglaze generates afterwards with ground-coat enamel melting has showed solution cavity effect, which comes with solution cavity defect
It says, can go deliberately to control the generation quantity of solution cavity, scope, it is much the same that the incompleteness U.S.A enable produces effect, quality
Stablize, be capable of the special double-deck reaction glaze of mass production.
Specific embodiment
In order that the present invention can be more clearly and readily understood, below according to specific embodiment, the present invention is made into
One step is described in detail.
Embodiment one
A kind of double-deck reaction glaze of solution cavity, glaze includes ground-coat enamel material and glaze material, the component of the ground-coat enamel material used in it
And each component mass parts are as follows:35 parts of potassium feldspar;3 parts of talcum;26 parts of Jiepai clay;17 parts of quartz;4 parts of zinc oxide;The overglaze
The component and each component mass parts of material are as follows:30 parts of potassium feldspar;3 parts of zinc oxide;10 parts of albite;8 parts of calcite;Quartz 15
Part;3 parts of Guizhou clay;7 parts of dolomite;Wherein, solution cavity particle is added in ground-coat enamel material;The component of solution cavity particle and each component mass parts
It is as follows:35 parts of potassium feldspar;6 parts of zinc oxide;12 parts of wollastonite;14 parts of dolomite;8 parts of vanadic anhydride;10 parts of borax.
A kind of the step of preparation method of the double-deck reaction glaze of solution cavity, method, is as follows:
A) ground-coat enamel material is stocked up according to each component and each component mass parts;
B) according to 1.6 ︰ 0.6 of mass ratio=1 ︰ of ground-coat enamel material ︰ ball ︰ water, when wet ball grinding 12 is small, the ground-coat enamel material mistake after ball milling
After 200 mesh sieves, 53~54 Baume concentration are modulated into, add in the solution cavity particle of 10g/ kg of water glaze, then take clean green body leaching panchromatic
Ground-coat enamel material or half color ground-coat enamel;
C) glaze material is stocked up according to each component and each component mass parts:
D) according to 1.6 ︰ 0.6 of mass ratio=1 ︰ of overglaze material ︰ ball ︰ water, when wet ball grinding 12 is small, the glaze material mistake after ball milling
After 200 mesh sieves, 52~54 Baume concentration are modulated into, clean green body is taken to soak panchromatic glaze material;
E) green body for having soaked glaze material is put into roller kilns to be fired in 1200 DEG C of oxidizing atmospheres.
Embodiment two
A kind of double-deck reaction glaze of solution cavity, glaze includes ground-coat enamel material and glaze material, the component of the ground-coat enamel material used in it
And each component mass parts are as follows:38 parts of potassium feldspar;6 parts of talcum;30 parts of Jiepai clay;23 parts of quartz;6 parts of zinc oxide;The overglaze
The component and each component mass parts of material are as follows:35 parts of potassium feldspar;6 parts of zinc oxide;15 parts of albite;12 parts of calcite;Quartz 18
Part;4 parts of Guizhou clay;10 parts of dolomite;Wherein, solution cavity particle is added in ground-coat enamel material;The component of solution cavity particle and each component quality
Part is as follows:40 parts of potassium feldspar;8 parts of zinc oxide;14 parts of wollastonite;16 parts of dolomite;10 parts of vanadic anhydride;16 parts of borax.
A kind of the step of preparation method of the double-deck reaction glaze of solution cavity, method, is as follows:
A) ground-coat enamel material is stocked up according to each component and each component mass parts;
B) according to 1.6 ︰ 0.6 of mass ratio=1 ︰ of ground-coat enamel material ︰ ball ︰ water, when wet ball grinding 14 is small, the ground-coat enamel material mistake after ball milling
After 200 mesh sieves, 53~54 Baume concentration are modulated into, add in the solution cavity particle of 10g/ kg of water glaze, then take clean green body leaching panchromatic
Ground-coat enamel material or half color ground-coat enamel;
C) glaze material is stocked up according to each component and each component mass parts:
D) according to 1.6 ︰ 0.6 of mass ratio=1 ︰ of overglaze material ︰ ball ︰ water, when wet ball grinding 14 is small, the glaze material mistake after ball milling
After 200 mesh sieves, 52~54 Baume concentration are modulated into, clean green body is taken to soak panchromatic glaze material;
E) green body for having soaked glaze material is put into roller kilns to be fired in 1200 DEG C of oxidizing atmospheres.
Embodiment three
A kind of double-deck reaction glaze of solution cavity, glaze includes ground-coat enamel material and glaze material, the component of the ground-coat enamel material used in it
And each component mass parts are as follows:36 parts of potassium feldspar;4 parts of talcum;28 parts of Jiepai clay;20 parts of quartz;5 parts of zinc oxide;The overglaze
The component and each component mass parts of material are as follows:32 parts of potassium feldspar;5 parts of zinc oxide;13 parts of albite;10 parts of calcite;Quartz 16
Part;3.5 parts of Guizhou clay;8 parts of dolomite;Wherein, solution cavity particle is added in ground-coat enamel material;The component of solution cavity particle and each component quality
Part is as follows:37 parts of potassium feldspar;7 parts of zinc oxide;13 parts of wollastonite;15 parts of dolomite;9 parts of vanadic anhydride;13 parts of borax.
A kind of the step of preparation method of the double-deck reaction glaze of solution cavity, method, is as follows:
A) ground-coat enamel material is stocked up according to each component and each component mass parts;
B) according to 1.6 ︰ 0.6 of mass ratio=1 ︰ of ground-coat enamel material ︰ ball ︰ water, when wet ball grinding 13 is small, the ground-coat enamel material mistake after ball milling
After 200 mesh sieves, 53~54 Baume concentration are modulated into, add in the solution cavity particle of 10g/ kg of water glaze, then take clean green body leaching panchromatic
Ground-coat enamel material or half color ground-coat enamel;
C) glaze material is stocked up according to each component and each component mass parts:
D) according to 1.6 ︰ 0.6 of mass ratio=1 ︰ of overglaze material ︰ ball ︰ water, when wet ball grinding 13 is small, the glaze material mistake after ball milling
After 200 mesh sieves, 52~54 Baume concentration are modulated into, clean green body is taken to soak panchromatic glaze material;
E) green body for having soaked glaze material is put into roller kilns to be fired in 1200 DEG C of oxidizing atmospheres.
The double-deck reaction glaze of solution cavity that three above embodiment is prepared passes through it has been observed that solution cavity can occur in its glaze paint
Effect meets desired effect.
Particular embodiments described above has carried out the purpose of the present invention, technical solution and advantageous effect further in detail
It describes in detail bright, it should be understood that the above is only a specific embodiment of the present invention, is not intended to limit the invention, it is all
Within the spirit and principles in the present invention, any modification, equivalent substitution, improvement and etc. done should be included in the guarantor of the present invention
Within the scope of shield.
Claims (2)
1. a kind of double-deck reaction glaze of solution cavity, it is characterised in that:Glaze includes ground-coat enamel material and glaze material, the ground-coat enamel used in it
The component and each component mass parts of material are as follows:35 parts~38 parts of potassium feldspar;3 parts~6 parts of talcum;26 parts~30 parts of Jiepai clay;Stone
17 parts~23 parts of English;4 parts~6 parts of zinc oxide;The component and each component mass parts of the glaze material are as follows:Potassium feldspar 30 parts~35
Part;3 parts~6 parts of zinc oxide;10 parts~15 parts of albite;8 parts~12 parts of calcite;15 parts~18 parts of quartz;3 parts of Guizhou clay~
4 parts;7 parts~10 parts of dolomite;Wherein, solution cavity particle is added in ground-coat enamel material;The component and each component mass parts of solution cavity particle are such as
Under:35 parts~40 parts of potassium feldspar;6 parts~8 parts of zinc oxide;12 parts~14 parts of wollastonite;14 parts~16 parts of dolomite;Five oxidations two
8 parts~10 parts of vanadium;10 parts~16 parts of borax.
2. the preparation method of the double-deck reaction glaze of a kind of solution cavity as described in claim 1, it is characterised in that the step of method is as follows:
A) ground-coat enamel material is stocked up according to each component and each component mass parts;
B) according to 1.6 ︰ 0.6 of mass ratio=1 ︰ of ground-coat enamel material ︰ ball ︰ water, when wet ball grinding 12~14 is small, the ground-coat enamel material mistake after ball milling
After 200 mesh sieves, 53~54 Baume concentration are modulated into, add in the solution cavity particle of 10g/ kg of water glaze, then take clean green body leaching panchromatic
Ground-coat enamel material or half color ground-coat enamel;
C) glaze material is stocked up according to each component and each component mass parts:
D) according to 1.6 ︰ 0.6 of mass ratio=1 ︰ of overglaze material ︰ ball ︰ water, when wet ball grinding 12~14 is small, the glaze material mistake after ball milling
After 200 mesh sieves, 52~54 Baume concentration are modulated into, clean green body is taken to soak panchromatic glaze material;
E) green body for having soaked glaze material is put into roller kilns to be fired in 1200 DEG C of oxidizing atmospheres.
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CN201711263853.4A CN108101365A (en) | 2017-12-05 | 2017-12-05 | Double-deck reaction glaze of solution cavity and preparation method thereof |
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CN201711263853.4A CN108101365A (en) | 2017-12-05 | 2017-12-05 | Double-deck reaction glaze of solution cavity and preparation method thereof |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108840567A (en) * | 2018-08-29 | 2018-11-20 | 湖南陶润会文化传播有限公司 | Double-deck Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze and preparation method thereof |
CN109160732A (en) * | 2018-08-29 | 2019-01-08 | 湖南陶润会文化传播有限公司 | Double-deck reaction particles glaze and preparation method thereof |
CN113651640A (en) * | 2021-08-20 | 2021-11-16 | 湖南陶润会文化传播有限公司 | Matt double-layer reaction glaze glazing decoration and preparation method |
CN113651533A (en) * | 2021-08-10 | 2021-11-16 | 湖南陶润会文化传播有限公司 | Reaction glaze with double-layer transmutation wire drawing effect and preparation method and application thereof |
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Cited By (4)
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CN108840567A (en) * | 2018-08-29 | 2018-11-20 | 湖南陶润会文化传播有限公司 | Double-deck Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze and preparation method thereof |
CN109160732A (en) * | 2018-08-29 | 2019-01-08 | 湖南陶润会文化传播有限公司 | Double-deck reaction particles glaze and preparation method thereof |
CN113651533A (en) * | 2021-08-10 | 2021-11-16 | 湖南陶润会文化传播有限公司 | Reaction glaze with double-layer transmutation wire drawing effect and preparation method and application thereof |
CN113651640A (en) * | 2021-08-20 | 2021-11-16 | 湖南陶润会文化传播有限公司 | Matt double-layer reaction glaze glazing decoration and preparation method |
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Inventor after: Wen Li Inventor after: Wen Zhiyong Inventor before: Wen Li Inventor before: Wen Zhiyong |
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Application publication date: 20180601 |