CN107382068A - Mobile graphic technique glaze and preparation method thereof - Google Patents
Mobile graphic technique glaze and preparation method thereof Download PDFInfo
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- CN107382068A CN107382068A CN201710604792.7A CN201710604792A CN107382068A CN 107382068 A CN107382068 A CN 107382068A CN 201710604792 A CN201710604792 A CN 201710604792A CN 107382068 A CN107382068 A CN 107382068A
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- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 238000000034 method Methods 0.000 title claims abstract description 16
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims abstract description 22
- 238000007650 screen-printing Methods 0.000 claims abstract description 16
- 229910021532 Calcite Inorganic materials 0.000 claims abstract description 12
- AYJRCSIUFZENHW-UHFFFAOYSA-L barium carbonate Chemical compound [Ba+2].[O-]C([O-])=O AYJRCSIUFZENHW-UHFFFAOYSA-L 0.000 claims abstract description 12
- 239000000463 material Substances 0.000 claims abstract description 12
- DLHONNLASJQAHX-UHFFFAOYSA-N aluminum;potassium;oxygen(2-);silicon(4+) Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[Al+3].[Si+4].[Si+4].[Si+4].[K+] DLHONNLASJQAHX-UHFFFAOYSA-N 0.000 claims abstract description 11
- 238000004040 coloring Methods 0.000 claims abstract description 11
- XGZVUEUWXADBQD-UHFFFAOYSA-L lithium carbonate Chemical compound [Li+].[Li+].[O-]C([O-])=O XGZVUEUWXADBQD-UHFFFAOYSA-L 0.000 claims abstract description 11
- 229910052808 lithium carbonate Inorganic materials 0.000 claims abstract description 11
- 150000004706 metal oxides Chemical group 0.000 claims abstract description 11
- 239000011787 zinc oxide Substances 0.000 claims abstract description 11
- CNLWCVNCHLKFHK-UHFFFAOYSA-N aluminum;lithium;dioxido(oxo)silane Chemical compound [Li+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O CNLWCVNCHLKFHK-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000010453 quartz Substances 0.000 claims abstract description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 6
- 229910052642 spodumene Inorganic materials 0.000 claims abstract description 6
- 229910052882 wollastonite Inorganic materials 0.000 claims abstract description 6
- 239000010456 wollastonite Substances 0.000 claims abstract description 6
- GFQYVLUOOAAOGM-UHFFFAOYSA-N zirconium(iv) silicate Chemical compound [Zr+4].[O-][Si]([O-])([O-])[O-] GFQYVLUOOAAOGM-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000000203 mixture Substances 0.000 claims description 20
- 238000000498 ball milling Methods 0.000 claims description 15
- 238000007639 printing Methods 0.000 claims description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 15
- 238000001035 drying Methods 0.000 claims description 12
- 230000008569 process Effects 0.000 claims description 11
- 239000011248 coating agent Substances 0.000 claims description 10
- 238000000576 coating method Methods 0.000 claims description 10
- AMWRITDGCCNYAT-UHFFFAOYSA-L hydroxy(oxo)manganese;manganese Chemical compound [Mn].O[Mn]=O.O[Mn]=O AMWRITDGCCNYAT-UHFFFAOYSA-L 0.000 claims description 10
- 229910044991 metal oxide Inorganic materials 0.000 claims description 10
- QPLDLSVMHZLSFG-UHFFFAOYSA-N Copper oxide Chemical compound [Cu]=O QPLDLSVMHZLSFG-UHFFFAOYSA-N 0.000 claims description 5
- 239000005751 Copper oxide Substances 0.000 claims description 5
- WGLPBDUCMAPZCE-UHFFFAOYSA-N Trioxochromium Chemical compound O=[Cr](=O)=O WGLPBDUCMAPZCE-UHFFFAOYSA-N 0.000 claims description 5
- 229910052656 albite Inorganic materials 0.000 claims description 5
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 5
- 229910000410 antimony oxide Inorganic materials 0.000 claims description 5
- 229910021538 borax Inorganic materials 0.000 claims description 5
- 229910000423 chromium oxide Inorganic materials 0.000 claims description 5
- 229910000428 cobalt oxide Inorganic materials 0.000 claims description 5
- IVMYJDGYRUAWML-UHFFFAOYSA-N cobalt(ii) oxide Chemical compound [Co]=O IVMYJDGYRUAWML-UHFFFAOYSA-N 0.000 claims description 5
- 229910000431 copper oxide Inorganic materials 0.000 claims description 5
- BDAGIHXWWSANSR-NJFSPNSNSA-N hydroxyformaldehyde Chemical compound O[14CH]=O BDAGIHXWWSANSR-NJFSPNSNSA-N 0.000 claims description 5
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims description 5
- 229910000480 nickel oxide Inorganic materials 0.000 claims description 5
- NDLPOXTZKUMGOV-UHFFFAOYSA-N oxo(oxoferriooxy)iron hydrate Chemical compound O.O=[Fe]O[Fe]=O NDLPOXTZKUMGOV-UHFFFAOYSA-N 0.000 claims description 5
- VTRUBDSFZJNXHI-UHFFFAOYSA-N oxoantimony Chemical compound [Sb]=O VTRUBDSFZJNXHI-UHFFFAOYSA-N 0.000 claims description 5
- GNRSAWUEBMWBQH-UHFFFAOYSA-N oxonickel Chemical compound [Ni]=O GNRSAWUEBMWBQH-UHFFFAOYSA-N 0.000 claims description 5
- 238000005245 sintering Methods 0.000 claims description 5
- 239000004328 sodium tetraborate Substances 0.000 claims description 5
- 235000010339 sodium tetraborate Nutrition 0.000 claims description 5
- 229910000018 strontium carbonate Inorganic materials 0.000 claims description 5
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 claims description 5
- 229910001887 tin oxide Inorganic materials 0.000 claims description 5
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 claims description 5
- 239000002904 solvent Substances 0.000 claims description 2
- 239000003086 colorant Substances 0.000 abstract description 5
- 239000003973 paint Substances 0.000 abstract 4
- 239000004927 clay Substances 0.000 abstract 1
- 210000003298 dental enamel Anatomy 0.000 abstract 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 abstract 1
- 230000008859 change Effects 0.000 description 2
- 238000007873 sieving Methods 0.000 description 2
- 239000000919 ceramic Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/02—Frit compositions, i.e. in a powdered or comminuted form
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/009—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/89—Coating or impregnation for obtaining at least two superposed coatings having different compositions
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Structural Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses a kind of mobile graphic technique glaze and preparation method thereof, the glaze paint of mobile graphic technique glaze includes the white ground glaze layer, color cover coat and the screen printing ink layer that set gradually from inside to outside；Wherein, the component and each component mass parts that white ground-coat enamel material used in white ground glaze layer includes are as follows：Potassium feldspar：35 parts~40 parts；Calcite：8 parts~12 parts；Jiepai clay：12 parts~16 parts；Wollastonite：8 parts~12 parts；Quartz：15 parts~25 parts；Aluminum oxide：4 parts~8 parts；Zirconium silicate：10 parts~15 parts；The component and each component mass parts that color glaze material used in color cover coat includes are as follows：Calcite：28 parts~34 parts；Spodumene：30 parts~35 parts；Barium carbonate：25 parts~30 parts；Lithium carbonate：5 parts~9 parts；Zinc oxide：3 parts~5 parts；Coloring metal oxide：2~4 parts.The present invention makes glaze paint deep mixed color occur, levels off to graduated colors, and the mobile performance of glaze paint is more preferable, and glaze paint is more attractive in appearance, deep to be favored by numerous clients.
Description
Technical Field
The invention relates to a flowing graphic craft glaze and a preparation method thereof.
Background
At present, because of the intense competition of the ceramic industry, products need transformation and upgrading, and a flowing graphic craft glaze with more characteristic than the prior in-glaze embossment is prepared.
Disclosure of Invention
The technical problem to be solved by the invention is to overcome the defects of the prior art and provide the flowing graphic process glaze, which enables the glaze to have colors with different depths and to approach to gradual change colors, has better flowing performance and more attractive appearance and is deeply favored by customers.
The technical scheme for realizing the technical problem of the invention is as follows: a flow pattern craft glaze, its glaze includes white ground coat, color cover coat and silk-screen printing ink layer set up sequentially from inside to outside; wherein,
the white ground glaze used for the white ground glaze layer comprises the following components in parts by mass: potassium feldspar: 35-40 parts; calcite: 8-12 parts; boundary plate mud: 12-16 parts; wollastonite: 8-12 parts; quartz: 15-25 parts; alumina: 4-8 parts; zirconium silicate: 10-15 parts;
the color surface glaze used for the color surface glaze layer comprises the following components in parts by mass: calcite: 28-34 parts; spodumene: 30-35 parts; barium carbonate: 25-30 parts; lithium carbonate: 5-9 parts of a solvent; zinc oxide: 3-5 parts; coloring metal oxide: 2-4 parts;
the printing ink used for the screen printing ink layer comprises the following components in parts by mass: potassium feldspar: 25-30 parts; albite: 10-15 parts; lithium carbonate: 7-8 parts; strontium carbonate: 6-8 parts; borax: 20-25 parts; zinc oxide: 3-6 parts; bone ash: 8 to 10 portions.
Further, the coloring metal oxide is one or a mixture of several of ferric oxide, chromium oxide, copper oxide, antimony oxide, nickel oxide, cobalt oxide, tin oxide and manganese oxide.
The invention also provides a preparation method of the flowing graphic process glaze, which comprises the following steps:
a) respectively preparing a white bottom glaze, a color surface glaze and printing ink; the preparation process of the white bottom glaze comprises the following steps: preparing a white base glaze material according to the following components in parts by mass: wet ball milling is carried out for 13-15 hours according to the mass ratio of glaze to ball to water being 1 to 1.6 to 0.8, and the ball milled glaze is sieved by a 200-mesh sieve and is modulated into 51-53 Baume concentration for later use; the preparation process of the color surface glaze material is as follows: preparing the color surface glaze according to the following components in parts by mass: wet ball milling is carried out for 13-15 hours according to the mass ratio of glaze to ball to water being 1 to 1.6 to 0.9, and the ball milled glaze is sieved by a 200-mesh sieve and is modulated into 51-53 Baume concentration for later use; the ink was prepared as follows: preparing the printing ink according to the following components in parts by mass: wet ball milling is carried out for 13-15 hours according to the mass ratio of glaze to ball to water being 1 to 1.6 to 0.5, and the ball milled glaze is sieved by a 200-mesh sieve and dried for standby;
b) taking a clean blank body, coating a white bottom glaze, drying, coating a color surface glaze outside according to the required color, and drying for later use;
c) the green body with the ground glaze and the surface glaze dried is subjected to silk-screen printing of corresponding images by using prepared ink;
d) and sintering the green body in a roller kiln at 1200 ℃.
After the technical scheme is adopted, the flowing graphic process glaze prepared by the invention has the advantages that the glaze surface has colors with different depths, the color tends to gradually change, the flowing performance of the glaze surface is better, the glaze surface is more attractive, and the flowing graphic process glaze is deeply favored by customers.
Detailed Description
In order that the present invention may be more clearly understood, the following detailed description of the present invention is given with reference to specific examples.
Example one
A flow pattern craft glaze, its glaze includes white ground coat, color cover coat and silk-screen printing ink layer set up sequentially from inside to outside; wherein,
the white ground glaze used for the white ground glaze layer comprises the following components in parts by mass: potassium feldspar: 35 parts of (B); calcite: 8 parts of a mixture; boundary plate mud: 12 parts of (1); wollastonite: 8-12 parts; quartz: 15 parts of (1); alumina: 4 parts of a mixture; zirconium silicate: 10 parts of (A);
the color surface glaze used for the color surface glaze layer comprises the following components in parts by mass: calcite: 28 parts of (1); spodumene: 30 parts of (1); barium carbonate: 25 parts of (1); lithium carbonate: 5 parts of a mixture; zinc oxide: 3 parts of a mixture; coloring metal oxide: 2 parts of (1);
the printing ink used for the screen printing ink layer comprises the following components in parts by mass: potassium feldspar: 25 parts of (1); albite: 10 parts of (A); lithium carbonate: 7 parts; strontium carbonate: 6 parts of (1); borax: 20 parts of (1); zinc oxide: 3 parts of a mixture; bone ash: 8 parts.
Wherein, the coloring metal oxide can be one or a mixture of several of ferric oxide, chromium oxide, copper oxide, antimony oxide, nickel oxide, cobalt oxide, tin oxide and manganese oxide.
The preparation method of the flowing graphic process glaze comprises the following steps:
a) respectively preparing a white bottom glaze, a color surface glaze and printing ink; the preparation process of the white bottom glaze comprises the following steps: preparing a white base glaze material according to the following components in parts by mass: wet ball milling for 13 hours according to the mass ratio of glaze to ball to water being 1 to 1.6 to 0.8, and modulating the ball milled glaze into 51 Baume for later use after passing through a 200-mesh sieve; the preparation process of the color surface glaze material is as follows: preparing the color surface glaze according to the following components in parts by mass: wet ball milling for 13 hours according to the mass ratio of glaze to ball to water being 1 to 1.6 to 0.9, and modulating the ball milled glaze into 51 Baume for later use after passing through a 200-mesh sieve; the ink was prepared as follows: preparing the printing ink according to the following components in parts by mass: wet ball milling is carried out for 13-15 hours according to the mass ratio of glaze to ball to water being 1 to 1.6 to 0.5, and the ball milled glaze is sieved by a 200-mesh sieve and dried for standby;
b) taking a clean blank body, coating a white bottom glaze, drying, coating a color surface glaze outside according to the required color, and drying for later use;
c) the green body with the ground glaze and the surface glaze dried is subjected to silk-screen printing of corresponding images by using prepared ink;
d) and sintering the green body in a roller kiln at 1200 ℃.
Example two
A flow pattern craft glaze, its glaze includes white ground coat, color cover coat and silk-screen printing ink layer set up sequentially from inside to outside; wherein,
the white ground glaze used for the white ground glaze layer comprises the following components in parts by mass: potassium feldspar: 40 parts of a mixture; calcite: 12 parts of (1); boundary plate mud: 16 parts of a mixture; wollastonite: 12 parts of (1); quartz: 25 parts of (1); alumina: 8 parts of a mixture; zirconium silicate: 15 parts of (1);
the color surface glaze used for the color surface glaze layer comprises the following components in parts by mass: calcite: 34 parts of (a); spodumene: 35 parts of (B); barium carbonate: 30 parts of (1); lithium carbonate: 9 parts of (1); zinc oxide: 5 parts of a mixture; coloring metal oxide: 4 parts of a mixture;
the printing ink used for the screen printing ink layer comprises the following components in parts by mass: potassium feldspar: 30 parts of (1); albite: 15 parts of (1); lithium carbonate: 8 parts of a mixture; strontium carbonate: 8 parts of a mixture; borax: 25 parts of (1); zinc oxide: 6 parts of (1); bone ash: 10 parts.
Wherein, the coloring metal oxide can be one or a mixture of several of ferric oxide, chromium oxide, copper oxide, antimony oxide, nickel oxide, cobalt oxide, tin oxide and manganese oxide.
The preparation method of the flowing graphic process glaze comprises the following steps:
a) respectively preparing a white bottom glaze, a color surface glaze and printing ink; the preparation process of the white bottom glaze comprises the following steps: preparing a white base glaze material according to the following components in parts by mass: wet ball milling for 15 hours according to the mass ratio of glaze to ball to water being 1 to 1.6 to 0.8, and modulating the ball milled glaze into 53 Baume concentration for later use after passing through a 200-mesh sieve; the preparation process of the color surface glaze material is as follows: preparing the color surface glaze according to the following components in parts by mass: wet ball milling for 15 hours according to the mass ratio of glaze to ball to water being 1 to 1.6 to 0.9, and modulating the ball milled glaze into 53 Baume concentration for later use after passing through a 200-mesh sieve; the ink was prepared as follows: preparing the printing ink according to the following components in parts by mass: wet ball milling for 15 hours according to the mass ratio of glaze to ball to water being 1 to 1.6 to 0.5, sieving the ball milled glaze with a 200-mesh sieve, and drying for later use;
b) taking a clean blank body, coating a white bottom glaze, drying, coating a color surface glaze outside according to the required color, and drying for later use;
c) the green body with the ground glaze and the surface glaze dried is subjected to silk-screen printing of corresponding images by using prepared ink;
d) and sintering the green body in a roller kiln at 1200 ℃.
EXAMPLE III
A flow pattern craft glaze, its glaze includes white ground coat, color cover coat and silk-screen printing ink layer set up sequentially from inside to outside; wherein,
the white ground glaze used for the white ground glaze layer comprises the following components in parts by mass: potassium feldspar: 38 parts of (B); calcite: 10 parts of (A); boundary plate mud: 14 parts of (1); wollastonite: 10 parts of (A); quartz: 20 parts of (1); alumina: 12 parts of (1); zirconium silicate: 13 parts;
the color surface glaze used for the color surface glaze layer comprises the following components in parts by mass: calcite: 31 parts of (B); spodumene: 33 parts of (B); barium carbonate: 23 parts; lithium carbonate: 7 parts; zinc oxide: 4 parts of a mixture; coloring metal oxide: 3 parts of a mixture;
the printing ink used for the screen printing ink layer comprises the following components in parts by mass: potassium feldspar: 28 parts of (1); albite: 12 parts of (1); lithium carbonate: 7 parts; strontium carbonate: 7 parts; borax: 23 parts; zinc oxide: 5 parts of a mixture; bone ash: 9 parts.
Wherein, the coloring metal oxide can be one or a mixture of several of ferric oxide, chromium oxide, copper oxide, antimony oxide, nickel oxide, cobalt oxide, tin oxide and manganese oxide.
The preparation method of the flowing graphic process glaze comprises the following steps:
a) respectively preparing a white bottom glaze, a color surface glaze and printing ink; the preparation process of the white bottom glaze comprises the following steps: preparing a white base glaze material according to the following components in parts by mass: wet ball milling is carried out for 13-15 hours according to the mass ratio of glaze to ball to water being 1 to 1.6 to 0.8, and the ball milled glaze is sieved by a 200-mesh sieve and is modulated into 51-53 Baume concentration for later use; the preparation process of the color surface glaze material is as follows: preparing the color surface glaze according to the following components in parts by mass: wet ball milling for 14 hours according to the mass ratio of glaze to ball to water of 1 to 1.6 to 0.9, and after the ball milled glaze is sieved by a 200-mesh sieve, modulating the glaze into 52 Baume concentration for later use; the ink was prepared as follows: preparing the printing ink according to the following components in parts by mass: wet ball milling for 14 hours according to the mass ratio of glaze to ball to water being 1 to 1.6 to 0.5, sieving the ball milled glaze with a 200-mesh sieve, and drying for later use;
b) taking a clean blank body, coating a white bottom glaze, drying, coating a color surface glaze outside according to the required color, and drying for later use;
c) the green body with the ground glaze and the surface glaze dried is subjected to silk-screen printing of corresponding images by using prepared ink;
d) and sintering the green body in a roller kiln at 1200 ℃.
The flowing graphic process glaze prepared by the three embodiments has the advantages that the glaze surface has colors with different depths, the color tends to be gradually changed, the flowing performance of the glaze surface is better, the glaze surface is more attractive, and the flowing graphic process glaze is deeply favored by customers.
The above-mentioned embodiments are intended to illustrate the objects, technical solutions and advantages of the present invention in further detail, and it should be understood that the above-mentioned embodiments are only exemplary embodiments of the present invention, and are not intended to limit the present invention, and any modifications, equivalents, improvements and the like made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (3)
1. A flowing pattern craft glaze is characterized in that the glaze surface of the flowing pattern craft glaze comprises a white ground glaze layer, a color surface glaze layer and a silk-screen printing ink layer which are sequentially arranged from inside to outside; wherein,
the white ground glaze used for the white ground glaze layer comprises the following components in parts by mass: potassium feldspar: 35-40 parts; calcite: 8-12 parts; boundary plate mud: 12-16 parts; wollastonite: 8-12 parts; quartz: 15-25 parts; alumina: 4-8 parts; zirconium silicate: 10-15 parts;
the color surface glaze used for the color surface glaze layer comprises the following components in parts by mass: calcite: 28-34 parts; spodumene: 30-35 parts; barium carbonate: 25-30 parts; lithium carbonate: 5-9 parts of a solvent; zinc oxide: 3-5 parts; coloring metal oxide: 2-4 parts;
the printing ink used for the screen printing ink layer comprises the following components in parts by mass: potassium feldspar: 25-30 parts; albite: 10-15 parts; lithium carbonate: 7-8 parts; strontium carbonate: 6-8 parts; borax: 20-25 parts; zinc oxide: 3-6 parts; bone ash: 8 to 10 portions.
2. The flow pattern process glaze according to claim 1, wherein: the coloring metal oxide is one or a mixture of several of ferric oxide, chromium oxide, copper oxide, antimony oxide, nickel oxide, cobalt oxide, tin oxide and manganese oxide.
3. A method of preparing a flowcharted process glaze according to claim 1 or 2, characterized in that the method comprises the steps of:
a) respectively preparing a white bottom glaze, a color surface glaze and printing ink; the preparation process of the white bottom glaze comprises the following steps: preparing a white base glaze material according to the following components in parts by mass: wet ball milling is carried out for 13-15 hours according to the mass ratio of glaze to ball to water being 1 to 1.6 to 0.8, and the ball milled glaze is sieved by a 200-mesh sieve and is modulated into 51-53 Baume concentration for later use; the preparation process of the color surface glaze material is as follows: preparing the color surface glaze according to the following components in parts by mass: wet ball milling is carried out for 13-15 hours according to the mass ratio of glaze to ball to water being 1 to 1.6 to 0.9, and the ball milled glaze is sieved by a 200-mesh sieve and is modulated into 51-53 Baume concentration for later use; the ink was prepared as follows: preparing the printing ink according to the following components in parts by mass: wet ball milling is carried out for 13-15 hours according to the mass ratio of glaze to ball to water being 1 to 1.6 to 0.5, and the ball milled glaze is sieved by a 200-mesh sieve and dried for standby;
b) taking a clean blank body, coating a white bottom glaze, drying, coating a color surface glaze outside according to the required color, and drying for later use;
c) the green body with the ground glaze and the surface glaze dried is subjected to silk-screen printing of corresponding images by using prepared ink;
d) and sintering the green body in a roller kiln at 1200 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710604792.7A CN107382068A (en) | 2017-07-24 | 2017-07-24 | Mobile graphic technique glaze and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710604792.7A CN107382068A (en) | 2017-07-24 | 2017-07-24 | Mobile graphic technique glaze and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107382068A true CN107382068A (en) | 2017-11-24 |
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| CN201710604792.7A Pending CN107382068A (en) | 2017-07-24 | 2017-07-24 | Mobile graphic technique glaze and preparation method thereof |
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| CN111517824A (en) * | 2020-04-24 | 2020-08-11 | 佛山科学技术学院 | Wear-resistant corrosion-resistant ceramic glaze as well as preparation method and application thereof |
| CN112125520A (en) * | 2020-09-24 | 2020-12-25 | 福建省春秋陶瓷实业有限公司 | Ceramic product with flowing pattern glaze and preparation method thereof |
| CN114163129A (en) * | 2021-12-31 | 2022-03-11 | 德化县京隆堂陶瓷有限责任公司 | Metal-texture in-glaze-pattern glazed ceramic and preparation method thereof |
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| CN112125520A (en) * | 2020-09-24 | 2020-12-25 | 福建省春秋陶瓷实业有限公司 | Ceramic product with flowing pattern glaze and preparation method thereof |
| CN114163129A (en) * | 2021-12-31 | 2022-03-11 | 德化县京隆堂陶瓷有限责任公司 | Metal-texture in-glaze-pattern glazed ceramic and preparation method thereof |
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