CN108840567A - Double-deck Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze and preparation method thereof - Google Patents
Double-deck Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze and preparation method thereof Download PDFInfo
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- CN108840567A CN108840567A CN201810994114.0A CN201810994114A CN108840567A CN 108840567 A CN108840567 A CN 108840567A CN 201810994114 A CN201810994114 A CN 201810994114A CN 108840567 A CN108840567 A CN 108840567A
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Classifications
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/89—Coating or impregnation for obtaining at least two superposed coatings having different compositions
Abstract
The invention discloses a kind of double-deck Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze and preparation method thereof, and the double-deck Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze contains ground coat enamel and overglaze；Wherein, the component and each component mass parts contained in the ground coat enamel material that the ground coat enamel uses is as follows：30~40 parts of potassium feldspar；30~40 parts of clues mud；12~15 parts of Jiepai clay；3~5 parts of zinc oxide；5~7 parts of calcite；13~18 parts of dolomite；10~12 parts of cobalt black；The overglaze includes the stream grain in glaze material and addition glaze material；The component and each component mass parts contained in glaze material is as follows：30~40 parts of potassium feldspar；20~25 parts of zinc oxide；18~20 parts of albite；13~15 parts of calcite；8~12 parts of Jiepai clay；5~8 parts of talcum；The component and each component mass parts of the stream grain are as follows：Feldspar：35~45 parts；10~15 parts of zinc oxide；12~15 parts of albite；7~9 parts of titanium oxide；12~15 parts of calcite；8~10 parts of wollastonite；10~12 parts of iron oxide red.The effect of the double-deck reaction glaze can not only be presented in the present invention, but also has stream grain effect, and people is allowed to be so fond that will not let out of one's hand, deep to be liked by users.
Description
Technical field
The present invention relates to a kind of double-deck Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze and preparation method thereof.
Background technique
Currently, being particular about the security performance of ceramics in ceramic industry, lead cadmium content must not be exceeded, and glaze is made to need to present
The double-deck reaction effect, and need to keep it more naturally beautiful plus stream grain effect.
Summary of the invention
The technical problem to be solved by the present invention is to overcome the deficiencies of existing technologies, a kind of double-deck Argyll Robertson pupil/sign Argyll-Robertson stream grain is provided
Glaze, the effect of the double-deck reaction glaze can not only be presented in it, but also has stream grain effect, and people is allowed to be so fond that will not let out of one's hand, deep by vast use
Like at family.
In order to solve the above technical problems, the technical scheme is that：A kind of bilayer Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze, it contains
Ground coat enamel and overglaze；Wherein,
The component and each component mass parts contained in the ground coat enamel material that the ground coat enamel uses is as follows：
30~40 parts of potassium feldspar；30~40 parts of clues mud；12~15 parts of Jiepai clay；3~5 parts of zinc oxide；Calcite 5~7
Part；13~18 parts of dolomite；10~12 parts of cobalt black；
The overglaze includes the stream grain in glaze material and addition glaze material；
The component and each component mass parts contained in glaze material is as follows：30~40 parts of potassium feldspar；20~25 parts of zinc oxide；Sodium
18~20 parts of feldspar；13~15 parts of calcite；8~12 parts of Jiepai clay；5~8 parts of talcum；
The component and each component mass parts of the stream grain are as follows：Feldspar：35~45 parts；10~15 parts of zinc oxide；Albite
12~15 parts；7~9 parts of titanium oxide；12~15 parts of calcite；8~10 parts of wollastonite；10~12 parts of iron oxide red.
Further, 20 grams of grain of stream is added in per kilogram glaze material.
Further, the stream grain is 80~100 mesh.
Further, after the stream grain is according to its component and each component mass parts stock, by ball milling, 70 mesh are crossed after drying
Sieve, is sintered, after 80~100 meshes in 1000 DEG C of drawer kiln.
The present invention also provides a kind of preparation method of double-deck Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze, the step of method contains, is as follows：
S1：Glaze material and ground coat enamel material are prepared respectively；And the stream grain of 80~100 mesh is added in glaze material obtained, it obtains
Overglaze stream pellet；Wherein, 20 grams of grain of stream is added in per kilogram glaze material；
S2：It will be dried after ground coat enamel material on clean green body；
S3：By overglaze stream pellet on the green body of first-class ground coat enamel material, enters and fired in 1200 DEG C of roller kilns.
Further, the preparation process of glaze material and ground coat enamel material is：1.7 ︰ 0.6 of mass ratio=1 ︰ of You Liao ︰ Qiu ︰ water, wet process
Ball milling 14~16 hours, the glaze after ball milling crossed 200 meshes.
After above-mentioned technical proposal, the double-deck Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze lead cadmium content that the present invention is prepared does not surpass
Mark, the bilayer Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze keep it more naturally beautiful, double plus stream grain effect in bilayer reaction glaze effect
It joined flow particles in the case where layer transmutation, people allowed to be so fond that will not let out of one's hand, it is deep to be liked by users.
Specific embodiment
In order that the present invention can be more clearly and readily understood, below according to specific embodiment, to the present invention make into
One step detailed description.
Embodiment one
A kind of bilayer Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze, it contains ground coat enamel and overglaze；Wherein,
The component and each component mass parts contained in the ground coat enamel material that the ground coat enamel uses is as follows：
30 parts of potassium feldspar；30 parts of clues mud；12 parts of Jiepai clay；3 parts of zinc oxide；5 parts of calcite；13 parts of dolomite；Cobalt black
10 parts；
The overglaze includes the stream grain in glaze material and addition glaze material；
The component and each component mass parts contained in glaze material is as follows：30 parts of potassium feldspar；20 parts of zinc oxide；Albite 18
Part；13 parts of calcite；8 parts of Jiepai clay；5 parts of talcum；
The component and each component mass parts of the stream grain are as follows：Feldspar：35 parts；10 parts of zinc oxide；12 parts of albite；Oxidation
7 parts of titanium；12 parts of calcite；8 parts of wollastonite；10 parts of iron oxide red.
20 grams of grain of stream is added in per kilogram glaze material.
The stream grain is 80~100 mesh.
After the stream grain is according to its component and each component mass parts stock, by ball milling, 70 meshes are crossed after drying, 1000
DEG C drawer kiln in be sintered, after 80~100 meshes.
The step of preparation method of the bilayer Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze, method contains, is as follows：
S1：Glaze material and ground coat enamel material are prepared respectively；And the stream grain of 80~100 mesh is added in glaze material obtained, it obtains
Overglaze stream pellet；Wherein, 20 grams of grain of stream is added in per kilogram glaze material；
S2：It will be dried after ground coat enamel material on clean green body；
S3：By overglaze stream pellet on the green body of first-class ground coat enamel material, enters and fired in 1200 DEG C of roller kilns.
The preparation process of glaze material and ground coat enamel material is：1.7 ︰ 0.6 of mass ratio=1 ︰ of You Liao ︰ Qiu ︰ water, wet ball grinding 14~
16 hours, the glaze after ball milling crossed 200 meshes.
Embodiment two
A kind of bilayer Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze, it contains ground coat enamel and overglaze；Wherein,
The component and each component mass parts contained in the ground coat enamel material that the ground coat enamel uses is as follows：
40 parts of potassium feldspar；40 parts of clues mud；15 parts of Jiepai clay；5 parts of zinc oxide；7 parts of calcite；18 parts of dolomite；Cobalt black
12 parts；
The overglaze includes the stream grain in glaze material and addition glaze material；
The component and each component mass parts contained in glaze material is as follows：40 parts of potassium feldspar；25 parts of zinc oxide；Albite 20
Part；15 parts of calcite；12 parts of Jiepai clay；8 parts of talcum；
The component and each component mass parts of the stream grain are as follows：Feldspar：45 parts；15 parts of zinc oxide；15 parts of albite；Oxidation
9 parts of titanium；15 parts of calcite；10 parts of wollastonite；12 parts of iron oxide red.
20 grams of grain of stream is added in per kilogram glaze material.
The stream grain is 80~100 mesh.
After the stream grain is according to its component and each component mass parts stock, by ball milling, 70 meshes are crossed after drying, 1000
DEG C drawer kiln in be sintered, after 80~100 meshes.
The step of preparation method of the bilayer Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze, method contains, is as follows：
S1：Glaze material and ground coat enamel material are prepared respectively；And the stream grain of 80~100 mesh is added in glaze material obtained, it obtains
Overglaze stream pellet；Wherein, 20 grams of grain of stream is added in per kilogram glaze material；
S2：It will be dried after ground coat enamel material on clean green body；
S3：By overglaze stream pellet on the green body of first-class ground coat enamel material, enters and fired in 1200 DEG C of roller kilns.
The preparation process of glaze material and ground coat enamel material is：1.7 ︰ 0.6 of mass ratio=1 ︰ of You Liao ︰ Qiu ︰ water, wet ball grinding 14~
16 hours, the glaze after ball milling crossed 200 meshes.
Embodiment three
A kind of bilayer Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze, it contains ground coat enamel and overglaze；Wherein,
The component and each component mass parts contained in the ground coat enamel material that the ground coat enamel uses is as follows：
35 parts of potassium feldspar；35 parts of clues mud；14 parts of Jiepai clay；4 parts of zinc oxide；6 parts of calcite；15 parts of dolomite；Cobalt black
11 parts；
The overglaze includes the stream grain in glaze material and addition glaze material；
The component and each component mass parts contained in glaze material is as follows：35 parts of potassium feldspar；22 parts of zinc oxide；Albite 19
Part；14 parts of calcite；10 parts of Jiepai clay；7 parts of talcum；
The component and each component mass parts of the stream grain are as follows：Feldspar：40 parts；12 parts of zinc oxide；13 parts of albite；Oxidation
8 parts of titanium；14 parts of calcite；9 parts of wollastonite；11 parts of iron oxide red.
20 grams of grain of stream is added in per kilogram glaze material.
The stream grain is 80~100 mesh.
After the stream grain is according to its component and each component mass parts stock, by ball milling, 70 meshes are crossed after drying, 1000
DEG C drawer kiln in be sintered, after 80~100 meshes.
The step of preparation method of the bilayer Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze, method contains, is as follows：
S1：Glaze material and ground coat enamel material are prepared respectively；And the stream grain of 80~100 mesh is added in glaze material obtained, it obtains
Overglaze stream pellet；Wherein, 20 grams of grain of stream is added in per kilogram glaze material；
S2：It will be dried after ground coat enamel material on clean green body；
S3：By overglaze stream pellet on the green body of first-class ground coat enamel material, enters and fired in 1200 DEG C of roller kilns.
The preparation process of glaze material and ground coat enamel material is：1.7 ︰ 0.6 of mass ratio=1 ︰ of You Liao ︰ Qiu ︰ water, wet ball grinding 14~
16 hours, the glaze after ball milling crossed 200 meshes.
Comparative example one
A kind of bilayer Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze, it contains ground coat enamel and overglaze；Wherein,
The component and each component mass parts contained in the ground coat enamel material that the ground coat enamel uses is as follows：
30 parts of potassium feldspar；30 parts of clues mud；12 parts of Jiepai clay；3 parts of zinc oxide；5 parts of calcite；13 parts of dolomite；Cobalt black
10 parts；
The overglaze includes the stream grain in glaze material and addition glaze material；
The component and each component mass parts contained in glaze material is as follows：30 parts of potassium feldspar；20 parts of zinc oxide；Albite 15
Part；13 parts of calcite；18 parts of Jiepai clay；5 parts of talcum；
The component and each component mass parts of the stream grain are as follows：Feldspar：35 parts；10 parts of zinc oxide；12 parts of albite；Oxidation
7 parts of titanium；12 parts of calcite；8 parts of wollastonite；10 parts of iron oxide red.
20 grams of grain of stream is added in per kilogram glaze material.
The stream grain is 80~100 mesh.
After the stream grain is according to its component and each component mass parts stock, by ball milling, 70 meshes are crossed after drying, 1000
DEG C drawer kiln in be sintered, after 80~100 meshes.
The step of preparation method of the bilayer Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze, method contains, is as follows：
S1：Glaze material and ground coat enamel material are prepared respectively；And the stream grain of 80~100 mesh is added in glaze material obtained, it obtains
Overglaze stream pellet；Wherein, 20 grams of grain of stream is added in per kilogram glaze material；
S2：It will be dried after ground coat enamel material on clean green body；
S3：By overglaze stream pellet on the green body of first-class ground coat enamel material, enters and fired in 1200 DEG C of roller kilns.
The preparation process of glaze material and ground coat enamel material is：You Liao ︰ Qiu ︰ water=1 ︰ 1.7 ︰ 0.6, wet ball grinding 14~16 hours,
Glaze after ball milling crosses 200 meshes.
Comparative example two
A kind of bilayer Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze, it contains ground coat enamel and overglaze；Wherein,
The component and each component mass parts contained in the ground coat enamel material that the ground coat enamel uses is as follows：
35 parts of potassium feldspar；35 parts of clues mud；14 parts of Jiepai clay；4 parts of zinc oxide；6 parts of calcite；15 parts of dolomite；Cobalt black
11 parts；
The overglaze includes the stream grain in glaze material and addition glaze material；
The component and each component mass parts contained in glaze material is as follows：35 parts of potassium feldspar；22 parts of zinc oxide；Albite 19
Part；14 parts of calcite；10 parts of Jiepai clay；7 parts of talcum；
The component and each component mass parts of the stream grain are as follows：Feldspar：40 parts；12 parts of zinc oxide；13 parts of albite；Oxidation
8 parts of titanium；14 parts of calcite；9 parts of wollastonite；11 parts of iron oxide red.
20 grams of grain of stream is added in per kilogram glaze material.
The stream grain is 80~100 mesh.
After the stream grain is according to its component and each component mass parts stock, by ball milling, 70 meshes are crossed after drying, 1000
DEG C drawer kiln in be sintered, after 80~100 meshes.
The step of preparation method of the bilayer Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze, method contains, is as follows：
S1：Glaze material and ground coat enamel material are prepared respectively；And the stream grain of 80~100 mesh is added in glaze material obtained, it obtains
Overglaze stream pellet；Wherein, 20 grams of grain of stream is added in per kilogram glaze material；
S2：It will be dried after ground coat enamel material on clean green body；
S3：By overglaze stream pellet on the green body of first-class ground coat enamel material, enters and fired in 1200 DEG C of roller kilns.
The preparation process of glaze material and ground coat enamel material is：You Liao ︰ Qiu ︰ water=1 ︰ 1.7 ︰ 0.6, wet ball grinding 16~20 hours,
Glaze after ball milling crosses 200 meshes.
Compare one：Overglaze mobile performance is too weak, keeps particle effect flow effect not obvious enough；
Compare two：Ball-milling Time is too long, overglaze hacking when glazing, the product contracting glaze for being sintered out；
Embodiment one is to embodiment three：Meet exploitation to require, properties are stablized.
Particular embodiments described above, to the technical problems to be solved by the invention, technical scheme and beneficial effects into
Further description of having gone is not used to limit it should be understood that the above is only a specific embodiment of the present invention
The system present invention, all within the spirits and principles of the present invention, any modification, equivalent substitution, improvement and etc. done should be included in
Within protection scope of the present invention.
Claims (6)
1. a kind of bilayer Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze, it is characterised in that it contains ground coat enamel and overglaze；Wherein,
The component and each component mass parts contained in the ground coat enamel material that the ground coat enamel uses is as follows：
30~40 parts of potassium feldspar；30~40 parts of clues mud；12~15 parts of Jiepai clay；3~5 parts of zinc oxide；5~7 parts of calcite；It is white
13~18 parts of marble；10~12 parts of cobalt black；
The overglaze includes the stream grain in glaze material and addition glaze material；
The component and each component mass parts contained in glaze material is as follows：30~40 parts of potassium feldspar；20~25 parts of zinc oxide；Albite
18~20 parts；13~15 parts of calcite；8~12 parts of Jiepai clay；5~8 parts of talcum；
The component and each component mass parts of the stream grain are as follows：Feldspar：35~45 parts；10~15 parts of zinc oxide；Albite 12~
15 parts；7~9 parts of titanium oxide；12~15 parts of calcite；8~10 parts of wollastonite；10~12 parts of iron oxide red.
2. bilayer Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze according to claim 1, it is characterised in that：Stream grain is added in per kilogram glaze material
20 grams.
3. bilayer Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze according to claim 1, it is characterised in that：The stream grain is 80~100 mesh.
4. bilayer Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze according to claim 1, it is characterised in that：The stream grain is according to its component and respectively
After constituent mass part stock, by ball milling, 70 meshes are crossed after drying, are sintered in 1000 DEG C of drawer kiln, after 80~100 mesh
Sieve.
5. a kind of preparation method of the double-deck Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze according to any one of claims 1 to 4, it is characterised in that
The step of method contains is as follows：
S1：Glaze material and ground coat enamel material are prepared respectively；And the stream grain of 80~100 mesh is added in glaze material obtained, obtain overglaze
Flow pellet；Wherein, 20 grams of grain of stream is added in per kilogram glaze material；
S2：It will be dried after ground coat enamel material on clean green body；
S3：By overglaze stream pellet on the green body of first-class ground coat enamel material, enters and fired in 1200 DEG C of roller kilns.
6. the preparation method according to claim 4, it is characterised in that：The preparation process of glaze material and ground coat enamel material is：You Liao ︰
1.7 ︰ 0.6 of the mass ratio of Qiu ︰ water=1 ︰, wet ball grinding 14~16 hours, the glaze after ball milling crossed 200 meshes.
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| CN201810994114.0A CN108840567A (en) | 2018-08-29 | 2018-08-29 | Double-deck Argyll Robertson pupil/sign Argyll-Robertson stream grain glaze and preparation method thereof |
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Cited By (1)
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| CN110790506A (en) * | 2019-12-18 | 2020-02-14 | 湖南华联瓷业股份有限公司 | Granular double-layer reaction glaze and preparation method thereof |
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