CN108096100A - A kind of plant base light repairs suncream and preparation method thereof - Google Patents
A kind of plant base light repairs suncream and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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Abstract
The present invention relates to a kind of plant base light to repair suncream and preparation method thereof, belongs to cosmetic technical field.The present invention passes through rabbit hair keratin cladding titanium dioxide, there is good skin-friendly using rabbit hair keratin, the characteristics of non-toxic and adsorptivity, the scattering process to ultraviolet light can be enhanced, it is easy to skin pore again to be disperseed to absorb, avoid due to grain diameter is big and the problem of block pore, and with reference to effective ingredients in plant, inhibit TYR enzyme activity so as to which melanin be blocked to generate, slow down the cutaneous anaphylaxis as caused by ultraviolet radioactive, actively repair the pyrimidine dimer generated in Skin Cell due to ultraviolet radioactive, so as to protect skin, prevent the malignant disease caused by the ultraviolet injuries such as melanoma and cutaneum carcinoma, repair the DNA structure of damaged cell, reach mild, it is non-stimulated, stability is good, have both anti-aging, the beauty functions such as whitening.
Description
Technical field
The present invention relates to a kind of plant base light to repair suncream and preparation method thereof, belongs to cosmetic technical field.
Background technology
Suncream shields to skin by reflection and scatters ultraviolet.Ultraviolet light is to cell DNA, film and is immunized
System has a negative effect, and suncream can provide cell and immune system protection, wherein titanium dioxide for suncream mainly into
/ mono-.The strong anti-uv-ray of titanium dioxide is since it is with high refractivity and high photolytic activity, anti-uv-ray
And its mechanism is related with its grain size：When grain size is larger, the barrier to ultraviolet light is based on reflecting, scatter, and to medium wave area
Effective with long-wavelength region ultraviolet light, sun-proof mechanism is simply to cover, and belongs to general physical sunscreen, and sun-proof ability is weaker；With
The reduction of grain size, light can be through the particle faces of titanium dioxide, reflection, scattering unobvious to long-wavelength region ultraviolet light, and right
The absorbability of medium wave area ultraviolet light is remarkably reinforced, and sun-proof mechanism is to absorb ultraviolet light, main to absorb medium wave area ultraviolet light.Thus
As it can be seen that titanium dioxide is different to the sun-proof mechanism of different wave length ultraviolet light, to the barrier of long-wavelength region ultraviolet light based on scattering,
To the barrier of medium wave area ultraviolet light based on absorbing.For nano-titanium dioxide since grain size is small, activity is big, can reflect, scatter purple
Outside line, and ultraviolet light can be absorbed, so as to there is stronger obstructing capacity to ultraviolet light.
When titanium dioxide fine particles grain size is equal to or less than the half of optical wavelength, the reflection, scattered quantum to light are maximum, shielding
Effect is best.The wavelength of ultraviolet light is between 190~400nm, therefore the grain size of nano-titanium dioxide cannot be more than 200nm, most
It is not more than 100nm well.But, though having preferable sun-proof result when titanium dioxide coarseness is too small, easily reunite, be unfavorable for
It is scattered, it is also easy to block the pore of skin, is unfavorable for ventilative and sweat exclusion, it is necessary to carry out modification to it.
The content of the invention
The technical problems to be solved by the invention：For titanium dioxide coarseness in suncream it is too small when easily reunite, it is unfavorable
In scattered, be also easy to block the pore of skin, be unfavorable for the problem of ventilative, provide a kind of plant base light repair suncream and its
Preparation method.
In order to solve the above technical problems, the technical solution adopted by the present invention is：
A kind of plant base light repairs suncream, including following weight parts raw material：
100~200 portions of plant mixed liquors, 200~400 parts of rabbit hair keratin solutions, 5~8 parts of sodium chloride, 30~40 parts of fourths two
Alcohol, 50~80 parts of glycerine, 0.5~0.8 part of xanthans, 3~5 parts of Arlacel-60s, 25~30 parts of dimethyl silicone polymers, 150~
200 parts of atoleines, 100~150 parts of carbonic acid dioctyl esters, 15~20 parts of beeswaxs, 5~8 portions of preservatives, 0.5~0.8 part of essence.
The plant mixed liquor mixes for 10~20 parts by weight butyl titanates with 100~200 parts by weight plant extraction liquids
It stands and is made.
The plant extraction liquid be scutellaria powder, combined-ear chrysanthemum powder, Antarctic ice microalgae powder add in mass fraction be 70% ethyl alcohol
Heating and refluxing extraction in solution, and be evaporated under reduced pressure concentration, then by macroporous resin column be adsorbed to it is colourless after eluted with ethanol solution,
Ethanol eluate is collected, and vacuum distillation is concentrated into no ethyl alcohol and is made.
The scutellaria powder, combined-ear chrysanthemum powder, Antarctic ice microalgae powder, the parts by weight of ethanol solution are 100~200 parts of scutellarias
Powder, 100~200 parts of combined-ear chrysanthemum powder, 50~100 parts of Antarctic ice microalgae powder, 1000~2000 parts of ethanol solutions.
The rabbit hair keratin solution is that be dissolved in mass fraction after rabbit hair drying and crushing be to be made in 2% sodium hydroxide solution
.
The mass ratio of the rabbit hair and sodium hydroxide solution is 1：5~1：20.
The preservative is any one in methyl hydroxybenzoate, propylben.
A kind of plant base light repairs the preparation method of suncream, concretely comprises the following steps：
（1）It is crushed being fitted into after scutellaria naturally dry in micronizer, crosses 300 mesh sieves, obtain scutellaria powder；
（2）It is crushed being fitted into after combined-ear chrysanthemum naturally dry in micronizer, crosses 300 mesh sieves, obtain combined-ear chrysanthemum powder；
（3）It is crushed being fitted into after Antarctic ice microalgae naturally dry in micronizer, crosses 300 mesh sieves, obtain Antarctic ice microalgae powder；
（4）Scutellaria powder, combined-ear chrysanthemum powder, Antarctic ice microalgae powder are taken, adds in ethanol solution, is heated to reflux at 60~80 DEG C
2~3h is extracted, obtains crude extract；
（5）Crude extract vacuum distillation is concentrated into no ethyl alcohol, and passes through macroporous resin column and is adsorbed to colourless, then is with mass fraction
It is colourless that 50% ethanol solution is eluted to washing lotion, collects ethanol eluate, and is evaporated under reduced pressure and is concentrated into no ethyl alcohol, obtains plant extract
Liquid；
（6）Butyl titanate is taken, adds in plant extraction liquid and 2~3h is stood after stirring evenly, obtain plant mixed liquor；
（7）It will be crushed after rabbit hair washing and drying, be re-dissolved in sodium hydroxide solution, obtain rabbit hair keratin solution；
（8）Plant mixed liquor is added dropwise in rabbit hair keratin solution, adds sodium chloride, butanediol, glycerine, xanthans,
30~40min is stirred at 70~80 DEG C, obtains A phases；
（9）Take Arlacel-60, dimethyl silicone polymer, atoleine, carbonic acid dioctyl ester, beeswax, at 70~80 DEG C stir 20~
30min obtains B phases；
（10）A is added in B phases, with 3000~4000r/min, 20~30min of emulsifying, 40 are cooled to after emulsification
~50 DEG C, preservative, essence are added, stirs evenly rear vacuum defoamation, plant base light is obtained and repairs suncream.
Compared with other methods, advantageous effects are the present invention：
（1）The present invention has conjugated double bond using the active ingredient flavone compound in scutellaria, structure, to it is ultraviolet have it is strong
It absorbs, especially the average UV line absorption rate highest in UVB areas, sun-proof so as to achieve the effect that, scutellaria also has both antibacterial, resists
It is scorching, clearing heat and detoxicating and other effects, and the active ingredient in combined-ear chrysanthemum contains more band conjugate double bond system compound, these chemical combination
Object is 3- methylene -6- respectively（1- Methylethyls）Cyclohexene, firpene, cyclohexene etc., the compound with conjugate double bond system
With stronger ultraviolet absorption effect, TYR enzyme activity can be inhibited so as to which melanin be blocked to generate, in combination with Antarctic Ice
Light repair enzyme in algae can effectively slow down the cutaneous anaphylaxis as caused by ultraviolet radioactive, actively repair in Skin Cell
The pyrimidine dimer generated due to ultraviolet radioactive, so as to protect skin, the prevention ultraviolet injuries such as melanoma and cutaneum carcinoma institute
Caused malignant disease repairs damaged cell；
（2）The present invention has good skin-friendly, nontoxicity by rabbit hair keratin cladding titanium dioxide using rabbit hair keratin
And the characteristics of adsorptivity, can enhance the scattering process to ultraviolet light and skin pore is disperseed to absorb, avoid by
It is big in grain diameter and the problem of block pore, and it is mild, non-stimulated, stability is good, have both the beauty work(such as anti-aging, whitening
Effect.
Specific embodiment
It is crushed being fitted into after scutellaria naturally dry in micronizer, crosses 300 mesh sieves, obtain scutellaria powder, by combined-ear chrysanthemum certainly
It is fitted into micronizer and crushes after so drying, cross 300 mesh sieves, obtain combined-ear chrysanthemum powder, will be packed into after Antarctic ice microalgae naturally dry
It is crushed in micronizer, crosses 300 mesh sieves, obtain Antarctic ice microalgae powder, take 100~200g scutellaria powder, 100~200g combined-ear chrysanthemums
Powder, 50~100g Antarctic ice microalgae powder add in 1~2L mass fractions in 70% ethanol solution, to be heated back at 60~80 DEG C
Stream extraction 2~3h, obtain crude extract, by crude extract vacuum distillation be concentrated into no ethyl alcohol, and pass through macroporous resin column be adsorbed to it is colourless,
It is colourless washing lotion to be eluted to the ethanol solution that mass fraction is 50%, collects ethanol eluate, and is evaporated under reduced pressure and is concentrated into no second again
Alcohol obtains plant extraction liquid, takes 10~20g butyl titanates, adds in 100~200g plant extraction liquids, with 300~400r/min
20~30min is stirred, 2~3h is stood, obtains plant mixed liquor, take 1~2kg rabbit hairs, be washed with deionized totally and is packed into baking
In case, dry 2~3h at 50~55 DEG C, then be transferred in pulverizer and be crushed to broken section of 1~5mm, by broken section of addition of the rabbit hair
10~20kg mass fractions are in 2% sodium hydroxide solution, under 80~85 DEG C of waters bath with thermostatic control, react 3~5h, filter to get filtrate,
Rabbit hair keratin solution, it is molten that 100~200g plants mixed liquor with 1~2g/min is added dropwise to 200~400g rabbit hair keratin
It in liquid, is continued stirring until and is added dropwise with 200~300r/min, add 5~8g sodium chloride, 30~40g butanediols, 50~
80g glycerine, 0.5~0.8g xanthans continue 30~40min of stirring at 70~80 DEG C, obtain A phases, take 3~5g Arlacel-60s, and 25
~30g dimethyl silicone polymers, 150~200g atoleines, 100~150g carbonic acid dioctyl esters, 15~20g beeswaxs, 70~
20~30min is stirred with 300~400r/min at 80 DEG C, B phases is obtained, A is added in B phases, with 3000~4000r/min homogeneous
20~30min is emulsified, 40~50 DEG C are cooled to after emulsification, adds 5~8g preservatives, 0.5~0.8g essence, stirring is
Vacuum defoamation after even obtains the plant base light and repairs suncream.
Example 1
It is crushed being fitted into after scutellaria naturally dry in micronizer, crosses 300 mesh sieves, obtain scutellaria powder, combined-ear chrysanthemum is dried in the air naturally
It is fitted into micronizer and crushes after dry, cross 300 mesh sieves, obtain combined-ear chrysanthemum powder, ultra micro will be packed into after Antarctic ice microalgae naturally dry
It is crushed in pulverizer, crosses 300 mesh sieves, obtain Antarctic ice microalgae powder, take 100g scutellaria powder, 100g combined-ear chrysanthemum powder, 50g Antarctic Ices
Algae powder adds in 1L mass fractions as in 70% ethanol solution, heating and refluxing extraction 2h, obtains crude extract at 60 DEG C, by crude extract
Vacuum distillation be concentrated into no ethyl alcohol, and pass through macroporous resin column be adsorbed to it is colourless, then with mass fraction be 50% ethanol solution wash
, collection ethanol eluate colourless to washing lotion is taken off, and is evaporated under reduced pressure and is concentrated into no ethyl alcohol, plant extraction liquid is obtained, takes four fourth of 10g metatitanic acids
Ester is added in 100g plant extraction liquids, is stirred 20min with 300r/min, is stood 2h, obtain plant mixed liquor, take the 1kg rabbit hairs, uses
Deionized water washes clean is simultaneously fitted into baking oven, the dry 2h at 50 DEG C, then is transferred in pulverizer and is crushed to broken section of 1mm,
The rabbit hair is added in into 10kg mass fractions as in 2% sodium hydroxide solution, under 80 DEG C of waters bath with thermostatic control, reaction 3h, filtering must filter for broken section
Liquid obtains rabbit hair keratin solution, and 100g plants mixed liquor is added dropwise to 1g/min in 200g rabbit hair keratin solutions, with
200r/min, which is continued stirring until, to be added dropwise, and adds 5g sodium chloride, 30g butanediols, 50g glycerine, 0.5g xanthans, at 70 DEG C
Under continue to stir 30min, obtain A phases, take 3g Arlacel-60s, 25g dimethyl silicone polymers, 150g atoleines, 100g carbonic acid two is pungent
Ester, 15g beeswaxs stir 20min with 300r/min at 70 DEG C, obtain B phases, A is added in B phases, with 3000r/min homogenized milks
Change 20min, 40 DEG C are cooled to after emulsification, adds 5g preservatives, 0.5g essence stirs evenly rear vacuum defoamation, obtains institute
It states plant base light and repairs suncream.
Example 2
It is crushed being fitted into after scutellaria naturally dry in micronizer, crosses 300 mesh sieves, obtain scutellaria powder, combined-ear chrysanthemum is dried in the air naturally
It is fitted into micronizer and crushes after dry, cross 300 mesh sieves, obtain combined-ear chrysanthemum powder, ultra micro will be packed into after Antarctic ice microalgae naturally dry
It is crushed in pulverizer, crosses 300 mesh sieves, obtain Antarctic ice microalgae powder, take 150g scutellaria powder, 150g combined-ear chrysanthemum powder, 75g Antarctic Ices
Algae powder adds in 1L mass fractions as in 70% ethanol solution, heating and refluxing extraction 2h, obtains crude extract at 70 DEG C, by crude extract
Vacuum distillation be concentrated into no ethyl alcohol, and pass through macroporous resin column be adsorbed to it is colourless, then with mass fraction be 50% ethanol solution wash
, collection ethanol eluate colourless to washing lotion is taken off, and is evaporated under reduced pressure and is concentrated into no ethyl alcohol, plant extraction liquid is obtained, takes four fourth of 15g metatitanic acids
Ester is added in 150g plant extraction liquids, is stirred 25min with 350r/min, is stood 2h, obtain plant mixed liquor, take the 1kg rabbit hairs, uses
Deionized water washes clean is simultaneously fitted into baking oven, the dry 2h at 52 DEG C, then is transferred in pulverizer and is crushed to broken section of 3mm,
The rabbit hair is added in into 15kg mass fractions as in 2% sodium hydroxide solution, under 82 DEG C of waters bath with thermostatic control, reaction 4h, filtering must filter for broken section
Liquid obtains rabbit hair keratin solution, and 150g plants mixed liquor is added dropwise to 2g/min in 300g rabbit hair keratin solutions, with
250r/min, which is continued stirring until, to be added dropwise, and adds 6g sodium chloride, 35g butanediols, 65g glycerine, 0.65g xanthans, 75
Continue to stir 35min at DEG C, obtain A phases, take 4g Arlacel-60s, 27g dimethyl silicone polymers, 175g atoleines, 125g carbonic acid two
Monooctyl ester, 17g beeswaxs stir 25min with 350r/min at 75 DEG C, obtain B phases, A is added in B phases, with 3500r/min homogeneous
25min is emulsified, 45 DEG C are cooled to after emulsification, adds 7g preservatives, 0.65g essence stirs evenly rear vacuum defoamation, obtains
The plant base light repairs suncream.
Example 3
It is crushed being fitted into after scutellaria naturally dry in micronizer, crosses 300 mesh sieves, obtain scutellaria powder, combined-ear chrysanthemum is dried in the air naturally
It is fitted into micronizer and crushes after dry, cross 300 mesh sieves, obtain combined-ear chrysanthemum powder, ultra micro will be packed into after Antarctic ice microalgae naturally dry
It is crushed in pulverizer, crosses 300 mesh sieves, obtain Antarctic ice microalgae powder, take 200g scutellaria powder, 200g combined-ear chrysanthemum powder, the 100g South Pole
Ice algae powder adds in 2L mass fractions as in 70% ethanol solution, heating and refluxing extraction 3h, obtains crude extract at 80 DEG C, will slightly carry
Liquid vacuum distillation be concentrated into no ethyl alcohol, and pass through macroporous resin column be adsorbed to it is colourless, then with mass fraction be 50% ethanol solution
It is colourless to be eluted to washing lotion, collects ethanol eluate, and is evaporated under reduced pressure and is concentrated into no ethyl alcohol, obtains plant extraction liquid, takes 20g metatitanic acids four
Butyl ester is added in 200g plant extraction liquids, is stirred 30min with 400r/min, is stood 3h, obtain plant mixed liquor, take the 2kg rabbit hairs,
It is washed with deionized clean and is fitted into baking oven, the dry 3h at 55 DEG C, then it is transferred in pulverizer that be crushed to 5mm broken
The rabbit hair is added in 20kg mass fractions as in 2% sodium hydroxide solution, under 85 DEG C of waters bath with thermostatic control, reaction 5h is filtered for broken section by section
Filtrate is obtained, rabbit hair keratin solution is obtained, 200g plants mixed liquor is added dropwise to 2g/min in 400g rabbit hair keratin solutions, with
300r/min, which is continued stirring until, to be added dropwise, and adds 8g sodium chloride, 40g butanediols, 80g glycerine, 0.8g xanthans, at 80 DEG C
Under continue to stir 40min, obtain A phases, take 5g Arlacel-60s, 30g dimethyl silicone polymers, 200g atoleines, 150g carbonic acid two is pungent
Ester, 20g beeswaxs stir 30min with 400r/min at 80 DEG C, obtain B phases, A is added in B phases, with 4000r/min homogenized milks
Change 30min, 50 DEG C are cooled to after emulsification, adds 8g preservatives, 0.8g essence stirs evenly rear vacuum defoamation, obtains institute
It states plant base light and repairs suncream.
Plant base light prepared by the present invention repairs suncream and the suncream of Guangdong company production is detected, specifically
Testing result such as following table table 1：
1 plant base light of table repairs suncream performance characterization
| Performance characterization | Example 1 | Example 2 | Example 3 | Comparative example |
| SPF measured values | 31.31 | 33.26 | 35.96 | 18.44 |
| Prevent tanned coefficient | PA++ | PA+++ | PA+++ | PA+ |
| UVB light transmittances | 2.5 | 2.3 | 2.2 | 10.3 |
| UVA light transmittances | 9.8 | 8.9 | 8.6 | 30.3 |
| Whether lotion occurs agglomeration | It is no | It is no | It is no | Slight caking, agglomeration |
The plant base light that as shown in Table 1 prepared by the present invention repairs suncream, prevents that tanned index is high, light transmittance is low, will not roll into a ball
Poly- phenomenon will not block pore, have fabulous sun-proof performance.
Claims (8)
1. a kind of plant base light repairs suncream, which is characterized in that including following weight parts raw material：
100~200 portions of plant mixed liquors, 200~400 parts of rabbit hair keratin solutions, 5~8 parts of sodium chloride, 30~40 parts of fourths two
Alcohol, 50~80 parts of glycerine, 0.5~0.8 part of xanthans, 3~5 parts of Arlacel-60s, 25~30 parts of dimethyl silicone polymers, 150~
200 parts of atoleines, 100~150 parts of carbonic acid dioctyl esters, 15~20 parts of beeswaxs, 5~8 portions of preservatives, 0.5~0.8 part of essence.
2. a kind of plant base light as described in claim 1 repairs suncream, which is characterized in that the plant mixed liquor for 10~
20 parts by weight butyl titanates mix standing with 100~200 parts by weight plant extraction liquids and are made.
3. a kind of plant base light as claimed in claim 2 repairs suncream, which is characterized in that the plant extraction liquid is scutellaria
Powder, combined-ear chrysanthemum powder, Antarctic ice microalgae powder add in mass fraction as heating and refluxing extraction in 70% ethanol solution, and depressurize steaming
Evaporate concentration, then by macroporous resin column be adsorbed to it is colourless after eluted with ethanol solution, collect ethanol eluate, and be evaporated under reduced pressure dense
No ethyl alcohol is reduced to be made.
4. a kind of plant base light as claimed in claim 3 repairs suncream, which is characterized in that the scutellaria powder, combined-ear chrysanthemum
Powder, Antarctic ice microalgae powder, the parts by weight of ethanol solution is 100~200 parts of scutellaria powder, 100~200 parts of combined-ear chrysanthemum powder,
50~100 parts of Antarctic ice microalgae powder, 1000~2000 parts of ethanol solutions.
5. a kind of plant base light as described in claim 1 repairs suncream, which is characterized in that the rabbit hair keratin solution is
Mass fraction is dissolved in after rabbit hair drying and crushing to be made in 2% sodium hydroxide solution.
6. a kind of plant base light as claimed in claim 5 repairs suncream, which is characterized in that the rabbit hair and sodium hydroxide are molten
The mass ratio of liquid is 1：5~1：20.
7. a kind of plant base light as described in claim 1 repairs suncream, which is characterized in that the preservative is Metagin
Any one in ester, propylben.
8. a kind of plant base light as described in claim 1~7 any one repairs the preparation method of suncream, feature exists
In concretely comprising the following steps：
（1）It is crushed being fitted into after scutellaria naturally dry in micronizer, crosses 300 mesh sieves, obtain scutellaria powder；
（2）It is crushed being fitted into after combined-ear chrysanthemum naturally dry in micronizer, crosses 300 mesh sieves, obtain combined-ear chrysanthemum powder；
（3）It is crushed being fitted into after Antarctic ice microalgae naturally dry in micronizer, crosses 300 mesh sieves, obtain Antarctic ice microalgae powder；
（4）Scutellaria powder, combined-ear chrysanthemum powder, Antarctic ice microalgae powder are taken, adds in ethanol solution, is heated to reflux at 60~80 DEG C
2~3h is extracted, obtains crude extract；
（5）Crude extract vacuum distillation is concentrated into no ethyl alcohol, and passes through macroporous resin column and is adsorbed to colourless, then is with mass fraction
It is colourless that 50% ethanol solution is eluted to washing lotion, collects ethanol eluate, and is evaporated under reduced pressure and is concentrated into no ethyl alcohol, obtains plant extract
Liquid；
（6）Butyl titanate is taken, adds in plant extraction liquid and 2~3h is stood after stirring evenly, obtain plant mixed liquor；
（7）It will be crushed after rabbit hair washing and drying, be re-dissolved in sodium hydroxide solution, obtain rabbit hair keratin solution；
（8）Plant mixed liquor is added dropwise in rabbit hair keratin solution, adds sodium chloride, butanediol, glycerine, xanthans,
30~40min is stirred at 70~80 DEG C, obtains A phases；
（9）Take Arlacel-60, dimethyl silicone polymer, atoleine, carbonic acid dioctyl ester, beeswax, at 70~80 DEG C stir 20~
30min obtains B phases；
（10）A is added in B phases, with 3000~4000r/min, 20~30min of emulsifying, 40 are cooled to after emulsification
~50 DEG C, preservative, essence are added, stirs evenly rear vacuum defoamation, plant base light is obtained and repairs suncream.
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Application publication date: 20180601 |