CN105078830B - A kind of natural anticorrosion children herbal sun-screening lotion and preparation method thereof - Google Patents
A kind of natural anticorrosion children herbal sun-screening lotion and preparation method thereof Download PDFInfo
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Abstract
The invention belongs to daily nursing product technical field, discloses a kind of natural anticorrosion children herbal sun-screening lotion and preparation method thereof.The sunscreen of the present invention is by cetyl glucoside, monoglyceride, C16~18Alcohol, 26# white oils, methyl-silicone oil, disodium edta, glycerine, propane diols, carbomer, allantoin, xanthan gum, triethanolamine, D panthenols, extract solution from aloe, extract solution of bamboo leaves, Lotus Leaf Extracts, American aloe extract and deionization are prepared.The product of the present invention is used as sun-proof component and preservative component by adding plant extraction liquid, can avoid the use of chemical synthesis sun-screening agent and preservative, reduce the irritation of product, improve the security of product, is formulated available for children.
Description
Technical field
The invention belongs to daily nursing product technical field, and in particular to a kind of natural anticorrosion children herbal sun-screening lotion and its system
Preparation Method.
Background technology
Compared with adult, child skin is structurally and functionally having huge difference, including：1) child skin
Thin, soft, the outer layer cuticula of its skin is cell monolayer, lacks hyaline layer；2) child skin water content is high, but due to skin
Barrier function is extremely low, and the fluid loss of skin is also larger；3) melanin content of child skin is low, and uvea is thin, and light sensitivity is high, purple
Outside line resilience is poor, is easily burnt by ultraviolet radiation.In addition, the outdoor activities time of children is longer, ultraviolet radiation accumulation
Amount increases therewith.Therefore more and more families are become using the cosmetics of sun-proof class to resist injury of the ultraviolet to child skin
Long selection, the development ＆ production of children sunscreen cosmetics also become one of hot spot of cosmetics development ＆ production.
Harmful ultraviolet radiation is can effectively prevent using sun care preparations, including skin tanning is easily led to, is made
Into DNA Damage and then trigger the UVB radiation (wavelength is 290~320nm) of cutaneum carcinoma and accelerate the actinic aging of skin
UVA radiation (wavelength is 320~400nm).At present, in the market children sunscreen class cosmetics are dazzling, and master is played in product formula
Wanting the component of sun-proof result substantially has two kinds of physical ultraviolet light screener and chemical type ultraviolet absorber, wherein physical sun-screening agent
Mainly have zinc oxide and titanium dioxide, chemical sun mainly have Octyl methoxycinnamate, benzophenone derivates and
Anthranilate class etc..In recent years, related component of sun triggers allergic dermatitis, irritant contact dermatitis and connect
The report for touching the adverse reactions such as property nettle rash emerges in an endless stream, and largely uses inorganic powder sun-screening agent in some products, causes skin
Clogging of pores, causes a skin inflammation, the reaction of the cutaneous lesions such as abscess, and many sunscreen products are come by using chemical synthesis sun-screening agent
SPF SPF (Sun Protection Factor) values and PA (Protection Anti UVA) value, but this is substantially improved
Class sun-screening agent photostability is poor, easy illumination or oxidative degradation, and then causes skin allergy, redness and inflammation.The skin of children is thin,
It is soft, easily stimulate and easy allergy, therefore in the formula design of children sunscreen cosmetics and during preparing, should select safety,
Gentle and efficient sun-screening agent, avoids using the strong chemical synthesis type sun-screening agent of irritation as far as possible.
In cosmetic formulations, reasonable employment preservative, which can make cosmetics reach the expected shelf-life, can simultaneously suppress to make up
In product may caused by microbial reproduction and consumer's secondary pollution when in use, but chemical synthesis preservative is but to occupy the
Two anaphylactogen for causing cutaneous anaphylaxis.The skin of children is thin, soft, to external irritant neurological susceptibility, therefore in children
It should be reduced to the greatest extent in cosmetic formulations and use or without using chemical synthesis preservative, reduce cosmetics for children in use
The stimulation produced to child skin.
The content of the invention
The shortcomings that in order to solve the above prior art and shortcoming, primary and foremost purpose of the invention are to provide a kind of natural
Anti-corrosion children's herbal sun-screening lotion.
Another object of the present invention is to provide a kind of preparation method of above-mentioned natural anticorrosion children herbal sun-screening lotion.
The object of the invention is achieved through the following technical solutions：
A kind of natural anticorrosion children herbal sun-screening lotion, is prepared by the component of following mass percentage：
The preparation method of above-mentioned natural anticorrosion children herbal sun-screening lotion, including following preparation process：
(1) by cetyl glucoside, monoglyceride, C16~18Heating stirring is molten after alcohol, 26# white oils and methyl-silicone oil mixing
Solution, is A phases；
(2) disodium edta, glycerine, propane diols, carbomer, allantoin, xanthan gum and deionized water are mixed
Heating stirring dissolves afterwards, is B1Phase；
(3) extract solution from aloe, extract solution of bamboo leaves and Lotus Leaf Extracts room temperature are mixed, is C1Phase；
(4) by B1It is added in A phases, homogeneous is uniformly mixed to obtain mixed liquor；
(5) by C1It is added in the mixed liquor of step (4), is defoamed after homogeneous, when stirring is cooled to 40~55 DEG C, by three
Monoethanolamine and D-pantothenyl aleohol are as B2Phase, American aloe extract is as C2It is added to, discharges after continuing stirring to room temperature, obtains natural
Anti-corrosion children's herbal sun-screening lotion.
Preferably, the heating stirring dissolving described in step (1) refers to be heated to 80~95 DEG C of stirring and dissolvings.
Preferably, the heating stirring dissolving described in step (2) refers to be heated to 85~95 DEG C of stirring and dissolvings.
Preferably, the homogeneous described in step (4) refers to the homogeneous 2~3 on 5000~10000 revs/min of homogenizer
Minute.
Preferably, after the homogeneous described in step (5) defoaming refer to homogeneous 2~after five minutes at 70~80 DEG C defoaming 3~
5 minutes.
Preferably, the stirring cooling described in step (5) refers to stir on 3000~5000 revs/min of mixer cold
But.
Preferably, the extract solution from aloe is prepared by the following method：Take dry aloe crust powder, add 10~
The Extraction solvent of 40 times of quality, the selected as mass fraction of solvent is 20%~60% ethanol solution, in 25~55 DEG C of temperature
Lower progress ultrasonic extraction 20~40 minutes, takes filtrate after fully being filtered with organic filter paper of 0.22nm specifications, filtrate is being rotated
0.2~0.3 times is concentrated in evaporimeter, then vacuum drying obtains fluffy solid at a temperature of 45~55 DEG C, pulverizes
The deionized water dissolving of 5~10 times of quality is added afterwards, obtains extract solution from aloe.
The anthraquinone analog compounds such as barbaloin that the extract solution from aloe that is extracted from aloe skin of the present invention contains, aloe-emodin
Can effective ultraviolet radiation-absorbing, slow down damage of the ultraviolet to skin.Effective sun-prevention component tool in extract solution from aloe
Have that sun-proof section is big, the advantages such as safe and sensitization is low, some of which component also has the function that disinfection.Lotus
Leaf, the leaf of bamboo are common plant leaf blades, its extracting solution possesses the effect of significantly restraining and sterilizing bacteria, common in being detected to cosmetics
Pathogenic bacteria such as Escherichia coli, staphylococcus aureus and fungi etc. have strong inhibitory action.American aloe extracting solution is a kind of
Naturally, gentle antiallergic extract, the high pure natural substance of several securities is mixed in proportion as natural antiseptic agent more than
Close addition to enter in cosmetics for children formula, not only ensure that the anti-corrosion effect in cosmetics for children formula, and reduce and match somebody with somebody
Stimulation of the square additive to child skin.
The present invention preparation method and obtained product has the following advantages that and beneficial effect：
(1) at present children sunscreen product on the market it is most of using add chemical synthesis sun-screening agent as it is effective it is sun-proof into
Point, this often easily causes the safety problems such as child skin allergy, inflammation；The present invention is used as natural sun-screening agent using extract solution from aloe
It instead of chemical synthesis sun-screening agent, the component design and product being prepared into does not stimulate gently, it is anti-to be that a suitable children use
Shine skin care item；The Multiple components such as the barbaloin that contains in the extract solution from aloe that the present invention uses, aloe-emodin, which are respectively provided with, to be resisted
The ability of ultraviolet radiation, the compounding of a variety of natural sun-prevention components can the significantly more efficient injury for resisting a variety of ultraviolets；This
The polysaccharide component contained in outer extract solution from aloe is a kind of natural moisture preserving agent and thickener well, not only increases the guarantor of product
Wet, moisture absorption effect, also reduces the cost of product；
(2) there is pharmacological effect, the wherein lotus leaf such as anti-inflammatory, antibacterial to carry for the lotus leaf that uses and bamboo extractive in the present invention
The lotus flavone component contained in liquid is taken to have very strong inhibition, bamboo to enteropathogenic E. Coli and staphylococcus aureus etc.
The components such as the bamboo-leaves flavones and alkaloid that contain in leaf extract have significantly inhibition to bacterium, saccharomycete and mould etc.,
The two is substituted into traditional chemical synthesis preservative into the antibacterial natural antiseptic agent of multiple-effect according to corresponding proportioning hybrid modulation, is made
The standby children's herbal sun-screening lotion formed has the security of higher；
(3) because it contains saponins material in American aloe extracting solution, so living with the good biology such as anti-inflammatory, antiallergic
Property, it with the addition of the extract in the present invention product double shielding barrier formd to user, not only greatly reduce
The risk of issuable skin allergy, can also act synergistically with lotus leaf and bamboo extractive when virgin user uses, into
One step improves the antibacterial bacteriostatic system of product；
(4) selection of the other compositions in inventive formulation, addition and preparation process can ensure the plant of the present invention
The stability of thing extract in formula, and its function can be given full play to.
Brief description of the drawings
Fig. 1 is the extract solution from aloe sun-prevention component absorbance change curve that various extracting conditions obtain in embodiment 1~3
Figure；
The UV, visible light spectrophotometric spectra figure of the children sunscreen breast of different plant extraction liquid additive amounts in Fig. 2 embodiments 4~6.
Embodiment
With reference to embodiment and attached drawing, the present invention is described in further detail, but embodiments of the present invention are unlimited
In this.
Embodiment 1
The aloe crust powder of the drying of 6g is taken, adds the Extraction solvent of 30 times of quality, the selection mass fraction point of solvent
Not Wei 20%, 30%, 40%, 50% and 60% ethanol solution, ultrasonic extraction 30 minutes left sides are carried out at a temperature of 25 DEG C ± 3 DEG C
The right side, takes filtrate after fully being filtered with organic filter paper of 0.22nm specifications, filtrate is concentrated to 0.3 times in Rotary Evaporators, turns
In the vacuum drying chamber moved on under the conditions of 55 DEG C it is dry after obtain fluffy solid, added after pulverizing 5 times of quality go from
Sub- water dissolving, it is spare to obtain extract solution from aloe.It with absolute ethyl alcohol constant volume is 5ml to take 1.5ml extract solution from aloe, takes 1ml dilutions
With deionized water constant volume it is 10ml after being reacted 30 minutes with 2% magnesium acetate methanol solutions of 1ml.With 1cm cuvettes, with volume ratio
For deionized water：Methanol=9:1 mixed liquor surveys its front and rear absorbance difference at 420nm of reaction, its absorbance for reference
Relative intensity is as shown in Figure 1 with the change curve of concentration of alcohol.It is bent according to the concentration absorption standard of Fig. 1 and barbaloin standard items
Line compares, and it is 100mg/g that the extract solution from aloe sun-prevention component content that 30% concentration of alcohol extracts, which can be calculated,.
Embodiment 2
The aloe crust powder of the drying of 6g is taken, adds the Extraction solvent of 30 times of quality, the second of the selected as 60% of solvent
Alcoholic solution, carries out ultrasonic extraction 30 minutes or so, with 0.22nm specifications at a temperature of 25 DEG C, 35 DEG C, 45 DEG C and 55 DEG C
Organic filter paper takes filtrate after fully filtering, and filtrate is concentrated to 0.3 times in Rotary Evaporators, is transferred to true under the conditions of 55 DEG C
Fluffy solid is obtained after drying in empty drying box, the deionized water dissolving of 5 times of quality is added after pulverizing, aloe is obtained and carries
Take liquid spare.It with absolute ethyl alcohol constant volume is 5ml to take 1.5ml extract solution from aloe, takes 1ml dilutions and 2% magnesium acetate methanol of 1ml
Solution reaction was 10ml with deionized water constant volume after 30 minutes.With 1cm cuvettes, using volume ratio as deionized water：Methanol=9:1
Mixed liquor survey its front and rear absorbance difference at 420nm of reaction for reference, its absorbance relative intensity is with Extracting temperature
Change curve is as shown in Figure 1.According to Fig. 1 compared with the concentration absorption standard curve of barbaloin standard items, 45 can be calculated
The extract solution from aloe sun-prevention component content extracted at a temperature of DEG C is 65mg/g.
Embodiment 3
The aloe crust powder of the drying of 6g is taken, is separately added into the Extraction solvent of 10 times, 20 times, 30 times and 40 times quality,
The ethanol solution of the selected as 40% of solvent, ultrasonic extraction 30 minutes or so is carried out at a temperature of 45 DEG C ± 3 DEG C, is advised with 0.22nm
Organic filter paper of lattice takes filtrate after fully filtering, and filtrate is concentrated to 0.3 times in Rotary Evaporators, is transferred under the conditions of 55 DEG C
Vacuum drying chamber in it is dry after obtain fluffy solid, the deionized water dissolving of 5 times of quality is added after pulverizing, obtains reed
Luxuriant growth extracting solution is spare.It with absolute ethyl alcohol constant volume is 5ml to take 1.5ml extract solution from aloe, takes 1ml dilutions and 2% magnesium acetates of 1ml
Methanol solution with deionized water constant volume is 10ml after reacting 30 minutes.With 1cm cuvettes, using volume ratio as deionized water：Methanol
=9:1 mixed liquor surveys its front and rear absorbance difference at 420nm of reaction for reference, its absorbance relative intensity is with extraction temperature
The change curve of degree is as shown in Figure 1.According to Fig. 1 compared with the concentration absorption standard curve of barbaloin standard items, it can calculate
It is 169mg/g to go out the extract solution from aloe sun-prevention component content that 10 times of Extraction solvents extract.
It can be seen that from Fig. 1 results：The recovery rate of sun-prevention component is mainly by the concentration of alcohol solvent, extraction in aloe crust
Temperature and solid-liquid ratio three are adjusted, improve the concentration of Extraction solvent in certain scope and Extracting temperature can improve effectively into
The recovery rate divided, but can decline therewith again after reaching extreme value.In extraction process, since solvent is excessive, increase solid-liquid ratio is certain
Equivalent to diluted effect in degree, therefore increase solid-liquid ratio reduces the recovery rate of active ingredient on the contrary.
Embodiment 4
As mass fraction, by cetyl glucoside 1.5%, monoglyceride 1%, C16-18Alcohol 2%, 26# white oils 8% and first
Base silicone oil 2.5% is heated to 90 DEG C of stirring and dissolvings after mixing, and is kept the temperature as A phases raw material spare.By disodium edta
0.02%th, glycerine 7%, propane diols 2%, carbomer 10%, allantoin 0.1%, xanthan gum 0.1%, deionized water 30% mix
90 DEG C or so stirring and dissolvings are heated to, as B1The insulation of phase raw material is spare.Treat A phases and B1When phase temperature is roughly the same, by B1Xiang Yuan
Material diameter is directly poured into A phases, then homogeneous 2 minutes on the homogenizer that condition is 6000 revs/min.By extract solution from aloe 15%
C is used as after (sun-prevention component content is about 0.5g), extract solution of bamboo leaves 2.5% and the mixing of 2.5% room temperature of Lotus Leaf Extracts1Phase raw material
Pour into straight in mixed liquor, add deionized water to continue homogeneous after reaching 97.6% to entirety and defoam 3 points after 3 minutes at 75 DEG C
Clock, is then transferred on the mixer that condition is 3500 revs/min and stirs cooling.When cooling temperature is to 40 DEG C, by triethanolamine
0.2% and D-pantothenyl aleohol 2% be used as B2Phase, American aloe extract 0.2% are used as C2It is added to, discharges, obtain after continuing stirring to room temperature
To natural anticorrosion children's herbal sun-screening lotion of the present embodiment.It is detected using Shimadzu UV-1780 ultraviolet-uisible spectrophotometers,
With 1cm cuvettes in the range of 290~400nm, with anhydrous ether：Absolute ethyl alcohol=1:To survey its saturating for reference for 1 mixed solvent
Rate is penetrated, experimental result carries out sun-proof result evaluation as shown in the sample 1 of Fig. 2, to the product of preparation, and what be can be calculated resists UVB
The SPF indexes of radiation are about：10, the PA indexes for resisting UVA radiation are about：+.
Embodiment 5
As mass fraction, by cetyl glucoside 1.5%, monoglyceride 1%, C16-18Alcohol 2%, 26# white oils 8% and first
Base silicone oil 2.5% is heated to 90 DEG C of stirring and dissolvings after mixing, and is kept the temperature as A phases raw material spare.By disodium edta
0.02%th, glycerine 7%, propane diols 2%, carbomer 10%, allantoin 0.1%, xanthan gum 0.1%, deionized water 30% mix
90 DEG C or so stirring and dissolvings are heated to, as B1The insulation of phase raw material is spare.Treat A phases and B1When phase temperature is roughly the same, by B1Xiang Yuan
Material diameter is directly poured into A phases, then homogeneous 2 minutes on the homogenizer that condition is 6000 revs/min.By extract solution from aloe 25%
C is used as after (sun-prevention component content is about 0.8g), extract solution of bamboo leaves 3% and the mixing of 2% room temperature of Lotus Leaf Extracts1Phase raw material is straight
Pour into mixed liquor, add deionized water to it is overall reach 97.6% after continue homogeneous 3 minutes after defoam 3 minutes at 75 DEG C, so
It is transferred to afterwards on the mixer that condition is 3500 revs/min and stirs cooling.When cooling temperature is to 40 DEG C, by triethanolamine 0.2%
B is used as with D-pantothenyl aleohol 2%2Phase, American aloe extract 0.2% are used as C2It is added to, discharges after continuing stirring to room temperature, obtains this
Natural anticorrosion children's herbal sun-screening lotion of embodiment.It is detected, is used using Shimadzu UV-1780 ultraviolet-uisible spectrophotometers
1cm cuvettes are in the range of 290~400nm, with anhydrous ether：Absolute ethyl alcohol=1:1 mixed solvent surveys its transmission for reference
Rate, experimental result carry out sun-proof result evaluation as shown in the sample 2 of Fig. 2, to the product of preparation, and what be can be calculated resists UVB spokes
The SPF indexes penetrated are about：12, the PA indexes for resisting UVA radiation are about：++.
Embodiment 6
As mass fraction, by cetyl glucoside 1.5%, monoglyceride 1%, C16-18Alcohol 2%, 26# white oils 8% and first
Base silicone oil 2.5% is heated to 90 DEG C of stirring and dissolvings after mixing, and is kept the temperature as A phases raw material spare.By disodium edta
0.02%th, glycerine 7%, propane diols 2%, carbomer 10%, allantoin 0.1%, xanthan gum 0.1%, deionized water 30% mix
90 DEG C or so stirring and dissolvings are heated to, as B1The insulation of phase raw material is spare.Treat A phases and B1When phase temperature is roughly the same, by B1Xiang Yuan
Material diameter is directly poured into A phases, then homogeneous 2 minutes on the homogenizer that condition is 6000 revs/min.By extract solution from aloe 40%
C is used as after (sun-prevention component content is about 1.3g), extract solution of bamboo leaves 3% and the mixing of 2% room temperature of Lotus Leaf Extracts1Phase raw material is straight
Pour into mixed liquor, add deionized water to it is overall reach 97.6% after continue homogeneous 3 minutes after defoam 3 minutes at 75 DEG C, so
It is transferred to afterwards on the mixer that condition is 3500 revs/min and stirs cooling.When cooling temperature is to 40 DEG C, by triethanolamine 0.2%
B is used as with D-pantothenyl aleohol 2%2Phase, American aloe extract 0.2% are used as C2It is added to, discharges after continuing stirring to room temperature, obtains this
Natural anticorrosion children's herbal sun-screening lotion of embodiment.It is detected, is used using Shimadzu UV-1780 ultraviolet-uisible spectrophotometers
1cm cuvettes are in the range of 290~400nm, with anhydrous ether：Absolute ethyl alcohol=1:1 mixed solvent surveys its transmission for reference
Rate, experimental result carry out sun-proof result evaluation as shown in the sample 3 of Fig. 2, to the product of preparation, and what be can be calculated resists UVB spokes
The SPF indexes penetrated are about：30, the PA indexes for resisting UVA radiation are about：+++.
As can be seen from the above results：With the dosage increase of extract solution from aloe, the children sunscreen breast being prepared is prevented
Index is shone linearly to rise.UVA radiation is to suffer from one of main inducing of malignant mela noma, from experimental result it can be seen that preparing
Product resist UVA radiation ability increasing degree it is larger, therefore children's plant sun of the present invention can be effectively protected
The tender skin of children.
Above-described embodiment is the preferable embodiment of the present invention, but embodiments of the present invention and from above-described embodiment
Limitation, other any Spirit Essences without departing from the present invention with made under principle change, modification, replacement, combine, simplification,
Equivalent substitute mode is should be, is included within protection scope of the present invention.
Claims (5)
- A kind of 1. natural anticorrosion children herbal sun-screening lotion, it is characterised in that：It is prepared by the component of following mass percentage：The method of the preparation includes following preparation process：(1) by cetyl glucoside, monoglyceride, C16~18Heating stirring dissolves after alcohol, 26# white oils and methyl-silicone oil mixing, is A Phase；(2) add after mixing disodium edta, glycerine, propane diols, carbomer, allantoin, xanthan gum and deionized water Thermal agitation is dissolved, and is B1Phase；(3) extract solution from aloe, extract solution of bamboo leaves and Lotus Leaf Extracts room temperature are mixed, is C1Phase；(4) by B1It is added in A phases, homogeneous is uniformly mixed to obtain mixed liquor；(5) by C1It is added in the mixed liquor of step (4), is defoamed after homogeneous, when stirring is cooled to 40~55 DEG C, by three ethanol Amine and D-pantothenyl aleohol are as B2Phase, American aloe extract is as C2It is added to, discharges after continuing stirring to room temperature, obtain natural anticorrosion Children's herbal sun-screening lotion.
- A kind of 2. natural anticorrosion children herbal sun-screening lotion according to claim 1, it is characterised in that：Described in step (1) Heating stirring dissolving refer to be heated to 80~95 DEG C of stirring and dissolvings；Heating stirring dissolving described in step (2) refers to heat To 85~95 DEG C of stirring and dissolvings.
- A kind of 3. natural anticorrosion children herbal sun-screening lotion according to claim 1, it is characterised in that：Described in step (4) Homogeneous refer to homogeneous 2~3 minutes on 5000~10000 revs/min of homogenizer.
- A kind of 4. natural anticorrosion children herbal sun-screening lotion according to claim 1, it is characterised in that：Described in step (5) Homogeneous after defoaming refer to homogeneous 2~defoamed 3~5 minutes at 70~80 DEG C after five minutes；The stirring cooling refers to Cooling is stirred on 3000~5000 revs/min of mixer.
- A kind of 5. natural anticorrosion children herbal sun-screening lotion according to claim 1, it is characterised in that：The aloe extraction Liquid is prepared by the following method：Dry aloe crust powder is taken, adds the Extraction solvent of 10~40 times of quality, the selection of solvent The ethanol solution for being 20%~60% for mass fraction, carries out ultrasonic extraction 20~40 minutes at a temperature of 25~55 DEG C, uses Organic filter paper of 0.22nm specifications takes filtrate after fully filtering, and filtrate is concentrated to 0.2~0.3 times in Rotary Evaporators, so Vacuum drying obtains fluffy solid at a temperature of 45~55 DEG C afterwards, and the deionized water of 5~10 times of quality is added after pulverizing Dissolving, obtains extract solution from aloe.
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| CN105411926A (en) * | 2015-12-03 | 2016-03-23 | 青蛙王子(中国)日化有限公司 | Skin-tendering essence rich in anthocyanin and preparation method of skin-tendering essence |
| CN107898734B (en) * | 2018-01-04 | 2021-08-31 | 上海紫邦生物医药有限公司 | Application of agave extract in preparing external itching-relieving and moisturizing personal care product |
| CN112972326B (en) * | 2021-02-24 | 2023-04-28 | 江西建昌帮食疗科技有限公司 | Sun-screening emulsion for pregnant and lying-in women and preparation method thereof |
| CN112999112B (en) * | 2021-02-26 | 2023-08-01 | 上海家化联合股份有限公司 | Sunscreen compositions for reducing transdermal penetration of sunscreens |
| CN116421559B (en) * | 2023-03-01 | 2023-11-17 | 杭州百诚医药科技股份有限公司 | Stable simethicone emulsion and preparation method thereof |
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