CN108095191A - A kind of tobacco plug plasticizer and its application - Google Patents

A kind of tobacco plug plasticizer and its application Download PDF

Info

Publication number
CN108095191A
CN108095191A CN201711105477.6A CN201711105477A CN108095191A CN 108095191 A CN108095191 A CN 108095191A CN 201711105477 A CN201711105477 A CN 201711105477A CN 108095191 A CN108095191 A CN 108095191A
Authority
CN
China
Prior art keywords
plasticizer
tobacco plug
triacetyl glycerine
cigarette
present
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711105477.6A
Other languages
Chinese (zh)
Inventor
刘惠芳
张月华
张健
寇智岭
张柳枝
杨恒
陈洁
王颖
郭书裴
张希瑶
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Tobacco Henan Industrial Co Ltd
Original Assignee
China Tobacco Henan Industrial Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Tobacco Henan Industrial Co Ltd filed Critical China Tobacco Henan Industrial Co Ltd
Priority to CN201711105477.6A priority Critical patent/CN108095191A/en
Publication of CN108095191A publication Critical patent/CN108095191A/en
Pending legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/06Use of materials for tobacco smoke filters
    • A24D3/08Use of materials for tobacco smoke filters of organic materials as carrier or major constituent
    • A24D3/10Use of materials for tobacco smoke filters of organic materials as carrier or major constituent of cellulose or cellulose derivatives
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/06Use of materials for tobacco smoke filters
    • A24D3/14Use of materials for tobacco smoke filters of organic materials as additive

Abstract

The present invention relates to a kind of tobacco plug plasticizer, the tobacco plug plasticizer is by triacetyl glycerine and triethyl citrate in mass ratio 0~1:3 compounding compositions.The present invention substitutes triacetyl glycerine as plasticizer using triethyl citrate, or both compounding use as filter stick plasticizer, plasticizer of the present invention is pollution-free, at low cost, to bond plasticization effect extremely strong.Find, which reduce environmental pollution, reduce production cost that there is preferable social and economic benefit in practical applications.

Description

A kind of tobacco plug plasticizer and its application
Technical field
The invention belongs to tobacco leaf production processing technique fields, and in particular to a kind of tobacco plug plasticizer mainly should For cigarette filter tip shaping enterprise.
Background technology
Cigarette filter stick(Filter stick)Filter medium generally all using acetate fiber, must in its molding process Suitable bonding plasticizer must be added in, makes dissolving bonding effect of bulk, the soft acetate fiber surface through bonding plasticizer, into Type is the round filter stick with appropriate hardness, to ensure in cigarette connection filter stick processing and aspiration procedure, does not generate distortion, wrinkle Folding, deformation, preferably adsorb harmful substances in flue gas so as to fulfill filter stick and rejection effect.
But the existing filter stick for cigarettes plasticizer used, have that synthesis cost is higher, and seriously polluted, corrosivity is strong, bonding The shortcomings of plasticization effect is bad.The plasticizer used in cigarette filter rod is mainly triacetyl glycerine at present, due to its higher price, Cigarette cost is added, while the mono ethyl ester of glycerine, double ethyl ester hygroscopicity are very strong, reduce the bonding plasticising of triacetyl glycerine Easily there is raw silk at the time of molding in effect, mouth stick, and filter stick is caused to form heat in suction and is collapsed.To sum up, Dichlorodiphenyl Acetate fiber is filtered at present The research of plasticizer is less in stick, it is necessary to it be furtherd investigate, to overcome defect existing in the prior art.
The content of the invention
Present invention aims to overcome that prior art defect, provide a kind of tobacco plug plasticizer, its main application in Cigarette filter tip shaping enterprise.
To achieve the above object, the present invention adopts the following technical scheme that:
A kind of tobacco plug plasticizer, the tobacco plug plasticizer press matter by triacetyl glycerine and triethyl citrate Measure ratio 0~1:3 compounding compositions.
The preparation method of above-mentioned tobacco plug plasticizer is specially:By triacetyl glycerine and triethyl citrate In proportion mixing to get.
The present invention also provides purposes of the above-mentioned tobacco plug plasticizer in cigarette filter rod is prepared.It is specifically, described Tobacco plug is with 7~9% that the additive amount of plasticizer is cigarette filter rod weight.
Triethyl citrate, molecular formula:C12H20O, molecular weight:276.28;For colourless, transparency liquid, being dissolved in most of has Solvent is insoluble in oils.
Compared to the prior art, the beneficial effects of the present invention are:
Triacetyl glycerine is substituted as plasticizer using triethyl citrate, or both compounding use as filter stick plasticizer, Plasticizer of the present invention is pollution-free, at low cost, bonding plasticization effect is stronger.Find in practical applications, which reduce environmental pollution, Production cost is reduced, there is preferable social and economic benefit.
Specific embodiment
Technical scheme is further discussed in detail with reference to embodiments, but protection scope of the present invention It is not limited thereto.
Embodiment 1
A kind of tobacco plug plasticizer, the tobacco plug plasticizer press matter by triacetyl glycerine and triethyl citrate Measure ratio 1:3 compounding compositions.
The preparation method of above-mentioned tobacco plug plasticizer is specially:By triacetyl glycerine and triethyl citrate In proportion mixing to get.
Reference examples:A kind of tobacco plug plasticizer, component are triacetyl glycerine.
Effect test:Triacetyl glycerine and triethyl citrate compound product are compared with pure triacetyl glycerine Experiment
1)Physical quality Analysis of test results
By tobacco plug plasticizer described in embodiment 1(That is triacetyl glycerine and triethyl citrate 1:3 compoundings), reference examples The tobacco plug plasticizer(I.e. pure triacetyl glycerine product), respectively as plasticizer to account for cigarette filter rod weight 8.2% additive amount is added in cigarette filter rod production technology, the former is experimental group, and the latter is control group.
Using identical material and raw material, rolled filter rod sample and cigarette sample under same equipment, same process conditions Product carry out physical quality Indexs measure respectively(A is experimental group sample, and B is control sample), as a result as shown in Tables 1 and 2.
1 filter stick physical quality testing result of table
2 cigarette physical quality testing result of table
As can be seen from Table 1 and Table 2:The physical quality index no significant difference of test group sample and control sample, is being produced In the range of product standard regulation.
2)The testing result of phthalic acid ester in filter stick
The testing result of phthalic acid ester in 3 filter stick of table(Unit is:mg/kg)
As can be seen from Table 3:The testing result no significant difference of phthalic acid ester in test group sample and control sample, It has no effect to the safety indexes of filter stick
3)Sensory Quality of Cigarette
Sensory quality assessment, comprehensive evaluation result such as table 4 are carried out to the cigarette sample that different groups roll.
The sensory quality assessment result of the different filter stick rolling cigarettes of table 4
As can be seen from Table 4:Compared with the control group, experimental group cigarette sample is in the conglobation property of flue gas, sugariness, fine and smooth degree, dry It is improved in terms of dry sense, pleasant impression etc., makes moderate progress in terms of aroma quality, perfume quantity, miscellaneous gas.
Synthesis result:The filter stick physical quality index no significant difference of experimental group sample and control sample, in product In the range of standard regulation;By being found to the detection of phthalic acid ester in rolled filter rod:Compound the new of triethyl citrate Type plasticizer has no effect to the quality of filter stick, and finished cigarettes are in the conglobation property of flue gas, sugariness, fine and smooth degree, dry sensation, remaining Taste etc. is improved, and is made moderate progress in terms of aroma quality, perfume quantity, miscellaneous gas.

Claims (4)

1. a kind of tobacco plug plasticizer, which is characterized in that the tobacco plug plasticizer is by triacetyl glycerine and lemon Lemon triethylenetetraminehexaacetic acid ester in mass ratio 0~1:3 compounding compositions.
2. the preparation method of tobacco plug plasticizer described in claim 1, which is characterized in that by triacetyl glycerine and lemon Triethylenetetraminehexaacetic acid ester in proportion mixing to get.
3. purposes of the tobacco plug plasticizer in cigarette filter rod is prepared described in claim 1.
4. purposes of the tobacco plug plasticizer as described in claim 1 in cigarette filter rod is prepared, which is characterized in that the cigarette Careless filter stick is with 7~9% that the additive amount of plasticizer is cigarette filter rod weight.
CN201711105477.6A 2017-11-10 2017-11-10 A kind of tobacco plug plasticizer and its application Pending CN108095191A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711105477.6A CN108095191A (en) 2017-11-10 2017-11-10 A kind of tobacco plug plasticizer and its application

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711105477.6A CN108095191A (en) 2017-11-10 2017-11-10 A kind of tobacco plug plasticizer and its application

Publications (1)

Publication Number Publication Date
CN108095191A true CN108095191A (en) 2018-06-01

Family

ID=62206521

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201711105477.6A Pending CN108095191A (en) 2017-11-10 2017-11-10 A kind of tobacco plug plasticizer and its application

Country Status (1)

Country Link
CN (1) CN108095191A (en)

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201536617U (en) * 2009-09-29 2010-08-04 菲尔创纳国际有限公司 Filter tip bar used for smoking tobacco
CN101827536A (en) * 2007-09-19 2010-09-08 菲尔特隆纳国际有限公司 Tobacco smoke filter
CN102883629A (en) * 2010-05-12 2013-01-16 英美烟草(投资)有限公司 Filter additive
CN103126073A (en) * 2013-03-05 2013-06-05 湖南中烟工业有限责任公司 Filter stick fiber base material additive capable of reducing tar content in main cigarette stream smoke and application
CN103945714A (en) * 2011-09-23 2014-07-23 英美烟草(投资)有限公司 Filter materials and uses thereof
CN104797149A (en) * 2012-10-10 2015-07-22 R.J.雷诺兹烟草公司 Filter material for a filter element of a smoking article, and associated system and method

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101827536A (en) * 2007-09-19 2010-09-08 菲尔特隆纳国际有限公司 Tobacco smoke filter
CN201536617U (en) * 2009-09-29 2010-08-04 菲尔创纳国际有限公司 Filter tip bar used for smoking tobacco
CN102883629A (en) * 2010-05-12 2013-01-16 英美烟草(投资)有限公司 Filter additive
CN103945714A (en) * 2011-09-23 2014-07-23 英美烟草(投资)有限公司 Filter materials and uses thereof
CN104797149A (en) * 2012-10-10 2015-07-22 R.J.雷诺兹烟草公司 Filter material for a filter element of a smoking article, and associated system and method
CN103126073A (en) * 2013-03-05 2013-06-05 湖南中烟工业有限责任公司 Filter stick fiber base material additive capable of reducing tar content in main cigarette stream smoke and application

Similar Documents

Publication Publication Date Title
Chen et al. Studies of chitosan: II. Preparation and characterization of chitosan/poly (vinyl alcohol)/gelatin ternary blend films
CN103965369B (en) Ganoderan, method for extraction and purification and the application as tobacco humectant thereof
EP3766364B1 (en) Tobacco humectant, and preparation method therefor and use thereof
CN103211304A (en) Preparation method of filter stick using cigarette harm-reducing synergistic agent containing glycerol triacetate
CN101427847A (en) Process for producing Zimbabwe tobacco clean oil and uses thereof
CN105146747A (en) Preparation method of endogenous oily humectant for tobaccos
CN109294332A (en) A kind of cigarette with anti-fake color shifting ink with and preparation method thereof and cigarette tipping paper
CN108095191A (en) A kind of tobacco plug plasticizer and its application
CN104818618B (en) A kind of wrinkle resistant ironing agent and preparation method thereof
CN109156866A (en) A kind of additive with tongue fur note style and features and include the cigarette of the additive
CN105639725A (en) Liquor aroma type spice and application thereof to cigarette
CN101032454A (en) Long-acting perfume
CN105077552B (en) Acanthopanax brachypus polysaccharide is as tobacco humectant application in Medicated cigarette
CN107927904A (en) Cigarette filter rod curing agent and its preparation and application
CN103980374B (en) Polysaccharides from morinda officinalis how, method for extraction and purification and the application as tobacco humectant thereof
CN103126063B (en) One grows tobacco sense organ humectant and the using method in tobacco thereof
CN1973701A (en) Additive for lowering the stimulation of cigarette smoke
CN105595297B (en) oatmeal essence
CN103126073B (en) Filter stick fiber base material additive capable of reducing tar content in main cigarette stream smoke and application
CN106723353B (en) Preparation method of activated carbon for cigarettes, activated carbon for cigarettes and application of activated carbon
CN109717505A (en) A kind of cigarette additive and its application
CN108425269A (en) A kind of cigarette paper and preparation method thereof added with tangerine peel powder
CN103980378B (en) Agaricus Blazei Murrill polysaccharide, method for extraction and purification and the application as tobacco humectant thereof
CN103666764A (en) Cooling peppermint tobacco flavor composition
CN104031161B (en) Herba Lysimachiae polysaccharide, method for extraction and purification and the application as tobacco humectant thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20180601