CN108084825A - A kind of antistatic floor coatings and the method for making the floor coatings - Google Patents
A kind of antistatic floor coatings and the method for making the floor coatings Download PDFInfo
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- CN108084825A CN108084825A CN201711424449.0A CN201711424449A CN108084825A CN 108084825 A CN108084825 A CN 108084825A CN 201711424449 A CN201711424449 A CN 201711424449A CN 108084825 A CN108084825 A CN 108084825A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/24—Electrically-conducting paints
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/30—Sulfur-, selenium- or tellurium-containing compounds
- C08K2003/3045—Sulfates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/001—Conductive additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K7/00—Use of ingredients characterised by shape
- C08K7/22—Expanded, porous or hollow particles
- C08K7/24—Expanded, porous or hollow particles inorganic
Abstract
The present invention relates to a kind of antistatic floor coatings and the methods for making the floor coatings, including following components, the mass percent of each component is 50 70wt% of water, 2 4wt% of dispersion moisture agent, silicon change 0.5 1wt% of antifoaming agent, 0.5 1wt%, PH neutralizer of foam inhibitor, 0.05 0.1wt%, 0.3 1wt% of thickener, 10 25wt% of color stuffing, 0.5 1wt% of single-walled carbon nanotube, 0.5 2wt% of 15 25wt% of resin emulsion, 0.2 0.3wt% of anticorrosion and bactericidal agent and aqueous leveling auxiliary agent, wherein the sum of mass percent to component is 100wt%.Single-walled carbon nanotube is added in antistatic floor coatings by the present invention, while antistatic, greatly reduce the additive amount of conductive material, instead of coating with the electrically conducting manner of electric conductivity material framework, the brushing thickness of coating is reduced, improves conductive stability, reduce coating application usage amount and maintaining cost, antistatic performance is excellent, lasting, from time, the influence of temperature, humidity, smooth, beautiful, the wear-resisting pressure-resistant, impact resistance of coating surface.
Description
Technical field
The present invention relates to a kind of antistatic floor coatings and the methods for making the floor coatings, belong to paint field.
Background technology
With the rapid development of modern science and technology, electronics and electrical equipment spread all over each corner, this equipment makes from being fabricated onto
With with this electromagnetic radiation and static radiation, electromagnetic pollution be acknowledged as atmosphere pollution, water pollution, noise pollution it
The fourth-largest public hazards afterwards.Electromagnetic radiation is classified as one of major pollutants that must be controlled by the United Nations's human environment conference.Separately
Outside, electromagnetic radiation also results in electromagnetic wave leakage, threatens security assurance information.Thus antistatic floor material extensive use
Organic solvent content in e-factory and military project, electromagnetic radiation protection etc., traditional solvent based coating is more than more than 40%,
Coating can volatilize substantial amounts of organic compound (voc) in use, and the physical and mental health of environment and people is caused to be harmful to
It influences, causes the situation to lose more than gain.And water paint is using water as solvent, safety and environmental protection, therefore aqueous antistatic coating is ground
Hair new product comes one after another.The existing conductive floor material in market can be summarized as at present：
Epoxy copper foil antistatic floor
Such is that China adopts time longest antistatic floor and Market Selection the most universal.Compared in antistatic
Field is more backward.Mainly by the way that good conductor copper foil is laid with ground in advance, then carry out floor construction, such material and
Technique drawback is more apparent.Due to relying on copper foil conduction, cause the conductive resistance rate of ground everywhere different, can not be formed and uniformly led
Electric face；It is significantly improved using the terrace cost of copper foil；Due to the copper foil being laid in advance, increase difficulty of construction, easy damaged, copper foil damage
After be difficult to repair, terrace also just no longer have value；And it is excessively high to the cleannes requirement on ground, dust can influence base's copper foil
It is conductive.
Conducting pigment class antistatic floor
Such material to add in conductive fiber, conductive black, nickel powder etc., by conductive filler be in contact with each other generate conduction
Property.The floor material that conduction is carried out by adding in pigment is just difficult to keep stable in process of production, due to addition pigment or has
Color pigment face layers of material, precipitation, thixotropy increase, levelability it is poor, the additive amount of conducting pigment influences electrical conductivity, simultaneously
Also color is made to be difficult to stablize, similary drying time shortens, and since the pigment of addition needs to uniformly disperse in system, obtains good
Wetting, increased dispersion moistening series auxiliary agent make again system become it is unstable.
Graphene conductive material
Graphene is advanced conductive material, and graphene is the most thin two-dimensional material found so far, is by carbon hexatomic ring group
Into two-dimensional periodic structure, there is unique, excellent performance in physics, chemistry etc., such as excellent electrical conductivity, higher
Specific surface area, higher tensile strength, higher light transmission rate, higher stability etc..But when the dosage of graphene is less than
When 1.0%, conducting particles is separated from each other mostly, and conductive network cannot be formed in film, and film electric resistance rate is very big, and electric conductivity is very
Difference.When graphene dosage reaches 2%, the content of conducting particles is interconnected to form effective conductive path, applies beyond diafiltration value
Film resistivity thus drastically reduces.Continue the dosage of increase graphene, conducting particles contacts with each other with linking more abundant, conduction
Access is more perfect, therefore resistivity continues to reduce.But, after due to exceeding percolation threshold, conductive path has been formed, thus
Resistivity declines slowly and tends to steady mouth relatively, excessively high graphene additive amount undoubtedly become system tie up it is tired it is scattered with
The stability of coating starts to be affected, and coating sticks increase, and coating performance and coating film forming are not ideal, since graphene is two
Material is tieed up with poor on the electrical efficiency of three-dimensional single-walled carbon nanotube, electron-transport speed is low.
The content of the invention
It is existing in the prior art in order to solve the problems, such as, the present invention provides a kind of antistatic floor coatings and make the terrace
The method of coating, by adding single-walled carbon nanotube so that coating possesses the electrical conductivity of superelevation.
The technical solution adopted in the present invention is：
A kind of antistatic floor coatings, including following components, the mass percent of each component is water 50-70wt%, dispersion moisture agent
2-4wt%, silicon change antifoaming agent 0.5-1wt%, foam inhibitor 0.5-1wt%, PH neutralizer 0.05-0.1wt%, thickener 0.3-1wt%,
Color stuffing 10-25wt%, single-walled carbon nanotube 0.5-1wt%, resin emulsion 15-25wt%, anticorrosion and bactericidal agent 0.2-0.3wt% and water
Property leveling auxiliary agent 0.5-2wt%, wherein the sum of mass percent to component is 100wt%.
In general, the resin emulsion can be water-based acrylic resin lotion, aqueous epoxy resin emulsion or aqueous poly- ammonia
Ester lotion.
Further, the single-walled carbon nanotube can be aqueous liquid dispersion, and the mass fraction of the aqueous liquid dispersion is dense
It spends for 0.01%-0.1%.
In general, dispersion moisture agent, silicon change antifoaming agent, foam inhibitor, PH neutralizers, thickener and aqueous leveling auxiliary agent is
Aqueous promoter.
The present invention also provides a kind of method for preparing antistatic floor coatings, this method comprises the following steps
S1 steps：The silicon of water, dispersion moisture agent, PH neutralizers and 1/2 amount is changed antifoaming agent to be mixed evenly, obtains auxiliary agent
Liquid；
S2 steps：Color stuffing and single-walled carbon nanotube are added in liquid additive, are disperseed under the rotating speed of 800r/min-1200r/min
30min obtains dispersion liquid；
S3 steps：Dispersion liquid by zirconium pearl grinder is ground, obtains lapping liquid；
S4 steps：The foam inhibitor of resin emulsion and 1/2 amount is added in lapping liquid, and is stirred, speed of agitator 650r/
Min-750r/min, a length of 10min during stirring, obtains antistatic floor coatings.
Preferably, wherein being additionally added the foam inhibitor of 1/2 amount in S1 steps, and the speed of agitator in S1 steps is
400r/min, a length of 10min during stirring.
Preferably, anticorrosion and bactericidal agent is added in S4 steps, 1/2 amount silicon changes antifoaming agent, thickener and aqueous leveling auxiliary agent.
It is stirred or disperses in general, experiment dispersion machine may be employed in S1 steps, S2 steps and S4 steps.
Beneficial effects of the present invention：
Single-walled carbon nanotube is added in antistatic floor coatings by the present invention, while antistatic, greatly reduces conduction
The additive amount of material instead of coating with the electrically conducting manner of electric conductivity material framework, reduces the brushing thickness of coating, improves
Conductive stability, reduces coating application usage amount and maintaining cost, and antistatic performance is excellent, lasting, from when
Between, the influence of temperature, humidity, smooth, beautiful, the wear-resisting pressure-resistant, impact resistance of coating surface.
In addition the specific surface area of single-walled carbon nanotube is than the specific surface area bigger of graphene, thus single-walled carbon nanotube is led
Electrical property is more more excellent than graphene, and single-walled carbon nanotube is nanometer materials in addition, thus it possesses quantum size effect, tool
Standby certain superconduction ability, thus improve the conductive capability of terrace.
Single-walled carbon nanotube is three-dimensional tubular structure, with respect to the planar structure with graphene, the conduction of single-walled carbon nanotube
Performance is more preferable.
Specific embodiment
The present invention provides a kind of antistatic floor coatings, and including following components, the mass percent of each component is water 50-
70wt%, dispersion moisture agent 2-4wt%, silicon change antifoaming agent 0.5-1wt%, foam inhibitor 0.5-1wt%, PH neutralizer 0.05-0.1wt%,
Thickener 0.3-1wt%, color stuffing 10-25wt%, single-walled carbon nanotube 0.5-1wt%, resin emulsion 15-25wt%, antisepsis and sterilization
Agent 0.2-0.3wt% and aqueous leveling auxiliary agent 0.5-2wt%, wherein the sum of mass percent to component is 100wt%.
The resin emulsion can be water-based acrylic resin lotion, aqueous epoxy resin emulsion and aqueous polyurethane emulsion
In any one.
The single-walled carbon nanotube can be aqueous liquid dispersion, and the mass fraction concentration of the aqueous liquid dispersion is 0.01%-
0.1%。
It is aqueous help that dispersion moisture agent, silicon, which change antifoaming agent, foam inhibitor, PH neutralizers, thickener and aqueous leveling auxiliary agent,
Agent.
Color stuffing is the general name of pigment and filler in the application, and pigment is coloring pigment, and pigment refers to aqueous color paste herein, fills out
Material refers to constitution filler, referred to dicalcium powder and/or blanc fixe.
The present invention also provides a kind of method for preparing antistatic floor coatings, this method comprises the following steps：
S1 steps：The silicon of water, dispersion moisture agent, PH neutralizers, the foam inhibitor of 1/2 amount and 1/2 amount is changed antifoaming agent to be mixed
Uniformly, liquid additive is obtained, speed of agitator 400r/min, a length of 10min during stirring；
S2 steps：Color stuffing and single-walled carbon nanotube are added in liquid additive, are disperseed under the rotating speed of 800r/min-1200r/min
30min obtains dispersion liquid；
S3 steps：Dispersion liquid by zirconium pearl grinder is ground, obtains lapping liquid；
S4 steps：Resin emulsion, the foam inhibitor of 1/2 amount, anticorrosion and bactericidal agent, 1/2 amount silicon are changed into antifoaming agent, thickener and aqueous flow
Flat auxiliary agent is added in lapping liquid, and is stirred, speed of agitator 650r/min-750r/min, a length of 10min during stirring,
Obtain antistatic floor coatings.
It is stirred or divides it is emphasized that experiment dispersion machine may be employed in S1 steps, S2 steps and S4 steps
It dissipates, a diameter of 50mm of dispersion impeller.
Claims (8)
1. a kind of antistatic floor coatings, it is characterised in that：Including following components, the mass percent of each component is water 50-
70wt%, dispersion moisture agent 2-4wt%, silicon change antifoaming agent 0.5-1wt%, foam inhibitor 0.5-1wt%, PH neutralizer 0.05-0.1wt%,
Thickener 0.3-1wt%, color stuffing 10-25wt%, single-walled carbon nanotube 0.5-1wt%, resin emulsion 15-25wt%, antisepsis and sterilization
Agent 0.2-0.3wt% and aqueous leveling auxiliary agent 0.5-2wt%, wherein the sum of mass percent to component is 100wt%.
2. antistatic floor coatings according to claim 1, it is characterised in that：The resin emulsion is water soluble acrylic acid tree
Fat liquor, aqueous epoxy resin emulsion or aqueous polyurethane emulsion.
3. antistatic floor coatings according to claim 1, it is characterised in that：The single-walled carbon nanotube is aqueous dispersion
Liquid, and the mass fraction concentration of the aqueous liquid dispersion is 0.01%-0.1%.
4. antistatic floor coatings according to claim 1, it is characterised in that：Dispersion moisture agent, silicon change antifoaming agent, suds
Agent, PH neutralizers, thickener and aqueous leveling auxiliary agent are aqueous promoter.
A kind of 5. method for preparing claim 1-4 any one of them antistatic floor coatings, it is characterised in that：This method bag
Include following steps
S1 steps：The silicon of water, dispersion moisture agent, PH neutralizers and 1/2 amount is changed antifoaming agent to be mixed evenly, obtains auxiliary agent
Liquid；
S2 steps：Color stuffing and single-walled carbon nanotube are added in liquid additive, are disperseed under the rotating speed of 800r/min-1200r/min
30min obtains dispersion liquid；
S3 steps：Dispersion liquid by zirconium pearl grinder is ground, obtains lapping liquid；
S4 steps：The foam inhibitor of resin emulsion and 1/2 amount is added in lapping liquid, and is stirred, speed of agitator 650r/
Min-750r/min, a length of 10min during stirring, obtains antistatic floor coatings.
6. the method according to claim 5 for preparing antistatic floor coatings, it is characterised in that：Wherein in S1 steps also
The foam inhibitor of 1/2 amount is added in, and the speed of agitator in S1 steps is 400r/min, a length of 10min during stirring.
7. the method according to claim 5 for preparing antistatic floor coatings, it is characterised in that：It is added in S4 steps anti-
Rotten fungicide, 1/2 amount silicon change antifoaming agent, thickener and aqueous leveling auxiliary agent.
8. the method according to claim 5 for preparing antistatic floor coatings, it is characterised in that：In S1 steps, S2 steps
It is stirred or disperses using experiment dispersion machine in S4 steps.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711424449.0A CN108084825A (en) | 2017-12-25 | 2017-12-25 | A kind of antistatic floor coatings and the method for making the floor coatings |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201711424449.0A CN108084825A (en) | 2017-12-25 | 2017-12-25 | A kind of antistatic floor coatings and the method for making the floor coatings |
Publications (1)
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| CN108084825A true CN108084825A (en) | 2018-05-29 |
Family
ID=62179293
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| CN201711424449.0A Pending CN108084825A (en) | 2017-12-25 | 2017-12-25 | A kind of antistatic floor coatings and the method for making the floor coatings |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108795294A (en) * | 2018-07-04 | 2018-11-13 | 淄博旭川环保科技有限公司 | A kind of preparation process of high molecular nanometer composite coating |
| CN109836969A (en) * | 2019-03-12 | 2019-06-04 | 严勇 | A kind of anti-static and abrasion-resistant epoxy flooring coating |
| CN110387185A (en) * | 2019-07-12 | 2019-10-29 | 厦门中思诺新材料有限公司 | A kind of preparation method of the Waterborne polyurethane floor paint with antibacterial functions |
| CN114181590A (en) * | 2021-12-31 | 2022-03-15 | 厦门安必信新材料科技有限公司 | Waterborne epoxy antistatic self-leveling floor finish paint composition and construction method |
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| CN102234476A (en) * | 2010-05-06 | 2011-11-09 | 天津五一天立油漆有限公司 | Waterborne acrylic polyurethane surface paint |
| CN104693926A (en) * | 2015-02-15 | 2015-06-10 | 淄博世纪联合新型建筑材料有限公司 | Preparation method of water-based floor paint and construction process of water-based floor paint |
| CN105860815A (en) * | 2016-04-22 | 2016-08-17 | 北京虹霞正升涂料有限责任公司 | Waterborne anti-static anti-corrosive thermal insulation coating and preparation method |
| CN206751720U (en) * | 2016-12-29 | 2017-12-15 | 上海正欧实业有限公司 | A kind of single-walled carbon nanotube conductive coating and conductive terrace |
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2017
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102234476A (en) * | 2010-05-06 | 2011-11-09 | 天津五一天立油漆有限公司 | Waterborne acrylic polyurethane surface paint |
| CN104693926A (en) * | 2015-02-15 | 2015-06-10 | 淄博世纪联合新型建筑材料有限公司 | Preparation method of water-based floor paint and construction process of water-based floor paint |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108795294A (en) * | 2018-07-04 | 2018-11-13 | 淄博旭川环保科技有限公司 | A kind of preparation process of high molecular nanometer composite coating |
| CN109836969A (en) * | 2019-03-12 | 2019-06-04 | 严勇 | A kind of anti-static and abrasion-resistant epoxy flooring coating |
| CN110387185A (en) * | 2019-07-12 | 2019-10-29 | 厦门中思诺新材料有限公司 | A kind of preparation method of the Waterborne polyurethane floor paint with antibacterial functions |
| CN114181590A (en) * | 2021-12-31 | 2022-03-15 | 厦门安必信新材料科技有限公司 | Waterborne epoxy antistatic self-leveling floor finish paint composition and construction method |
| CN114181590B (en) * | 2021-12-31 | 2022-07-22 | 厦门安必信新材料科技有限公司 | Waterborne epoxy antistatic self-leveling floor finish paint composition and construction method |
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Application publication date: 20180529 |