CN108049029B - 一种干爽高吸附热风无纺布 - Google Patents

一种干爽高吸附热风无纺布 Download PDF

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CN108049029B
CN108049029B CN201810053702.4A CN201810053702A CN108049029B CN 108049029 B CN108049029 B CN 108049029B CN 201810053702 A CN201810053702 A CN 201810053702A CN 108049029 B CN108049029 B CN 108049029B
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郑勇城
施纯妙
傅仁杰
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FUJIAN GUAN HONG INDUSTRIAL Co Ltd
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Abstract

本发明涉及一种无纺布，更具体涉及一种干爽高吸附的热风无纺布。本发明提供的热风无纺布的原料及原料重量份包括：ES复合纤维40‑50份，超吸水纤维20‑40份，蚕丝纤维10‑30份，甲壳素纤维10‑20份；所述的ES复合纤维为掺杂了银的PE/PP皮芯型复合纤维和/或掺杂了银的PE/PET皮芯型复合纤维；所述的ES复合纤维表面涂敷有纺丝油剂，所述的纺丝油剂包括：10‑15wt％的抗静电剂，25‑35wt％的芳香植物提取物，0.05‑0.1wt％的金属螯合剂，其余为去离子水。该热风无纺布高度吸水，液体穿透速度快，回渗量小，柔软度好，抗菌且对肌肤无刺激，舒适度好。

Description

一种干爽高吸附热风无纺布
技术领域
本发明涉及一种无纺布，更具体涉及一种干爽高吸附的热风无纺布。
背景技术
热风无纺布隶属于热风粘合(热轧、热风)无纺布中的一种，是在纤维梳理成后，利用烘燥设备上的热风穿透纤网，使之受热而得以粘合生成的无纺布。热轧粘合是指用一对热轧辊对纤网进行加热，同时加以一定压力的热粘合方式；热风粘合是指在烘燥设备上利用热风穿透纤网使之受热熔融而产生粘合的生产方式。
ES纤维是一种最理想的热粘纤维，ES纤维是英文“Ethylene-Propylene Side BySide”的缩写，即低熔点双组分复合纤维，由两种具有不同低熔点的切片通过双螺杆纺丝机挤出，采用复合纺丝方法而制成，主要用于非织造布热粘法加工。当梳理后的纤维网通过热轧式或热风贯通式进行热粘合时，低熔点组分在纤维的交叉点上形成熔融粘着，而冷却后，非交叉点的纤维仍保持原来的状态，这是一种“点状粘合”而不是“区粘合”的形式，因而采用ES纤维加工而成的非织造布具有良好的蓬松性、柔软性和湿弹性，被广泛地用于纸尿布或生理用卫生巾等卫生用品、擦拭装置等清扫用品、面罩等医疗用品等领域。
中国发明CN 103603139B提供了一种热粘合无纺布及其制备方法，该热粘合无纺布包括60wt％以上的热塑性纤维，所述热合无纺布表面具有凹凸，并且克重为25g/m2～35g/m 2,综合柔软度≤55nN，吸水性≥600％，液体穿透性≤3s。本发明生产流程简单、能耗小，以及产品表面柔软、蓬松度高、不易变形，即手感好、使用更加舒适；
中国发明CN 103600552 A提供了一种柔软无纺布，该柔软无纺布包括最上层、中间层和最下层，所述最上层是聚乙烯醇纤维，所述中间层是稀释剂，所述最下层是金属纤维，所述聚乙烯醇纤维占柔软无纺布主体重量的34％-38％，所述稀释剂占柔软无纺布主体重量的9％-15％，所述金属纤维占柔软无纺布主体重量的51％-52％，本发明提供一种柔软无纺布，具有生产成本较低、纤网均匀性较好和手感柔软等优点。
近年来，人们对生活品质和健康的关注度越来越高，妇女卫生巾、婴儿纸尿裤、成人纸尿裤和护理垫等一次性卫生用品的需求量逐年攀升，且对其品质的要求也越来越多。如目前的纸尿裤，传统面层多次亲水性差，或尿液下渗速度缓慢，致使尿液长期滞留于人体皮肤与纸尿裤面层即表层之间，潮湿感重，使用舒适度差，且潮湿环境易滋生细菌；女性在经期敏感部位的皮肤最易受损伤或感染，调查表明，73％的女性会在经期感到局部皮肤瘙痒、灼痛，这主要是由于现有的卫生巾制品由无纺布制成，卫生巾表面材质粗糙低劣，性能差。
发明内容
为解决上述技术问题，本发明的目的在于提供一种高度吸水，液体穿透速度快，回渗量小，柔软度好，抗菌且对肌肤无刺激，舒适度好的干爽高吸附热风无纺布。
本发明提供了一种热风无纺布，该热风无纺布的原料及原料重量份包括：ES复合纤维40-50份，超吸水纤维20-40份，蚕丝纤维10-30份，甲壳素纤维10-20份。
进一步地，所述的ES复合纤维为掺杂了银的PE/PP皮芯型复合纤维和/或掺杂了银的PE/PET皮芯型复合纤维；其中，所述的掺杂了银的PE/PP皮芯型复合纤维的原料及其重量份组成为：纳米银0.001-0.005份，PE 30-50份，PP 30-50份；所述的掺杂了银的PE/PET皮芯型复合纤维的原料及其重量份组成为：纳米银0.001-0.005份，PE 30-50份，PET 30-50份。
进一步地，所述的ES复合纤维表面涂敷有纺丝油剂，所述的纺丝油剂包括：10-15wt％的抗静电剂，25-35wt％的芳香植物提取物，0.05-0.1wt％的金属螯合剂，其余为去离子水。
其中，所述的抗静电剂为烷基磷酸酯盐；
其中，所述的芳香植物提取物为本领域常规使用的任何芳香植物提取物，优选为玫瑰花提取物、桂花提取物、茉莉花提取物、柠檬提取物、薰衣草提取物、紫薇花提取物和蔷薇花提取物中的一种或多种。
其中，所述的金属螯合剂为乙二胺四乙酸二钠。
其中，所述的纺丝油剂与ES复合纤维的重量比为0.8％-1％。
本发明还提供了上述的热风无纺布在制备卫生材料中的应用，所述的卫生材料包括纸尿裤、卫生巾、护垫、成人失禁裤等。
本发明的有益效果在于：
1.本发明提供的热风无纺布，采用热风粘合技术加工而得，使用的ES纤维为低熔点双组分复合纤维，具有良好的蓬松性、柔软性，且本发明提供的热风无纺布，使用的ES复合纤维的原材料中掺杂了少量纳米银，赋予了ES复合纤维优异的抗菌性。
2.本发明提供的热风无纺布，通过在制备ES复合纤维的过程中使用的纺丝油剂添加天然芳香植物提取物的方法，使得天然芳香植物提取物在热风无纺布中分布更加均匀，天然芳香植物提取物具有优良的抗菌性，且其香味可掩盖异味，使得热风无纺布制备的卫生材料在使用时，使用者体验更加。另外，芳香植物提取物为天然来源，对肌肤无刺激，舒适度更好。
3.本发明提供的热风无纺布，添加了超吸水纤维，大大提高了热风无纺布的吸水性。
4.本发明提供的热风无纺布添加的蚕丝纤维使得制备得到的热风无纺布丝滑不易起毛，干爽，亲肤性好。
5.本发明提供的热风无纺布，添加了甲壳素纤维，使制备得到的热风无纺布具有优异的抗菌功能性，提高了热风无纺布的使用性能。
具体实施方式
以下结合具体实施例对本发明做进一步详备说明，但本发明不限于以下实施例。
实施例1
一种热风无纺布，该热风无纺布的原料及原料重量百分比为：
ES复合纤维50份，超吸水纤维(购自南通江潮纺织科技有限公司)40份，蚕丝纤维(购自吴江市倪氏绢纺厂)30份，甲壳素纤维(购自青岛欣玲丽绣品厂)20份；
其中，ES复合纤维的原材料组成为：
纳米银0.001份，PE(购自新疆独山子石油化工总厂)30份，PP(购自辽阳石油化纤公司)30份；纳米银在皮层PE和芯层PP中等量掺杂；
ES复合纤维制备过程中的纺丝油剂的重量百分比组成为：
10％的十二磷酸烷基酯钾盐(购自长沙江龙化工科技有限公司)，25％的薰衣草提取物(西安源森生物科技有限公司)，0.05％的EDTA-2Na，去离子水补至100％。
使用上述ES复合纤维原材料及纺丝油剂通过挤出、喷丝、拉伸、上油、二次拉伸、烘干、切断等步骤制备ES复合纤维，以及使用上述热风无纺布原材料经过开松混合、梳理、热风粘合、冷却定型等步骤制备热风无纺布所使用的工艺及设备均为本领域公知的。
实施例2
一种热风无纺布，各原料来源同实施例1，该热风无纺布的原料及原料重量百分比为：ES复合纤维40份，超吸水纤维20份，蚕丝纤维10份，甲壳素纤维10份；
其中，ES复合纤维的原材料组成为：纳米银0.005份，PE 50份，PP 50份；纳米银在皮层PE和芯层PP中等量掺杂；
ES复合纤维制备过程中的纺丝油剂的重量百分比组成为：15％的十二磷酸烷基酯钾盐，35％的柠檬提取物(西安源森生物科技有限公司)，0.1％的EDTA-2Na，去离子水补至100％。
制备方法同实施例1。
实施例3
一种热风无纺布，各原料来源同实施例1，该热风无纺布的原料及原料重量百分比为：ES复合纤维50份，超吸水纤维30份，蚕丝纤维10份，甲壳素纤维10份；
其中，ES复合纤维的原材料组成为：纳米银0.004份，PE 50份，PP 50份；纳米银在皮层PE和芯层PP中等量掺杂；
ES复合纤维制备过程中的纺丝油剂的重量百分比组成为：12％的十二磷酸烷基酯钾盐，30％的玫瑰花提取物(西安源森生物科技有限公司)，0.05％的EDTA-2Na，去离子水补至100％。
制备方法同实施例1。
实施例4
一种热风无纺布，各原料来源同实施例1，该热风无纺布的原料及原料重量百分比为：ES复合纤维50份，超吸水纤维40份，蚕丝纤维10份，甲壳素纤维10份；
其中，ES复合纤维的原材料组成为：纳米银0.004份，PE 50份，PP 50份；纳米银在皮层PE和芯层PP中等量掺杂；
ES复合纤维制备过程中的纺丝油剂的重量百分比组成为：12％的十二磷酸烷基酯钾盐，30％的玫瑰花提取物，0.05％的EDTA-2Na。
制备方法同实施例1。
实施例5
一种热风无纺布，各原料来源同实施例1，该热风无纺布的原料及原料重量百分比为：ES复合纤维50份，超吸水纤维30份，蚕丝纤维10份，甲壳素纤维10份；
其中，ES复合纤维的原材料组成为：纳米银0.004份，PE 50份，PP 50份；纳米银在皮层PE和芯层PP中等量掺杂；
ES复合纤维制备过程中的纺丝油剂的重量百分比组成为：12％的十二磷酸烷基酯钾盐，35％的玫瑰花提取物(西安源森生物科技有限公司)，0.05％的EDTA-2Na，去离子水补至100％。
制备方法同实施例1。
对比例1
一种热风无纺布，同实施例3，差别仅在于该热风无纺布的原料不含超吸水纤维。
对比例2
一种热风无纺布，同实施例3，差别仅在于该热风无纺布的原料不含蚕丝纤维。
对比例3
一种热风无纺布，同实施例3，差别仅在于该热风无纺布的原料不含甲壳素纤维。
对比例4
一种热风无纺布，同实施例3，差别仅在于ES复合纤维的原料中不含纳米银。
对比例5
一种热风无纺布，同实施例3，差别仅在于纺丝油剂中不含玫瑰花提取物。
实验例
将上述实施例及对比例制备得到的热风无纺布进行检测：
1.吸水性测试
取面积相同的各热风无纺布，称量G1，放入盛有测试溶液的烧杯中，浸泡30min后取出，自然悬挂30min后立即精密称量G2，根据公式：吸水倍率＝(G2-G1)/G1×100％计算热风无纺布的吸水倍率。
测试溶液是渗透性能测试专用的标准合成试液，配方见GB8939附录B。
2.渗透性能测试
渗透性能主要衡量液体在热风无纺布上的渗透及扩散效果，通过测试热风无纺布的单次和多次穿透时间进行表征，方法为：将人工尿液单次或多次(五次)通过穿透盘滴在热风无纺布上，测试尿液穿透热风无纺布的时间。
3.回渗量测试
测试热风无纺布对已流过的液体返渗到表面的抵抗性，方法为测试有多少被吸收的人工尿液又回到了热风无纺布的表面。
4.抑菌率测试
抑菌率的测试方法参考GB15979《一次性使用卫生用品卫生标准》，测试其对金黄色葡萄球菌、大肠杆菌、白色念珠菌的20分钟抑菌率。
实施例1-5及对比例1-5的热风无纺布的检测数据见表1：
表1

Claims (1)

1.一种热风无纺布，其特征在于，所述的热风无纺布的原料及原料重量份包括：ES复合纤维40-50份，超吸水纤维20-40份，蚕丝纤维10-30份，甲壳素纤维10-20份；
所述的ES复合纤维为掺杂了银的PE/ PP皮芯型复合纤维和/或掺杂了银的PE/PET皮芯型复合纤维；
所述的ES复合纤维表面涂敷有纺丝油剂；
所述的纺丝油剂包括：10-15wt％的抗静电剂，25-35wt％的芳香植物提取物，0.05-0.1wt％的金属螯合剂，其余为去离子水；
所述的掺杂了银的PE/PP皮芯型复合纤维的原料及其重量份组成为：纳米银0.001-0.005份，PE 30-50份，PP 30-50份；
所述的掺杂了银的PE/PET皮芯型复合纤维的原料及其重量份组成为：纳米银0.001-0.005份，PE 30-50份，PET 30-50份；
所述的抗静电剂为烷基磷酸酯盐；
所述的芳香植物提取物为玫瑰花提取物、桂花提取物、茉莉花提取物、柠檬提取物、薰衣草提取物、紫薇花提取物和蔷薇花提取物中的一种或多种；
所述的金属螯合剂为乙二胺四乙酸二钠；
所述的纺丝油剂与ES复合纤维的重量比为0.8％-1％。
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