CN108035176A - A kind of method that can colour carbon fiber - Google Patents

A kind of method that can colour carbon fiber Download PDF

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Publication number
CN108035176A
CN108035176A CN201810038260.6A CN201810038260A CN108035176A CN 108035176 A CN108035176 A CN 108035176A CN 201810038260 A CN201810038260 A CN 201810038260A CN 108035176 A CN108035176 A CN 108035176A
Authority
CN
China
Prior art keywords
carbon fiber
maintained
power section
sputtering power
vacuum
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810038260.6A
Other languages
Chinese (zh)
Inventor
王银川
余荣沾
刘琼溪
张欣
陈博昊
梁媛
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
GUANGDONG XINFENG TECHNOLOGY CO., LTD.
Original Assignee
Beijing Nano Chromophore Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Beijing Nano Chromophore Technology Co Ltd filed Critical Beijing Nano Chromophore Technology Co Ltd
Priority to CN201810038260.6A priority Critical patent/CN108035176A/en
Publication of CN108035176A publication Critical patent/CN108035176A/en
Pending legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/06—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the coating material
    • C23C14/14—Metallic material, boron or silicon
    • C23C14/18—Metallic material, boron or silicon on other inorganic substrates
    • C23C14/185—Metallic material, boron or silicon on other inorganic substrates by cathodic sputtering
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/34—Sputtering
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/80—Inorganic fibres

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Textile Engineering (AREA)
  • Chemical Or Physical Treatment Of Fibers (AREA)
  • Physical Vapour Deposition (AREA)

Abstract

The present invention provides a kind of method that can colour carbon fiber, and this method utilizes vacuum deposition method, forms plurality of color film layer in carbon fiber surface, makes carbon fiber surface face colouring.

Description

A kind of method that can colour carbon fiber
Technical field
It is a kind of color method of carbon fiber the invention belongs to innovate textile field
Background technology
At present, traditional dyeing technology cannot colour on carbon fiber, class graphite knot of its reason mainly due to carbon fiber Chemical inertness is presented in structure, its surface, lacks the chemical group with compared with high reaction activity, and the low valence bond between dye molecule closes Effect, makes its extremely difficult dyeing, this significantly limit the application field of carbon fiber
In order to which in carbon fiber surface face colouring, there is an urgent need to a kind of new coloring principle and method by the mankind.
The content of the invention
In order to solve the above technical problem, the present invention provides a kind of method that can colour carbon fiber, and this method is using very Empty sedimentation, forms plurality of color film layer in carbon fiber surface, makes carbon fiber surface face colouring.
The present invention technical solution be：
A kind of method that can colour carbon fiber, it includes：
1. carrying out pre-treatment to carbon fiber, surface blot is removed.
Room is unreeled 2. being involved on carbon fiber, guarantee unreels room vacuum and is maintained at 0.5-2.5E-1MPa sections；
3. carbon fiber makes carbon fiber temperature rise to 50 DEG C, heating chamber vacuum is maintained at 0.5-2.5E into heating chamber- 1MPa sections
4. carbon fiber is maintained at 3-8E into prechamber, house vacuum degree-2MPa；
5. when coating chamber vacuum reaches 1E-3During more than Pa, carbon fiber is into coating chamber, target Ti, sputtering power section 200-25000W, target Cu, sputtering power section are 400-30000W, and target Zn, sputtering power section is 200-35000W targets Material stainless steel, sputtering power section are 100-38000W, target stainless steel, and sputtering power section is 200-31000W, carbon fiber Into winding room, ensure that winding room vacuum is maintained at 0.5-2.5E-1Pa sections；
6. carbon fiber ensures that winding room vacuum is maintained at 0.5-2.5E into winding room-1MPa sections；
7. finished fabric is taken out, sampling detection.
Beneficial effects of the present invention are：
A kind of colouring method compared with prior art, method that can colour carbon fiber of the present invention, can be in carbon fiber Surface forms plurality of color film layer, makes carbon fiber that multiple color be presented, so as to meet the standard of GB/T 2660-2017.
Brief description of the drawings
Fig. 1 is present invention process flow chart
Embodiment
Embodiment is described in detail below in conjunction with attached drawing.
Embodiment 1
As shown in Figure 1, a kind of method that can colour carbon fiber, it includes：
1. carrying out pre-treatment to carbon fiber, surface blot is removed.
Room is unreeled 2. being involved on carbon fiber, guarantee unreels room vacuum and is maintained at 0.5-2.5E-1MPa sections；
3. carbon fiber makes carbon fiber temperature rise to 50 DEG C, heating chamber vacuum is maintained at 0.5-2.5E into heating chamber- 1MPa sections
4. carbon fiber is maintained at 3-8E into prechamber, house vacuum degree-2MPa；
5. when coating chamber vacuum reaches 1E-3During more than Pa, carbon fiber is into coating chamber, target Ti, sputtering power section 200-25000W, target Cu, sputtering power section are 400-30000W, and target Zn, sputtering power section is 200-35000W targets Material stainless steel, sputtering power section are 100-38000W, target stainless steel, and sputtering power section is 200-31000W, carbon fiber Into winding room, ensure that winding room vacuum is maintained at 0.5-2.5E-1Pa sections；
6. carbon fiber ensures that winding room vacuum is maintained at 0.5-2.5E into winding room-1MPa sections；
7. finished fabric is taken out, sampling detection.
Embodiment 2
As shown in Figure 1, a kind of method that can colour carbon fiber, it includes：
1. carrying out pre-treatment to carbon fiber, surface blot is removed.
Room is unreeled 2. being involved on carbon fiber, guarantee unreels room vacuum and is maintained at 0.5E-1MPa sections；
3. carbon fiber makes carbon fiber temperature rise to 50 DEG C, heating chamber vacuum is maintained at 0.5E into heating chamber-1MPa areas Between
4. carbon fiber is maintained at 3E into prechamber, house vacuum degree-2MPa；
5. when coating chamber vacuum reaches 1E-3During more than Pa, carbon fiber is into coating chamber, target Ti, sputtering power section 200-25000W, target Cu, sputtering power section are 400-30000W, and target Zn, sputtering power section is 200-35000W targets Material stainless steel, sputtering power section are 100-38000W, target stainless steel, and sputtering power section is 200-31000W, carbon fiber Into winding room, ensure that winding room vacuum is maintained at 0.5-2.5E-1Pa sections；
6. carbon fiber ensures that winding room vacuum is maintained at 0.5E into winding room-1MPa sections；
7. finished fabric is taken out, sampling detection.
Embodiment 3
As shown in Figure 1, a kind of method that can colour carbon fiber, it includes：
1. carrying out pre-treatment to carbon fiber, surface blot is removed.
Room is unreeled 2. being involved on carbon fiber, guarantee unreels room vacuum and is maintained at 2.5E-1MPa sections；
3. carbon fiber makes carbon fiber temperature rise to 50 DEG C, heating chamber vacuum is maintained at 2.5E into heating chamber-1MPa areas Between
4. carbon fiber is maintained at 8E into prechamber, house vacuum degree-2MPa；
5. when coating chamber vacuum reaches 1E-3During more than Pa, carbon fiber is into coating chamber, target Ti, sputtering power section 200-25000W, target Cu, sputtering power section are 400-30000W, and target Zn, sputtering power section is 200-35000W targets Material stainless steel, sputtering power section are 100-38000W, target stainless steel, and sputtering power section is 200-31000W, carbon fiber Into winding room, ensure that winding room vacuum is maintained at 0.5-2.5E-1Pa sections；
6. carbon fiber ensures that winding room vacuum is maintained at 2.5E into winding room-1MPa sections；
7. finished fabric is taken out, sampling detection.
Coloring experiment
According to GB/T 2660-2017, the carbon fiber of the method for the invention coloring is in color fastness to water, perspiration resistance color jail Degree, colour fastness to rubbing, fastness to soaping, colour fasteness to dry cleaning, color fastness to light meet the mark of GB/T 2660-2017 It is accurate.
The present invention elaborates and has been cited embodiment, but those skilled in the art made according to above-described embodiment it is aobvious And be clear to various schemes, modification, change, these schemes, modification, change should all belong to the present invention claim protection Scope.

Claims (3)

  1. A kind of 1. method that can colour carbon fiber, it is characterised in that it includes：
    1. carrying out pre-treatment to carbon fiber, surface blot is removed.
    Room is unreeled 2. being involved on carbon fiber, guarantee unreels room vacuum and is maintained at 0.5-2.5E-1MPa sections；
    3. carbon fiber makes carbon fiber temperature rise to 50 DEG C, heating chamber vacuum is maintained at 0.5-2.5E into heating chamber-1MPa areas Between
    4. carbon fiber is maintained at 3-8E into prechamber, house vacuum degree-2MPa；
    5. when coating chamber vacuum reaches 1E-3During more than Pa, carbon fiber into coating chamber, target Ti, sputtering power section be 200- 25000W, target Cu, sputtering power section are 400-30000W, target Zn, sputtering power section for 200-35000W targets not Become rusty steel, and sputtering power section is 100-38000W, target stainless steel, and sputtering power section is 200-31000W, and carbon fiber is into receipts Room is rolled up, ensures that winding room vacuum is maintained at 0.5-2.5E-1Pa sections；
    6. carbon fiber ensures that winding room vacuum is maintained at 0.5-2.5E into winding room-1MPa sections；
    7. finished fabric is taken out, sampling detection.
  2. 2. a kind of method that can colour carbon fiber as claimed in claim 1, it is characterised in that it includes：
    1. carrying out pre-treatment to carbon fiber, surface blot is removed.
    Room is unreeled 2. being involved on carbon fiber, guarantee unreels room vacuum and is maintained at 0.5E-1MPa sections；
    3. carbon fiber makes carbon fiber temperature rise to 50 DEG C, heating chamber vacuum is maintained at 0.5E into heating chamber-1MPa sections
    4. carbon fiber is maintained at 3E into prechamber, house vacuum degree-2MPa；
    5. when coating chamber vacuum reaches 1E-3During more than Pa, carbon fiber into coating chamber, target Ti, sputtering power section be 200- 25000W, target Cu, sputtering power section are 400-30000W, target Zn, sputtering power section for 200-35000W targets not Become rusty steel, and sputtering power section is 100-38000W, target stainless steel, and sputtering power section is 200-31000W, and carbon fiber is into receipts Room is rolled up, ensures that winding room vacuum is maintained at 0.5-2.5E-1Pa sections；
    6. carbon fiber ensures that winding room vacuum is maintained at 0.5E into winding room-1MPa sections；
    7. finished fabric is taken out, sampling detection.
  3. 3. a kind of method that can colour carbon fiber as claimed in claim 1, it is characterised in that it includes：
    1. carrying out pre-treatment to carbon fiber, surface blot is removed.
    Room is unreeled 2. being involved on carbon fiber, guarantee unreels room vacuum and is maintained at 2.5E-1MPa sections；
    3. carbon fiber makes carbon fiber temperature rise to 50 DEG C, heating chamber vacuum is maintained at 2.5E into heating chamber-1MPa sections
    4. carbon fiber is maintained at 8E into prechamber, house vacuum degree-2MPa；
    5. when coating chamber vacuum reaches 1E-3During more than Pa, carbon fiber into coating chamber, target Ti, sputtering power section be 200- 25000W, target Cu, sputtering power section are 400-30000W, target Zn, sputtering power section for 200-35000W targets not Become rusty steel, and sputtering power section is 100-38000W, target stainless steel, and sputtering power section is 200-31000W, and carbon fiber is into receipts Room is rolled up, ensures that winding room vacuum is maintained at 0.5-2.5E-1Pa sections；
    6. carbon fiber ensures that winding room vacuum is maintained at 2.5E into winding room-1MPa sections；
    7. finished fabric is taken out, sampling detection.
CN201810038260.6A 2018-01-16 2018-01-16 A kind of method that can colour carbon fiber Pending CN108035176A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810038260.6A CN108035176A (en) 2018-01-16 2018-01-16 A kind of method that can colour carbon fiber

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810038260.6A CN108035176A (en) 2018-01-16 2018-01-16 A kind of method that can colour carbon fiber

Publications (1)

Publication Number Publication Date
CN108035176A true CN108035176A (en) 2018-05-15

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Family Applications (1)

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CN201810038260.6A Pending CN108035176A (en) 2018-01-16 2018-01-16 A kind of method that can colour carbon fiber

Country Status (1)

Country Link
CN (1) CN108035176A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112813709A (en) * 2020-12-30 2021-05-18 盐城工学院 Dyeing method of carbon fiber

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112813709A (en) * 2020-12-30 2021-05-18 盐城工学院 Dyeing method of carbon fiber

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PB01 Publication
PB01 Publication
TA01 Transfer of patent application right
TA01 Transfer of patent application right

Effective date of registration: 20181221

Address after: 529000 First Floor of No.6 Jinzhang Avenue, Changsha District, Kaiping City, Jiangmen City, Guangdong Province

Applicant after: GUANGDONG XINFENG TECHNOLOGY CO., LTD.

Address before: 100080 Tianchuang Science and Technology Building, 8th Caihefang Road, Haidian District, Beijing, 12th floor 211B

Applicant before: Beijing nano chromophore Technology Co., Ltd.

WD01 Invention patent application deemed withdrawn after publication
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20180515