CN108029695A - A kind of fumigating disinfectant composition for animals, preparation method and applications - Google Patents
A kind of fumigating disinfectant composition for animals, preparation method and applications Download PDFInfo
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- CN108029695A CN108029695A CN201711450895.9A CN201711450895A CN108029695A CN 108029695 A CN108029695 A CN 108029695A CN 201711450895 A CN201711450895 A CN 201711450895A CN 108029695 A CN108029695 A CN 108029695A
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- animals
- disinfectant composition
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/64—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/18—Vapour or smoke emitting compositions with delayed or sustained release
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/02—Saturated carboxylic acids or thio analogues thereof; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/16—Heavy metals; Compounds thereof
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- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- Agronomy & Crop Science (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Toxicology (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
A kind of fumigating disinfectant composition for animals of the present invention, is made of following percentage by weight raw material：Sodium dichloroisocyanurate 60% 80%, zinc stearate 7% 10%, cornstarch 5% 10%, potassium permanganate 5% 10%.It is of the invention to select safe efficient, wide spectrum sodium dichloroisocyanurate to form synergist as host agent, the another three kinds of raw materials of selection, and the proportioning of four kinds of raw materials is continued to optimize by experiment, maximumlly to play the advantages of sootiness sterilizes；The fumigating disinfectant composition of the formula, is easy to use quick, and Disinfection Effect is good, not only can be that follow-up cultivation work is laid a solid foundation, but also can shorten the empty house phase of livestock and poultry cultivation, and then shortens the whole production cycle.
Description
Technical field
The invention belongs to disinfectant technical field, is related to a kind of solid fumigation disinfectant composition for animals and preparation method thereof
And application.
Background technology
As the continuous progress of breeding production theory and increasingly complexity, the feeding management of breeding environment are paid attention to all the more.
Sterilizing part not only can be that good environmental basis was established in cultivation work as key therein, but also can be in outbreak of disease
Control its sprawling.The selection of disinfectant is Bu Tong varied according to use environment and condition, if but classify according to disinfection way,
Then mainly there are liquid spray, dry powder spreading and smog to fumigate three kinds.In breeding production, sootiness disinfection is that poultry house passes through a system
Row cleaning, disinfection, dried final step.
Traditional fumigating disinfectant is made of formalin and potassium permanganate, by the quick release of formaldehyde gas, is reached
Kill the purpose of pathogenic microorganism.But formaldehyde is regarded as the 1st class carcinogenic substance by the World Health Organization in June, 2004
Matter --- there is the material of clear and definite carcinogenicity to human body.Also, in practical operation in use, the strong and stimulating of formaldehyde, strong sensitization
With high residue also great pressure is brought to the health production of animal and the trouble free service of poultry feeders.At present, in the market ratio
It is chlorine-containing disinfectant relatively successfully to substitute formaldehyde, the fumigating disinfectant of potassium permanganate, but the chlorine-containing disinfectant of one-component, burning
Not exclusively, smoke is inefficient, how to solve it on formula the defects of, gives full play to that fumigating disinfectant is easy to use, disinfection
Thoroughly the advantages of is main purpose.
The content of the invention
A kind of the defects of it is an object of the invention to solve existing one-component fumigating disinfectant, there is provided solid fumigation for animals
Antiseptic composition, preparation method and applications.
To achieve these goals, technical solution provided by the invention is：
A kind of fumigating disinfectant composition for animals, is made of following percentage by weight raw material：Sodium dichloroisocyanurate 60%-
80%, zinc stearate 7%-10%, cornstarch 5%-10%, potassium permanganate 5%-10%；
The sum of described each component mass percent=100%.
Preferably, it is made of following percentage by weight raw material：Sodium dichloroisocyanurate 75.8%, zinc stearate 9.0% are beautiful
Rice starch 7.6%, potassium permanganate 7.6%.
The present invention also resides in the preparation method for disclosing the fumigating disinfectant composition for animals, comprises the following steps that：In proportion
Various raw materials are taken, sodium dichloroisocyanurate is individually packaged as host agent, zinc stearate, cornstarch and potassium permanganate are uniformly mixed
Synergist is packaged as after conjunction.
Wherein, 58% should be no less than containing effective chlorine in the host agent.
The present invention, which also resides in, to be disclosed the fumigating disinfectant composition for animals and is applied in the empty house disinfection of livestock and poultry cultivation.
Its application process step is as follows：
(1) host agent of fumigating disinfectant composition for animals and synergist are mixed, is mixed according to every cubic metre of disinfection space
Agent amount calculates total dosage for 0.79-1.32 grams；
(2) fumigating disinfectant composition for animals is placed in container, is uniformly positioned over each position of the empty house of livestock and poultry to be sterilized；
(3) ignite after starting smoke, speed away, when closed poultry house 12-24 is small, after ventilation.
It should be noted that the present invention uses sodium dichloroisocyanurate, for host agent, the effective percentage of sodium dichloroisocyanurate contains
Amount is high, and up to 60%-62%, broad-spectrum high efficacy, sterilizing power are strong, easily stored, be readily transported.And the Ministry of Public Health《Food disinfectant
Raw material (composition) list (version in 2009)》(defend and do supervision hair (2010) 17) confirms that it can be directly used for sterilized food, food and drink
Tool and the directly material of instrument, equipment or the packaging material for food of contact food and container, it was demonstrated that dichloroisocyanuric acid
The security of sodium.
The mechanism of action of sodium dichloroisocyanurate sterilization is mainly the synergy of hypochlorous acid and nascent oxygen.Hypochlorous acid is made
Negatively charged phage surface is diffused into for neutral small molecule, penetration cell wall enters inside thalline, destroys phosphate dehydrogenase.And
Nascent oxygen can aoxidize bacterium protein, both achieve the purpose that broad-spectrum sterilization at collective effect.
Zinc stearate, cornstarch and potassium permanganate group in the solid fumigation disinfectant composite formula for animals of the present invention
Into synergist.Stearate is to increase cigarette auxiliary agent, and cornstarch is fuel, and potassium permanganate is oxygenate.Experiment proof, single two
Chlorine isocyanuric acid sodium is difficult to light, and smoke is slow, and cigarette is few and heavy；After coordinating synergist use, it is not only easy to light, has burnt
Entirely, and smoke is rapid, smog is more and light, suspension time length.It is more advantageous to having the gas of disinfection to be full of, is suspended in entirely
Disinfection space, to each corner fully thoroughly sterilize.
Solid fumigation disinfectant composition for animals in the present invention, should use after the empty house clear water rinsing, drying of livestock and poultry.
The present invention has the advantages and positive effects of：
The present invention selects safe efficient, wide spectrum sodium dichloroisocyanurate to select another three kinds of raw materials composition to increase as host agent
Agent is imitated, and the proportioning of four kinds of raw materials is continued to optimize by experiment, maximumlly to play the advantages of sootiness sterilizes；The cigarette of the formula
Smoked antiseptic composition, is easy to use quick, and Disinfection Effect is good, not only can be that follow-up cultivation work is laid a solid foundation, but also
The empty house phase of livestock and poultry cultivation can be shortened, and then shorten the whole production cycle.
Embodiment
In order to understand the present invention, the present invention is further illustrated with embodiment below, but do not limit the present invention.
Embodiment 1
Solid fumigation disinfectant composition for animals, every cubic metre of space dosage to be sterilized is 0.79 gram, its component is：Dichloro
0.6 gram of isocyanuric acid sodium, 0.07 gram of zinc stearate, 0.06 gram of cornstarch, 0.06 gram of potassium permanganate.Each original is weighed in proportion
Material, sodium dichloroisocyanurate are packaged as host agent, and zinc stearate, cornstarch, potassium permanganate, which are uniformly mixed, is packaged as synergist.
Embodiment 2
Solid fumigation disinfectant composition for animals, every cubic metre of space dosage to be sterilized is 1.06 grams, its component is：Dichloro
0.8 gram of isocyanuric acid sodium, 0.10 gram of zinc stearate, 0.08 gram of cornstarch, 0.08 gram of potassium permanganate.Each original is weighed in proportion
Material, sodium dichloroisocyanurate are packaged as host agent, and zinc stearate, cornstarch, potassium permanganate, which are uniformly mixed, is packaged as synergist.
Embodiment 3
Solid fumigation disinfectant composition for animals, every cubic metre of space dosage to be sterilized is 1.32 grams, its component is：Dichloro
1.0 grams of isocyanuric acid sodium, 0.12 gram of zinc stearate, 0.10 gram of cornstarch, 0.10 gram of potassium permanganate.Each original is weighed in proportion
Material, sodium dichloroisocyanurate are packaged as host agent, and zinc stearate, cornstarch, potassium permanganate, which are uniformly mixed, is packaged as synergist.
The solid fumigation disinfectant composition for animals of embodiment 1-3, should make after the empty house of livestock and poultry and clear water rinsing, drying
With.The host agent of sanitizing composition and synergist are uniformly mixed, it is empty according to every cubic metre of disinfection according to the volume in space to be sterilized
Between need mixture dosage be 0.79-1.32 grams, calculate total dosage.After weighing places, light successively from the inside to the outside rapidly, it is close
Close poultry house 12-24 it is small when, hatching egg fumigation be no more than 60 minutes, open a window ventilation.
4 disinfection effect test of embodiment
Test objective：For the Disinfection Effect of more different sterilization methods, disappeared using the solid fumigation for animals of embodiment 1-3
Toxic agent composition and formaldehyde, potassium permanganate (28ml:14g/m3) traditional sootiness sterilization tested.
Test method (one)：Hatching egg detection method (cotton swab swabs method)
By every group of egg (10) numbering 1-10.Tip is put well downward, and each egg is existed with the circle of a diameter of 1.5cm
Stub end draws symmetrical two regions.Drawn before sootiness on the left of each egg and determine region cotton swab libation at an ancient wedding ceremony physiological saline smearing,
Cotton swab is fractureed and is immersed in 500ul physiological saline, room temperature places 30min, sways instrument vibration 15s with rotation afterwards, and pipettor is inhaled
Taking 50ul, spreader coating is uniform, and spin for some time, after agar is by moisture absorption, puts on General nutrition agar plate
24h is cultivated in 37 DEG C of constant incubators, takes out and counts.Repeated after sootiness in the encircled of right side such as preceding operation.
Every batch of detects 10 pieces of the hatching egg of different sootiness positions, calculates average band bacterium number.Next group fumigation is carried out after 3d
Experiment.
Result of the test is as shown in the table：
| Disinfection way | Dosage/m3 | *Sterilizing rate |
| Embodiment 1 | 0.79g | 91.15% |
| Embodiment 2 | 1.06g | 93.87% |
| Embodiment 3 | 1.32g | 94.17% |
| Formaldehyde, potassium permanganate | 28ml:14g | 91.20% |
*Viable count × 100% before sterilizing rate (%)=(viable count after viable count-disinfection before disinfection)/disinfection
Result of the test shows, in the case of 25 DEG C of room temperature, relative humidity 65%-75%, uses for animals solid of the present invention
Body fumigating disinfectant composition 0.79-1.32g/m3Sootiness disinfection is carried out to hatching egg, sterilizing rate, can be with first up to more than 90%
Aldehyde, traditional sootiness sterilization of potassium permanganate are equal to.
Test method (two)：Henhouse detection method (plate sedimentation)
3 identical henhouses of size are selected, measure the total number of bacteria in air before sootiness disinfection with plate sedimentation respectively,
Further according to the weight of fumigating disinfectant composition used in the calculating of henhouse volume, respectively using the sootiness sterilization pair of embodiment 1-3
Sky house carries out sootiness disinfection, after, the total number of bacteria in plate sedimentation measure air is reused, calculates sterilizing rate.
Wherein, the specific operation process of plate sedimentation is as follows：Every henhouse chooses 10 test points, in each test point
1 nutrient agar plate is placed, uncap sampling 5min.After sampling, plate lid is covered, is inverted into 37 DEG C of constant temperature
Culture 24h, afterwards, measures each culture dish colony quantity, the average bacteriological for calculating and recording every henhouse is total in incubator
Number.
Result of the test is as shown in the table：
| Disinfection way | Dosage/m3 | *Sterilizing rate |
| Embodiment 1 | 0.79g | 92.38% |
| Embodiment 2 | 1.06g | 94.03% |
| Embodiment 3 | 1.32g | 94.92% |
*Viable count × 100% before sterilizing rate (%)=(viable count after viable count-disinfection before disinfection)/disinfection
Result of the test shows, in the case of 25 DEG C of room temperature, relative humidity 65%-75%, uses for animals solid of the present invention
Body fumigating disinfectant composition 0.79-1.32g/m3, sootiness disinfection is carried out to empty henhouse, sterilizing rate is up to more than 90%.
5 toxotest of embodiment
Use the solid fumigation disinfectant composition for animals and formaldehyde, potassium permanganate (28ml of embodiment 1-3:14g/m3)
Traditional sootiness sterilization is contrasted, and carries out sootiness disinfection to every group of 100 pieces of hatching eggs respectively.Then hatched, record is incubated
The index such as survival rate, the process have carried out toxicity research from side within rate, rate of healthy chick and 7 ages in days.
Result of the test is as shown in the table：
| Disinfection way | Dosage/m3 | Incubation rate | Rate of healthy chick | Survival rate in 7 ages in days |
| Embodiment 1 | 0.79g | 68.89% | 56.67% | 83.65% |
| Embodiment 2 | 1.06g | 70.11% | 65.52% | 91.08% |
| Embodiment 3 | 1.32g | 68.97% | 56.32% | 81.67% |
| Formaldehyde, potassium permanganate | 28ml:14g | 68.29% | 56.10% | 82.14% |
| Blank control | 0 | 70.79% | 64.04% | 87.30% |
Result of the test shows, uses the solid fumigation disinfectant composition 0.79-1.32g/m for animals of the present invention3And first
Aldehyde, potassium permanganate traditional sootiness disinfection methods after the hatching egg hatched, except the result of the test and blank control group of embodiment 2
As a result close outer, other 3 groups incubation rates, rate of healthy chick, 3 index results of survival rate are all not much different in 7 ages in days, but all lower slightly
In blank control group.The above results illustrate that embodiment 2 uses solid fumigation disinfectant composition 1.06g/ for animals of the invention
m3Disinfection Effect is moderate, and corresponding toxicity is relatively low, and follow-up hatching of breeding eggs, chick are survived favorably.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
With within principle, any modification, equivalent replacement, improvement and so on, should all be included in the protection scope of the present invention god.
Claims (6)
- A kind of 1. fumigating disinfectant composition for animals, it is characterised in thatIt is made of following percentage by weight raw material：Sodium dichloroisocyanurate 60%-80%, zinc stearate 7%-10%, corn form sediment Powder 5%-10%, potassium permanganate 5%-10%；The sum of described each component mass percent=100%.
- 2. a kind of fumigating disinfectant composition for animals according to claim 1, it is characterised in that by following percentage by weight Raw material forms：Sodium dichloroisocyanurate 75.8%, zinc stearate 9.0%, cornstarch 7.6%, potassium permanganate 7.6%.
- 3. according to the preparation method of any fumigating disinfectant composition for animals of claim 1 or 2, it is characterised in that press Ratio takes various raw materials, and sodium dichloroisocyanurate is individually packaged as host agent, and zinc stearate, cornstarch and potassium permanganate is equal Synergist is packaged as after even mixing.
- 4. the preparation method of fumigating disinfectant composition for animals according to claim 3, it is characterised in that in the host agent 58% should be no less than containing effective chlorine.
- 5. should in the empty house disinfection of livestock and poultry cultivation according to any fumigating disinfectant composition for animals of claim 1 or 2 With.
- 6. a kind of fumigating disinfectant composition for animals according to claim 5 is applied in the empty house disinfection of livestock and poultry cultivation, It is characterized in that, its application process step is as follows：(1) host agent of fumigating disinfectant composition for animals and synergist are mixed, agent is mixed according to every cubic metre of disinfection space Measure and calculate total dosage for 0.79-1.32 grams；(2) fumigating disinfectant composition for animals is placed in container, is uniformly positioned over each position of the empty house of livestock and poultry to be sterilized；(3) ignite after starting smoke, speed away, when closed poultry house 12-24 is small, after ventilation.
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| CN201711450895.9A CN108029695A (en) | 2017-12-27 | 2017-12-27 | A kind of fumigating disinfectant composition for animals, preparation method and applications |
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| CN201711450895.9A CN108029695A (en) | 2017-12-27 | 2017-12-27 | A kind of fumigating disinfectant composition for animals, preparation method and applications |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101411336A (en) * | 2008-11-27 | 2009-04-22 | 河北科技大学 | Aerosol disinfectant for edible fungus and preparation method thereof |
| CN101584319A (en) * | 2009-06-11 | 2009-11-25 | 汪文华 | Smoke disinfectant for hygiene sterilization and preparation method thereof |
-
2017
- 2017-12-27 CN CN201711450895.9A patent/CN108029695A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101411336A (en) * | 2008-11-27 | 2009-04-22 | 河北科技大学 | Aerosol disinfectant for edible fungus and preparation method thereof |
| CN101584319A (en) * | 2009-06-11 | 2009-11-25 | 汪文华 | Smoke disinfectant for hygiene sterilization and preparation method thereof |
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Application publication date: 20180515 |