CN110272669A - A kind of surface spray liniment and its preparation and application - Google Patents
A kind of surface spray liniment and its preparation and application Download PDFInfo
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- CN110272669A CN110272669A CN201910497701.3A CN201910497701A CN110272669A CN 110272669 A CN110272669 A CN 110272669A CN 201910497701 A CN201910497701 A CN 201910497701A CN 110272669 A CN110272669 A CN 110272669A
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- spray liniment
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D129/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal, or ketal radical; Coating compositions based on hydrolysed polymers of esters of unsaturated alcohols with saturated carboxylic acids; Coating compositions based on derivatives of such polymers
- C09D129/02—Homopolymers or copolymers of unsaturated alcohols
- C09D129/04—Polyvinyl alcohol; Partially hydrolysed homopolymers or copolymers of esters of unsaturated alcohols with saturated carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/08—Metals
- C08K2003/0806—Silver
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/32—Phosphorus-containing compounds
- C08K2003/321—Phosphates
- C08K2003/328—Phosphates of heavy metals
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
Abstract
The invention discloses a kind of surface spray liniment and its preparation and application.The surface spray liniment is made of component A and B component, wherein the component A, according to parts by weight, comprising: 1~5 part of polyvinyl alcohol rubber powder, 2~10 parts of anion nanometer solution, 0.1~3 part of titanium dioxide, 0.1~1 part of graphene oxide, 100 parts of water；The B component, according to parts by weight, comprising: 80~100 parts of alcohol, 1~10 part of Nano silver solution, 0~1 part of essence.The surface spray liniment is made of component A and B component, wherein the main function of component A is to generate negative oxygen ion and antibacterial, moreover it is possible to which the degradation of formaldehyde under ultraviolet light irradiation, the main function of B component are to kill the bacterium on spray attachment object and eliminate peculiar smell；The surface spray liniment is used for cloth, cladding, wallpaper, woodwork and other items, can play sterilization, the anion concentration in increase air, inhibit the effect of formaldehyde, use simple and convenient.
Description
Technical field
The present invention relates to daily-use chemical industry technical field, in particular to a kind of surface spray liniment and its preparation and application.
Background technique
With the promotion of people's living standard, the requirement to environment is also higher and higher.In real life, household or office
There is formaldehyde or the germ for being harmful to human body in wallpaper and woodwork and other items in the human body environments such as room circle, and underwear, socks and
Shirt internal layer etc. directly contacts the clothing of human skin, and there is also numerous germs, directly affect the health of human body.Although for net
Change air and antibacterial surface spray liniment product more and more enters in people's lives, but existing surface spray liniment is most
Be only capable of bacteriostasis, and deodorization, and effective time is short, can not the pernicious gases such as PARA FORMALDEHYDE PRILLS(91,95) eliminated,.Therefore it needs to prepare a kind of high
Effect, environmental protection and surface spray liniment harmless to humans.
Summary of the invention
The purpose of the present invention is intended to provide a kind of surface spray liniment and its preparation and application, is asked with solving above-mentioned technology
Topic.
To achieve the goals above, the technical solution of the present invention is as follows:
In a first aspect, a kind of surface spray liniment provided by the invention, is made of component A and B component, wherein the A group
Point, according to parts by weight, comprising: 1~5 part of polyvinyl alcohol rubber powder, 2~10 parts of anion nanometer solution, titanium dioxide 0.1~3
Part, 0.1~1 part of graphene oxide, 100 parts of water；The B component, according to parts by weight, comprising: alcohol 80~100 part, nanometer
1~10 part of silver-colored solution, 0~1 part of essence.
Preferably, the anion nanometer solution is to be made using following methods:
It is ground after solitary mountain flour, Tourmaline mountain flour and water mixing, homogeneous, takes supernatant after standing, obtain anion nanometer
Solution, wherein the weight ratio of the Tourmaline mountain flour and the solitary mountain flour is 5~10:1, the weight of the Tourmaline mountain flour
It is the 1~5% of the weight of the water.
Preferably, the mass concentration of the alcohol is 75~95%.
Preferably, the silver content of the Nano silver solution is 25~1000ppm.
Preferably, the component A is to be made using following methods: will polyvinyl alcohol rubber powder and water mix after heating infusion at
Glue adjusts the temperature to 40~60 DEG C, anion nanometer solution, titanium dioxide, graphene oxide is added in glue, middling speed is equal
It is cooling after matter, obtain component A.
It is further preferred that the condition of the middling speed homogeneous are as follows: speed of agitator is 400~800r/min, homogenizing time 1
~10 minutes.
Preferably, the B component is to be made using following methods: after alcohol, Nano silver solution, essence are mixed, through height
Fast homogeneous obtains B component.
It is further preferred that the condition of the high speed homogenization are as follows: speed of agitator is 1000~2000r/min, homogenizing time
It is 1~10 minute.
Preferably, the component A, according to parts by weight, comprising: 3 parts of polyvinyl alcohol rubber powder, 5 parts of anion nanometer solution,
1 part of titanium dioxide, 0.3 part of graphene oxide, 100 parts of deionized water.
Preferably, the B component, according to parts by weight, comprising: 95 parts of alcohol, 5 parts of Nano silver solution, essence 0.5~1
Part.
Second aspect, a kind of application method of such as surface spray liniment of first aspect provided by the invention, including walk as follows
It is rapid:
By B component even application on the surface of spray attachment object, after spontaneously drying, by component A even application in the spray attachment
The surface of object.
Preferably, any one of the spray attachment object in cloth, cladding, wallpaper, woodwork.
Compared with prior art, the beneficial effects of the present invention are:
Surface spray liniment of the invention is made of component A and B component, wherein the main function of component A is to generate negative oxygen
Ion and antibacterial, moreover it is possible to can be to kill with degradation of formaldehyde, the main function of B component under ultraviolet light irradiation thin on spray attachment object
Bacterium and elimination peculiar smell；Component A and B component can also be used alone, and can also arrange in pairs or groups use, especially B component, can be independent
Using on clothing, user travels outside, and when no time washes underwear, socks and shirt, can be sprayed on underwear, socks and lining
Shirt internal layer plays the role of sterilization, eliminates the unusual smell, and noresidue；Component A and B component collocation in use, as cloth, cladding,
The surface spray liniment of wallpaper, woodwork can play sterilization, the anion concentration in increase air, inhibit the effect of formaldehyde, make
Convenience simply to use.
Specific embodiment
Specific embodiments of the present invention will be further explained below.It should be noted that for these implementations
The explanation of mode is used to help understand the present invention, but and does not constitute a limitation of the invention.In addition, invention described below
Technical characteristic involved in each embodiment can be combined with each other as long as they do not conflict with each other.
Anion nanometer solution in following example 1~4 is to be made using following methods: by solitary mountain flour, Tourmaline
20nm is not more than by the partial size that nano-level grinder is ground to solitary mountain flour and Tourmaline mountain flour after mountain flour and water mixing, by true
Empty nanometer shears homogenizer homogeneous, and supernatant is taken after standing, obtains anion nanometer solution, wherein the Tourmaline mountain flour
Weight ratio with the solitary mountain flour is 9:1, and the weight of the Tourmaline mountain flour is the 4% of the weight of the water.
Embodiment 1
A kind of preparation method of surface spray liniment provided in this embodiment, includes the following steps:
(1) following raw materials according to parts by weight: 3 parts of polyvinyl alcohol rubber powder, 5 parts of anion nanometer solution, dioxy are weighed
Change 1 part of titanium, 0.3 part of graphene oxide, 100 parts of deionized water, will polyvinyl alcohol rubber powder and water mix after heating infusion at glue,
50 DEG C are adjusted the temperature to, anion nanometer solution, titanium dioxide, graphene oxide are added in glue, it is cold after middling speed homogeneous
But, component A, the condition of the middling speed homogeneous are obtained are as follows: speed of agitator 600r/min, homogenizing time are 5 minutes；
(2) following raw materials according to parts by weight: 95 parts of alcohol, 5 parts of Nano silver solution, 0.5 part of essence are weighed, by wine
After essence, Nano silver solution, essence mixing, B component, the condition of the high speed homogenization are obtained through high speed homogenization are as follows: speed of agitator is
1500r/min, homogenizing time are 5 minutes, and the mass concentration of the alcohol is 85%, and the silver content of the Nano silver solution is
500ppm。
Embodiment 2~4
Beneficial effect in order to further illustrate the present invention, using raw material shown in table 1 according to the preparation method of embodiment 1
Surface spray liniment is made.
The dosage of each raw material of table 1 counts
Embodiment 5
A kind of preparation method of surface spray liniment provided in this embodiment, includes the following steps:
(1) solitary mountain flour and Tuo Ma are ground to by nano-level grinder after mixing solitary mountain flour, Tourmaline mountain flour and water
The partial size of beautiful jade mountain flour is not more than 20nm, shears homogenizer homogeneous by vacuum nano, supernatant is taken after standing, obtains anion
Nano-solution, wherein the weight ratio of the Tourmaline mountain flour and the solitary mountain flour is 5:1, the weight of the Tourmaline mountain flour
It is the 1% of the weight of the water；Weigh following raw materials according to parts by weight: 1 part of polyvinyl alcohol rubber powder, anion nanometer solution
2 parts, 3 parts of titanium dioxide, 0.1 part of graphene oxide, 100 parts of deionized water are heated after mixing polyvinyl alcohol rubber powder and water and are endured
It is cooked into glue, adjusts the temperature to 40 DEG C, anion nanometer solution, titanium dioxide, graphene oxide are added in glue, middling speed is equal
It is cooling after matter, obtain component A, the condition of the middling speed homogeneous are as follows: speed of agitator 400r/min, homogenizing time are 10 minutes；
(2) following raw materials according to parts by weight: 90 parts of alcohol, 10 parts of Nano silver solution, 0.5 part of essence are weighed, by wine
After essence, Nano silver solution, essence mixing, B component, the condition of the high speed homogenization are obtained through high speed homogenization are as follows: speed of agitator is
1000r/min, homogenizing time are 10 minutes, and the mass concentration of the alcohol is 75%, and the silver content of the Nano silver solution is
25ppm。
Embodiment 6
A kind of preparation method of surface spray liniment provided in this embodiment, includes the following steps:
(1) solitary mountain flour and Tuo Ma are ground to by nano-level grinder after mixing solitary mountain flour, Tourmaline mountain flour and water
The partial size of beautiful jade mountain flour is not more than 20nm, shears homogenizer homogeneous by vacuum nano, supernatant is taken after standing, obtains anion
Nano-solution, wherein the weight ratio of the Tourmaline mountain flour and the solitary mountain flour is 10:1, the weight of the Tourmaline mountain flour
It is the 5% of the weight of the water；Weigh following raw materials according to parts by weight: 5 parts of polyvinyl alcohol rubber powder, anion nanometer solution
10 parts, 0.1 part of titanium dioxide, 1 part of graphene oxide, 100 parts of deionized water are heated after mixing polyvinyl alcohol rubber powder and water and are endured
It is cooked into glue, adjusts the temperature to 60 DEG C, anion nanometer solution, titanium dioxide, graphene oxide are added in glue, middling speed is equal
It is cooling after matter, obtain component A, the condition of the middling speed homogeneous are as follows: speed of agitator 800r/min, homogenizing time are 3 minutes；
(2) following raw materials according to parts by weight: 99 parts of alcohol, 1 part of Nano silver solution, 1 part of essence are weighed, by alcohol,
After Nano silver solution, essence mixing, B component, the condition of the high speed homogenization are obtained through high speed homogenization are as follows: speed of agitator is
2000r/min, homogenizing time are 3 minutes, and the mass concentration of the alcohol is 95%, and the silver content of the Nano silver solution is
1000ppm。
Comparative example 1
Surface spray is made using preparation method similar to Example 1 in beneficial effect in order to further illustrate the present invention
The difference of paint, this comparative example and embodiment 1 is only that graphene oxide is not used in this comparative example in component A.
Effect example 1 is tested except effect of formaldehyde
Beneficial effect in order to further illustrate the present invention, 7 pieces of wood-based plate for selecting 30cm × 30cm size, is respectively put into
In the identical closed container of 7 sizes, the resulting surface spray liniment of 1~6 dose of comparative example of above-described embodiment 1 is sprayed on 7 respectively
On block artificial board, and the removal rate of formaldehyde is detected, test method is as follows: the wood-based plate of 30cm × 30cm size being put into closed
In container for 24 hours after, the concentration of formaldehyde value in the closed container is measured using methylene oxide detecting instrument, closed container is opened, surface is sprayed
The B component even application of paint sprays surface after the B component on artificial board spontaneously dries on the surface of artificial board
The component A even application of agent closes closed container and detects the formaldehyde in the closed container after for 24 hours on the surface of artificial board
Concentration value calculates the removal rate of formaldehyde, and statistical result is as shown in table 2, and calculation formula is as follows:
The removal rate (%) of formaldehyde=(the concentration of formaldehyde value measured after the concentration of formaldehyde value-spraying measured before spraying )/spray
Concentration of formaldehyde value × 100% measured before painting.
Table 2 removes effect of formaldehyde test result
| Serial number | The source of surface spray liniment | The removal rate (%) of formaldehyde |
| 1 | Embodiment 1 | 96.72 |
| 2 | Embodiment 2 | 95.42 |
| 3 | Embodiment 3 | 92.41 |
| 4 | Embodiment 4 | 93.27 |
| 5 | Embodiment 5 | 85.42 |
| 6 | Embodiment 6 | 89.34 |
| 7 | Comparative example 1 | 74.39 |
The test of 2 fungistatic effect of effect example
Inhibition zone test is carried out according to " disinfection technology standard " 2002No2.1.8.2:
(1) strain: Escherichia coli, staphylococcus aureus, Candida albicans is tested；
(2) preparing 8 diameters is 7mm filter paper dick, spare after high-temperature sterilization；
(3) filter paper after above-mentioned 7 sterilizings is impregnated respectively using the surface spray liniment of above-described embodiment 1~6 and comparative example 1
Piece, until filter paper to soaking completely, then takes out filter paper, the culture for being coated with 200 μ L bacterium solutions is placed on through naturally dry
In ware, then culture dish is put into incubator, 7d cultivated under the conditions of 37 DEG C, as processing group 1~7；
(4) filter paper after a sterilizing is impregnated in ethanol to soaking completely, naturally dry, which is placed on, is coated with 200
In the culture dish of μ L bacterium solution, then culture dish is put into incubator, 7d cultivated under the conditions of 37 DEG C, as blank control group；
(5) growing state of bacterium in processing group and blank group culture dish is observed respectively and tests the size of inhibition zone, is surveyed
Test result is as shown in table 3.
3 fungistatic effect test result of table
Above the embodiments of the present invention are described in detail, but the present invention is not limited to described embodiments.It is right
For those skilled in the art, in the case where not departing from the principle of the invention and spirit, these embodiments are carried out more
Kind change, modification, replacement and modification, still fall in protection scope of the present invention.
Claims (9)
1. a kind of surface spray liniment, which is characterized in that be made of component A and B component, wherein the component A, in parts by weight
Meter, comprising: 1~5 part of polyvinyl alcohol rubber powder, 2~10 parts of anion nanometer solution, 0.1~3 part of titanium dioxide, graphene oxide
0.1~1 part, 100 parts of water；The B component, according to parts by weight, comprising: 80~100 parts of alcohol, 1~10 part of Nano silver solution,
0~1 part of essence.
2. surface spray liniment according to claim 1, which is characterized in that the anion nanometer solution is to use following sides
Method is made:
It is ground after solitary mountain flour, Tourmaline mountain flour and water mixing, homogeneous, takes supernatant after standing, obtain anion nanometer solution,
Wherein, the weight ratio of the Tourmaline mountain flour and the solitary mountain flour is 5~10:1, and the weight of the Tourmaline mountain flour is described
The 1~5% of the weight of water.
3. surface spray liniment according to claim 1, which is characterized in that the mass concentration of the alcohol is 75~95%.
4. surface spray liniment according to claim 1, which is characterized in that the silver content of the Nano silver solution be 25~
1000ppm。
5. surface spray liniment according to claim 1, which is characterized in that the component A is to be made using following methods: will
Heating infusion adjusts the temperature to 40~60 DEG C, by anion nanometer solution, dioxy at glue after polyvinyl alcohol rubber powder and water mixing
Change titanium, graphene oxide are added in glue, cooling after middling speed homogeneous, obtain component A.
6. surface spray liniment according to claim 5, which is characterized in that the condition of the middling speed homogeneous are as follows: speed of agitator
For 400~800r/min, homogenizing time is 1~10 minute.
7. surface spray liniment according to claim 1, which is characterized in that the B component is to be made using following methods: will
After alcohol, Nano silver solution, essence mixing, B component is obtained through high speed homogenization.
8. surface spray liniment according to claim 7, which is characterized in that the condition of the high speed homogenization are as follows: speed of agitator
For 1000~2000r/min, homogenizing time is 1~10 minute.
9. a kind of application method of such as surface spray liniment according to any one of claims 1 to 8, which is characterized in that including such as
Lower step:
By B component even application on the surface of spray attachment object, after spontaneously drying, by component A even application in the spray attachment object
Surface.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111973466A (en) * | 2020-08-26 | 2020-11-24 | 中山市凯蕾护理用品有限公司 | Antibacterial and deodorant composition and preparation method and application thereof |
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| CN109852167A (en) * | 2018-12-27 | 2019-06-07 | 东易生态科技(广州)有限公司 | It is a kind of that liquid occurring applied to the anion sprayed on object or material |
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| KR100532097B1 (en) * | 2002-08-28 | 2005-11-29 | 삼성전자주식회사 | Watersoluble polymer antibiotic agent and ink composition comprising the same |
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