CN108018119A - A kind of method that ozone is efficiently mutually mixed with vegetable oil - Google Patents
A kind of method that ozone is efficiently mutually mixed with vegetable oil Download PDFInfo
- Publication number
- CN108018119A CN108018119A CN201711344414.6A CN201711344414A CN108018119A CN 108018119 A CN108018119 A CN 108018119A CN 201711344414 A CN201711344414 A CN 201711344414A CN 108018119 A CN108018119 A CN 108018119A
- Authority
- CN
- China
- Prior art keywords
- ozone
- vegetable oil
- oil
- tank
- ultrasonication
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/02—Refining fats or fatty oils by chemical reaction
- C11B3/08—Refining fats or fatty oils by chemical reaction with oxidising agents
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The invention discloses a kind of method that ozone and vegetable oil efficiently mutually mix, include the following steps：1) vegetable oil is pumped into storage tank, applies ultrasonication, seal, vacuumize afterwards；Under vacuum conditions, tank implants oil is heated；2) under normal pressure state, ozone and oxygen are pressed 1:0.2~0.4 volume ratio mixing, is passed through vacuum breaker degree in the vegetable oil in storage tank by mixed gas with the speed of 0.5~2g/min afterwards；3) vegetable oil in tank is stirred with the speed of 15~30r/min, while applies ultrasonication, the condition of ultrasonication is：200~300W of power, 40~60Hz of frequency, 0.5~3h of time；4) tank implants oil pump is gone out immediately after ultrasonication, sealed packaging preserves afterwards.By the method for the present invention ozone can be made efficiently mutually to be mixed with vegetable oil, reduce the oxidation reaction of ozone and vegetable oil.
Description
Technical field
The present invention relates to a kind of ozone and the mutual mixing method of vegetable oil.
Background technology
Ozone (O3) super oxygen is also known as, it is oxygen (O2) allotrope, at normal temperatures, it is that one kind has off-odor
Light blue gas.At present, ozone has multiple use in terms of medical treatment in the world：Such as ward, the air sterillization of operating room, profit
Medical instrument sterilization is carried out with Ozone Water, dental disorder treatment (operation on oral cavity and holding oral cavity are sterile) is carried out using ozone, is adopted
With ozone and radiation physical therapy combined treatment cancer, Ozone Water treatment gynaecological disease, injecting ozone Gases for Treating fistula hemorrhoid, varication are drunk
Deng.In healthcare, Japan, the popular strong gas (air containing low concentration ozone) of suction of TaiWan, China are taken a shower with salubrity with Ozone Water
Body kills body bacterium and beauty.The high-tech beauty of current trend, beauty is carried out wherein just having using ozone.
Since ozone is extremely unstable in water, under room temperature the half-life period of ozone in water be about 5 minutes, 30 minutes after in water
Concentration is extremely low.Research finds, ozone quite stable in monounsaturated fatty acids, and ozone oil, which is made, can preserve more than 2 years, at present
Most commonly used is ozonisation olive oil, but the olive oil in China is mainly by import.Therefore, Chinese patent (application number
201410376761.7) a kind of ozonisation borneol tea oil is disclosed, it includes ozone, borneol and tea oil, wherein per 1L tea oil
The content of middle borneol is 30~50g, and in 25-30 DEG C of temperature, pressure is under 0.5~1.5bar, and control ozone leads in every 1L tea oil
It is 13.5g~20.0g to enter total amount.The ozonisation borneol tea oil of the technical solution, raw material is cheap and easy to get, and antibacterial effect can obtain
It is obviously improved, there is good anti-inflammatory, analgesic, bactericidal effect, effectively facilitates the healing of wound, be more advantageous to the rehabilitation of patient
, be more easy to be accepted by patients can stably be sustained out ozone, can kill Escherichia coli, S. aureus L-forms, white in a short time
Candida albicans etc., especially has chronic wounds such as diabetes and acute wounds the ozonisation borneol tea of the effect of fine
Oil.But among practice, during ozone is passed through vegetable oil, ozone can occur with the unrighted acid of vegetable oil
Reaction, aoxidize vegetable oil, cause ozone largely to lose, while vegetable oil aoxidized after degree of unsaturation be greatly reduced,
Ozone just can not be passed through in vegetable oil and be mixed with；In addition, ozone is difficult uniformly mutually to be mixed with vegetable oil, planting ozone
Dispersed and dissolving in thing oil.
The content of the invention
In view of the above-mentioned problems, the present invention provides a kind of method that ozone and vegetable oil efficiently mutually mix, by present invention side
Method can be such that ozone is efficiently mutually mixed with vegetable oil, reduce the oxidation reaction of ozone and vegetable oil.
The present invention is achieved through the following technical solutions.
A kind of method that ozone is efficiently mutually mixed with vegetable oil, includes the following steps：
1) vegetable oil is pumped into storage tank, applies ultrasonication, the condition of ultrasonication is：Power 200~
300W, 40~60Hz of frequency, 0.5~3h of time, seal, vacuumize afterwards, make vacuum up to 0.90~0.98MPa；In vacuum
Under environment, tank implants oil is heated, tank implants oil is heated to 60~65 DEG C with 1~2 DEG C/min of heating rate, Zhi Houwei
Hold 0.90~0.98MPa of vacuum in tank, the time of 60~65 DEG C of tank implants oil temperature is 1~3h；By the step, i.e.,
Under ultrasonic wave, vacuum environment it is persistently overheating can in advance by vegetable oil air remove；
2) under normal pressure state, ozone and oxygen are pressed 1:0.2~0.4 volume ratio mixing, afterwards by mixed gas with 0.5
The speed of~2g/min is passed through vacuum breaker degree in the vegetable oil in storage tank；Due to ozone after ozone and vegetable oil generation oxidation reaction
Oxygen is reduced into, therefore by the step, ozone and oxygen mix is passed through vegetable oil in advance, vegetable oil and ozone can be suppressed
Oxidation reaction；
3) vegetable oil in tank is stirred with the speed of 15~30r/min, while applies ultrasonication, ultrasonic wave
The condition of processing is：200~300W of power, 40~60Hz of frequency, 0.5~3h of time；After ozone and oxygen are passed through vegetable oil,
Ozone can be made to be evenly distributed in vegetable oil by the mechanical effect of slow mechanical agitation and ultrasonic wave and dissolved；
4) tank implants oil pump is gone out immediately after ultrasonication, sealed packaging preserves afterwards.
As concrete technical scheme, the intake of ozone and oxygen is calculated as 40 with the weight of vegetable oil in the step (2)
~60g/kg.
As concrete technical scheme, the vegetable oil is tea oil, one kind in olive oil.
Embodiment
With reference to embodiment, the present invention is described further, it is pointed out that implementation below is only
It is the indicative explaination done in the form of enumerating to the present invention, but protection scope of the present invention is not limited to that, Suo Youben
The technical staff in field each falls within protection scope of the present invention with the equivalent replacement that the spirit of the present invention is the present invention.
Embodiment 1
A kind of method that ozone is efficiently mutually mixed with vegetable oil, includes the following steps：
1) vegetable oil is pumped into storage tank, applies ultrasonication, the condition of ultrasonication is：Power 200~
300W, 40~60Hz of frequency, 0.5~3h of time, seal, vacuumize afterwards, make vacuum up to 0.90~0.98MPa；In vacuum
Under environment, tank implants oil is heated, tank implants oil is heated to 60~65 DEG C with 1~2 DEG C/min of heating rate, Zhi Houwei
Hold 0.90~0.98MPa of vacuum in tank, the time of 60~65 DEG C of tank implants oil temperature is 1~3h；
2) under normal pressure state, ozone and oxygen are pressed 1:0.2~0.4 volume ratio mixing, afterwards by mixed gas with 0.5
The speed of~2g/min is passed through vacuum breaker degree in the vegetable oil in storage tank；
3) vegetable oil in tank is stirred with the speed of 15~30r/min, while applies ultrasonication, ultrasonic wave
The condition of processing is：200~300W of power, 40~60Hz of frequency, 0.5~3h of time；
4) tank implants oil pump is gone out immediately after ultrasonication, sealed packaging preserves afterwards.
Embodiment 2
A kind of method that ozone is efficiently mutually mixed with vegetable oil, includes the following steps：
1) vegetable oil is pumped into storage tank, applies ultrasonication, the condition of ultrasonication is：200~300W of power,
40~60Hz of frequency, 0.5~3h of time, seal, vacuumize afterwards, make vacuum up to 0.90~0.98MPa；In vacuum environment
Under, tank implants oil is heated, tank implants oil is heated to 60~65 DEG C with 1~2 DEG C/min of heating rate, maintains tank afterwards
Interior 0.90~0.98MPa of vacuum, the time of 60~65 DEG C of tank implants oil temperature are 1~3h；
2) under normal pressure state, ozone and oxygen are pressed 1:0.2~0.4 volume ratio mixing, afterwards by mixed gas with 0.5
The speed of~2g/min is passed through vacuum breaker degree in the vegetable oil in storage tank；Wherein, the intake of ozone and oxygen is with vegetable oil
Weight is calculated as 40~60g/kg；
3) vegetable oil in tank is stirred with the speed of 15~30r/min, while applies ultrasonication, ultrasonic wave
The condition of processing is：200~300W of power, 40~60Hz of frequency, 0.5~3h of time；
4) tank implants oil pump is gone out immediately after ultrasonication, sealed packaging preserves afterwards.
Embodiment 3
A kind of method that ozone is efficiently mutually mixed with tea oil, includes the following steps：
1) tea oil is pumped into storage tank, applies ultrasonication, the condition of ultrasonication is：200~300W of power,
40~60Hz of frequency, 0.5~3h of time, seal, vacuumize afterwards, make vacuum up to 0.90~0.98MPa；In vacuum environment
Under, tea oil in tank is heated, tea oil in tank is heated to 60~65 DEG C with 1~2 DEG C/min of heating rate, remains true in tank afterwards
The time of 60~65 DEG C of tea oil temperature is 1~3h in 0.90~0.98MPa of reciprocal of duty cycle, tank；
2) under normal pressure state, ozone and oxygen are pressed 1:0.2~0.4 volume ratio mixing, afterwards by mixed gas with 0.5
The speed of~2g/min is passed through vacuum breaker degree in the tea oil in storage tank；Wherein, the intake of ozone and oxygen is with the weight of tea oil
It is calculated as 40~60g/kg；
3) tea oil in tank is stirred with the speed of 15~30r/min, while applies ultrasonication, at ultrasonic wave
The condition of reason is：200~300W of power, 40~60Hz of frequency, 0.5~3h of time；
4) tea oil in tank is pumped out immediately after ultrasonication, sealed packaging preserves afterwards.
Embodiment 4
A kind of method that ozone is efficiently mutually mixed with olive oil, includes the following steps：
1) olive oil is pumped into storage tank, applies ultrasonication, the condition of ultrasonication is：Power 200~
300W, 40~60Hz of frequency, 0.5~3h of time, seal, vacuumize afterwards, make vacuum up to 0.90~0.98MPa；In vacuum
Under environment, olive oil in tank is heated, olive oil in tank is heated to 60~65 DEG C with 1~2 DEG C/min of heating rate, Zhi Houwei
Hold 0.90~0.98MPa of vacuum in tank, the time of 60~65 DEG C of olive oil temperature is 1~3h in tank；
2) under normal pressure state, ozone and oxygen are pressed 1:0.2~0.4 volume ratio mixing, afterwards by mixed gas with 0.5
The speed of~2g/min is passed through vacuum breaker degree in the olive oil in storage tank；Wherein, the intake of ozone and oxygen is with olive oil
Weight is calculated as 40~60g/kg；
3) olive oil in tank is stirred with the speed of 15~30r/min, while applies ultrasonication, ultrasonic wave
The condition of processing is：200~300W of power, 40~60Hz of frequency, 0.5~3h of time；
4) olive oil in tank is pumped out immediately after ultrasonication, sealed packaging preserves afterwards.
Claims (3)
1. a kind of method that ozone is efficiently mutually mixed with vegetable oil, it is characterised in that include the following steps：
1) vegetable oil is pumped into storage tank, applies ultrasonication, the condition of ultrasonication is：200~300W of power, frequency
40~60Hz, 0.5~3h of time, seal, vacuumize afterwards, make vacuum up to 0.90~0.98MPa；Under vacuum conditions, it is right
The oil heating of tank implants, 60~65 DEG C are heated to 1~2 DEG C/min of heating rate by tank implants oil, remain true in tank afterwards
0.90~0.98MPa of reciprocal of duty cycle, the time of 60~65 DEG C of tank implants oil temperature are 1~3h；
2) under normal pressure state, ozone and oxygen are pressed 1:0.2~0.4 volume ratio mixing, afterwards by mixed gas with 0.5~
The speed of 2g/min is passed through vacuum breaker degree in the vegetable oil in storage tank；
3) vegetable oil in tank is stirred with the speed of 15~30r/min, while applies ultrasonication, ultrasonication
Condition be：200~300W of power, 40~60Hz of frequency, 0.5~3h of time；
4) tank implants oil pump is gone out immediately after ultrasonication, sealed packaging preserves afterwards.
2. the method that ozone as claimed in claim 1 is efficiently mutually mixed with vegetable oil, it is characterised in that ozone in the step (2)
Intake 40~60g/kg is calculated as with the weight of vegetable oil.
3. the efficient mutual mixed method of ozone as claimed in claim 1 and vegetable oil, it is characterised in that the vegetable oil is tea oil,
One kind in olive oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711344414.6A CN108018119A (en) | 2017-12-14 | 2017-12-14 | A kind of method that ozone is efficiently mutually mixed with vegetable oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711344414.6A CN108018119A (en) | 2017-12-14 | 2017-12-14 | A kind of method that ozone is efficiently mutually mixed with vegetable oil |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108018119A true CN108018119A (en) | 2018-05-11 |
Family
ID=62073637
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711344414.6A Pending CN108018119A (en) | 2017-12-14 | 2017-12-14 | A kind of method that ozone is efficiently mutually mixed with vegetable oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108018119A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110663700A (en) * | 2019-09-12 | 2020-01-10 | 河北众成七星生物科技有限公司 | Ozone disinfectant and preparation method thereof |
| EP4309506A1 (en) * | 2022-07-22 | 2024-01-24 | Tarullo, Angelo | Improved device for lipid matrices gasification in a temperature controlled environment |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2131673C1 (en) * | 1998-04-17 | 1999-06-20 | Педдер Валерий Викторович | Method of preparing ozonized oil "otrisan" |
| CN2851264Y (en) * | 2005-12-24 | 2006-12-27 | 邸维民 | Ultrasonic vacuum oil purifying device |
| JP2007262120A (en) * | 2006-03-27 | 2007-10-11 | Otech Labo:Kk | Method for producing ozonized vegetable oil |
| CN102406549A (en) * | 2011-09-08 | 2012-04-11 | 李明利 | Device and method for efficiently producing stable ozone (O3) ointment |
| CN107057859A (en) * | 2016-11-11 | 2017-08-18 | 郑州中仁臭氧技术服务有限公司 | A kind of process units and method for efficiently producing ozone carburetion |
-
2017
- 2017-12-14 CN CN201711344414.6A patent/CN108018119A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2131673C1 (en) * | 1998-04-17 | 1999-06-20 | Педдер Валерий Викторович | Method of preparing ozonized oil "otrisan" |
| CN2851264Y (en) * | 2005-12-24 | 2006-12-27 | 邸维民 | Ultrasonic vacuum oil purifying device |
| JP2007262120A (en) * | 2006-03-27 | 2007-10-11 | Otech Labo:Kk | Method for producing ozonized vegetable oil |
| CN102406549A (en) * | 2011-09-08 | 2012-04-11 | 李明利 | Device and method for efficiently producing stable ozone (O3) ointment |
| CN107057859A (en) * | 2016-11-11 | 2017-08-18 | 郑州中仁臭氧技术服务有限公司 | A kind of process units and method for efficiently producing ozone carburetion |
Non-Patent Citations (3)
| Title |
|---|
| （美）汉森等: "《溶出度试验技术》", 30 November 2007, 中国医药科技出版社 * |
| 王宇成: "《最新色谱分析检测方法及应用技术实用手册 第4卷》", 31 December 2004, 银声音像出版社 * |
| 王细洋: "《现代制造技术》", 30 June 2017, 国防工业出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110663700A (en) * | 2019-09-12 | 2020-01-10 | 河北众成七星生物科技有限公司 | Ozone disinfectant and preparation method thereof |
| EP4309506A1 (en) * | 2022-07-22 | 2024-01-24 | Tarullo, Angelo | Improved device for lipid matrices gasification in a temperature controlled environment |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN1203864C (en) | Spray formulation of providone iodine | |
| CN103800979A (en) | Health-care gas generator | |
| CN101072592B (en) | Application of liquid composition for treating wounds and burns in the drugs | |
| CN108295352A (en) | Health care gas generating system | |
| CN108018119A (en) | A kind of method that ozone is efficiently mutually mixed with vegetable oil | |
| CN1850108A (en) | Medical hemostasis anti-adhesive irrigation solution | |
| CN1592627A (en) | Carbon dioxide compositions for external use and process for producing the same | |
| CN1751577A (en) | Composite sterilizing agent contg. silver and zinc, prepn. method and application thereof | |
| CN106994132A (en) | A kind of oral cavity disinfection sanitizer | |
| Gulafsha et al. | Miracle of ozone in dentistry: An overview | |
| CN107028977A (en) | A kind of ozone carburetion complex compound and its preparation method and application | |
| CN108057350A (en) | A kind of solubilization method of ozone in tea oil | |
| CN101972271B (en) | Chlorine dioxide mucous membrane gel and preparation method thereof | |
| CN108096429A (en) | A kind of mouth sprays for alleviating oral peculiar smell and preparation method thereof | |
| Captain | Ozonated Water, Ozonated Water, Ozonated Oil and its Products | |
| CN106491643B (en) | A kind of preparation facilities and preparation method of plasma-activated hydrogen peroxide solution | |
| US20150209470A1 (en) | Oxygenated Oil Ointment | |
| CN103156882A (en) | Injection for one-needle removal of hemorrhoids and mole and wart removal paste and preparation method of injection and paste | |
| CN109464455A (en) | A kind of creme for preventing and treating pet body surface bacterium and fungi | |
| CN116602986A (en) | Composite preparation for human tissue | |
| CN202705164U (en) | Sterile water supply device | |
| CA2299205A1 (en) | Super-oxygenated water solutions and methods of use | |
| CN104127396B (en) | A kind of antibacterials and its preparation method and application | |
| CN105596362A (en) | Energy liquid powder mineral supplement and activation method | |
| CN1090960C (en) | Preparation of onychomycosis liquor |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20180511 |
|
| WD01 | Invention patent application deemed withdrawn after publication |