CN108002902A - One kind sustained release fertilizer granules and its production method - Google Patents

One kind sustained release fertilizer granules and its production method Download PDF

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Publication number
CN108002902A
CN108002902A CN201711235907.6A CN201711235907A CN108002902A CN 108002902 A CN108002902 A CN 108002902A CN 201711235907 A CN201711235907 A CN 201711235907A CN 108002902 A CN108002902 A CN 108002902A
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CN
China
Prior art keywords
fertilizer
sustained release
production method
agent
plant growth
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711235907.6A
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Chinese (zh)
Inventor
孟祥光
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jinzhou Shuofeng Pesticide Group Co Ltd
Original Assignee
Jinzhou Shuofeng Pesticide Group Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jinzhou Shuofeng Pesticide Group Co Ltd filed Critical Jinzhou Shuofeng Pesticide Group Co Ltd
Priority to CN201711235907.6A priority Critical patent/CN108002902A/en
Publication of CN108002902A publication Critical patent/CN108002902A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B7/00Fertilisers based essentially on alkali or ammonium orthophosphates
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/60Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/80Soil conditioners
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00Fertilisers characterised by their form
    • C05G5/30Layered or coated, e.g. dust-preventing coatings

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  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Soil Sciences (AREA)
  • Plant Pathology (AREA)
  • Fertilizers (AREA)

Abstract

One kind sustained release fertilizer granules and its production method, are consisted of the following compositions by mass percentage:Pesticide 0.01%~80%;Fertilizer 5%~90%;Plant growth regulator 0.1%~10%;Auxiliary agent 1%~12%;Filler surplus;The dinotefuran or Diacloden, the auxiliary agent are at least one of wetting agent, tackifier, dispersant, emulsifying agent.Pesticide, plant growth regulator, auxiliary agent and water are added in sand mill, agricultural-chemical suspension liquid is made in clipped sand milling;Fertilizer and filler are mixed, are granulated, Drying and cooling, screening, are made fertiliser granulates;Agricultural-chemical suspension liquid is sprayed into coating on fertiliser granulates, is uniformly mixed, medicine fertilizer particle is made and obtains product.Advantage is:The efficient medicine fertilizer that pesticide, fertilizer, plant growth regulator make, which has, simplifies operation, saves labour, plays the role of obvious effect of increasing production and improving quality to crop, can effectively prevent field subterranean pest-insect.

Description

One kind sustained release fertilizer granules and its production method
Technical field
The invention belongs to medicament-fertilizer mixture field, and the present invention relates to one kind sustained release fertilizer granules and its production method.
Background technology
Medicine fertilizer is the new technology agriculturally used in recent years, refers to have and kills suppression crop pests or plant growth tune One or more kinds of functions in section, and nutrition can be provided for crops or have at the same time provide nutrition and improve fertilizer and The multi-Functional Fertilizers of pesticide utilization rate, have and simplify operation, save labour, raising fertilizer efficiency and drug effect, reduce pesticide cost, reduce The features such as hazard of pesticides.
Medicine fertilizer report of the domestic and foreign literature report containing dinotefuran, Diacloden is more, but is related to itself and plant growth regulator And the report that fertilizer is applied together is actually rare, only Ba Sifu companies application PCT Patent WO2010092032A refer to it is short Strong element is mixed and applies for Chinese patent CN102307478A at the same time.But containing one kind in dinotefuran, Diacloden, plant growth regulating The ternary composition of agent and fertilizer has no report.
The content of the invention
The technical problem to be solved in the present invention is to provide one kind sustained release fertilizer granules and its production method, the medicament-fertilizer mixture Double action with pesticide and fertilizer, can both prevent crop pests, and improve plant vitality and insect pest ability, and can Soil is improved, adjusts the soil nitrogen, phosphorus, the content of potassium, plant growth regulator can also improve crops quality, and it is mixed to improve medicine fertilizer The utilization rate of agent, saves labour turnover.
The present invention technical solution be:
One kind sustained release fertilizer granules, are consisted of the following compositions by mass percentage:
The dinotefuran or Diacloden, the auxiliary agent are at least one of wetting agent, tackifier, dispersant, emulsifying agent.
Further, it is described a kind of containing Diacloden, plant growth regulator, fertilizer mixture, had by mass fraction by following Imitate component composition:
Further, the plant growth regulator is 6- benzylaminopurines, paclobutrazol, indolebutyric acid, heteroauxin At least one of.
Further, the fertilizer is at least one of organic fertilizer, inorganic fertilizer, micro- fertilizer.
Further, the inorganic fertilizer is nitrogenous fertilizer, phosphate fertilizer and potash fertilizer, and the nitrogenous fertilizer is one in urea, nitramine, sulphur ammonium Kind;Micro- fertilizer is at least one of zinc sulfate, boric acid, cobalt chloride;The organic fertilizer is humic acid, in plant ash, stalk At least one.
Further, in terms of material content, auxiliary agent is by mass percentage into being grouped into:4%~5% wetting agent, 4% ~5% dispersant, 0.2%~2% thickener.
Further, the auxiliary agent is aromatics sulphur including suitable surfactant (wetting agent, tackifier or dispersant) Acid such as wetting agent sodium lignosulfonate, dispersant morwetD425, dispersant NNO, wetting agent morwetEFW, wetting agent dodecane Base sodium sulphate, Lignosite;Thickener (assigns the mobility that preparaton improves, i.e., has high viscosity under static state And there is the compound of low viscosity in whipping process) example be polysaccharide and organic and inorganic clay, as soluble starch, Xanthans, organic boron-moisten soil, sodium carboxymethylcellulose.
Further, filler for mineral soil at least one of such as kaolin, diatomite, ground synthetic material, with And the product such as shuck powder from plant.
Further, the preparation method of the efficient medicine fertilizer is as follows:
Pesticide, plant growth regulator, auxiliary agent and water are added in sand mill, agricultural-chemical suspension liquid is made in clipped sand milling;Will Fertilizer and filler mixing, are granulated, Drying and cooling, screening, are made fertiliser granulates;Agricultural-chemical suspension liquid is sprayed into coating in fertiliser granulates On, it is uniformly mixed, medicine fertilizer particle is made and obtains product.
Further, the preparation method of the efficient medicine fertilizer is as follows:
Added after pesticide, fertilizer, plant growth regulator, auxiliary agent and filler are measured in mixer, start stirring, be uniformly mixed Afterwards, it is put into intermediate bunker, is crushed by ultrafine crusher.The material crushed addition adhesive is mixed, is treated After mixing, it is granulated by comminutor, up to dinotefuran/Diacloden Granular pesticide fertilizer product.
The beneficial effects of the invention are as follows:
The efficient medicine fertilizer that pesticide, fertilizer, plant growth regulator make, which has, to be simplified operation, saves labour, improves fertilizer efficiency and medicine Effect, reduce agriculture this features such as.And energy storage can be promoted, and improving cell permeability, regulation of physiological functions, increases chlorophyll content, Rate of photosynthisis is improved, strengthens the activity of enzyme, promotes mineral absorption, promotes seed to sprout, root system root of hair, improves ripe, increase Protein content and amount of dry matter, play the role of crop obvious effect of increasing production and improving quality, can effectively prevent field Subterranean pest-insect, the especially prevention to the snout moth's larva of rice, rice water weevil, grub, and improve the yield of crops.
Embodiment
The present invention is further described with reference to specific embodiment, but does not limit the invention to these tools Body embodiment.One skilled in the art would recognize that present invention encompasses may include in Claims scope All alternatives, improvement project and equivalents.
Embodiment 1
Efficient medicine fertilizer mass percentage is as follows:
Preparation method:
By 5kg dinotefuran, 6- benzylaminopurine 1kg and 30kg water, 5kg sodium lignin sulfonates and 4kg dispersants The organic boron-moisten soil of morwetD425,2kg is added in sand mill, and agricultural-chemical suspension liquid is made in clipped sand milling;By 10kg urea, 20kg potassium dihydrogen phosphates, 5kg humic acid, the mixing of 48kg shucks powder, are granulated, Drying and cooling, screening, are made fertiliser granulates;Will Agricultural-chemical suspension liquid sprays coating on fertiliser granulates, is uniformly mixed, medicine fertilizer particle is made and obtains product.
Embodiment 2
Efficient medicine fertilizer mass percentage is as follows:
Processing method:It is processed using " dry method ", specifically by recipe requirements, by various auxiliary agents, filler, adds after active compound metering In mixer, stirring is started, after mixing, is put into intermediate bunker, is crushed by ultrafine crusher.By what is crushed Material add adhesive mixed, it is to be mixed uniformly after, be granulated by comminutor, up to 10% dinotefuran granules medicine fertilizer production Product.
Embodiment 3
Efficient medicine fertilizer mass percentage is as follows:
Processing method:It is processed using " dry method ", specifically by recipe requirements, by various auxiliary agents, filler, adds after active compound metering In mixer, stirring is started, after mixing, is put into intermediate bunker, is crushed by ultrafine crusher.By what is crushed Material add adhesive mixed, it is to be mixed uniformly after, be granulated by comminutor, up to 20% Diacloden granular pesticide fertilizer produce Product.
The prevention peanut grub field trial report of dinotefuran medicament-fertilizer mixture:
1st, crop title:Peanut
2nd, subjects:Subterranean pest-insect
3rd, test medicine:Medicament-fertilizer mixture prepared by the embodiment of the present invention 1,2;
Comparison medicament:10% chlopyrifos granule;
4th, reagent agent experimental design
1 reagent agent experimental design 1 of table, for studying thing:Peanut (white sand 1016)
5th, processing area:Each 33 square metres of cell (4 ridges, 0.55 meter of row spacing, ridge grow 15 meters), 7 processing, 3 repetitions, at random Arrangement;
Cell distribution such as table 1:
Table 1
S1 S2 S3 S4 S5 S6 S7
S5 S6 S7 S1 S2 S3 S4
S2 S3 S4 S5 S6 S7 S1
6th, dispenser period and method are fertile using byfurrow method dispenser when May 4, peanut seeding closed ridge.May 11 was sowed
7th, investigation result and analysis
1) drug effect:Inquiry agency is investigated with plant in all sprout seedling stage and florescence of peanut, records aggrieved strain number, investigation result such as table 2:
Table 2
Investigate the date:July 15
2) yield application form
Survey the production date:September 24 days
3) security:7 days after dispenser, crop growth is observed within 15 days, 30 days normally without poisoning generation;
4) interpretation of result:
By result above as it can be seen that the anti-subterranean pest-insect effect highest of 1,30,000 grams/acre of embodiment (commodity amount), preventive effect reach 83.33%, per mu yield is also up to 197.10 kilograms;Secondly 2 medicine of embodiment fertilizer 30,000 grams/acre (commodity amounts), preventive effect are 78.79%, yield is 193.76 thousand grams/acre.Each embodiment has insecticidal activity.
It these are only the specific embodiment of the present invention, be not intended to limit the invention, for those skilled in the art For member, the invention may be variously modified and varied.Any modification within the spirit and principles of the invention, being made, Equivalent substitution, improvement etc., should all be included in the protection scope of the present invention.

Claims (10)

1. one kind sustained release fertilizer granules and its production method, it is characterized in that:Consisted of the following compositions by mass percentage:
The dinotefuran or Diacloden, the auxiliary agent are at least one of wetting agent, tackifier, dispersant, emulsifying agent.
2. sustained release fertilizer granules according to claim 1, it is characterized in that:It is described a kind of containing Diacloden, plant growth tune Agent, fertilizer mixture are saved, is made of by mass fraction following active ingredient:
3. sustained release fertilizer granules according to claim 1, it is characterized in that:The plant growth regulator is 6- benzyl ammonia At least one of base purine, paclobutrazol, indolebutyric acid, heteroauxin.
4. sustained release fertilizer granules according to claim 1 and its production method, it is characterized in that:The fertilizer is organic At least one of fertilizer, inorganic fertilizer, micro- fertilizer.
5. sustained release fertilizer granules according to claim 1 and its production method, it is characterized in that:The inorganic fertilizer is nitrogen Fertilizer, phosphate fertilizer and potash fertilizer, the nitrogenous fertilizer is urea, one kind in nitramine, sulphur ammonium;Micro- fertilizer is zinc sulfate, in boric acid, cobalt chloride At least one;The organic fertilizer is at least one of humic acid, plant ash, stalk.
6. sustained release fertilizer granules according to claim 1 and its production method, it is characterized in that:In terms of material content, help Agent is by mass percentage into being grouped into:4%~5% wetting agent, 4%~5% dispersant and 0.2%~2% thickener.
7. sustained release fertilizer granules according to claim 1, it is characterized in that:The auxiliary agent include wetting agent, thickener and Dispersant, the wetting agent are sodium lignosulfonate, wetting agent morwetEFW, wetting agent, lauryl sodium sulfate or lignosulphonic acid Calcium;The dispersant is dispersant morwetD425 or dispersant NNO;The thickener is soluble starch, xanthans, organic Boron-moisten soil or sodium carboxymethylcellulose.
8. sustained release fertilizer granules according to claim 1 and its production method, it is characterized in that:Filler is kaolin, silicon At least one of diatomaceous earth, or ground synthetic material, or come from the product shuck powder of plant.
9. a kind of production method of sustained release fertilizer granules as claimed in claim 1, it is characterized in that:
Specific preparation process is as follows:
Pesticide, plant growth regulator, auxiliary agent and water are added in sand mill, agricultural-chemical suspension liquid is made in clipped sand milling;Will Fertilizer and filler mixing, are granulated, Drying and cooling, screening, are made fertiliser granulates;Agricultural-chemical suspension liquid is sprayed into coating in fertiliser granulates On, it is uniformly mixed, slow releasing medicinal fertilizer particle is made.
10. a kind of production method of sustained release fertilizer granules as claimed in claim 1, it is characterized in that:
Specific preparation process is as follows:
Added after pesticide, fertilizer, plant growth regulator, auxiliary agent and filler are measured in mixer, start stirring, be uniformly mixed Afterwards, it is put into intermediate bunker, is crushed by ultrafine crusher, the material crushed addition adhesive is mixed, is treated After mixing, it is granulated by comminutor, up to dinotefuran/Diacloden Granular pesticide fertilizer product.
CN201711235907.6A 2017-11-30 2017-11-30 One kind sustained release fertilizer granules and its production method Pending CN108002902A (en)

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Application Number Priority Date Filing Date Title
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Application Number Priority Date Filing Date Title
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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110590452A (en) * 2019-09-30 2019-12-20 中国有色桂林矿产地质研究院有限公司 Preparation method of porous material for slowly-releasing degradable film coated with pesticide fertilizer
CN110590451A (en) * 2019-09-30 2019-12-20 中国有色桂林矿产地质研究院有限公司 Preparation method of selenium-loaded slow-release degradable film-coated porous material
CN112136815A (en) * 2020-10-27 2020-12-29 中诚国联(河南)生物科技有限公司 Preparation and application of pesticide-fertilizer granules containing metalaxyl-M and azoxystrobin
CN112624851A (en) * 2020-12-30 2021-04-09 广西金裕隆农药化工有限公司 Preparation method of urea formaldehyde slow-release granular pesticide fertilizer
CN113372163A (en) * 2021-06-17 2021-09-10 深圳诺普信农化股份有限公司 Clothianidin special pesticide fertilizer and preparation method thereof
CN115043686A (en) * 2022-06-06 2022-09-13 青海国润农业科技有限公司 Regular round granular potash fertilizer granulation auxiliary agent and preparation method thereof

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CN102060618A (en) * 2010-12-13 2011-05-18 湖南大方农化有限公司 Preparation method of water dispersible granule medicinal fertilizer
CN104585215A (en) * 2015-02-09 2015-05-06 湖南神隆超级稻丰产工程有限公司 Method for simply and efficiently producing seeds and cultivating hybrid rice
CN105037024A (en) * 2015-07-09 2015-11-11 广西兄弟农药厂(普通合伙) Pesticide-fertilizer granules containing Monosultap and Thiamethoxam
CN105218232A (en) * 2015-09-28 2016-01-06 广西洪喜肥业有限公司 A kind of longan and Specialized fertilizer for litchi and production method thereof
CN105541506A (en) * 2016-01-06 2016-05-04 联保作物科技有限公司 Paddy-field pesticide-fertilizer sustained release granules and preparing method and application method thereof
CN105601447A (en) * 2016-02-04 2016-05-25 锦州硕丰农药集团有限公司 Dinotefuran slow release pesticide-fertilizer mixture and production method thereof
CN106818732A (en) * 2016-12-15 2017-06-13 东莞市联洲知识产权运营管理有限公司 A kind of rice terrace floating granula and preparation method and application

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102060618A (en) * 2010-12-13 2011-05-18 湖南大方农化有限公司 Preparation method of water dispersible granule medicinal fertilizer
CN104585215A (en) * 2015-02-09 2015-05-06 湖南神隆超级稻丰产工程有限公司 Method for simply and efficiently producing seeds and cultivating hybrid rice
CN105037024A (en) * 2015-07-09 2015-11-11 广西兄弟农药厂(普通合伙) Pesticide-fertilizer granules containing Monosultap and Thiamethoxam
CN105218232A (en) * 2015-09-28 2016-01-06 广西洪喜肥业有限公司 A kind of longan and Specialized fertilizer for litchi and production method thereof
CN105541506A (en) * 2016-01-06 2016-05-04 联保作物科技有限公司 Paddy-field pesticide-fertilizer sustained release granules and preparing method and application method thereof
CN105601447A (en) * 2016-02-04 2016-05-25 锦州硕丰农药集团有限公司 Dinotefuran slow release pesticide-fertilizer mixture and production method thereof
CN106818732A (en) * 2016-12-15 2017-06-13 东莞市联洲知识产权运营管理有限公司 A kind of rice terrace floating granula and preparation method and application

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110590452A (en) * 2019-09-30 2019-12-20 中国有色桂林矿产地质研究院有限公司 Preparation method of porous material for slowly-releasing degradable film coated with pesticide fertilizer
CN110590451A (en) * 2019-09-30 2019-12-20 中国有色桂林矿产地质研究院有限公司 Preparation method of selenium-loaded slow-release degradable film-coated porous material
CN110590452B (en) * 2019-09-30 2022-04-15 中国有色桂林矿产地质研究院有限公司 Preparation method of porous material for slowly-releasing degradable film coated with pesticide fertilizer
CN112136815A (en) * 2020-10-27 2020-12-29 中诚国联(河南)生物科技有限公司 Preparation and application of pesticide-fertilizer granules containing metalaxyl-M and azoxystrobin
CN112624851A (en) * 2020-12-30 2021-04-09 广西金裕隆农药化工有限公司 Preparation method of urea formaldehyde slow-release granular pesticide fertilizer
CN113372163A (en) * 2021-06-17 2021-09-10 深圳诺普信农化股份有限公司 Clothianidin special pesticide fertilizer and preparation method thereof
CN115043686A (en) * 2022-06-06 2022-09-13 青海国润农业科技有限公司 Regular round granular potash fertilizer granulation auxiliary agent and preparation method thereof

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