CN107982422A - A kind of preparation method of stir-baked RHIZOMA POLYGONATI with yellow rice wine medicine materical crude slice - Google Patents
A kind of preparation method of stir-baked RHIZOMA POLYGONATI with yellow rice wine medicine materical crude slice Download PDFInfo
- Publication number
- CN107982422A CN107982422A CN201711473625.XA CN201711473625A CN107982422A CN 107982422 A CN107982422 A CN 107982422A CN 201711473625 A CN201711473625 A CN 201711473625A CN 107982422 A CN107982422 A CN 107982422A
- Authority
- CN
- China
- Prior art keywords
- sealwort
- preparation
- yellow rice
- stir
- rice wine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/896—Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
- A61K36/8969—Polygonatum (Solomon's seal)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/13—Preparation or pretreatment of starting material involving cleaning, e.g. washing or peeling
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/15—Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
Landscapes
- Health & Medical Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Alternative & Traditional Medicine (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Medical Informatics (AREA)
- Medicinal Chemistry (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Pharmacology & Pharmacy (AREA)
- Epidemiology (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a kind of preparation method of stir-baked RHIZOMA POLYGONATI with yellow rice wine medicine materical crude slice, described method includes following steps：(1) select；(2) clean；(3) wine steams；(4) it is predrying；(5) cut into slices；(6) demulcen；(7) it is dry；(6) pack.The extract content ＞ 45% for the stir-baked RHIZOMA POLYGONATI with yellow rice wine medicine materical crude slice that the present invention is prepared, Siberian solomonseal rhizome polysaccharide content ＞ 7%, quality is high, meets stir-baked RHIZOMA POLYGONATI with yellow rice wine prepared slice quality standard；And the method for the present invention has the advantages of simple, to save time and the energy, suitable for industrialized production.
Description
Technical field
The present invention relates to Technology of Processing Chinese Herbal Medicines field, is steamed more particularly, to one kind by yellow rice wine and prepares stir-baked RHIZOMA POLYGONATI with yellow rice wine medicine materical crude slice
Method.
Background technology
Stir-baked RHIZOMA POLYGONATI with yellow rice wine function is with curing mainly：Enrich blood enriching yin, beneficial to spirit and marrow.For blood deficiency chlorosis, palpitation and severe palpitation, irregular menstruation, collapses
Leak down blood, the deficiency of liver-yin and kidney-yin, soreness and weakness of waist and knees, osteopyrexia and fever, night sweat seminal emission, Heat Diabetes, dizziness, tinnitus, poliosis.
Conventional method concocting method have two kinds record in《Chinese Pharmacopoeia》Version one in 2015, be respectively " (1) takes sealwort,
Stew method according to wine, stew to wine and exhaust, take out, dry to crust mucus it is slightly dry when, cut sheet or block, it is dry, to obtain the final product.(2) sealwort is taken,
According to the method for steaming, steam to black profit, take out, shine to when about most probably doing, cut sheet or block, it is dry, to obtain the final product." conventionally produced efficiency is low,
Yield is low, and energy consumption is big, is not suitable for large-scale industrial production.
The content of the invention
In view of the above-mentioned problems existing in the prior art, the applicant provides a kind of preparation side of stir-baked RHIZOMA POLYGONATI with yellow rice wine medicine materical crude slice
Method.The method of the present invention is by selecting, cleaning, wine steaming, predrying, cutting, demulcen, drying and packaging step are formed, the method for the present invention
It is a kind of stir-baked RHIZOMA POLYGONATI with yellow rice wine medicine materical crude slice preparation method that is simple, efficient, saving the energy.
Technical scheme is as follows：
A kind of preparation method of stir-baked RHIZOMA POLYGONATI with yellow rice wine medicine materical crude slice, described method includes following steps：
(1) select：High-quality sealwort medicinal material is selected, goes out decontamination；
(2) clean：The sealwort medicinal material selected is eluriated using medicine-washing machine, after washing, standing drains away the water；
(3) wine steams：Sealwort after cleaning is mixed with wine, place 4~8h, be placed in steamer, carried out by steam
Steam, and collect concoction；
(4) it is predrying：The sealwort that step (3) steams is placed in predrying in baking oven, is dried to water content as 10~15%；
(5) cut into slices：Step (4) pre-dried sealwort is cut into the sealwort piece that thickness is 2~4mm；
(6) demulcen：Sealwort piece made from step (5) is placed in the concoction of step (3) collection, infiltrates 6~12h；
(7) it is dry：It will be placed in by the sealwort piece of step (6) processing in baking oven, be dried to water content less than 13%；
(6) pack：Dried sealwort piece is vacuum-packed, is placed at aeration-drying and stores, the stir-baked RHIZOMA POLYGONATI with yellow rice wine drink is made
Piece.
Medicine-washing machine is tumbling-box type medicine-washing machine in step (2).
Wine described in step (3) is yellow rice wine；The steaming time is 6~14h.
Predrying temperature described in step (4) is 60~80 DEG C.
Section uses turn table type slicer described in step (5).
Drying temperature described in step (7) is 60~80 DEG C.
The present invention is beneficial to be had technical effect that：
The concoction that the present invention steams during steaming is used for demulcen so that its active ingredient can as often as possible enter wine
Play a role, do not waste raw material in sealwort decoction piece.This process carries out demulcen without using other juice, eliminates for other juice
The preparation of liquid.
The extract content ＞ 45% for the stir-baked RHIZOMA POLYGONATI with yellow rice wine medicine materical crude slice that the present invention is prepared, Siberian solomonseal rhizome polysaccharide content ＞ 7%, quality
Height, meets stir-baked RHIZOMA POLYGONATI with yellow rice wine prepared slice quality standard, and preparation method is simple, saves time and the energy, suitable for industrialized production.
Embodiment
With reference to embodiment, the present invention is specifically described.
Embodiment 1
A kind of preparation method of stir-baked RHIZOMA POLYGONATI with yellow rice wine medicine materical crude slice, described method includes following steps：
(1) select：High-quality sealwort medicinal material is selected, goes out decontamination；
(2) clean：The sealwort medicinal material selected is eluriated using tumbling-box type medicine-washing machine, after washing, standing drains away the water；
(3) wine steams：Sealwort after cleaning is mixed with yellow rice wine, place 8h, be placed in steamer, steamed by steam
7h processed, and collect concoction；
(4) it is predrying：The sealwort that step (3) steams is placed in predrying in 60 DEG C of baking ovens, is dried to water content as 15%；
(5) cut into slices：Use turn table type slicer that step (4) pre-dried sealwort is cut into sealwort piece of the thickness for 4mm；
(6) demulcen：Sealwort piece made from step (5) is placed in the concoction of step (3) collection, infiltrates 12h；
(7) it is dry：It will be placed in by the sealwort piece of step (6) processing in baking oven, be dried to water content as 12%；
(6) pack：Dried sealwort piece is vacuum-packed, is placed at aeration-drying and stores, the stir-baked RHIZOMA POLYGONATI with yellow rice wine drink is made
Piece.
Embodiment 2
A kind of preparation method of stir-baked RHIZOMA POLYGONATI with yellow rice wine medicine materical crude slice, described method includes following steps：
(1) select：High-quality sealwort medicinal material is selected, goes out decontamination；
(2) clean：The sealwort medicinal material selected is eluriated using tumbling-box type medicine-washing machine, after washing, standing drains away the water；
(3) wine steams：Sealwort after cleaning is mixed with yellow rice wine, place 4h, be placed in steamer, steamed by steam
11h processed, and collect concoction；
(4) it is predrying：The sealwort that step (3) steams is placed in predrying in 70 DEG C of baking ovens, is dried to water content as 12%；
(5) cut into slices：Use turn table type slicer that step (4) pre-dried sealwort is cut into sealwort piece of the thickness for 2mm；
(6) demulcen：Sealwort piece made from step (5) is placed in the concoction of step (3) collection, infiltrates 6h；
(7) it is dry：It will be placed in by the sealwort piece of step (6) processing in baking oven, be dried to water content as 13%；
(6) pack：Dried sealwort piece is vacuum-packed, is placed at aeration-drying and stores, the stir-baked RHIZOMA POLYGONATI with yellow rice wine drink is made
Piece.
Embodiment 3
A kind of preparation method of stir-baked RHIZOMA POLYGONATI with yellow rice wine medicine materical crude slice, described method includes following steps：
(1) select：High-quality sealwort medicinal material is selected, goes out decontamination；
(2) clean：The sealwort medicinal material selected is eluriated using tumbling-box type medicine-washing machine, after washing, standing drains away the water；
(3) wine steams：Sealwort after cleaning is mixed with yellow rice wine, place 6h, be placed in steamer, steamed by steam
9h processed, and collect concoction；
(4) it is predrying：The sealwort that step (3) steams is placed in predrying in 80 DEG C of baking ovens, is dried to water content as 10%；
(5) cut into slices：Use turn table type slicer that step (4) pre-dried sealwort is cut into sealwort piece of the thickness for 3mm；
(6) demulcen：Sealwort piece made from step (5) is placed in the concoction of step (3) collection, infiltrates 10h；
(7) it is dry：It will be placed in by the sealwort piece of step (6) processing in baking oven, be dried to water content as 10%；
(6) pack：Dried sealwort piece is vacuum-packed, is placed at aeration-drying and stores, the stir-baked RHIZOMA POLYGONATI with yellow rice wine drink is made
Piece.
Embodiment 4
Difference from Example 1 is only that, step (3) be passed through steam steam 6 it is small when, glutinous rehmannia section after steaming
There is gold zone.Remaining step is same as Example 1.
Embodiment 5
Difference from Example 1 is only that, step (3) be passed through steam steam 14 it is small when, glutinous rehmannia is broken after steaming
Face corvinus.Remaining step is same as Example 1.
Embodiment 6
Difference from Example 1 is only that it is 10% that water content is dried at 80 DEG C, remaining step and 1 phase of embodiment
Together.
Embodiment 7
Difference from Example 1 is only that, step (7) is dried to water content 13% at 75 DEG C, remaining step and reality
It is identical to apply example 1.
Test case：
The stir-baked RHIZOMA POLYGONATI with yellow rice wine medicine materical crude slice that Example 1~7 is prepared respectively, smashes, respectively takes lg, adds 70% ethanol 20ml,
Be heated to reflux 1 it is small when, filter, filtrate is evaporated, and residue adds water l0ml to make dissolving, adds n-butanol shaking extraction 2 times, each 20ml,
Merge n-butanol liquid, be evaporated, residue adds methanol lml to make dissolving, as test solution.Separately take sealwort control medicinal material lg, same to method
Control medicinal material solution is made.Tested according to thin-layered chromatography (general rule 0502), draw each l0 μ l of above two solution, put respectively in same
On one silica gel g thin-layer plate, with petroleum ether (60~90 DEG C)-acetic ether-methanoic acid (5:2:0.1) it is solvent, is unfolded, takes out,
Dry, spray with 5% vanillin-sulfuric acid solution, it is clear to be heated to spot development at 105 DEG C.In test sample chromatography, with comparison medicine
Wood color is composed on corresponding position, shows the spot of same color.The content value of each component of measure is as shown in table 1.
Table 1
| Extract content | Siberian solomonseal rhizome polysaccharide content | |
| Embodiment 1 | 45.8% | 7.2% |
| Embodiment 2 | 46.2% | 7.5% |
| Embodiment 3 | 47.5% | 7.9% |
| Embodiment 4 | 44.8% | 6.3% |
| Embodiment 5 | 44.3% | 6.7% |
| Embodiment 6 | 44.5% | 6.1% |
| Embodiment 7 | 43.7% | 6.5% |
The extract content for the stir-baked RHIZOMA POLYGONATI with yellow rice wine medicine materical crude slice that the method for the present invention is prepared can be high it can be seen from the data of table 1
Up to 45.8-47.5%, Siberian solomonseal rhizome polysaccharide content is 7.2-7.9%, and quality is high, meets stir-baked RHIZOMA POLYGONATI with yellow rice wine prepared slice quality standard.
Applicant states that the present invention illustrates the method detailed of the present invention, but not office of the invention by above-described embodiment
It is limited to above-mentioned method detailed, that is, does not mean that the present invention has to rely on above-mentioned method detailed and could implement.Technical field
Technical staff it will be clearly understood that any improvement in the present invention, equivalence replacement and auxiliary element to each raw material of product of the present invention
Addition, selection of concrete mode etc., all fall within protection scope of the present invention and the open scope.
Claims (6)
1. a kind of preparation method of stir-baked RHIZOMA POLYGONATI with yellow rice wine medicine materical crude slice, it is characterised in that described method includes following steps：
(1) select：High-quality sealwort medicinal material is selected, goes out decontamination；
(2) clean：The sealwort medicinal material selected is eluriated using medicine-washing machine, after washing, standing drains away the water；
(3) wine steams：Sealwort after cleaning is mixed with wine, place 4~8h, be placed in steamer, steamed by steam,
And collect concoction；
(4) it is predrying：The sealwort that step (3) steams is placed in predrying in baking oven, is dried to water content as 10~15%；
(5) cut into slices：Step (4) pre-dried sealwort is cut into the sealwort piece that thickness is 2~4mm；
(6) demulcen：Sealwort piece made from step (5) is placed in the concoction of step (3) collection, infiltrates 6~12h；
(7) it is dry：It will be placed in by the sealwort piece of step (6) processing in baking oven, be dried to water content less than 13%；
(6) pack：Dried sealwort piece is vacuum-packed, is placed at aeration-drying and stores, the stir-baked RHIZOMA POLYGONATI with yellow rice wine medicine materical crude slice is made.
2. preparation method according to claim 1, it is characterised in that medicine-washing machine is tumbling-box type medicine-washing machine in step (2).
3. preparation method according to claim 1, it is characterised in that wine described in step (3) is yellow rice wine；It is described when steaming
Between be 6~14h.
4. preparation method according to claim 1, it is characterised in that predrying temperature described in step (4) is 60~80
℃。
5. preparation method according to claim 1, it is characterised in that section is cut into slices using rotating disc type described in step (5)
Machine.
6. preparation method according to claim 1, it is characterised in that drying temperature described in step (7) is 60~80 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711473625.XA CN107982422A (en) | 2017-12-29 | 2017-12-29 | A kind of preparation method of stir-baked RHIZOMA POLYGONATI with yellow rice wine medicine materical crude slice |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711473625.XA CN107982422A (en) | 2017-12-29 | 2017-12-29 | A kind of preparation method of stir-baked RHIZOMA POLYGONATI with yellow rice wine medicine materical crude slice |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107982422A true CN107982422A (en) | 2018-05-04 |
Family
ID=62043321
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711473625.XA Pending CN107982422A (en) | 2017-12-29 | 2017-12-29 | A kind of preparation method of stir-baked RHIZOMA POLYGONATI with yellow rice wine medicine materical crude slice |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107982422A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108562685A (en) * | 2018-06-26 | 2018-09-21 | 成都中医药大学 | A kind of sealwort, mulberry leaf and radix polygonati officinalis compatibe drug composition quality detection method |
| CN108936648A (en) * | 2018-07-25 | 2018-12-07 | 贵州京源生态农业发展有限公司 | A kind of preparation method of anti-mildew rhizoma polygonati piece |
| CN112516247A (en) * | 2020-12-31 | 2021-03-19 | 安顺市长寿欣新中药发展有限公司 | Preparation method of traditional Chinese medicine rhizoma polygonati decoction pieces |
| CN113876887A (en) * | 2021-10-01 | 2022-01-04 | 浙江禾田兴生物科技有限公司 | Rhizoma polygonati processing method |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104147351A (en) * | 2013-12-14 | 2014-11-19 | 郑州瑞龙制药股份有限公司 | Method for preparing wine processed polygonatum kingianum decoction piece |
| CN105412579A (en) * | 2015-11-23 | 2016-03-23 | 宁国千方中药发展有限公司 | Preparing method for manyflower solomonseal rhizome decoction pieces |
| CN107224522A (en) * | 2017-06-26 | 2017-10-03 | 四川农业大学 | A kind of Preparation process method of stir-baked RHIZOMA POLYGONATI with yellow rice wine |
-
2017
- 2017-12-29 CN CN201711473625.XA patent/CN107982422A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104147351A (en) * | 2013-12-14 | 2014-11-19 | 郑州瑞龙制药股份有限公司 | Method for preparing wine processed polygonatum kingianum decoction piece |
| CN105412579A (en) * | 2015-11-23 | 2016-03-23 | 宁国千方中药发展有限公司 | Preparing method for manyflower solomonseal rhizome decoction pieces |
| CN107224522A (en) * | 2017-06-26 | 2017-10-03 | 四川农业大学 | A kind of Preparation process method of stir-baked RHIZOMA POLYGONATI with yellow rice wine |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108562685A (en) * | 2018-06-26 | 2018-09-21 | 成都中医药大学 | A kind of sealwort, mulberry leaf and radix polygonati officinalis compatibe drug composition quality detection method |
| CN108562685B (en) * | 2018-06-26 | 2020-05-12 | 成都中医药大学 | Quality detection method for rhizoma polygonati, folium mori and radix polygonati officinalis combined pharmaceutical composition |
| CN108936648A (en) * | 2018-07-25 | 2018-12-07 | 贵州京源生态农业发展有限公司 | A kind of preparation method of anti-mildew rhizoma polygonati piece |
| CN112516247A (en) * | 2020-12-31 | 2021-03-19 | 安顺市长寿欣新中药发展有限公司 | Preparation method of traditional Chinese medicine rhizoma polygonati decoction pieces |
| CN113876887A (en) * | 2021-10-01 | 2022-01-04 | 浙江禾田兴生物科技有限公司 | Rhizoma polygonati processing method |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107982422A (en) | A kind of preparation method of stir-baked RHIZOMA POLYGONATI with yellow rice wine medicine materical crude slice | |
| CN106334029A (en) | Method for preparing prepared rehmannia root decoction pieces | |
| CN104106692A (en) | Buckwheat tea bag and preparation method thereof | |
| CN104432381B (en) | A kind of honeysuckle health-care beverage and preparation method thereof | |
| CN103285305B (en) | Preparation method of prepared rehmannia root decoction piece | |
| CN103893274B (en) | A kind of concocting method of wine Herba Cistanches | |
| CN109646572A (en) | A kind of concocting method of sealwort decoction piece | |
| CN106109624A (en) | A kind of Herba Potentillae Discoloris fresh squeezing spray-dried powders decoction pieces and preparation technology thereof | |
| CN103013669B (en) | Preparation method of tobacco leaf moisturizing liquor for lowering tar content and benzopyrene content | |
| CN103071006A (en) | Preparation method and quality inspection method of traditional Chinese medicine for treating kidney failure | |
| CN103099830A (en) | Processing method of vinegar-baked bupleurum root and applications thereof | |
| CN106109544A (en) | A kind of Herba Euphorbiae Humifusae is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof | |
| CN106085750A (en) | A kind of processing method of Rhizoma Bistortae Radix ziziphi mauritianae health promoting wine | |
| CN103446195A (en) | Preparation method of ginkgo biloba extract | |
| CN102416028A (en) | Preparation method of cooked panax notoginseng extract and total ripe panax notoginseng saponins | |
| CN102727548A (en) | New technology and method for extracting ginseng stem and leaf total saponin | |
| CN103417626A (en) | Energy-saving preparation method for high-purity baical skullcap root extract | |
| CN103480177A (en) | Extraction technology optimization method | |
| CN104367622A (en) | Method for extracting alkaloids from herba leonuri | |
| CN110251562A (en) | A kind of preparation method of wine fruit of glossy privet medicine materical crude slice | |
| CN108066383A (en) | A kind of wine-prepared fructus corni medicine materical crude slice and preparation method thereof | |
| CN108126000A (en) | Arasaponin extracts preparation method in fresh Radix Notoginseng | |
| CN110251583A (en) | A kind of preparation method of steamed FRUCTUS SCHISANDRAE with vinegar medicine materical crude slice | |
| CN113616733A (en) | Rhizoma polygonati processing method | |
| CN102940724A (en) | Preparation method of traditional Chinese medicine compound capsule for diminishing inflammation |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180504 |
|
| RJ01 | Rejection of invention patent application after publication |