CN107982172A - A kind of radiation protection containing lily leaf extract, anti-apolexis composition and preparation method thereof - Google Patents
A kind of radiation protection containing lily leaf extract, anti-apolexis composition and preparation method thereof Download PDFInfo
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- CN107982172A CN107982172A CN201711363484.6A CN201711363484A CN107982172A CN 107982172 A CN107982172 A CN 107982172A CN 201711363484 A CN201711363484 A CN 201711363484A CN 107982172 A CN107982172 A CN 107982172A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
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- Veterinary Medicine (AREA)
- Dermatology (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Medicines Containing Plant Substances (AREA)
- Cosmetics (AREA)
Abstract
The present invention provides a kind of radiation protection containing lily leaf extract, anti-apolexis composition, include the component of following parts by weight：6 10 parts of lily leaf extract, 6 10 parts of side Bao Mao nonirrigated farmlands chrysanthemum extract, 35 parts of daye tea extract.The free radical scavenging activity of said composition is high, and anti-aging effects are good, and said composition also has preferable radiation-proof effect, and safe and non-stimulating.
Description
Technical field
The present invention relates to a kind of radiation protection containing lily leaf extract, anti-apolexis composition with and preparation method thereof.
Background technology
Skin is the largest organ for being covered in human body surface, due to directly being contacted with external environment, aoxidized, dried,
The stimulation of a variety of tension-causing factors such as ultraviolet, is highly susceptible to injure.Meanwhile and because age, diet and habits and customs etc.
The influence of internal factor, causes the decline of skin function and hereditary abnormalization, so that skin is more prone to aging.
In recent years, as the continuous improvement of people's living standard and itself health care consciousness, people become more concerned with itself
" anti-aging " of organ.According to investigations：After 20 years old (especially women), the aging of worry skin is begun to.It is so anti-aging
Cosmetics have become one of product of vast female consumer active demand.
Ionising radiation (such as x-ray, neutron, proton, α or β particles, gamma-rays) can be directly or by secondary reaction infringement group
Knit.High dose radiation can produce visible body effect within a couple of days.DNA changes caused by low dose can produce illuminated person
Chronic disease, makes relation between the healing or death of their offspring's development genetics defect degree of injury and cell very
It is complicated.Harmful ionized radiation source is including being used for high-energy X-ray, radium and other naturally occurring radioactive substances of diagnose and treat (such as
Radon), nuclear reactor, cyclotron, linear accelerator, variable gradient synchrotron, the cobalt of the sealing for treating cancerous swelling
With caesium and be largely used to medicine and industry artificially generated radioactive substance.After sufficiently high dose irradiation, it can occur
Meronecrosis.High sublethal dose can slow down DNA synthesis or cell is become polypoid by reducing mitosis rate, and
The propagation of interference cell.It can be produced after being carried out continuously the tissue (such as enteric epithelium, marrow, sexual gland) of renewal via radiation dose-dependent
Progressive hypoplasia, atrophy, final fibrosis.It is some to be damaged but can still provide for mitotic cell, before its death also
Abnormal offspring (such as huge metamylocyte, the excessive neutrophil of leaflet) can be produced through 1 or 2 cyclostage.Have
According to the report, separately add the time-to-live of animal of the animal survival time than only receiving background exposure of very low dose irradiation long.It is long
People are finding radioprotectant since phase, but do not find out a preferable medicine yet so far and be used to treat and prevent radiation institute
The toxic side effect of cause.
Lily is Liliaceae lilium perennial herb bulbous plant, is mainly distributed on east Asia, Europe, North America etc.
Northern Hemisphere Temperate Region in China, the whole world have had found a kind more than hundred, and China is its most important area of origin, originate in kind more than 50, are
Lily NATURAL DISTRIBUTION center.Lily is removed containing the battalion such as starch, protein, fat and calcium, phosphorus, iron, vitamin B1, B2, C
It is outer to support element, also containing some special nutritional ingredients, a variety of alkaloids of such as colchicin.These component comprehensive functions are in people
Body, the work(not only with good nutritious tonifying, but also have one to a variety of Seasonal diseases caused by dry in autumn
Fixed preventive and therapeutic effect.Say that fresh lily bulb has mental-tranquilization in the traditional Chinese medical science, the effect of moistening the lung and relieve the cough, have very much to the people of eak after being ill
Benefit.Bulbus Lilii extract Yin nourishing and lung moistening, clearing away the heart fire and tranquillizing.For yin chronic cough, blood-stained sputum, dysphoria palpitates with fear, insomnia and dreamful sleep, spirit is all of a sudden
Hu.In the prior art by compound less of Flos Lilii viriduli extract and other compositions.
The content of the invention
It is an object of the present invention to provide a kind of radiation protection containing lily leaf extract, anti-apolexis composition and its
Preparation method, which not only has preferable anti-senescence function, but also can play the role of radiation protection.
To achieve the above object, the technical solution used in the present invention：It is a kind of anti-aging containing lily leaf extract, net
White composition, includes the component of following parts by weight：It is 6-10 parts of lily leaf extract, 6-10 parts of side Bao Mao nonirrigated farmlands chrysanthemum extract, big
3-5 parts of leaf tea extract.
Single extract is usually used in the prior art and carries out anti-aging or radiation protection, but its effect is not managed as far as possible
Thinking, present inventor has found by numerous studies, and lily leaf extract, side Bao Mao nonirrigated farmlands chrysanthemum extract are compounded, its
Anti-aging effects are significantly better than independent extract；Lily leaf extract, daye tea extract are compounded, its radiation-proof effect
It is significantly better than independent extract.
Preferably, the weight ratio of the lily leaf extract and side Bao Mao nonirrigated farmlands chrysanthemum extract is 1:1.Present inventor
Find by numerous studies, match herein, its anti-aging effects is optimal.
Preferably, the weight ratio of the lily leaf extract and daye tea extract is 2:1.Present inventor is through excessive
Quantity research is found, is matched herein, its radiation-proof effect is optimal.
Preferably, the radiation protection, anti-apolexis composition further include preservative, pH adjusting agent, thickener, emulsifying agent, perfume (or spice)
Essence, pigment and water.
Preferably, the emulsifying agent is selected from ceteareth -6, ceteareth -25, glycerol monostearate
Ester, the emollient be selected from White Mineral Oil, stearic acid, cetostearyl alcohol, olive oil, octanoic acid/certain herbaceous plants with big flowers acid triglyceride, shea butter,
Jojoba oil, silicone oil, the skin moisturizer are selected from glycerine, propane diols, 1,3 butanediols.
The present invention provides radiation protection described above, the preparation method of anti-apolexis composition, the preparation method be by
Each component raw material precise by weight ratio, is sufficiently mixed and stirs evenly, that is, obtains the composition.
Preferably, the radiation protection, the formulation of anti-apolexis composition are aqua, creme, finish, washing lotion or emulsion.
The present invention provides a kind of radiation protection, anti-aging skin care product, including oil phase, water phase, the water mutually includes above-mentioned institute
The radiation protection stated, anti-apolexis composition.
Preferably, the radiation protection, anti-aging skin care product further include essence and preservative.
The beneficial effects of the present invention are：The present invention provides a kind of anti-aging containing lily leaf extract, white group net
Compound, the free radical scavenging activity of said composition is high, and anti-aging effects are good, and said composition also has preferable radiation-proof effect, and
It is and safe and non-stimulating.
Embodiment
Each raw material involved by following embodiments is the commercially available universal product unless otherwise instructed.
The preparation method of lily leaf extract of the present invention is：10 times of water is added after Bulbus Lilii leaf is smashed to pieces to carry out it
Extraction, 90-95 DEG C of the temperature of extraction, extraction time are 4 times, and water extract is obtained after concentrate drying；Bulbus Lilii leaf after extraction
Ethanol is added in powder, alcohol content is reached more than 70wt% and is extracted, ethanol extract is obtained after concentrate drying, water is extracted
Thing and ethanol extract merge, up to lily leaf extract.
Embodiment 1
Radiation protection of the present invention, a kind of embodiment of anti-apolexis composition, the composition include following parts by weight
Component：8 parts of lily leaf extract, 8 parts of side Bao Mao nonirrigated farmlands chrysanthemum extract, 4 parts of daye tea extract.
Embodiment 2
Radiation protection of the present invention, a kind of embodiment of anti-apolexis composition, the composition include following parts by weight
Component：6 parts of lily leaf extract, 10 parts of side Bao Mao nonirrigated farmlands chrysanthemum extract, 4 parts of daye tea extract.
Embodiment 3
Radiation protection of the present invention, a kind of embodiment of anti-apolexis composition, the composition include following parts by weight
Component：10 parts of lily leaf extract, 6 parts of side Bao Mao nonirrigated farmlands chrysanthemum extract, 4 parts of daye tea extract.
Comparative example 1
The formula of comparative example 1 is：16 parts by weight of lily leaf extract, 4 parts by weight of daye tea extract.
Comparative example 2
The formula of comparative example 2 is：16 parts by weight of side Bao Mao nonirrigated farmlands chrysanthemum extract., 4 parts by weight of daye tea extract.
The preparation method of embodiment 1-3 and comparative example 1,2：Each component raw material is pressed into above-mentioned weight proportion precise,
It is sufficiently mixed and stirs evenly, you can.
1-3 senile-resistant efficacy evaluation tests of the embodiment of the present invention
Free radical is the intermediate product of biochemical reaction during vital movement, and the biology related with life aging is freely
Base is mainly some oxygen containing free radicals, and antioxidant can provide proton to peroxide radical, it is thus possible to suppress lipid
Autoxidizable chain reaction.Usually make DPPH to examine antioxidant to put forward protogenic ability.DPPH be it is a kind of it is very stable from
By base, its methanol solution has extremely strong absorbance at 517nm, but when by oxidant (AH) or radical reduction, its extinction
Degree can be reduced or disappeared.Thus, it can judge whether sample has the energy for removing free radical using absorbance of the sample at 517nm
Power.
The composition of 1-3 of the embodiment of the present invention and comparative example 1-2 are taken, the solution of 4mg cosmetics/ml is configured to PBS,
Respectively with 1mL methanol solutions, 1ml DPPH free radicals methanol solution (2 × 10-4Mol/L), it is sufficiently mixed uniformly, stands 30min
Afterwards, with absorbance at spectrophotometric measurement 517nm, and its free radical scavenging activity is calculated with formula.Free radical scavenging activity (%)=
[(Ac-As/Ac)] × 100%, As：Absorbance of the sample containing determinand at 517nm；Ac：Sample without determinand
Absorbance at 517nm, the results are shown in Table 1 for the free radical scavenging activity (%) of 1-3 compositions of the embodiment of the present invention.
The free radical scavenging activity (%) of 1 1-3 compositions of the embodiment of the present invention of table
| Tested material | Free radical scavenging activity |
| Embodiment 1 | 93.4% |
| Embodiment 2 | 91.4% |
| Embodiment 3 | 91.5% |
| Comparative example 1 | 89.7% |
| Comparative example 2 | 89.4% |
As shown in Table 1：Adding lily leaf extract or side Bao Mao nonirrigated farmlands chrysanthemum extract in the composition can reach anti-ageing
Old effect, and lily leaf extract and the addition of side Bao Mao nonirrigated farmlands chrysanthemum extract compounding are in the composition, anti-aging effects collaboration increases
Effect, is significantly higher than the free radical scavenging activity highest of independent addition, wherein embodiment 1, and anti-aging ability is most strong.
Embodiment 4
Radiation protection of the present invention, a kind of embodiment of anti-apolexis composition, the composition include following parts by weight
Component：8 parts of lily leaf extract, 8 parts of side Bao Mao nonirrigated farmlands chrysanthemum extract, 4 parts of daye tea extract.
Embodiment 5
Radiation protection of the present invention, a kind of embodiment of anti-apolexis composition, the composition include following parts by weight
Component：6 parts of lily leaf extract, 8 parts of side Bao Mao nonirrigated farmlands chrysanthemum extract, 5 parts of daye tea extract.
Embodiment 6
Radiation protection of the present invention, a kind of embodiment of anti-apolexis composition, the composition include following parts by weight
Component：10 parts of lily leaf extract, 8 parts of side Bao Mao nonirrigated farmlands chrysanthemum extract, 3 parts of daye tea extract.
Comparative example 3
The formula of comparative example 3 is：16 parts of lily leaf extract, 8 parts of side Bao Mao nonirrigated farmlands chrysanthemum extract.
Comparative example 4
The formula of comparative example 4 is：8 parts of side Bao Mao nonirrigated farmlands chrysanthemum extract, 16 parts of daye tea extract.
The preparation method of embodiment 4-6 and documents 3-4：Each component raw material is accurately claimed by above-mentioned weight proportion
Amount, is sufficiently mixed and stirs evenly, you can.
4-6 anti-radiation effect evaluation tests of the embodiment of the present invention
Experimental method is as follows：
84 cleaning grade male Kunming strain mices are randomly divided into 7 groups：Blank group, model group, control group 1, control group 2,
Test group 1 (dosage 5g/kg), test group 2 (dosage 5g/kg), test group 3 (dosage 5g/kg), every group 12.Except sky
White group is outer, remaining group mouse is used60Co rays carry out a subtotal body irradiation, and irradiation total absorbed dose is 2.0Gy.Each dose of composition
Amount group mouse in60Co radiation the previous day gavage gives corresponding dosage, and blank group and model group animal gavage give isodose life
Brine is managed, each group is administered with the daily gavage of physiological saline once, continuous seven days.Each group animal is the 7th after pre-irradiation, irradiation
It adopts tail peripheral blood twice, surveys leucocyte (WBC) number.
Influence of the composition of 4-6 of the embodiment of the present invention to irradiated mice peripheral white blood cell the results are shown in Table 2.
Influence of the Chinese medicine composition of 2 4-6 of the embodiment of the present invention of table to irradiated mice peripheral white blood cell
| Group | Pre-irradiation WBC (× 109) | 7th day WBC (× 10 after irradiation9) |
| Blank group | 7.55±0.15 | 8.15±0.21 |
| Model group | 7.72±0.14 | 3.45±0.22* |
| Control group 1 (comparative example 3) | 7.66±0.23 | 6.10±0.25** |
| Control group 2 (comparative example 4) | 7.80±0.14 | 6.11±0.13** |
| Test group 1 (embodiment 4) | 7.82±0.20 | 7.26±0.11** |
| Test group 2 (embodiment 5) | 7.68±0.31 | 6.71±0.20** |
| Test group 3 (embodiment 6) | 7.87±0.25 | 6.69±0.21** |
* model group P ＜ 0.01 compared with blank group；* P ＜ 0.01 compared with model group.
As seen from the above table, model group is compared with blank group,607 days leukocyte counts significantly reduce after Co radiation exposures, have very
Significant difference (P ＜ 0.01), that is, test modeling success.Using above-mentioned composition, murine interleukin, which counts, to be had in various degree
Rising, tool is very significant (P ＜ 0.01) compared with model group, and the radiation-proof effect of embodiment 4 is best, adopts
It can reach radiation-proof effect with lily leaf extract or daye tea extract, and lily leaf extract and daye tea extract are answered
Match somebody with somebody, its radiation-proof effect is synergistic, is significantly higher than exclusive use.
The present composition has the function that body peripheral white blood cells caused by improving radiation injury reduce, that is, has pre-
Anti- and treatment radiation injury effect.
Present composition safety testing
Test material and method
Animal：Regular grade large ear rabbit 4,2.3-2.7 kilograms of weight, body looks into animal no abnormality seen.
Environmental condition：Room temperature：22 DEG C -23 DEG C, relative humidity：66% -68%；
Test method：
Foundation《Cosmetics health specification》(version in 2007) acute skin irritation test, before experiment 24 it is small when, will test
Back part of animal backbone diamond wool is cut, 3 centimetres of 3 cm x of unhairing scope.Tested 0.5 gram of no originality is taken directly to be applied to right side skin
On skin, with clean gauze cover, with nonirritant immobilization with adhesive tape 2 it is small when.Other side is negative control.After removing tested material
1 it is small when, 24 it is small when, 48 it is small when 72 it is small when observe and animal subject contact site dermoreaction and keep a record.
Under this experimental condition, 1-6 of embodiment of the present invention compositions press White Rabbit acute skin irritation test skin thorn
It is nonirritant to swash strength grading.
The Security test of 1-6 compositions of the embodiment of the present invention：
1-6 of embodiment of the present invention compositions safety, the examination of human body patch are demonstrated by zoopery and human body patch test
Test and carried out by our company professional.
Finally, it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention rather than the present invention is protected
The limitation of scope is protected, although being explained in detail with reference to preferred embodiment to the present invention, those of ordinary skill in the art should
Understand, can be to technical scheme technical scheme is modified or replaced equivalently, without departing from the essence of technical solution of the present invention
And scope.
Claims (9)
1. a kind of radiation protection containing lily leaf extract, anti-apolexis composition, it is characterised in that include the group of following parts by weight
Point：6-10 parts of lily leaf extract, 6-10 parts of side Bao Mao nonirrigated farmlands chrysanthemum extract, 3-5 parts of daye tea extract.
2. radiation protection according to claim 1, anti-apolexis composition, it is characterised in that the lily leaf extract and side
The weight ratio of spore hair nonirrigated farmland chrysanthemum extract is 1:1.
3. radiation protection according to claim 1, anti-apolexis composition, it is characterised in that the lily leaf extract and big
The weight ratio of leaf tea extract is 2:1.
4. radiation protection according to claim 1, anti-apolexis composition, it is characterised in that the anti-aging, net white composition
Further include preservative, pH adjusting agent, thickener, emulsifying agent, essence, pigment and water.
5. radiation protection according to claim 1, anti-apolexis composition, it is characterised in that it is hard that the emulsifying agent is selected from spermaceti
Lipidol polyethers -6, ceteareth -25, glycerin monostearate, the emollient are selected from White Mineral Oil, stearic acid, spermaceti
Stearyl alcohol, olive oil, octanoic acid/certain herbaceous plants with big flowers acid triglyceride, shea butter, jojoba oil, silicone oil, the skin moisturizer are selected from sweet
Oil, propane diols, 1,3 butanediols.
6. a kind of radiation protection as described in claim 1-5 is any, the preparation method of anti-apolexis composition, it is characterised in that institute
It is by each component raw material precise by weight ratio to state preparation method, is sufficiently mixed and stirs evenly, that is, obtains the combination
Thing.
7. radiation protection according to claim 1, anti-apolexis composition, it is characterised in that the anti-aging, net white composition
Formulation be aqua, creme, finish, washing lotion or emulsion.
8. a kind of radiation protection, anti-aging skin care product, it is characterised in that including oil phase, water phase, the water mutually includes such as claim
Any radiation protections of 1-5, anti-apolexis composition.
9. radiation protection according to claim 8, anti-aging skin care product, it is characterised in that the radiation protection, antisenility skin care
Product further include essence and preservative.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711363484.6A CN107982172A (en) | 2017-12-14 | 2017-12-14 | A kind of radiation protection containing lily leaf extract, anti-apolexis composition and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711363484.6A CN107982172A (en) | 2017-12-14 | 2017-12-14 | A kind of radiation protection containing lily leaf extract, anti-apolexis composition and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113288848A (en) * | 2021-06-16 | 2021-08-24 | 吉林洁洁宝生物科技有限公司 | Edible oat mask powder and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101766555A (en) * | 2008-12-31 | 2010-07-07 | 云南恒冠实业有限公司 | Anti-aging, wrinkle-eliminating and anti-wrinkle cosmetic composition |
-
2017
- 2017-12-14 CN CN201711363484.6A patent/CN107982172A/en not_active Withdrawn
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101766555A (en) * | 2008-12-31 | 2010-07-07 | 云南恒冠实业有限公司 | Anti-aging, wrinkle-eliminating and anti-wrinkle cosmetic composition |
Non-Patent Citations (1)
| Title |
|---|
| 王建新等: "《化妆品植物原料大全》", 30 June 2012, 中国纺织出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113288848A (en) * | 2021-06-16 | 2021-08-24 | 吉林洁洁宝生物科技有限公司 | Edible oat mask powder and preparation method thereof |
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Application publication date: 20180504 |