CN107951778B - Shower gel composition and preparation method thereof - Google Patents
Shower gel composition and preparation method thereof Download PDFInfo
- Publication number
- CN107951778B CN107951778B CN201711406482.0A CN201711406482A CN107951778B CN 107951778 B CN107951778 B CN 107951778B CN 201711406482 A CN201711406482 A CN 201711406482A CN 107951778 B CN107951778 B CN 107951778B
- Authority
- CN
- China
- Prior art keywords
- weight
- extract
- parts
- camellia seed
- shower gel
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Dermatology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a Chinese herbal medicine shower gel containing camellia seed hulls, momordica grosvenori and perilla frutescens, which comprises the following components in parts by weight: 0.75-1.75 parts by weight of camellia seed hull extract; 0.05-0.45 part by weight of a momordica grosvenori extract; 0.3 to 0.7 part by weight of perilla frutescens; 10-15 parts by weight of glycerol; 55-85 parts of a foaming agent; 10-10 parts by weight of DOE-1204.5; 7-15 parts of pearlescent slurry; 0.3-0.7 parts of kasong; 100-200 parts by volume of water. The invention also provides a preparation method of the shower gel. The bath cream containing the camellia seed hulls, the momordica grosvenori and the perilla frutescens is stable in performance, natural, safe, strong in detergency and easy to clean, and has the effects of moisturizing, protecting skin, diminishing inflammation, whitening and the like, and all the selected ingredients are natural ingredients and high-grade washing and protecting product additives.
Description
Technical Field
The invention relates to the technical field of daily chemicals, and particularly relates to a bath composition and a preparation method thereof.
Background
The shower gel is a washing product generally composed of a surfactant and other auxiliary components, such as a bubble film stabilizer, essence, a thickening agent, a chelating agent, a skin care agent, a pigment and the like, is a necessary product for the life of modern people, is a popular consumer product with the consumption of daily chemical products second to that of a shampoo product, and can meet the requirements of people on the quality of life, so that the daily washing product is not only clean, but also more environment-friendly, healthy and natural. At present, bath products are developing towards the direction of nature, function and environmental protection, so most bath products with natural nutrient components are popular with consumers in the market.
The camellia seed hulls are hulls of camellia seeds or camellia seeds, and are portions of the hulls which naturally fall off in the process of drying the camellia seeds in the sun, the camellia seeds are often used for oil extraction, and the hulls of the camellia seeds are often discarded, so that the environment is polluted. Modern chemical and pharmacological research shows that the main components of the camellia seed hulls are triterpenoid saponin, tea flavone, anthocyanin, tea polyphenol, xylose and the like. The triterpenoid saponin is a natural nonionic surfactant, has the effects of emulsifying, dispersing, wetting, reducing the surface tension of water and the like, and also has good decontamination capability; the camellia seed hulls contain tea flavonoids, anthocyanins and other components, have remarkable antioxidation, can protect the skin, particularly can prevent skin damage and aging, and enable the skin to have luster; tea polyphenol is an effective and comprehensive antioxidant, has the functions of absorbing ultraviolet rays, sterilizing, diminishing inflammation and inhibiting certain fungi, has good stability, and can exert efficacy for a long time.
Momordica grosvenori, the dry fruit of Momordica grosvenori of the family Georgia, it is a common Chinese medicine, the taste is sweet and cool, return to the lung, large intestine channel, is known as "the immortal fruit" by people, it has effects of moistening dryness, promoting the production of body fluid, modern chemistry, pharmacological research show that fructus Siraitiae Grosvenori principal ingredients are fructus Siraitiae Grosvenori saponin, fructus Siraitiae Grosvenori saponin is not merely non-ionic natural surfactant, and have apparent antioxidation, scavenge free radical activity, improve the metabolism of whole body skin, and stability is very good, can play effects such as diminishing inflammation, resisting bacteria, whitening, sun-.
Perilla frutescens, an annual plant, is the dried whole plant of Perilla frutescens of the family Labiatae. Pungent, warm and nontoxic, and its root, stem, leaf, flower and seed can be used as a common Chinese medicine. The theory of traditional Chinese medicine considers that it dispels cold, relieves exterior syndrome, regulates qi and relieves epigastric distention. Modern chemical and pharmacological research shows that perilla contains chemical substances such as perillaldehyde, perillanol, linalool, menthol, perillanone, limonene, eugenol and the like, has multiple effects of special fragrance, antibiosis, antiphlogosis, antipyretic, analgesia, antivirus, itching relieving and the like, has special fragrance, and also has the effects of removing skin odor, improving skin microcirculation, promoting skin metabolism, eliminating excessive accumulation of pigments in tissues, removing skin stains and scars, treating skin blister, bruise, mange, delaying skin aging and the like.
There is no shower gel using camellia seed hulls as the main component of a detergent, and there is no report on a bath composition consisting of camellia seed hulls, momordica grosvenori and beefsteak plant.
Disclosure of Invention
The invention aims to provide a bath lotion containing camellia seed hulls, momordica grosvenori and perilla frutescens, which comprises the following components in parts by weight:
0.75-1.75 parts by weight of camellia seed shell extract
0.05 to 0.45 weight portion of momordica grosvenori extract
0.3 to 0.7 part by weight of common perilla extract
10-15 parts by weight of glycerin
55-85 parts by weight of foaming agent
DOE-1204.5-10 parts by weight
7-15 parts by weight of pearlescent slurry
0.3 to 0.7 part by weight of kasong
100-200 parts by volume of water.
Wherein the weight portions by volume are g: and (3) ml.
Preferably, the composition comprises the following components in proportion:
1.05-1.45 parts by weight of camellia seed hull extract
0.15 to 0.35 weight part of momordica grosvenori extract
0.4 to 0.6 part by weight of common perilla extract
11.5 to 13.5 parts by weight of glycerin
45-55 parts of coconut oil foaming agent
10-20 parts by weight of amino acid foaming agent
DOE-1206.5-8.5 parts by weight
9-13 parts by weight of pearlescent slurry
0.4 to 0.6 part by weight of kasong
130-170 parts by volume of water.
Preferably, the composition comprises the following components in proportion:
camellia seed husk extract 1.25 weight parts
0.25 part by weight of momordica grosvenori extract
Perilla frutescens extract 0.5 parts by weight
Glycerol: 12.5 parts by weight
Coconut oil foaming agent 50 parts by weight
15 parts by weight of amino acid foaming agent
DOE-1207.5 parts by weight
11 parts by weight of pearlescent slurry
0.5 part by weight of kasong
150 parts by volume of water.
The camellia seed husk extract is obtained by adopting the following method:
extracting from oil tea seed hull by water extraction and alcohol extraction; preferably, the preparation method is as follows: mashing the camellia seed hull cake into camellia seed hull powder, adding 7-8 times of water, extracting twice in a water bath at 90 ℃, filtering with hot gauze, adding alum for flocculation, carrying out suction filtration and concentration, adding 95% ethanol for 3 times of extraction, decoloring with active carbon, recovering ethanol, and drying at constant temperature to obtain a powdery camellia seed hull extract.
The fructus momordicae extract is obtained by adopting the following method:
extracting fructus Siraitiae Grosvenorii with alcohol; preferably, the preparation method is as follows: pulverizing fructus Siraitiae Grosvenorii, adding 20 times of 70% ethanol, ultrasonic extracting for 30 min twice, filtering, mixing filtrates, concentrating, and drying at constant temperature to obtain powdered fructus Siraitiae Grosvenorii extract.
The common perilla extract is a common perilla volatile oil extract. The preparation method of the common perilla extract comprises the following steps: and (3) putting the perilla frutescens powder into a volatile oil extractor, and adding water for distillation for 6 hours to obtain the perilla frutescens volatile oil extract.
The pearlescent slurry is ethylene glycol distearate emulsion.
The coconut oil foaming agent is; the amino acid foaming agent is.
The shower gel contains essential oil, the dosage of the essential oil is 0.05-0.15 weight part, preferably 0.1 weight part,
the invention also provides a method for preparing the shower gel, which comprises the following steps:
(1) heating and mixing the camellia seed hull extract, the momordica grosvenori extract, the perilla frutescens extract, the glycerol, the coconut oil foaming agent, the amino acid foaming agent and the DOE-120 at 70-80 ℃, adding water and stirring until all the components are dissolved uniformly.
(2) Cooling the mixture obtained in the step (1), adding the pearlescent slurry, and uniformly stirring;
(3) and (3) cooling the mixture obtained in the step (2), adding the kasong and the essential oil, uniformly stirring, and cooling to obtain the shower gel containing the camellia seed hulls, the momordica grosvenori and the perilla frutescens.
In the step (2), the temperature is reduced to below 50 ℃; in the step (3), the temperature is reduced to 35 ℃.
The DOE-120 is a high-efficiency thickener, is chemically named methyl glucoside polyoxyethylene (120) ether dioleate, and is a light yellow waxy solid;
the invention has the beneficial effects that:
(1) compared with the existing shower gel products on the market, the shower gel provided by the invention is simple in preparation method, easy to operate, wide in raw materials and suitable for large-scale production.
(2) The shower gel disclosed by the invention is stable in performance, natural and safe, strong in detergency, easy to clean, and has the effects of moistening skin, protecting skin, diminishing inflammation, whitening and the like.
The present invention is described in further detail with reference to the following embodiments, but the present invention is not limited thereto, and various other modifications, substitutions and alterations can be made without departing from the basic technical idea of the present invention based on the above-mentioned contents of the present invention and common technical knowledge and conventional means in the art.
Detailed Description
The present invention will be further illustrated by way of examples.
Example 1 preparation of a body wash composition of the invention
(1) Mashing the camellia seed hull cake, sieving with a 80-mesh sieve to obtain camellia seed hull powder, weighing 140g of the camellia seed hull powder, adding 980ml of water, carrying out water bath at 90 ℃ for 1.5 hours, extracting twice, filtering with hot gauze, adding alum for flocculation, carrying out suction filtration and concentration, adding 95% ethanol for extraction for 3 times, decoloring with activated carbon, recovering ethanol, and drying the concentrate at constant temperature of 60 ℃ to obtain a powdery camellia seed hull extract.
(2) Pulverizing fructus Siraitiae Grosvenorii, sieving with 80 mesh sieve to obtain fructus Siraitiae Grosvenorii powder, weighing 72g fructus Siraitiae Grosvenorii powder, adding 712ml 70% ethanol, ultrasonic extracting for 30 min twice, vacuum filtering, mixing filtrates, concentrating, and drying at constant temperature to obtain powdered fructus Siraitiae Grosvenorii extract.
(3) Pulverizing the decoction pieces of common perilla, sieving with 40 mesh sieve, extracting with volatile oil extractor, distilling with water for 6 hr, and extracting to obtain common perilla volatile oil.
(4) Heating and mixing 1.25g of camellia seed hull extract, 0.25g of momordica grosvenori extract, 0.5g of perilla frutescens extract, 12.5g of glycerol, 50g of coconut oil foaming agent, 15g of amino acid foaming agent and DOE-1207.5 g in a water bath at 70-80 ℃, adding 150ml of water and stirring until all the components are uniformly dissolved.
(5) And (4) cooling the mixture obtained in the step (4) to below 50 ℃, adding 11g of pearlescent slurry, and quickly and uniformly stirring.
(6) And (3) cooling the mixture obtained in the step (5) to below 35 ℃, adding 0.5g of cason and a proper amount (0.1g) of essential oil, and uniformly stirring, wherein the total mass of the shower gel is the sum of the mass of each component. Standing at room temperature until bubbles disappear to obtain the bath lotion containing Camellia seed husk, fructus Siraitiae Grosvenorii and herba Stachydis Japonicae components.
Example 2 preparation of a body wash composition of the invention
(1) Mashing the camellia seed hull cake, sieving with a 80-mesh sieve to obtain camellia seed hull powder, weighing 140g of the camellia seed hull powder, adding 980ml of water, carrying out water bath at 90 ℃ for 1.5 hours, extracting twice, filtering with hot gauze, adding alum for flocculation, carrying out suction filtration and concentration, adding 95% ethanol for extraction for 3 times, decoloring with activated carbon, recovering ethanol, and drying the concentrate at constant temperature of 60 ℃ to obtain a powdery camellia seed hull extract.
(2) Pulverizing fructus Siraitiae Grosvenorii, sieving with 80 mesh sieve to obtain fructus Siraitiae Grosvenorii powder, weighing 72g fructus Siraitiae Grosvenorii powder, adding 712ml 70% ethanol, ultrasonic extracting for 30 min twice, vacuum filtering, mixing filtrates, concentrating, and drying at constant temperature to obtain powdered fructus Siraitiae Grosvenorii extract.
(3) Pulverizing the decoction pieces of common perilla, sieving with 40 mesh sieve, extracting with volatile oil extractor, distilling with water for 6 hr, and extracting to obtain common perilla volatile oil.
(4) Heating and mixing 1.05g of camellia seed hull extract, 0.35g of momordica grosvenori extract, 0.4g of perilla frutescens extract, 13.5g of glycerol, 45g of coconut oil foaming agent, 20g of amino acid foaming agent and DOE-1206.5 g in a water bath at 70-80 ℃, adding 130ml of water and stirring until all the components are uniformly dissolved.
(5) And (4) cooling the mixture obtained in the step (4) to below 50 ℃, adding 13g of pearlescent slurry, and quickly and uniformly stirring.
(6) And (3) cooling the mixture obtained in the step (5) to below 35 ℃, adding 0.4g of cason and a proper amount (0.1g) of essential oil, and uniformly stirring, wherein the total mass of the shower gel is the sum of the mass of each component. Standing at room temperature until bubbles disappear to obtain the bath lotion containing Camellia seed husk, fructus Siraitiae Grosvenorii and herba Stachydis Japonicae components.
Example 3 preparation of a body wash composition of the invention
(1) Mashing the camellia seed hull cake, sieving with a 80-mesh sieve to obtain camellia seed hull powder, weighing 140g of the camellia seed hull powder, adding 980ml of water, carrying out water bath at 90 ℃ for 1.5 hours, extracting twice, filtering with hot gauze, adding alum for flocculation, carrying out suction filtration and concentration, adding 95% ethanol for extraction for 3 times, decoloring with activated carbon, recovering ethanol, and drying the concentrate at constant temperature of 60 ℃ to obtain a powdery camellia seed hull extract.
(2) Pulverizing fructus Siraitiae Grosvenorii, sieving with 80 mesh sieve to obtain fructus Siraitiae Grosvenorii powder, weighing 72g fructus Siraitiae Grosvenorii powder, adding 712ml 70% ethanol, ultrasonic extracting for 30 min twice, vacuum filtering, mixing filtrates, concentrating, and drying at constant temperature to obtain powdered fructus Siraitiae Grosvenorii extract.
(3) Pulverizing the decoction pieces of common perilla, sieving with 40 mesh sieve, extracting with volatile oil extractor, distilling with water for 6 hr, and extracting to obtain common perilla volatile oil.
(4) Heating and mixing 1.45g of camellia seed hull extract, 0.15g of momordica grosvenori extract, 0.5g of perilla frutescens extract, 11.5g of glycerol, 55g of coconut oil foaming agent, 10g of amino acid foaming agent and DOE-1208.5 g in a water bath at 70-80 ℃, adding 170ml of water and stirring until all the components are uniformly dissolved.
(5) And (4) cooling the mixture obtained in the step (4) to below 50 ℃, adding 9g of pearlescent slurry, and quickly and uniformly stirring.
(6) And (3) cooling the mixture obtained in the step (5) to below 35 ℃, adding 0.6g of cason and a proper amount (0.05g) of essential oil, and uniformly stirring, wherein the total mass of the shower gel is the sum of the mass of each component. Standing at room temperature until bubbles disappear to obtain the bath lotion containing Camellia seed husk, fructus Siraitiae Grosvenorii and herba Stachydis Japonicae components.
Example 4 preparation of a body wash composition of the invention
(1) Mashing the camellia seed hull cake, sieving with a 80-mesh sieve to obtain camellia seed hull powder, weighing 140g of the camellia seed hull powder, adding 980ml of water, carrying out water bath at 90 ℃ for 1.5 hours, extracting twice, filtering with hot gauze, adding alum for flocculation, carrying out suction filtration and concentration, adding 95% ethanol for extraction for 3 times, decoloring with activated carbon, recovering ethanol, and drying the concentrate at constant temperature of 60 ℃ to obtain a powdery camellia seed hull extract.
(2) Pulverizing fructus Siraitiae Grosvenorii, sieving with 80 mesh sieve to obtain fructus Siraitiae Grosvenorii powder, weighing 72g fructus Siraitiae Grosvenorii powder, adding 712ml 70% ethanol, ultrasonic extracting for 30 min twice, vacuum filtering, mixing filtrates, concentrating, and drying at constant temperature to obtain powdered fructus Siraitiae Grosvenorii extract.
(3) Pulverizing the decoction pieces of common perilla, sieving with 40 mesh sieve, extracting with volatile oil extractor, distilling with water for 6 hr, and extracting to obtain common perilla volatile oil.
(4) Heating and mixing 0.75g of camellia seed hull extract, 0.45g of momordica grosvenori extract, 0.3g of perilla frutescens extract, 15g of glycerol, 45g of coconut oil foaming agent, 10g of amino acid foaming agent and 10g of DOE-12010 in a water bath at 70-80 ℃, adding 100ml of water and stirring until all the components are dissolved uniformly.
(5) And (4) cooling the mixture obtained in the step (4) to below 50 ℃, adding 7g of pearlescent slurry, and quickly and uniformly stirring.
(6) And (3) cooling the mixture obtained in the step (5) to below 35 ℃, adding 0.7g of cason and a proper amount (0.15g) of essential oil, and uniformly stirring, wherein the total mass of the shower gel is the sum of the mass of each component. Standing at room temperature until bubbles disappear to obtain the bath lotion containing Camellia seed husk, fructus Siraitiae Grosvenorii and herba Stachydis Japonicae components.
Example 5 preparation of a body wash composition of the invention
(1) Mashing the camellia seed hull cake, sieving with a 80-mesh sieve to obtain camellia seed hull powder, weighing 140g of the camellia seed hull powder, adding 980ml of water, carrying out water bath at 90 ℃ for 1.5 hours, extracting twice, filtering with hot gauze, adding alum for flocculation, carrying out suction filtration and concentration, adding 95% ethanol for extraction for 3 times, decoloring with activated carbon, recovering ethanol, and drying the concentrate at constant temperature of 60 ℃ to obtain a powdery camellia seed hull extract.
(2) Pulverizing fructus Siraitiae Grosvenorii, sieving with 80 mesh sieve to obtain fructus Siraitiae Grosvenorii powder, weighing 72g fructus Siraitiae Grosvenorii powder, adding 712ml 70% ethanol, ultrasonic extracting for 30 min twice, vacuum filtering, mixing filtrates, concentrating, and drying at constant temperature to obtain powdered fructus Siraitiae Grosvenorii extract.
(3) Pulverizing the decoction pieces of common perilla, sieving with 40 mesh sieve, extracting with volatile oil extractor, distilling with water for 6 hr, and extracting to obtain common perilla volatile oil.
(4) Heating and mixing 1.75g of camellia seed hull extract, 0.05g of momordica grosvenori extract, 0.7g of perilla frutescens extract, 10g of glycerol, 65g of coconut oil foaming agent, 20g of amino acid foaming agent and DOE-1204.5 g in a water bath at 70-80 ℃, adding 200ml of water and stirring until all the components are dissolved uniformly.
(5) And (4) cooling the mixture obtained in the step (4) to below 50 ℃, adding 15g of pearlescent slurry, and quickly and uniformly stirring.
(6) And (3) cooling the mixture obtained in the step (5) to below 35 ℃, adding 0.3g of cason and a proper amount (0.1g) of essential oil, and uniformly stirring, wherein the total mass of the shower gel is the sum of the mass of each component. Standing at room temperature until bubbles disappear to obtain the bath lotion containing Camellia seed husk, fructus Siraitiae Grosvenorii and herba Stachydis Japonicae components.
The beneficial effects of the invention are illustrated by way of experimental examples as follows:
experimental example 1 shower gel Performance test
The shower gel prepared in example 1 was taken and tested for the following properties:
(1) degree of foaming: two 10ml EP tubes were prepared, to which a drop of ordinary shower gel and a drop of homemade shower gel were added, respectively, and the degree of foaming was observed by vigorously shaking the tubes with a lid.
(2) Clarity: the EP tube with observed foaming was placed flat for 5 minutes and the water clarity was observed.
(3) pH value: and the pH test paper is used for detection, the pH value is between 5 and 6, the weak acidity is achieved, the skin environment can be protected, and the cleaning power is strong.
(4) And (3) permeability: the common shower gel and the self-made shower gel are respectively and directly smeared on the skin, and the absorption condition and the comfort degree of the skin to the shower gel are observed.
(5) Salinity melting: uniformly dividing a small amount of salt into two parts, placing the two parts on a culture dish at intervals, dripping a drop of common shower gel and self-made shower gel respectively, stirring the two parts by using a toothpick, and observing the dissolution condition of the salt in the shower gel.
(6) Stability: dividing the self-made shower gel into two parts, placing one part in a refrigerator at the temperature of-20 ℃, placing the other part in an oven at the temperature of 40 ℃, taking out after 24 hours, placing to the room temperature, and observing whether the shower gel is stable.
(7) Appearance, odor, color, consistency, rinse feel, lather feel were assessed in comparison to a normal body wash in 20 volunteers.
The results are shown in Table 1.
Table 1 shower gel performance test
| Detecting the index | Bath lotion containing camellia seed hull, fructus momordicae and perilla frutescens |
| Appearance of the product | 75% of volunteers considered uniform and glossy |
| Colour(s) | 75% of volunteers consider that |
| Smell(s) | 50% of volunteers considered as general |
| Consistency of | 55% of volunteers considered moderate |
| Feeling of rinsing | 80% of volunteers considered no adverse sensation of flushing |
| Foam feel | 75% of volunteers represent |
| Degree of foaming | A large amount of the traditional Chinese medicine is similar to that of common shower gel |
| Clarity of reaction | Clear and similar to common bath lotion |
| pH value | PH 6, the same as common bath lotion |
| Osmotic power | Feel more moist than common shower gel |
| Salinity melting degree | Has higher solubility than common bath lotion |
| Stability of | Uniform and stable, and no separation and water separation |
Experimental example 2 whitening Performance test of body wash
The body wash prepared in example 1, and a commercially available body wash with whitening effect were taken for testing:
the first, experimental principle: the whitening capacity is reflected by testing the capacity of the bath cream for inhibiting the generation of melanin, a tyrosine standard solution is used for reacting with potato juice rich in tyrosinase, a sample emulsion is added at the same time, whether the content of the melanin generated after the reaction is different or not is observed, the highest absorption peak of the melanin is between 320nm and 410nm, and the OD400 is measured by using a spectrophotometer for evaluation.
II, an experimental method: fresh potato pellet juice (1 mL) was added using 4mL of tyrosine standard solution (0.5mol/L) and divided into two groups, one group with 1mL of whitened sample and the other group without any treatment as a blank Control (CK). After the reaction was carried out for 15 minutes by adding dissolved oxygen to a constant temperature shaking table (30 ℃ C., 200rpm), 2mL of the reacted solution was put into a centrifuge tube and centrifuged at 12000rpm for 3 minutes, and the supernatant was taken out to measure the OD 400.
Thirdly, experimental results:
note: the larger the difference in OD400, the better whitening effect.
Fourthly, experimental conclusion:
compared with other shower creams, the shower gel provided by the invention has a remarkably better whitening effect.
The foregoing descriptions of specific embodiments of the present invention are presented for purposes of illustration and example. It should be understood, however, that there is no intent to limit the invention to the particular forms disclosed, but on the contrary, the intention is to cover all modifications, equivalents, and alternatives falling within the spirit and scope of the invention as defined by the appended claims.
Claims (5)
1. The Chinese herbal medicine shower gel is characterized in that: comprises the following components in proportion:
camellia seed husk extract 1.25 weight parts
0.25 part by weight of momordica grosvenori extract
Perilla frutescens extract 0.5 parts by weight
12.5 parts by weight of glycerol
Coconut oil foaming agent 50 parts by weight
15 parts by weight of amino acid foaming agent
DOE-1207.5 parts by weight
11 parts by weight of pearlescent slurry
0.5 part by weight of kasong
150 parts by weight of water;
the camellia seed husk extract is obtained by adopting the following method:
pulverizing camellia seed hulls, adding 7-8 times of water, extracting twice in a water bath at 90 ℃, filtering with hot gauze, adding alum for flocculation, performing suction filtration and concentration, adding 95% ethanol for 3 times for extraction and dissolution, decoloring with active carbon, recovering ethanol, and drying at constant temperature to obtain a powdery camellia seed hull extract;
the fructus momordicae extract is obtained by adopting the following method:
pulverizing fructus Siraitiae Grosvenorii, adding 20 times of 70% ethanol, ultrasonic extracting for 30 min twice, filtering, mixing filtrates, concentrating, and drying at constant temperature to obtain powdered fructus Siraitiae Grosvenorii extract;
the common perilla extract is obtained by the following method:
and (3) putting the perilla frutescens powder into a volatile oil extractor, and adding water for distillation for 6 hours to obtain the perilla frutescens volatile oil extract.
2. The body wash of claim 1, wherein: the pearlescent slurry is ethylene glycol distearate emulsion.
3. The body wash of claim 1, wherein: the shower gel contains 0.05-0.15 part by weight of essential oil.
4. A method of preparing the body wash of claim 3, wherein: the method comprises the following steps:
(1) heating and mixing the camellia seed hull extract, the momordica grosvenori extract, the perilla frutescens extract, the glycerol, the coconut oil foaming agent, the amino acid foaming agent and the DOE-120 at 70-80 ℃, adding water and stirring until all the components are dissolved uniformly;
(2) cooling the mixture obtained in the step (1), adding the pearlescent slurry, and uniformly stirring;
(3) and (3) cooling the mixture obtained in the step (2), adding the kasong and the essential oil, uniformly stirring, and cooling to obtain the shower gel containing the camellia seed hulls, the momordica grosvenori and the perilla frutescens.
5. The method of claim 4, wherein: in the step (2), the temperature is reduced to below 50 ℃; in the step (3), the temperature is reduced to 35 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711406482.0A CN107951778B (en) | 2017-12-22 | 2017-12-22 | Shower gel composition and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711406482.0A CN107951778B (en) | 2017-12-22 | 2017-12-22 | Shower gel composition and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107951778A CN107951778A (en) | 2018-04-24 |
| CN107951778B true CN107951778B (en) | 2021-06-04 |
Family
ID=61955843
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711406482.0A Active CN107951778B (en) | 2017-12-22 | 2017-12-22 | Shower gel composition and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107951778B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114404315B (en) * | 2022-01-17 | 2023-12-08 | 上海澄穆生物科技有限公司 | Application of 11-O-mogroside V and pharmaceutically acceptable salt thereof as CB2 receptor agonist in cosmetics |
| CN115844787A (en) * | 2022-12-29 | 2023-03-28 | 福建片仔癀化妆品有限公司 | Preparation method of face cream with natural fragrance |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100792040B1 (en) * | 2006-11-01 | 2008-01-04 | 하인숙 | Cleansing soap |
| JP2011140523A (en) * | 2011-04-15 | 2011-07-21 | Lion Corp | Foul breath inhibitor and oral cavity composition for foul breath inhibition |
| CN103860439A (en) * | 2014-04-09 | 2014-06-18 | 赵月 | Whitening and moisturizing skin-care composition and preparation method thereof |
| CN104887577A (en) * | 2015-06-03 | 2015-09-09 | 桂林电子科技大学 | Preparation method of momordica grosvenori compound gel |
| CN104940102A (en) * | 2015-06-20 | 2015-09-30 | 青岛克立克信息技术有限公司 | Facial mask with moisturizing function |
| CN106070202A (en) * | 2006-02-15 | 2016-11-09 | 博塔诺凯普有限公司 | The application of microencapsulated essential oils |
| CN106176361A (en) * | 2010-12-30 | 2016-12-07 | 玫琳凯有限公司 | Topical skin composition and application thereof |
| CN106466280A (en) * | 2015-08-20 | 2017-03-01 | 哈尔滨灵草舒生物科技有限公司 | A kind of Radix Polygalae mind tranquilizing and the heart calming bath gel and preparation method thereof |
| CN106667841A (en) * | 2017-01-13 | 2017-05-17 | 华南理工大学 | Tea-seed foot washing powder as well as preparation method and application thereof |
-
2017
- 2017-12-22 CN CN201711406482.0A patent/CN107951778B/en active Active
Patent Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106070202A (en) * | 2006-02-15 | 2016-11-09 | 博塔诺凯普有限公司 | The application of microencapsulated essential oils |
| KR100792040B1 (en) * | 2006-11-01 | 2008-01-04 | 하인숙 | Cleansing soap |
| CN106176361A (en) * | 2010-12-30 | 2016-12-07 | 玫琳凯有限公司 | Topical skin composition and application thereof |
| JP2011140523A (en) * | 2011-04-15 | 2011-07-21 | Lion Corp | Foul breath inhibitor and oral cavity composition for foul breath inhibition |
| CN103860439A (en) * | 2014-04-09 | 2014-06-18 | 赵月 | Whitening and moisturizing skin-care composition and preparation method thereof |
| CN105326686A (en) * | 2014-04-09 | 2016-02-17 | 赵月 | Whitening and moisturizing skin care mask |
| CN104887577A (en) * | 2015-06-03 | 2015-09-09 | 桂林电子科技大学 | Preparation method of momordica grosvenori compound gel |
| CN104940102A (en) * | 2015-06-20 | 2015-09-30 | 青岛克立克信息技术有限公司 | Facial mask with moisturizing function |
| CN106466280A (en) * | 2015-08-20 | 2017-03-01 | 哈尔滨灵草舒生物科技有限公司 | A kind of Radix Polygalae mind tranquilizing and the heart calming bath gel and preparation method thereof |
| CN106667841A (en) * | 2017-01-13 | 2017-05-17 | 华南理工大学 | Tea-seed foot washing powder as well as preparation method and application thereof |
Non-Patent Citations (2)
| Title |
|---|
| Antioxidant, Anti-Tyrosinase and Anti-Inflammatory Activities of Oil Production Residues from Camellia tenuifloria;Shu-Yuan Chiou等;《International Journal of Molecular Sciences》;20151231(第16期);第29522-29541页 * |
| 油茶活性成分作为护肤因子在化妆品领域的研究进展;陈健等;《中国美容医学》;20130131;第22卷(第1期);第223-225页 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN107951778A (en) | 2018-04-24 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103756808B (en) | A kind of natural washing liquid of preservative free and preparation method thereof | |
| CN105754768B (en) | A kind of Baby Care handmade soap containing natural Sasanguasaponin and preparation method thereof | |
| CN102080028B (en) | Dryopteris erythrosora/soapberry natural biomass detergent and preparation method thereof | |
| CN105832582A (en) | Preparing method for camellia oil emulsion | |
| CN102895152A (en) | Preparation method for rose extract and cosmetic | |
| US11337915B2 (en) | Shampoo composition for improving scalp and hair conditions | |
| CN104434650B (en) | A kind of relax skin whitening, moisturizing of pressure of allaying excitement is energized emulsion and preparation method thereof | |
| CN103550131B (en) | Pure natural hair care hair color shampoo and preparation method thereof | |
| KR20100044502A (en) | Cleaning solution for body by using natural material | |
| CN106434028A (en) | Fruit and vegetable washing salt for removing pesticide residues and preparation method thereof | |
| CN105997827A (en) | Compound camellia oil moisturizer and preparation method thereof | |
| CN107951778B (en) | Shower gel composition and preparation method thereof | |
| CN105310935B (en) | A kind of disposable sleep mask of black fruit fructus lycii combination | |
| WO2018112857A1 (en) | Moisturizing skin-care lotion | |
| CN103550130B (en) | Folium Nelumbinis tea bran shampoo and preparation method thereof | |
| CN104825361A (en) | Natural shampoo containing camellia saponin | |
| KR20160105187A (en) | A kitchen antimicrobial detergent containing an eco-friendly antimicrobial agent | |
| CN104906004A (en) | Peach blossom toner and making method thereof | |
| CN109609261A (en) | A kind of aurelia extractive liquid oleosa and the preparation method and application thereof | |
| CN105106082A (en) | Handmade acne removing soap containing aloes | |
| CN108078905A (en) | Anticreep shampoo for men only and its processing method | |
| CN105232402B (en) | A kind of composition with skin-care effect | |
| CN107375087A (en) | A kind of shower cream and preparation method thereof | |
| KR101539744B1 (en) | A kitchen antimicrobial detergent containing an eco-friendly antimicrobial agent for preventing atopic dermatitis | |
| CN105441230A (en) | Camellia oil cold processed soap |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |