CN107951619A - A kind of steam eye patch and preparation method thereof - Google Patents

A kind of steam eye patch and preparation method thereof Download PDF

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Publication number
CN107951619A
CN107951619A CN201711336060.0A CN201711336060A CN107951619A CN 107951619 A CN107951619 A CN 107951619A CN 201711336060 A CN201711336060 A CN 201711336060A CN 107951619 A CN107951619 A CN 107951619A
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China
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parts
essential oil
potato
eye patch
steam eye
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CN201711336060.0A
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Chinese (zh)
Inventor
李恪言
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Liuzhou Elephant Line Education Science And Technology Co Ltd
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Liuzhou Elephant Line Education Science And Technology Co Ltd
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Priority to CN201711336060.0A priority Critical patent/CN107951619A/en
Publication of CN107951619A publication Critical patent/CN107951619A/en
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61F—FILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
    • A61F9/00—Methods or devices for treatment of the eyes; Devices for putting-in contact lenses; Devices to correct squinting; Apparatus to guide the blind; Protective devices for the eyes, carried on the body or in the hand
    • A61F9/04—Eye-masks ; Devices to be worn on the face, not intended for looking through; Eye-pads for sunbathing
    • A61F9/045—Eye-shades or visors; Shields beside, between or below the eyes
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61H—PHYSICAL THERAPY APPARATUS, e.g. DEVICES FOR LOCATING OR STIMULATING REFLEX POINTS IN THE BODY; ARTIFICIAL RESPIRATION; MASSAGE; BATHING DEVICES FOR SPECIAL THERAPEUTIC OR HYGIENIC PURPOSES OR SPECIFIC PARTS OF THE BODY
    • A61H33/00—Bathing devices for special therapeutic or hygienic purposes
    • A61H33/06—Artificial hot-air or cold-air baths; Steam or gas baths or douches, e.g. sauna or Finnish baths
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/32—Burseraceae (Frankincense family)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
    • A61K36/534—Mentha (mint)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/63—Oleaceae (Olive family), e.g. jasmine, lilac or ash tree
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/73—Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/81—Solanaceae (Potato family), e.g. tobacco, nightshade, tomato, belladonna, capsicum or jimsonweed
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/88—Liliopsida (monocotyledons)
    • A61K36/899—Poaceae or Gramineae (Grass family), e.g. bamboo, corn or sugar cane
    • A61K36/8998—Hordeum (barley)
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K5/00—Heat-transfer, heat-exchange or heat-storage materials, e.g. refrigerants; Materials for the production of heat or cold by chemical reactions other than by combustion
    • C09K5/16—Materials undergoing chemical reactions when used
    • C09K5/18—Non-reversible chemical reactions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/02—Recovery or refining of essential oils from raw materials
    • C11B9/025—Recovery by solvent extraction
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/02—Recovery or refining of essential oils from raw materials
    • C11B9/027—Recovery of volatiles by distillation or stripping
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61H—PHYSICAL THERAPY APPARATUS, e.g. DEVICES FOR LOCATING OR STIMULATING REFLEX POINTS IN THE BODY; ARTIFICIAL RESPIRATION; MASSAGE; BATHING DEVICES FOR SPECIAL THERAPEUTIC OR HYGIENIC PURPOSES OR SPECIFIC PARTS OF THE BODY
    • A61H33/00—Bathing devices for special therapeutic or hygienic purposes
    • A61H33/06—Artificial hot-air or cold-air baths; Steam or gas baths or douches, e.g. sauna or Finnish baths
    • A61H2033/068—Steam baths
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61H—PHYSICAL THERAPY APPARATUS, e.g. DEVICES FOR LOCATING OR STIMULATING REFLEX POINTS IN THE BODY; ARTIFICIAL RESPIRATION; MASSAGE; BATHING DEVICES FOR SPECIAL THERAPEUTIC OR HYGIENIC PURPOSES OR SPECIFIC PARTS OF THE BODY
    • A61H2205/00—Devices for specific parts of the body
    • A61H2205/02—Head
    • A61H2205/022—Face
    • A61H2205/024—Eyes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids

Abstract

The present invention relates to steam eye patch processing technique field, more particularly to a kind of steam eye patch and preparation method thereof, the steam eye patch of the application is made of hot radical material and essential oil material, wherein, hot radical material is by bamboo charcoal, iron powder, water-absorbing resin, NaHCO3, vermiculite, wormwood, green tea slag and water composition；Essential oil material is made of potato composite essential oil, osmanthus essential oil, apple essential oil, mint extract, Fructus Hordei Germinatus essential oil, olive oil, fatty acid glyceride and water；The hot radical material of the application is heatable, so that derived essential oil volatilizees, eyes are made to releive, containing abundant vitamin E component in the essential oil material of the application, which has heat resistanceheat resistant, antiacid, anti-photosensitizing effect, it can inhibit the lipid peroxidation reaction in ocular lens body, make peripheral vasodilation, improve blood circulation, pre- Anti-myopic eye occurrence and development, it can effectively relieve stress, there is good effect of easing stress.

Description

A kind of steam eye patch and preparation method thereof
【Technical field】
The present invention relates to steam eye patch processing technique field, more particularly to a kind of steam eye patch and preparation method thereof.
【Background technology】
Eyes are one of important organs of human body, and however as the popularization of electronic product, electromagnetic hazard is serious, more and more Teenager due to eye be accustomed to it is bad, cause ciliary muscle to be chronically at contraction state with eye is unhygienic, constantly filled in eyeball Blood, intraocular pressure increase accordingly, meanwhile, the anxiety and oppression eyeball of extraocular muscle, hamper the circulation of blood, are easy to cause false Myopia, after pseudo-myopia cannot be corrected effectively with eye custom, it will become permanent myopia, A nearsighted person by pseudo-myopia Prolonged reading, writes, sees TV, will feel that eyes are dry and astringent, eyelid is heavy, and eyeball acid is swollen, eye socket pain, then regarding thing It is fuzzy, there is slur, reading is serial, serious the symptoms such as giddy, headache, nausea occur.However, with rhythm of life Quickening, the pressure of people is also increasing, comes self study, life, the pressure of work so that many people are chronically at insomnia shape In state, because of the sleep of deficiency, cause position blood supply difficult, obstacle, eye water shortage occur for metabolism.
To solve the above-mentioned problems, at present, occur the series of products of steam eye patch on the market, its principle is：In eye The inner side of cover, reaches heater by moisture and oxidized metal.The independent package bag of eyeshade is opened, the oxygen in air touches Exothermic oxidation reaction occurs for the oxidized metal in heater so that the moisture evaporation in heater, sends steam.So as to allow patch Steam is sustained out, a variety of discomforts at pasted position are cleared up using the warm of steam；But steam eye patch now on the market, It is mostly single steam eye patch, only there is heating release steam, its temperature discharged is higher than human body temperature, to promoting Blood circulation has certain help, but effect unobvious；Its vapor discharged has eyes the moist feeling of moment, but to eye The permanent moisturizing of eyeball does not act on.Steam eye patch also, sprays artificial flavors on eyeshade, nervous system and hematopoiesis to people System produces certain injury, to calming the nerves, promoting no any help of sleeping, in addition it is harmful.
Therefore, it is necessary to produce a kind of plant that can effectively discharge pressure, lift eyesight and will not be damaged to human body Thing component essential oil eyeshade.
【The content of the invention】
In view of the above, it is necessary to which pressure, lifting eyesight can effectively be discharged and will not be caused to human body by producing one kind The plant component essential oil eyeshade of injury.
To reach above-mentioned purpose, the technical solution adopted in the present invention is：
A kind of steam eye patch, it is 10-15 that the steam eye patch is made of according to mass ratio hot radical material and essential oil material:1 Composition.
Further, the hot radical material comprises the following components in parts by weight：17 parts of -28 parts of bamboo charcoals, 12 parts of -24 parts of iron Powder, 10 parts of -16 parts of water-absorbing resins, 4 parts of -8 parts of NaHCO3, 16 portions of -24 parts of vermiculites, 13 parts of -27 parts of wormwoods, 17 portions of -29 portions of green tea Slag and 13 parts -17 parts of water.
Further, the essential oil material comprises the following components in parts by weight：50 parts of -60 parts of potato composite essential oils, 12 parts of -17 parts of osmanthus essential oils, 9 parts of -17 parts of apple essential oils, 10 parts of -21 parts of mint extracts, 21 parts of -32 parts of Fructus Hordei Germinatus essential oils, 7 - 15 parts of olive oil of part, 16 parts of -27 parts of fatty acid glycerides and 13 parts of -23 parts of water.
Further, potato essential oil and weight of the potato composite essential oil by percentage by weight for 70%-90% The auxiliary material essential oil that percentage is 10%-30% forms.
Further, the potato essential oil is made by potato；The auxiliary material essential oil by following parts by weight component system ：17 parts -29 parts of Chinese toon wood skin, 13 parts -31 parts of Radix agastaches, 24 parts -32 parts of Semen sesami nigrum and 34 parts -46 parts of the leaf of bamboo.
Further, the potato composite essential oil preparation method include potato extraction of essential oil, auxiliary material extraction of essential oil and Essential oil mixes three steps and is made, and comprises the following steps that：
(1) potato extraction of essential oil：
Step S1：Potato is puffing：Potato is cut into the potato block that thickness is 1-3mm, then potato block is put into Temperature is to soak 1-2h in 0-2 DEG C of frozen water, potato block is taken out drain be totally submerged keep 1-2s in rapeseed oil after take Go out, be put into steamer cook, mashed into paste, it is 9MPa-10MPa that mashed potato then is put into pressure condition, temperature 100 Keep 10min-15min in DEG C -105 DEG C of hot wind, pressure release, then it is 0MPa-2MPa that mashed potato is put into pressure condition, temperature It is puffing to keep 5min-10min to complete potato in 0 DEG C -5 DEG C of cold wind；
Step S2：Cellulase treatment：By potatos of the step S1 after puffing and biology enzyme I solution according to solid-liquid mass ratio For 1:1-2 mixing immersions, 20min-30min is stood in the insulating box that temperature is 27 DEG C, is then concentrated, drying goes to remove water Get potato flour；Wherein, biology enzyme I solution is made of the raw material of following parts by weight：30 parts -35 parts of amylase, 20 Parts -25 parts carbohydrase, 5 parts -10 parts of aspergillus oryzae, 10 parts -20 parts of barbaloin and 250 parts of -300 parts of mass percents are 1% sodium hydroxide solution；The enzyme activity of the amylase is 800u/g-1000u/g；The enzyme activity of the carbohydrase is 1000u/g-1200u/g；The living bacteria count of the aspergillus oryzae is 3.1 × 107~6.7 × 107CFU/g；
Step S3：Microwave treatment：After the potato flour of step S2 is cooled to room temperature, it is laid in plate, tiling is thick Spend for 1mm-3mm, be placed on microwave oven turntable and carry out microwave treatment, the frequency of the microwave treatment is 2300MHZ, and power is 1000W, total duration 180s；
Step S4：Supercritical CO2Extraction：By in the potato flour input extraction kettle after step S3 microwave treatments, pressing When power is 15-20MPa, with liquid CO2Static extracting 30-40min, then progressively discharges pressure, carries out supercritical CO2Dynamic extracts Take, dynamic extraction technological parameter is：When temperature is heated to 40-50 DEG C, pressurize to system, pressure reaches 40-50MPa Afterwards, CO is adjusted2Flow is 15-25L/min, keeps constant temperature and pressure to discharge after carrying out cycling extraction 2-4h, in 800-1000r/min Under conditions of be centrifuged to obtain potato essential oil.
(2) auxiliary material extraction of essential oil：
Step A1：Auxiliary material is puffing：Each raw material is weighed by above-mentioned parts by weight to be crushed respectively, by -50 mesh sieve net of 30 mesh Screening, is then 1 according to solid-liquid mass ratio by ethanol solution that Chinese toon wood skin powder and percentage by volume are 75%:2 mixing；By the leaves of pulse plants The butanol solution that spiceleaf powder is 10% with percentage by volume is 1 according to solid-liquid mass ratio:1 mixing；By Semen sesami nigrum powder and body The ethanol solution that product percentage is 75% is 1 according to solid-liquid mass ratio:1 mixing；By leaf of bamboo powder and water according to solid-liquid mass ratio For 1:1 mixing；Then each powder soak is placed in the refrigerator-freezer that temperature is -2 DEG C~0 DEG C and refrigerates 24h-26h；Filtering, takes each Powder mixes, and it is 8MPa-9MPa to be put into after being infiltrated in rapeseed oil mixed-powder being put into pressure condition, and temperature is 110 DEG C -120 DEG C hot wind in keep 20min-25min, pressure release, then it is 0MPa-2MPa that mashed potato is put into pressure condition, temperature for 0 DEG C- 15min-20min is kept to complete auxiliary material in 5 DEG C of cold wind puffing；
Step A2：Cellulase treatment：By auxiliary materials of the step S1 after puffing and biology enzyme II solution according to solid-liquid mass ratio For 1:1-2 mixing immersions, 20min-30min is stood in the insulating box that temperature is 27 DEG C, is then concentrated, drying goes to remove water Get auxiliary material dry powder；Wherein, biology enzyme II solution is made of the raw material of following parts by weight：15 parts -25 parts of pectase, 30 Cellulase, 20 parts -30 parts of amylase, 10 parts -20 parts of aspergillus flavus and 300 parts of -350 parts of mass percents of -50 parts of part For 2% sodium chloride solution；The enzyme activity of the pectase is 1200u/g-1500u/g；The enzyme activity of the cellulase is 1500u/g-2000u/g；The enzyme activity of the amylase is 900u/g-1200u/g；The living bacteria count of the aspergillus flavus is 3.9×108~6.7 × 108CFU/g；
Step A3：Supercritical CO2Extraction：The auxiliary material dry powder of step S2 is put into extraction kettle, is 15-20MPa in pressure When, with liquid CO2Static extracting 20-30min, then progressively discharges pressure, carries out supercritical CO2Dynamic extraction, dynamic extraction work Skill parameter is：When temperature is heated to 50-60 DEG C, pressurize to system, after pressure reaches 30-40MPa, adjust CO2Flow For 15-25L/min, keep constant temperature and pressure to discharge after carrying out cycling extraction 3-5h, carried out under conditions of 800-1000r/min from The isolated auxiliary material essential oil of the heart.
(3) essential oil mixes：
Potato essential oil and auxiliary material essential oil are weighed according to percentage by weight, is 75% by potato essential oil and percentage by volume Ethanol solution according to 2:1 is mixed, and 5min-7min is stirred under the speed conditions of 500-800r/min, is then added Auxiliary material essential oil, continues to stir 6min-8min, rotary evaporation concentration goes moisture removal that potato composite precision described herein is made Oil.
Present invention also provides a kind of preparation method for preparing steam eye patch, this method comprises the following steps：
(1) each material composition is weighed by the parts by weight；
(2) potato composite essential oil, osmanthus essential oil, apple essential oil and Fructus Hordei Germinatus essential oil are mixed, and are put into mixer Blend of essential oils is made in stirring, and the mixing time is 25min-35min；Speed of agitator is 100r/min-300r/min；Then Blend of essential oils is put into temperature to be freezed in -5 DEG C~0 DEG C refrigerator-freezer, cooling time obtains freezing essential oil for 2h-4h；
(3) the obtained freezing essential oil of step (2) is placed on and thawed under room temperature, until temperature is 10 DEG C~15 DEG C, so Fatty acid glyceride, water and olive oil is added into blend of essential oils again afterwards to be stirred to obtain essential oil emulsion with high speed dispersor, The mixing time is 15min-20min, speed of agitator 400r/min-600r/min；
(4) by NaHCO3It is put into water and obtains salting liquid；The whole strain of wormwood is dried, until moisture content is 3%, Ran Houjin Row crushes, selects to obtain wormwood powder by 60 mesh sieve mesh screens；Green tea slag is dried, until moisture content is 3%, is then carried out Crush, select to obtain green tea ground-slag end by 60 mesh sieve mesh screens；Bamboo charcoal, wormwood powder, green tea ground-slag end and water-absorbing resin are poured into Stirring 5min-10min obtains solid mixt under conditions of rotating speed is 100r/min-300r/min in mixer；Salt is molten Liquid is poured into above-mentioned solid mixt, and stirring 1min-3min obtains liquid under conditions of rotating speed is 200r/min-400r/min State mixture, then again adds iron powder in liquefied mixture, is stirred under conditions of rotating speed is 100r/min-200r/min Hot radical material is made by vibrating screen screening, sealing, cooling again after 2min-5min；
(5) take hermetically sealable film, ventilated membrane, sterile-cloth to carry out corresponding to cutting, from outside to inside according to hermetically sealable film, ventilated membrane, The order of sterile-cloth is arranged, and under vacuum, to hot radical material is filled between hermetically sealable film and ventilated membrane, ventilative Even spread essential oil emulsion between film and sterile-cloth, and hermetically sealable film, ventilated membrane and sterile-cloth overlapping edge portions are carried out Suture, obtain the steam eye patch.
Green tea used in this application is pekoe tea；It is 1 that green tea slag, which is pekoe tea with boiling water by solid-liquid mass ratio,:3 mixing leachings Steep filtering after 30min, immersion 3 times, dry be made to 3%.
The present invention has the advantages that：
1st, the steam eye patch of the application is made of hot radical material and essential oil material, wherein, hot radical material by bamboo charcoal, iron powder, Water-absorbing resin, NaHCO3, vermiculite, wormwood, green tea slag and water composition；Wherein hot radical material energy efficient heat generation；Essential oil material is by horse Bell potato composite essential oil, osmanthus essential oil, apple essential oil, mint extract, Fructus Hordei Germinatus essential oil, olive oil, fatty acid glyceride and water Composition；Wherein, potato composite essential oil includes the derived essential oil extracted from potato and the auxiliary material essential oil extracted from auxiliary material Component, by potato essential oil and auxiliary material essential oil compounding use, can improve the DPPH free radical scavenging activities of potato derived essential oil, Improve the inoxidizability of essential oil.The essential oil extracted in potato essential oil contains abundant lactone component, can effectively improve essential oil perfume The essential oil extracted in gas Chinese toon wood skin is relatively enriched with oxygenatedchemicals, can improve the oxidation resistance of essential oil；The essence extracted in Radix agastaches Oil can improve the sterilizing ability of essential oil, so as to improve oxidation resistance compared with beneficiation of hydrocarbons compound；The essential oil extracted in Semen sesami nigrum Compared with enrichment oxygenatedchemicals component, so as to improve oxidation resistance；The essential oil extracted in the leaf of bamboo is relatively enriched with oxygenatedchemicals component, So as to improve oxidation resistance.Make when containing Chinese toon wood skin, Semen sesami nigrum and several components mutual cooperations of the leaf of bamboo in auxiliary material derived essential oil With rear, the oxygenatedchemicals component that can significantly improve essential oil improves the oxidation resistance of essential oil, so that with very strong suppression body The ability of extracellular tyrosinase enzymatic activity.
2nd, although the application potato composite essential oil has very strong oxidation resistance, but wherein containing abundant dimension life Plain C components, can decompose under the conditions of fever, and substantially reduce the activity of potato composite essential oil, in this regard, the essence of the application eyeshade Light wood material by also allocated osmanthus essential oil, apple essential oil, mint extract, Fructus Hordei Germinatus essential oil, olive oil, fatty acid glyceride and Water, the apple essential oil and Fructus Hordei Germinatus essential oil used in essential oil material contain vitamin E component, which has heat resistanceheat resistant, antiacid, anti- Photosensitizing effect, can inhibit the lipid peroxidation reaction in ocular lens body, make peripheral vasodilation, improve blood circulation, and prevention is near Depending on eye occurrence and development；Containing abundant antioxidant content in osmanthus essential oil, apple essential oil, mint extract, can effectively alleviate Pressure, has good effect of easing stress.
3rd, the application potato first carries out puffing, microwave treatment and cellulase treatment during essential oil is extracted, due to Its essential oil of the potato of the application and Vitamin C content ratio starch and protein content component are low, and starch, protein material With viscosity, the small-molecule substance such as essential oil and vitamin C cannot be separated out effectively, if, it is impossible to its potato is pre-processed The output capacity of essential oil will be largely effected on, is soaked in the present frozen water of potato, can remove most starch material, Ma Ling Potato chips will cause most starch chain and protein hydrogen bonds to be broken after high pressure, low pressure are puffing, with biology after crushing Enzyme and microwave are handled, and can effectively remove content of starch, destroy the molecular structure of starch and protein, and this temperature, pressure Power will not destroy derived essential oil again, will can effectively facilitate the precipitation efficiency of essential oil, improve the essential oil yield of potato；Meanwhile this Apply for the supercritical CO used2Extraction prepares potato essential oil, and this method is easy to operate, ripe, and preparation rate is high, purity It is high miscellaneous few；The characteristics of the application is directed to starch in potato, protein content is more is configured with biology enzyme I solution, forms sediment in enzyme solutions Powder enzyme can effectively starch-splitting, carbohydrase starch can be decomposed into the glucose of small molecule, aspergillus oryzae containing abundant viable bacteria into Point, can effective decomposing protein, barbaloin can effectively improve aspergillus oryzae activity, sodium hydroxide solution can be biology enzyme I solution carry For enzymolysis environment preferably；The characteristics of it is mostly plant component that the application, which is directed in auxiliary material, and content of cellulose is high is configured with biology Enzyme II solution, pectase can effectively decompose the pectin composition in plant in enzyme solutions, and cellulase can be decomposed effectively in plant Cellulose components, amylase can effectively decompose starch enzyme component in plant, in aspergillus flavus containing abundant viable bacteria component, can be effective Promote the decomposition of cellulose, sodium chloride solution can provide enzymolysis environment preferably for biology enzyme II solution.
【Embodiment】
All features disclosed in this specification, or disclosed all methods or during the step of, except mutually exclusive Feature and/or step beyond, can combine in any way.
Any feature disclosed in this specification (including any accessory claim, summary), unless specifically stated, each Feature is an example in a series of equivalent or similar characteristics.
Embodiment 1：
It is 10 that the steam eye patch of the present embodiment is made of according to mass ratio hot radical material and essential oil material:1 composition；Wherein, Hot radical material comprises the following components in parts by weight：17 parts of bamboo charcoals, 12 parts of iron powders, 10 parts of water-absorbing resins, 4 parts of NaHCO3, 16 parts Vermiculite, 13 parts of wormwoods, 17 parts of green tea slags and 13 parts of water；Essential oil material comprises the following components in parts by weight：50 portions of potatos Composite essential oil, 12 parts of osmanthus essential oils, 9 parts of apple essential oils, 10 parts of mint extracts, 21 parts of Fructus Hordei Germinatus essential oils, 7 parts of olive oil, 16 Part fatty acid glyceride and 13 parts of water.
The extracting method of osmanthus essential oil is in the present embodiment：It is 2% by dried sweet-scented osmanthus and mass percent that moisture content is 3% Sodium chloride solution according to mass ratio be 1:3 are mixed, and are then placed into handling 2.0h in steam distillation generator, condensation Distilled crude extract is collected afterwards, and water-oil separating takes upper strata fluid to be put into -30 DEG C of refrigerator-freezers, stands 12h, precipitation, takes supernatant, that is, obtain Osmanthus essential oil, recovery rate 12.3%, after testing, (53.42%) containing α-terpinenes in essential oil.
The extracting method of apple essential oil is in the present embodiment：It is 2% that fresh apple pulp, which is smashed to pieces with mass percent, Sodium chloride solution is 1 according to mass ratio:2 are mixed, and are then placed into handling 3h in steam distillation generator, are received after condensation Collect distilled crude extract, water-oil separating takes upper strata fluid to be put into -20 DEG C of refrigerator-freezers, stands 10h, precipitation, takes supernatant, that is, obtain apple Meat essential oil；Apple Seeds are crushed, after mixing with petroleum ether solution according to mass ratio be 1:2 are mixed, and are then placed into water steaming Decatize slips and 2h is handled in generator, distilled crude extract is collected after condensation, water-oil separating takes upper strata fluid to be put into -30 DEG C of refrigerator-freezers, quiet 10h, precipitation are put, supernatant is taken, that is, obtains Apple Seeds essential oil, apple grunt essential oil and Apple Seeds essential oil are mixed to get apple essence Oil, the recovery rate of apple essential oil are 15.9%, and after testing, (26.35%) containing 1,8- cineoles in essential oil, content of vitamin E is 13.05%.
The extracting method of mint extract is in the present embodiment：The whole strain of dried peppermint that moisture content is 5% is crushed to 80 mesh, Obtain Herba Menthae powder；Then it is 1 according to solid-liquid mass ratio by ethanol solution that Herba Menthae powder and percentage by volume are 75%：2 are mixed Close, mixture is put into the refluxing extraction device that temperature is 105 DEG C carries out refluxing extraction afterwards, extraction time 2h, filters off Except filter residue, take filtrate to carry out rotary evaporation and be concentrated into paste, until the relative density of paste is 2.35g/cm3Obtain described thin Lotus extract, general flavone content is 156.36mg/g in extract, total phenol content 74.35, content of vitamin E is 57.09mg/g。
The extracting method of Fructus Hordei Germinatus essential oil is in the present embodiment：According to plumule and proportion of ethanol it is 1 by barley germs:2 into Row grinding, is then placed into handling 2h in steam distillation generator, and distilled crude extract is collected after condensation, and water-oil separating takes upper strata Fluid is put into -20 DEG C of refrigerator-freezers, stands 10h, precipitation, takes supernatant, that is, obtain Fructus Hordei Germinatus essential oil, the recovery rate of wherein essential oil is 4.36%, the alcohol containing (+/-)-terpenes -4- (12.36%) in Fructus Hordei Germinatus essential oil, terpinolene (9.64%), content of vitamin E is 5.36%.
In the present embodiment, potato essential oil and percentage by weight that potato composite essential oil is 70% by percentage by weight are 30% auxiliary material essential oil composition, the potato essential oil of the present embodiment are made by potato；Auxiliary material essential oil by following parts by weight into Divide and be made：17 parts of Chinese toon wood skin, 13 parts of Radix agastaches, 24 parts of Semen sesami nigrum and 34 parts of the leaf of bamboo.
In the present embodiment, potato composite essential oil preparation method includes potato extraction of essential oil, auxiliary material extraction of essential oil and essence Three steps of oil mixing are made, and comprise the following steps that：
(1) potato extraction of essential oil：
Step S1：Potato is puffing：Potato is cut into the potato block that thickness is 1mm, then potato block is put into temperature Spend in the frozen water for 0 DEG C and soak 1h, potato block is taken out to drain to be totally submerged in rapeseed oil and is taken out after holding 1s, is put into steaming Cooked in pot, mashed into paste, it is 9MPa that mashed potato then is put into pressure condition, and temperature is to be kept in 100 DEG C of hot wind 10min, pressure release, then it is 0MPa that mashed potato is put into pressure condition, keeps 5min to complete potato in the cold wind that temperature is 0 DEG C It is puffing；
Step S2：Cellulase treatment：By potatos of the step S1 after puffing and biology enzyme I solution according to solid-liquid mass ratio For 1:1 mixing immersion, 20min is stood in the insulating box that temperature is 27 DEG C, is then concentrated, drying goes moisture removal to obtain horse Bell potato dry powder；Wherein, biology enzyme I solution is made of the raw material of following parts by weight：30 parts of amylase, 20 parts of carbohydrase, 5 parts Aspergillus oryzae, 10 parts of barbaloin and 250 parts of mass percents be 1% sodium hydroxide solution；The enzyme activity of the amylase For 800u/g；The enzyme activity of the carbohydrase is 1000u/g；The living bacteria count of the aspergillus oryzae is 3.1 × 107；
Step S3：Microwave treatment：After the potato flour of step S2 is cooled to room temperature, it is laid in plate, tiling is thick Spend for 1mm, be placed on microwave oven turntable and carry out microwave treatment, the frequency of the microwave treatment is 2300MHZ, and power is 1000W, total duration 180s；
Step S4：Supercritical CO2Extraction：By in the potato flour input extraction kettle after step S3 microwave treatments, pressing When power is 15-20MPa, with liquid CO2Static extracting 30min, then progressively discharges pressure, carries out supercritical CO2Dynamic extraction, Dynamic extraction technological parameter is：When temperature is heated to 40 DEG C, pressurize to system, after pressure reaches 40MPa, adjust CO2 Flow is 15L/min, keeps constant temperature and pressure to discharge after carrying out cycling extraction 2h, is centrifuged under conditions of 800r/min Obtain potato essential oil.
(2) auxiliary material extraction of essential oil：
Step A1：Auxiliary material is puffing：Each raw material is weighed by above-mentioned parts by weight to be crushed respectively, is selected by 30 mesh sieve mesh screens, Then it is 1 according to solid-liquid mass ratio by ethanol solution that Chinese toon wood skin powder and percentage by volume are 75%:2 mixing；By Radix agastaches The butanol solution that powder is 10% with percentage by volume is 1 according to solid-liquid mass ratio:1 mixing；By Semen sesami nigrum powder and volume hundred The ethanol solution that fraction is 75% is 1 according to solid-liquid mass ratio:1 mixing；According to solid-liquid mass ratio it is 1 by leaf of bamboo powder and water:1 Mixing；Then each powder soak is placed in the refrigerator-freezer that temperature is -2 DEG C and refrigerates 24h；Filtering, takes each powder to mix, is put into dish It is 8MPa that mixed-powder is put into pressure condition after being infiltrated in seed oil, and temperature is that 20min is kept in 110 DEG C of hot wind, pressure release, then It is 0MPa that mashed potato is put into pressure condition, keeps 15min to complete auxiliary material in the cold wind that temperature is 0 DEG C puffing；
Step A2：Cellulase treatment：By auxiliary materials of the step S1 after puffing and biology enzyme II solution according to solid-liquid mass ratio For 1:1 mixing immersion, 20min is stood in temperature is 27 DEG C of insulating box, is then concentrated, dry to go moisture removal to obtain auxiliary Expect dry powder；Wherein, biology enzyme II solution is made of the raw material of following parts by weight：15 parts of pectase, 30 parts of cellulase, 20 The sodium chloride solution that the amylase, 10 parts of aspergillus flavus and 300 parts of mass percents of part are 2%；The enzyme activity of the pectase For 1200u/g；The enzyme activity of the cellulase is 1500u/g；The enzyme activity of the amylase is 900u/g；The aspergillus flavus Living bacteria count be 3.9 × 108；
Step A3：Supercritical CO2Extraction：The auxiliary material dry powder of step S2 is put into extraction kettle, when pressure is 15MPa, With liquid CO2Static extracting 20min, then progressively discharges pressure, carries out supercritical CO2Dynamic extraction, dynamic extraction technological parameter For：When temperature is heated to 50 DEG C, pressurize to system, after pressure reaches 30MPa, adjust CO2Flow is 15L/min, is protected Hold after constant temperature and pressure carries out cycling extraction 3h and discharge, be centrifuged to obtain auxiliary material essential oil under conditions of 800r/min.
(3) essential oil mixes：
Potato essential oil and auxiliary material essential oil are weighed according to percentage by weight, is 75% by potato essential oil and percentage by volume Ethanol solution according to 2:1 is mixed, and 5min is stirred under the speed conditions of 500r/min, then adds auxiliary material essential oil, Continue to stir 6min, rotary evaporation concentration goes moisture removal to be made.
The preparation method of the present embodiment steam eye patch includes the following steps：
(1) each material composition is weighed by the parts by weight；
(2) potato composite essential oil, osmanthus essential oil, apple essential oil and Fructus Hordei Germinatus essential oil are mixed, and are put into mixer Blend of essential oils is made in stirring, and the mixing time is 25min；Speed of agitator is 100r/min；Then blend of essential oils is put Enter temperature to be freezed in -5 DEG C of refrigerator-freezers, cooling time obtains freezing essential oil for 2h；
(3) the obtained freezing essential oil of step (2) is placed on and thawed under room temperature, until temperature is 10 DEG C, then again to Fatty acid glyceride, water and olive oil is added in blend of essential oils to be stirred to obtain essential oil emulsion with high speed dispersor, it is described to stir It is 15min, speed of agitator 400r/min to mix the time；
(4) by NaHCO3It is put into water and obtains salting liquid；The whole strain of wormwood is dried, until moisture content is 3%, Ran Houjin Row crushes, selects to obtain wormwood powder by 60 mesh sieve mesh screens；Green tea slag is dried, until moisture content is 3%, is then carried out Crush, select to obtain green tea ground-slag end by 60 mesh sieve mesh screens；Bamboo charcoal, wormwood powder, green tea ground-slag end and water-absorbing resin are poured into Stirring 10min obtains solid mixt under conditions of rotating speed is 300r/min in mixer；Salting liquid is poured into above-mentioned consolidate In state mixture, stirring 3min obtains liquefied mixture under conditions of rotating speed is 400r/min, and iron powder then is added liquid again In state mixture, it is made again by vibrating screen screening, sealing, cooling after 5min is stirred under conditions of rotating speed is 200r/min Hot radical material；
(5) take hermetically sealable film, ventilated membrane, sterile-cloth to carry out corresponding to cutting, from outside to inside according to hermetically sealable film, ventilated membrane, The order of sterile-cloth is arranged, and under vacuum, to hot radical material is filled between hermetically sealable film and ventilated membrane, ventilative Even spread essential oil emulsion between film and sterile-cloth, and hermetically sealable film, ventilated membrane and sterile-cloth overlapping edge portions are carried out Suture, obtain the steam eye patch.
Embodiment 2：
It is 15 that the steam eye patch of the present embodiment is made of according to mass ratio hot radical material and essential oil material:1 composition；Wherein, Hot radical material comprises the following components in parts by weight：28 parts of bamboo charcoals, 24 parts of iron powders, 16 parts of water-absorbing resins, 8 parts of NaHCO3, 24 parts Vermiculite, 27 parts of wormwoods, 29 parts of green tea slags and 17 parts of water；Essential oil material comprises the following components in parts by weight：60 portions of potatos Composite essential oil, 17 parts of osmanthus essential oils, 17 parts of apple essential oils, 21 parts of mint extracts, 32 parts of Fructus Hordei Germinatus essential oils, 15 parts of olive oil, 27 parts of fatty acid glycerides and 23 parts of water.
The extracting method of osmanthus essential oil in the present embodiment, the extracting method of apple essential oil, the extracting method of mint extract, The extracting method of Fructus Hordei Germinatus essential oil and embodiment 1 are completely the same.
Wherein, the potato essential oil and percentage by weight that potato composite essential oil is 90% by percentage by weight are 10% Auxiliary material essential oil forms, and the potato essential oil of the present embodiment is made by potato；The auxiliary material essential oil of the present embodiment is by following parts by weight Component be made：29 parts of Chinese toon wood skin, 31 parts of Radix agastaches, 32 parts of Semen sesami nigrum and 46 parts of the leaf of bamboo.
In the present embodiment, potato composite essential oil preparation method includes potato extraction of essential oil, auxiliary material extraction of essential oil and essence Three steps of oil mixing are made, and comprise the following steps that：
(1) potato extraction of essential oil：
Step S1：Potato is puffing：Potato is cut into the potato block that thickness is 3mm, then potato block is put into temperature Spend in the frozen water for 2 DEG C and soak 2h, potato block is taken out to drain to be totally submerged in rapeseed oil and is taken out after holding 2s, is put into steaming Cooked in pot, mashed into paste, it is 10MPa that mashed potato then is put into pressure condition, and temperature is to be kept in 105 DEG C of hot wind 15min, pressure release, then it is 2MPa that mashed potato is put into pressure condition, keeps 5min-10min to complete in the cold wind that temperature is 5 DEG C Potato is puffing；
Step S2：Cellulase treatment：By potatos of the step S1 after puffing and biology enzyme I solution according to solid-liquid mass ratio For 1:2 mixing immersions, 30min is stood in the insulating box that temperature is 27 DEG C, is then concentrated, drying goes moisture removal to obtain horse Bell potato dry powder；Wherein, biology enzyme I solution is made of the raw material of following parts by weight：35 parts of amylase, 25 parts of carbohydrase, 10 The sodium hydroxide solution that the aspergillus oryzae, 20 parts of barbaloin and 300 parts of mass percents of part are 1%；The enzyme activity of the amylase Power is 1000u/g；The enzyme activity of the carbohydrase is 1200u/g；The living bacteria count of the aspergillus oryzae is 6.7 × 107CFU/ g；
Step S3：Microwave treatment：After the potato flour of step S2 is cooled to room temperature, it is laid in plate, tiling is thick Spend for 3mm, be placed on microwave oven turntable and carry out microwave treatment, the frequency of the microwave treatment is 2300MHZ, and power is 1000W, total duration 180s；
Step S4：Supercritical CO2Extraction：By in the potato flour input extraction kettle after step S3 microwave treatments, pressing When power is 20MPa, with liquid CO2Static extracting 40min, then progressively discharges pressure, carries out supercritical CO2Dynamic extraction, dynamic Extraction process parameter is：When temperature is heated to 50 DEG C, pressurize to system, after pressure reaches 50MPa, adjust CO2Flow For 25L/min, keep constant temperature and pressure to discharge after carrying out cycling extraction 4h, be centrifuged under conditions of 1000r/min To potato essential oil.
(2) auxiliary material extraction of essential oil：
Step A1：Auxiliary material is puffing：Each raw material is weighed by above-mentioned parts by weight to be crushed respectively, is selected by 50 mesh sieve mesh screens, Then it is 1 according to solid-liquid mass ratio by ethanol solution that Chinese toon wood skin powder and percentage by volume are 75%:2 mixing；By Radix agastaches The butanol solution that powder is 10% with percentage by volume is 1 according to solid-liquid mass ratio:1 mixing；By Semen sesami nigrum powder and volume hundred The ethanol solution that fraction is 75% is 1 according to solid-liquid mass ratio:1 mixing；According to solid-liquid mass ratio it is 1 by leaf of bamboo powder and water:1 Mixing；Then each powder soak is placed in the refrigerator-freezer that temperature is 0 DEG C and refrigerates 26h；Filtering, takes each powder to mix, is put into dish It is 9MPa that mixed-powder is put into pressure condition after being infiltrated in seed oil, and temperature is that 25min is kept in 120 DEG C of hot wind, pressure release, then It is 2MPa that mashed potato is put into pressure condition, keeps 20min to complete auxiliary material in the cold wind that temperature is 5 DEG C puffing；
Step A2：Cellulase treatment：By auxiliary materials of the step S1 after puffing and biology enzyme II solution according to solid-liquid mass ratio For 1:2 mixing immersions, 30min is stood in temperature is 27 DEG C of insulating box, is then concentrated, dry to go moisture removal to obtain auxiliary Expect dry powder；Wherein, biology enzyme II solution is made of the raw material of following parts by weight：25 parts of pectase, 50 parts of cellulase, 30 The sodium chloride solution that the amylase, 20 parts of aspergillus flavus and 350 parts of mass percents of part are 2%；The enzyme activity of the pectase For 1500u/g；The enzyme activity of the cellulase is 2000u/g；The enzyme activity of the amylase is 1200u/g；It is described yellow bent Mould living bacteria count is 6.7 × 108CFU/g；
Step A3：Supercritical CO2Extraction：The auxiliary material dry powder of step S2 is put into extraction kettle, when pressure is 20MPa, With liquid CO2Static extracting 30min, then progressively discharges pressure, carries out supercritical CO2Dynamic extraction, dynamic extraction technological parameter For：When temperature is heated to 60 DEG C, pressurize to system, after pressure reaches 40MPa, adjust CO2Flow is 25L/min, is protected Hold after constant temperature and pressure carries out cycling extraction 5h and discharge, be centrifuged to obtain auxiliary material essential oil under conditions of 1000r/min.
(3) essential oil mixes：
Potato essential oil and auxiliary material essential oil are weighed according to percentage by weight, is 75% by potato essential oil and percentage by volume Ethanol solution according to 2:1 is mixed, and 7min is stirred under the speed conditions of 800r/min, then adds auxiliary material essential oil, Continue to stir 8min, rotary evaporation concentration goes moisture removal to be made.
The preparation method of the present embodiment steam eye patch includes the following steps：
(1) each material composition is weighed by the parts by weight；
(2) potato composite essential oil, osmanthus essential oil, apple essential oil and Fructus Hordei Germinatus essential oil are mixed, and are put into mixer Blend of essential oils is made in stirring, and the mixing time is 35min；Speed of agitator is 300r/min；Then blend of essential oils is put Enter temperature to be freezed in 0 DEG C of refrigerator-freezer, cooling time obtains freezing essential oil for 4h；
(3) the obtained freezing essential oil of step (2) is placed on and thawed under room temperature, until temperature is 15 DEG C, then again to Fatty acid glyceride, water and olive oil is added in blend of essential oils to be stirred to obtain essential oil emulsion with high speed dispersor, it is described to stir It is 20min to mix the time, and speed of agitator is -600r/min；
(4) by NaHCO3It is put into water and obtains salting liquid；The whole strain of wormwood is dried, until moisture content is 3%, Ran Houjin Row crushes, selects to obtain wormwood powder by 60 mesh sieve mesh screens；Green tea slag is dried, until moisture content is 3%, is then carried out Crush, select to obtain green tea ground-slag end by 60 mesh sieve mesh screens；Bamboo charcoal, wormwood powder, green tea ground-slag end and water-absorbing resin are poured into Stirring 10min obtains solid mixt under conditions of rotating speed is 300r/min in mixer；Salting liquid is poured into above-mentioned consolidate In state mixture, stirring 3min obtains liquefied mixture under conditions of rotating speed is 400r/min, and iron powder then is added liquid again In state mixture, it is made again by vibrating screen screening, sealing, cooling after 5min is stirred under conditions of rotating speed is 200r/min Hot radical material；
(5) take hermetically sealable film, ventilated membrane, sterile-cloth to carry out corresponding to cutting, from outside to inside according to hermetically sealable film, ventilated membrane, The order of sterile-cloth is arranged, and under vacuum, to hot radical material is filled between hermetically sealable film and ventilated membrane, ventilative Even spread essential oil emulsion between film and sterile-cloth, and hermetically sealable film, ventilated membrane and sterile-cloth overlapping edge portions are carried out Suture, obtain the steam eye patch.
Embodiment 3：
It is 12 that the steam eye patch of the present embodiment is made of according to mass ratio hot radical material and essential oil material:1 composition；Wherein, Hot radical material comprises the following components in parts by weight：19 parts of bamboo charcoals, 20 parts of iron powders, 10 parts of -16 parts of water-absorbing resins, 6 parts of NaHCO3、 18 parts of vermiculites, 19 parts of wormwoods, 21 parts of green tea slags and 15 parts of water；Essential oil material comprises the following components in parts by weight：55 portions of horses Bell potato composite essential oil, 15 parts of osmanthus essential oils, 12 parts of apple essential oils, 18 parts of mint extracts, 28 parts of Fructus Hordei Germinatus essential oils, 12 portions of olives Oil, 20 parts of fatty acid glycerides and 20 parts of water.
The extracting method of osmanthus essential oil in the present embodiment, the extracting method of apple essential oil, the extracting method of mint extract, The extracting method of Fructus Hordei Germinatus essential oil and embodiment 1 are completely the same.
Wherein, the potato essential oil and percentage by weight that potato composite essential oil is 80% by percentage by weight are 20% Auxiliary material essential oil forms, and the potato essential oil of the present embodiment is made by potato；The auxiliary material essential oil of the present embodiment is by following parts by weight Component be made：21 parts of Chinese toon wood skin, 21 parts of Radix agastaches, 24 parts of Semen sesami nigrum and 40 parts of the leaf of bamboo.
In the present embodiment, potato composite essential oil preparation method includes potato extraction of essential oil, auxiliary material extraction of essential oil and essence Three steps of oil mixing are made, and comprise the following steps that：
(1) potato extraction of essential oil：
Step S1：Potato is puffing：Potato is cut into the potato block that thickness is 2mm, then potato block is put into temperature Spend in the frozen water for 1 DEG C and soak 1.5h, potato block is taken out to drain to be totally submerged in rapeseed oil and is taken out after holding 2s, is put into Cooked in steamer, mashed into paste, it is 9MPa that mashed potato then is put into pressure condition, and temperature is to be kept in 103 DEG C of hot wind 12min, pressure release, then it is 1MPa that mashed potato is put into pressure condition, keeps 8min to complete potato in the cold wind that temperature is 2 DEG C It is puffing；
Step S2：Cellulase treatment：By potatos of the step S1 after puffing and biology enzyme I solution according to solid-liquid mass ratio For 1:2 mixing immersions, 25min is stood in the insulating box that temperature is 27 DEG C, is then concentrated, drying goes moisture removal to obtain horse Bell potato dry powder；Wherein, biology enzyme I solution is made of the raw material of following parts by weight：32 parts of amylase, 22 parts of carbohydrase, 8 parts Aspergillus oryzae, 15 parts of barbaloin and 270 parts of mass percents be 1% sodium hydroxide solution；The enzyme activity of the amylase For 900u/g；The enzyme activity of the carbohydrase is 1100u/g；The living bacteria count of the aspergillus oryzae is 4.7 × 107CFU/g；
Step S3：Microwave treatment：After the potato flour of step S2 is cooled to room temperature, it is laid in plate, tiling is thick Spend for 2mm, be placed on microwave oven turntable and carry out microwave treatment, the frequency of the microwave treatment is 2300MHZ, and power is 1000W, total duration 180s；
Step S4：Supercritical CO2Extraction：By in the potato flour input extraction kettle after step S3 microwave treatments, pressing When power is 18MPa, with liquid CO2Static extracting 35min, then progressively discharges pressure, carries out supercritical CO2Dynamic extraction, dynamic Extraction process parameter is：When temperature is heated to 45 DEG C, pressurize to system, after pressure reaches 45MPa, adjust CO2Flow For 20L/min, keep constant temperature and pressure to discharge after carrying out cycling extraction 3h, be centrifuged to obtain under conditions of 900r/min Potato essential oil.
(2) auxiliary material extraction of essential oil：
Step A1：Auxiliary material is puffing：Each raw material is weighed by above-mentioned parts by weight to be crushed respectively, is selected by 40 mesh sieve mesh screens, Then it is 1 according to solid-liquid mass ratio by ethanol solution that Chinese toon wood skin powder and percentage by volume are 75%:2 mixing；By Radix agastaches The butanol solution that powder is 10% with percentage by volume is 1 according to solid-liquid mass ratio:1 mixing；By Semen sesami nigrum powder and volume hundred The ethanol solution that fraction is 75% is 1 according to solid-liquid mass ratio:1 mixing；According to solid-liquid mass ratio it is 1 by leaf of bamboo powder and water:1 Mixing；Then each powder soak is placed in the refrigerator-freezer that temperature is -1 DEG C and refrigerates 25h；Filtering, takes each powder to mix, is put into dish It is 9MPa that mixed-powder is put into pressure condition after being infiltrated in seed oil, and temperature is that 23min is kept in 115 DEG C of hot wind, pressure release, then It is 1MPa that mashed potato is put into pressure condition, keeps 18min to complete auxiliary material in the cold wind that temperature is 3 DEG C puffing；
Step A2：Cellulase treatment：By auxiliary materials of the step S1 after puffing and biology enzyme II solution according to solid-liquid mass ratio For 1:1 mixing immersion, 25min is stood in temperature is 27 DEG C of insulating box, is then concentrated, dry to go moisture removal to obtain auxiliary Expect dry powder；Wherein, biology enzyme II solution is made of the raw material of following parts by weight：20 parts of pectase, 40 parts of cellulase, 25 The sodium chloride solution that the amylase, 15 parts of aspergillus flavus and 330 parts of mass percents of part are 2%；The enzyme activity of the pectase For 1300u/g；The enzyme activity of the cellulase is 1800u/g；The enzyme activity of the amylase is 1100u/g；It is described yellow bent Mould living bacteria count is 5.7 × 108CFU/g；
Step A3：Supercritical CO2Extraction：The auxiliary material dry powder of step S2 is put into extraction kettle, when pressure is 17MPa, With liquid CO2Static extracting 25min, then progressively discharges pressure, carries out supercritical CO2Dynamic extraction, dynamic extraction technological parameter For：When temperature is heated to 55 DEG C, pressurize to system, after pressure reaches 35MPa, adjust CO2Flow is 20L/min, is protected Hold after constant temperature and pressure carries out cycling extraction 4h and discharge, be centrifuged to obtain auxiliary material essential oil under conditions of 900r/min.
(3) essential oil mixes：
Potato essential oil and auxiliary material essential oil are weighed according to percentage by weight, is 75% by potato essential oil and percentage by volume Ethanol solution according to 2:1 is mixed, and 6min is stirred under the speed conditions of 700r/min, then adds auxiliary material essential oil, Continue to stir 7min, rotary evaporation concentration goes moisture removal to be made.
The preparation method of the present embodiment steam eye patch includes the following steps：
(1) each material composition is weighed by the parts by weight；
(2) potato composite essential oil, osmanthus essential oil, apple essential oil and Fructus Hordei Germinatus essential oil are mixed, and are put into mixer Blend of essential oils is made in stirring, and the mixing time is 30min；Speed of agitator is 200r/min；Then blend of essential oils is put Enter temperature to be freezed in -3 DEG C of refrigerator-freezers, cooling time obtains freezing essential oil for 3h；
(3) the obtained freezing essential oil of step (2) is placed on and thawed under room temperature, until temperature is 12 DEG C, then again to Fatty acid glyceride, water and olive oil is added in blend of essential oils to be stirred to obtain essential oil emulsion with high speed dispersor, it is described to stir It is 17min, speed of agitator 500r/min to mix the time；
(4) by NaHCO3It is put into water and obtains salting liquid；The whole strain of wormwood is dried, until moisture content is 3%, Ran Houjin Row crushes, selects to obtain wormwood powder by 60 mesh sieve mesh screens；Green tea slag is dried, until moisture content is 3%, is then carried out Crush, select to obtain green tea ground-slag end by 60 mesh sieve mesh screens；Bamboo charcoal, wormwood powder, green tea ground-slag end and water-absorbing resin are poured into Stirring 7min obtains solid mixt under conditions of rotating speed is 200r/min in mixer；Salting liquid is poured into above-mentioned solid-state In mixture, stirring 2min obtains liquefied mixture under conditions of rotating speed is 300r/min, and iron powder then is added liquid again In mixture, heat is made by vibrating screen screening, sealing, cooling again after 3min is stirred under conditions of rotating speed is 150r/min Sill；
(5) take hermetically sealable film, ventilated membrane, sterile-cloth to carry out corresponding to cutting, from outside to inside according to hermetically sealable film, ventilated membrane, The order of sterile-cloth is arranged, and under vacuum, to hot radical material is filled between hermetically sealable film and ventilated membrane, ventilative Even spread essential oil emulsion between film and sterile-cloth, and hermetically sealable film, ventilated membrane and sterile-cloth overlapping edge portions are carried out Suture, obtain the steam eye patch.
(1) the research control experiment of potato composite essential oil characteristic：
Control group 1：
The potato composite essential oil of this control group contains only potato essential oil, without using auxiliary material essential oil, other preparation methods with Embodiment 1 is identical.
Control group 2：
The potato composite essential oil of this control group contains only auxiliary material essential oil, without potato essential oil, other preparation methods and reality It is identical to apply example 1.
Control group 3：
The auxiliary material essential oil of this control group potato composite essential oil only contains Radix agastaches, Semen sesami nigrum and several components of the leaf of bamboo, i.e., The auxiliary material essence that the potato essential oil and percentage by weight that the potato essential oil of this control group is 70% by percentage by weight are 30% Oil composition, wherein, potato essential oil is made by potato；Auxiliary material essential oil is made by the component of following parts by weight：13 parts of wrinkled giant hyssop Leaf, 24 parts of Semen sesami nigrum and 34 parts of leaf of bamboo composition, other preparation methods are identical with embodiment 1.
Control group 4：
The auxiliary material essential oil of this control group potato composite essential oil only contains Chinese toon wood skin, Semen sesami nigrum and several components of the leaf of bamboo, i.e., The auxiliary material essence that the potato essential oil and percentage by weight that the potato essential oil of this control group is 70% by percentage by weight are 30% Oil composition, wherein, potato essential oil is made by potato；Auxiliary material essential oil is made by the component of following parts by weight：17 parts of Chinese toon wood Skin, 24 parts of Semen sesami nigrum and 34 parts of leaf of bamboo composition, other preparation methods are identical with embodiment 1.
Control group 5：
The auxiliary material essential oil of this control group potato composite essential oil only contains Chinese toon wood skin, Radix agastaches and several components of the leaf of bamboo, i.e., The auxiliary material essence that the potato essential oil and percentage by weight that the potato essential oil of this control group is 70% by percentage by weight are 30% Oil composition, wherein, potato essential oil is made by potato；Auxiliary material essential oil is made by the component of following parts by weight：17 parts of Chinese toon wood Skin, 13 parts of Radix agastaches and 34 parts of leaf of bamboo composition, other preparation methods are identical with embodiment 1.
Control group 6：
The auxiliary material essential oil of this control group potato composite essential oil only contains Chinese toon wood skin, Radix agastaches and several components of Semen sesami nigrum, That is the auxiliary material that the potato essential oil and percentage by weight that the potato essential oil of this control group is 70% by percentage by weight are 30% Essential oil forms, wherein, potato essential oil is made by potato；Auxiliary material essential oil is made by the component of following parts by weight：17 parts of Chinese toon Wood skin, 13 parts of Radix agastaches and 24 parts of Semen sesami nigrum composition, other preparation methods are identical with embodiment 1.
Control group 7：
Without expanding treatment in the potato essential oil producing process of this control group potato composite essential oil, but directly will Potato flour is digested, supercritical CO2Extraction, other preparation methods are identical with embodiment 1.
Control group 8：
Without enzymolysis in the potato essential oil producing process of this control group potato composite essential oil, but carry out potato Puffing, supercritical CO2Extraction, other preparation methods are identical with embodiment 1.
Control group 9：
Only pass through supercritical CO in the potato essential oil producing process of this control group potato composite essential oil2Extraction, it is other Preparation method is identical with embodiment 1.
Control group 10：
Without expanding treatment in the auxiliary material essential oil producing process of this control group potato composite essential oil, but directly will be auxiliary Feed powder end is digested, supercritical CO2Extraction, other preparation methods are identical with embodiment 1.
Control group 11：
Without enzymolysis in the auxiliary material essential oil producing process of this control group potato composite essential oil, but carry out auxiliary material powder Through puffing, supercritical CO2Extraction, other preparation methods are identical with embodiment 1.
Control group 12：
Only pass through supercritical CO in the auxiliary material essential oil producing process of this control group potato composite essential oil2Extraction, other systems Preparation Method is identical with embodiment 1.
Test experiments 1：
Measure in embodiment 1-3 and control group 1-12, the yield of the potato composite essential oil of preparation, Vitamin C content with And DPPH radical scavenging activities, concrete condition are shown in Table 1：
Table 1
Group Refined oil rate (%) Vitamin C content (%) DPPH free radical scavenging activities (%)
Embodiment 1 78.36 18.22 87.36
Embodiment 2 79.32 17.36 88.94
Embodiment 3 76.35 17.31 90.16
Control group 1 76.52 0.22 61.03
Control group 2 77.48 12.36 38.26
Control group 3 74.51 13.02 72.36
Control group 4 75.26 12.03 71.02
Control group 5 76.11 13.21 73.06
Control group 6 75.03 12.02 68.26
Control group 7 51.02 8.36 45.61
Control group 8 53.21 6.32 38.56
Control group 9 55.31 7.25 36.14
Control group 10 47.26 17.03 46.98
Control group 11 41.06 17.22 37.68
Control group 12 50.44 17.30 34.16
As seen from the above table, the refined oil rate of embodiment 1-3 is suitable with control group 1-6 higher than control group 7-12, illustrates this Shen Please puffing, biological enzymolysis, supercritical CO in method of extraction of essential oil2Extraction phase combination can effectively improve refined oil rate：Embodiment 1-3 In ascorbic content apparently higher than control group 1, illustrate to contain more rich vitamin C component in potato essential oil；Embodiment The Vitamin C content of 1-3 apparently higher than control group 7-9 and control group 10-12, illustrate in potato method of extraction of essential oil it is puffing, Biological enzymolysis, supercritical CO2Extraction phase combination can effectively improve Vitamin C content；The DPPH free radical scavenging activities of embodiment 1-3 Apparently higher than control group 1-12, illustrate that the essential oil of the application and method of extraction of essential oil can effectively remove the raising of DPPH free radicals The antioxygen rate of essential oil.
Test experiments 2：
Measure in embodiment 1 and control group 1-12, the oily substance component content of potato composite essential oil, concrete condition is shown in Table 2：
Table 2
Group Terpenoid (%) Ketone compounds (%) Ester type compound (%) Hydrocarbon compound (%) Oxygenatedchemicals (%)
Embodiment 1 16.25 9.36 54.36 11.06 8.97
Control group 1 17.26 11.36 48.36 13.25 9.77
Control group 2 19.40 46.35 13.25 12.36 8.64
Control group 3 23.02 16.25 47.15 8.25 5.33
Control group 4 21.25 17.26 46.29 5.36 9.84
Control group 5 26.35 17.06 45.98 9.36 1.25
Control group 6 24.25 16.34 46.09 10.03 3.29
Control group 7 26.35 16.97 31.02 8.64 17.02
Control group 8 24.19 17.36 33.06 9.13 16.26
Control group 9 23.14 17.09 31.02 11.31 17.44
Control group 10 26.35 16.88 32.54 9.26 14.97
Control group 11 28.35 16.46 17.25 23.25 14.69
Control group 12 30.25 14.28 13.25 24.26 17.96
As seen from the above table, the ester type compound component of embodiment 1 is above control group 1-12, and ketone compounds component is low In control group 1-12, illustrate, the ester-containing amount of potato essential oil of the application is high, and amount containing ketone is low, illustrates the potato essential oil of the application Its fragrance does not have other control groups to be pungent.
(2) steam eye patch characteristic test is tested：
Steam eye patch is prepared according to following test group, and is tested, the collocation method of test group steam eye patch is as follows：
Test group 1：Steam eye patch is produced according to the method for embodiment 1；
Test group 2：Steam eye patch is configured according to following component, the steam eye patch of this test group is by hot radical material and essential oil material Material composition is 10 according to mass ratio:1 composition, the wherein component of hot radical material are consistent with embodiment 1, and essential oil material is by following weight The component composition of part：50 parts of potato composite essential oils (the potato composite essential oil of this test group is free of auxiliary material derived essential oil, only by Potato essential oil form), 12 parts of osmanthus essential oils, 9 parts of apple essential oils, 10 parts of mint extracts, 21 parts of Fructus Hordei Germinatus essential oils, 7 parts of olives Olive oil, 16 parts of fatty acid glycerides and 13 parts of water.Other preparation methods and embodiment 1 are completely the same.
Test group 3：Steam eye patch is configured according to following component, the steam eye patch of this test group is by hot radical material and essential oil material Material composition is 10 according to mass ratio:1 composition, the wherein component of hot radical material are consistent with embodiment 1, and essential oil material is by following weight The component composition of part：12 parts of osmanthus essential oils, 9 parts of apple essential oils, 10 parts of mint extracts, 21 parts of Fructus Hordei Germinatus essential oils, 7 portions of olives Oil, 16 parts of fatty acid glycerides and 13 parts of water.Other preparation methods and embodiment 1 are completely the same.
Test group 4：Steam eye patch is configured according to following component, the steam eye patch of this test group is by hot radical material and essential oil material Material composition is 10 according to mass ratio:1 composition, the wherein component of hot radical material are consistent with embodiment 1, and essential oil material is by following weight The component composition of part：50 parts of potato composite essential oils, 9 parts of apple essential oils, 10 parts of mint extracts, 21 parts of Fructus Hordei Germinatus essential oils, 7 parts Olive oil, 16 parts of fatty acid glycerides and 13 parts of water.Other preparation methods and embodiment 1 are completely the same.
Test group 5：Steam eye patch is configured according to following component, the steam eye patch of this test group is by hot radical material and essential oil material Material composition is 10 according to mass ratio:1 composition, the wherein component of hot radical material are consistent with embodiment 1, and essential oil material is by following weight The component composition of part：50 parts of potato composite essential oils, 12 parts of osmanthus essential oils, 10 parts of mint extracts, 21 parts of Fructus Hordei Germinatus essential oils, 7 Part olive oil, 16 parts of fatty acid glycerides and 13 parts of water.Other preparation methods and embodiment 1 are completely the same.
Test group 6：Steam eye patch is configured according to following component, the steam eye patch of this test group is by hot radical material and essential oil material Material composition is 10 according to mass ratio:1 composition, the wherein component of hot radical material are consistent with embodiment 1, and essential oil material is by following weight The component composition of part：50 parts of potato composite essential oils, 12 parts of osmanthus essential oils, 9 parts of apple essential oils, 21 parts of Fructus Hordei Germinatus essential oils, 7 parts of olives Olive oil, 16 parts of fatty acid glycerides and 13 parts of water.Other preparation methods and embodiment 1 are completely the same.
Test group 7：Steam eye patch is configured according to following component：Steam eye patch is configured according to following component, this test group It is 10 that steam eye patch is made of according to mass ratio hot radical material and essential oil material:1 composition, the wherein component of hot radical material and implementation Example 1 is consistent, and essential oil material comprises the following components in parts by weight：50 parts of potato composite essential oils, 12 parts of osmanthus essential oils, 9 parts of apples Fruit essential oil, 10 parts of mint extracts, 7 parts of olive oil, 16 parts of fatty acid glycerides and 13 parts of water.Other preparation methods and embodiment 1 is completely the same.
Test group 8：Steam eye patch is configured according to following component：Steam eye patch is configured according to following component, this test group It is 10 that steam eye patch is made of according to mass ratio hot radical material and essential oil material:1 composition, the wherein component of hot radical material and implementation Example 1 is consistent, and essential oil material comprises the following components in parts by weight：50 parts of potato composite essential oils, 12 parts of osmanthus essential oils, 9 parts of apples Fruit essential oil, 10 parts of mint extracts, 21 parts of Fructus Hordei Germinatus essential oils, 7 parts of olive oil and 13 parts of water.Other preparation methods and embodiment 1 It is completely the same.
Test group 9：Steam eye patch is configured according to following component, hot radical material, which is used only, in the steam eye patch of this test group does not make With essential oil material.Other preparation methods and embodiment 1 are completely the same.
Control group：Without using any hot radical material and essential oil material, only it is applicable in hermetically sealable film, ventilated membrane, sterile-cloth and carries out Cut, suture.
Loose pressure measure of merit, evaluation：
Test site：Liuzhou senior middle school
Experimental subjects：Liuzhou high school student totally 100 people, and student is divided into 10 groups, every group of 10 people, the age is 16-18 Sui, Average age 17.5 years old；
Experiment content：In just common eye 40min, i.e., same set of paper is made to student in 40min, is terminated after 40min Paper test, wears the test group 1-9 of the application and the eyeshade 10min of control group to student again afterwards；After removing eyeshade, continue Keep quite 5min, is then used using infra red thermograph test 40min at the moment, after 40min eyes, after wearing eyeshade 10min The average face surface temperature of each tester；And wear the forward and backward average pulse of eyeshade.Specifically it is shown in Table 3：
Table 3
As seen from the above table, test group 1-9 and control group 40min the forward and backward facial temperature change of paper pressure test with And average pulse is not much different, it was demonstrated that after the paper Pressure stimulation of 40min is carried out, the student of test group 1-9 and control group is It is obvious to be in nervous, excitatory state, and after wearing the eyeshade 10min of test group 1-9 and control group, the facial temperature of test group 1, Average pulse is significantly lower than test group 2-9 and control group, and in test group 2-9 and control group test group 9, control group cooling Speed, pulse decrease speed are least obvious, illustrate, the eyeshade of the application can make one effectively to discharge pressure, make one to loosen, Er Qieqi To loosen effect be the application derived essential oil, it is and indispensable.
Pseudo-myopia curative effect is tested：
Test site：Liuzhou People's Hospital ophthalmology
Experimental subjects：Totally 100 people, myopia degree are 200 degree to Liuzhou People's Hospital ophthalmology pseudo-myopia patient, and will be suffered from Person is divided into 4 groups, and every group of 20 people, the age is 15-17 Sui, average age 16.5 years old；
Experiment content：Daily after just common eye 4h, the eyeshade of the test group 1-3 of the application, test group 9 and control group is used 30min；Use 2 times daily, 30d is used continuously, test 50 degree of eyesight lifting, 100 degree of lifting, 150 degree of lifting, lifting after 30d 200 degree of number.Specifically it is shown in Table 4：
Table 4
Group Lifted 50 degree (people) Lifted 100 degree (people) Lifted 150 degree (people) Lifted 200 degree (people) Unchanged (people)
Test group 1 10 5 3 1 1
Test group 2 9 4 0 0 7
Test group 3 8 3 0 0 9
Test group 9 0 0 0 0 20
Control group 0 0 0 0 20
As seen from the above table, the eyeshade of test group 1 can improve the eyesight of pseudo-myopia patient after long-term use, play lifting The effect of eyesight, and the effect that test group 2-3 improves pseudo-myopia patient's vision does not have test group 1 greatly, test group 9 and control group Not having improves the effect of pseudo-myopia patient's vision, illustrates, the eyeshade of the application can make one to be effectively improved pseudo-myopia, and What is played a role is the derived essential oil of the application, and indispensable.
In conclusion refined oil rate, raising essence can be effectively improved by preparing potato composite essential oil using the method for the present invention Oily oxidation resistance, and its fragrance is more comfortable；Meanwhile it can reach using the application steam eye patch and make one effectively to loosen, release Power is bled off pressure, improves eyesight, lifts the purpose of pseudo-myopia patient's vision.
Embodiment described above only expresses the several embodiments of the present invention, its description is more specific and detailed, but simultaneously Therefore limitation of the scope of the invention cannot be interpreted as.It should be pointed out that for those of ordinary skill in the art, Without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to the protection model of the present invention Enclose.Therefore, protection scope of the present invention should be determined by the appended claims.

Claims (9)

1. a kind of steam eye patch, it is characterised in that the steam eye patch is made of according to mass ratio hot radical material and essential oil material For 10-15:1 composition.
2. steam eye patch according to claim 1, it is characterised in that the hot radical material is by following parts by weight into packet Into：17 parts of -28 parts of bamboo charcoals, 12 parts of -24 parts of iron powders, 10 parts of -16 parts of water-absorbing resins, 4 parts of -8 parts of NaHCO3, 16 parts of -24 parts of vermiculites, 13 parts of -27 parts of wormwoods, 17 parts of -29 parts of green tea slags and 13 parts -17 parts of water.
3. steam eye patch according to claim 1, it is characterised in that the essential oil material is by following parts by weight into packet Into：50 parts of -60 parts of potato composite essential oils, 12 parts of -17 parts of osmanthus essential oils, 9 parts of -17 parts of apple essential oils, 10 parts of -21 parts of peppermints carry Take thing, 21 parts of -32 parts of Fructus Hordei Germinatus essential oils, 7 parts of -15 parts of olive oil, 16 parts of -27 parts of fatty acid glycerides and 13 parts of -23 parts of water.
4. steam eye patch according to claim 3, it is characterised in that the potato composite essential oil is by percentage by weight The auxiliary material essential oil that the potato essential oil and percentage by weight of 70%-90% is 10%-30% forms.
5. steam eye patch according to claim 4, it is characterised in that the potato essential oil is made by potato；It is described Auxiliary material essential oil is made by the component of following parts by weight：17 parts -29 parts of Chinese toon wood skin, 13 parts -31 parts of Radix agastaches, 24 parts -32 parts Semen sesami nigrum and 34 parts -46 parts of the leaf of bamboo.
6. steam eye patch according to claim 4, it is characterised in that the potato composite essential oil preparation method includes horse Bell potato extraction of essential oil, auxiliary material extraction of essential oil and essential oil mix three steps and are made.
7. steam eye patch according to claim 6, it is characterised in that the potato extraction of essential oil is swollen by potato Change, cellulase treatment, microwave treatment and supercritical CO2Four steps of extraction obtain；The biology enzyme I that the cellulase treatment uses Solution is made of the raw material of following parts by weight：30 parts -35 parts of amylase, 20 parts -25 parts of carbohydrase, 5 parts -10 parts of meter Qu The sodium hydroxide solution that mould, 10 parts -20 parts of barbaloin and 250 parts of -300 parts of mass percents are 1%；The enzyme of the amylase Vigor is 800u/g-1000u/g；The enzyme activity of the carbohydrase is 1000u/g-1200u/g；Effective viable bacteria of the aspergillus oryzae Number is 3.1 × 107~6.7 × 107CFU/g。
8. steam eye patch according to claim 6, it is characterised in that the auxiliary material extraction of essential oil is puffing, raw by auxiliary material Thing enzymatic treatment and supercritical CO2Four steps of extraction obtain；The biology enzyme II solution that the cellulase treatment uses by weighing as follows The raw material of amount part is made：15 parts -25 parts of pectase, 30 parts -50 parts of cellulase, 20 parts -30 parts of amylase, 10 parts - The sodium chloride solution that 20 parts of aspergillus flavus and 300 parts of -350 parts of mass percents are 2%；The enzyme activity of the pectase is 1200u/g-1500u/g；The enzyme activity of the cellulase is 1500u/g-2000u/g；The enzyme activity of the amylase is 900u/g-1200u/g；The living bacteria count of the aspergillus flavus is 3.9 × 108~6.7 × 108CFU/g。
A kind of 9. preparation method for preparing any one steam eye patch as described in claim 1-8, it is characterised in that the method Include the following steps：
(1) each material composition is weighed by the parts by weight；
(2) potato composite essential oil, osmanthus essential oil, apple essential oil and Fructus Hordei Germinatus essential oil are mixed, and is put into mixer and stirs Blend of essential oils is made, the mixing time is 25min-35min；Speed of agitator is 100r/min-300r/min；Then by essence Oil mixture is put into temperature to be freezed in -5 DEG C~0 DEG C refrigerator-freezer, and cooling time obtains freezing essential oil for 2h-4h；
(3) the obtained freezing essential oil of step (2) is placed on and thawed under room temperature, until temperature is 10 DEG C~15 DEG C, Ran Houzai Fatty acid glyceride, water and olive oil is added into blend of essential oils to be stirred to obtain essential oil emulsion with high speed dispersor, it is described Mixing time is 15min-20min, speed of agitator 400r/min-600r/min；
(4) by NaHCO3It is put into water and obtains salting liquid；The whole strain of wormwood is dried, until moisture content is 3%, then carries out powder It is broken, select to obtain wormwood powder by 60 mesh sieve mesh screens；Green tea slag is dried, until moisture content is 3%, then carries out powder It is broken, select to obtain green tea ground-slag end by 60 mesh sieve mesh screens；Bamboo charcoal, wormwood powder, green tea ground-slag end and water-absorbing resin are poured into and stirred Mix in machine rotating speed be 100r/min-300r/min under conditions of stirring 5min-10min obtain solid mixt；By salting liquid Pour into above-mentioned solid mixt, stirring 1min-3min obtains liquid under conditions of rotating speed is 200r/min-400r/min Mixture, then again adds iron powder in liquefied mixture, is stirred under conditions of rotating speed is 100r/min-200r/min Hot radical material is made by vibrating screen screening, sealing, cooling again after 2min-5min；
(5) hermetically sealable film, ventilated membrane, sterile-cloth is taken to carry out corresponding to cutting, from outside to inside according to hermetically sealable film, ventilated membrane, sterile The order of cloth is arranged, and under vacuum, to filling hot radical material between hermetically sealable film and ventilated membrane, in ventilated membrane and Even spread essential oil emulsion between sterile-cloth, and hermetically sealable film, ventilated membrane and sterile-cloth overlapping edge portions are sutured , obtain the steam eye patch.
CN201711336060.0A 2017-12-14 2017-12-14 A kind of steam eye patch and preparation method thereof Pending CN107951619A (en)

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Application publication date: 20180424