CN107929791A - diaper and preparation method thereof - Google Patents

diaper and preparation method thereof Download PDF

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Publication number
CN107929791A
CN107929791A CN201711248102.5A CN201711248102A CN107929791A CN 107929791 A CN107929791 A CN 107929791A CN 201711248102 A CN201711248102 A CN 201711248102A CN 107929791 A CN107929791 A CN 107929791A
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CN
China
Prior art keywords
parts
diaper
antiseptic
synergist
nano
Prior art date
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Pending
Application number
CN201711248102.5A
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Chinese (zh)
Inventor
林少洪
孙建松
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Dongguan Aiyi Pure Biological Technology Co Ltd
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Dongguan Aiyi Pure Biological Technology Co Ltd
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Priority to CN201711248102.5A priority Critical patent/CN107929791A/en
Publication of CN107929791A publication Critical patent/CN107929791A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L15/00Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
    • A61L15/16Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
    • A61L15/22Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons containing macromolecular materials
    • A61L15/28Polysaccharides or their derivatives
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L15/00Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
    • A61L15/16Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
    • A61L15/18Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons containing inorganic materials
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L15/00Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
    • A61L15/16Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
    • A61L15/20Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons containing organic materials
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L15/00Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
    • A61L15/16Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
    • A61L15/42Use of materials characterised by their function or physical properties
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L15/00Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
    • A61L15/16Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
    • A61L15/42Use of materials characterised by their function or physical properties
    • A61L15/44Medicaments
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L15/00Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
    • A61L15/16Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
    • A61L15/42Use of materials characterised by their function or physical properties
    • A61L15/46Deodorants or malodour counteractants, e.g. to inhibit the formation of ammonia or bacteria
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2300/00Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
    • A61L2300/10Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices containing or releasing inorganic materials
    • A61L2300/102Metals or metal compounds, e.g. salts such as bicarbonates, carbonates, oxides, zeolites, silicates
    • A61L2300/104Silver, e.g. silver sulfadiazine
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2300/00Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
    • A61L2300/40Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices characterised by a specific therapeutic activity or mode of action
    • A61L2300/404Biocides, antimicrobial agents, antiseptic agents

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  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Epidemiology (AREA)
  • Hematology (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Inorganic Chemistry (AREA)
  • Absorbent Articles And Supports Therefor (AREA)

Abstract

The invention discloses a kind of diaper and preparation method thereof, the diaper includes top layer, and the top layer is sprayed with antiseptic, and the antiseptic is made of the raw material of following weight parts:0.5 1.5 parts of decanoin, 0.5 3.5 parts of sodium carboxymethylcellulose, 0.05 0.5 parts of nano-silver water solution, 0.1 0.5 parts of surfactant, 0.1 0.5 parts of synergist, 95 105 parts of water.Diaper of the present invention, by after skin-material adds antiseptic, having high-efficiency antimicrobial, ventilative comfortably thermal diffusivity is good, non-stimulated to skin, the effect of can playing cleaning, deodorization, disinfection and sterilize.

Description

Diaper and preparation method thereof
Technical field
The present invention relates to a kind of amenities, and in particular to a kind of diaper and preparation method thereof.
Background technology
Disposable sanitary articles are also referred to as the disposable product of absorbability, including sanltary towel, panty liner, tampon, baby Youngster's paper nappy, adult diapers and other adult-incontinence articles, pet pads etc..During disposable sanitary articles use, product Mostly with user's direct skin contact, therefore, except should possess in itself to product health, in addition to security feature, should also be most Reduce to limits due to contact skin and cause the discomfort of user.In particular it is necessary to there is ventilative, smooth, quick suction Wet, moisture-inhibiting, anti-down fluidity and skin contact comfort.Skin contact comfort, also known as skin-friendly, refer to clothes with human body To the tactile comfort of fabric during skin contact.
The surface layer of diaper requires flexible, breathable, can keep the dry-ness of skin.In the market is generally using hot wind, hot rolling Non-woven material.But with the development in market, consumer to functional surface layer demand such as diaper antibacterial, comfortable also by Step rises.
The content of the invention
The technical problem to be solved in the present invention is to provide a kind of diaper and preparation method thereof.
To solve the above problems, the present invention adopts the following technical scheme that:
A kind of diaper, including top layer, the top layer are sprayed with antiseptic, the antiseptic by following weight parts original Material composition:0.5-1.5 parts of decanoin, 0.5-3.5 parts of sodium carboxymethylcellulose, 0.05-0.5 parts of nano-silver water solution, 0.1-0.5 parts of surfactant, 0.1-0.5 parts of synergist, 95-105 parts of water.
Preferably, the synergist is mixtures one or more in citric acid, cinnamic acid, salicylic acid.
It is highly preferred that the synergist is mixed by citric acid, cinnamic acid, salicylic acid, the citric acid, Chinese cassia tree Sour, salicylic mass ratio is (1-3):(1-3):(1-3).
Preferably, the surfactant is Dodecyl Polyglucosides, Plantacare 818, n- octyl group-β-D- pyrans Portugal One or more mixture in polyglycoside.
It is highly preferred that the surfactant is by Dodecyl Polyglucosides, Plantacare 818, n- octyl group-β-D- pyrans Glucoside mixes, the Dodecyl Polyglucosides, Plantacare 818, the quality of n- octyl group-β-D- glucopyranosides Than for (1-3):(1-3):(1-3).
Preferably, the mass concentration of nano silver is 80-120 μ g/mL in the nano-silver water solution, is prepared by following methods Form:Silver nitrate solid is dissolved in the water, preparation obtains solution A;Sodium cellulose glycolate and sodium carboxymethylcellulose is molten In Xie Yushui, preparation obtains solution B;Take 0.05-0.2mL solution As to be mixed with 15-25mL solution Bs, control its pH value 7-11 it Between, when reaction 3-18 is small at 20-80 DEG C, obtain the nano-silver water solution.
Preferably, the fountain height of antiseptic is 100-500g/m in the top layer2
Preferably, the material on the top layer is cotton.
Preferably, the diaper can be to be obtained in the commercially available baby paper diaper top layer sprinkling antiseptic, The commercially available baby paper diaper is as helped precious suitable paper diaper, cotton epoch paper diaper, shellfish shellfish bear paper diaper.
Present invention also offers the preparation method of above-mentioned diaper, and antiseptic is uniformly sprayed at paper diaper surface layer to obtain the final product.
Specifically, in the present invention:
Decanoin, No. CAS:621-71-6.
Sodium carboxymethylcellulose, No. CAS:9004-32-4.
Citric acid, No. CAS:77-92-9.
Cinnamic acid, No. CAS:621-82-9.
Salicylic acid, No. CAS:69-72-7.
Dodecyl Polyglucosides, No. CAS:110615-47-9.
Plantacare 818, No. CAS:68515-73-1.
N- octyl group-β-D- glucopyranosides, No. CAS:29836-26-8.
Diaper of the present invention, by after skin-material adds antiseptic, having high-efficiency antimicrobial, ventilative comfortable, thermal diffusivity It is good, it is non-stimulated to skin, the effect of cleaning, deodorization, disinfection can be played and sterilized.
Embodiment
Here is that the preferred embodiment of the present invention is described in detail, so that advantages and features of the invention can be easier to It is readily appreciated by one skilled in the art, so as to make a clearer definition of the protection scope of the present invention.
Embodiment 1
Antiseptic raw material (parts by weight):0.9 part of decanoin, 2 parts of sodium carboxymethylcellulose, nano-silver water solution 0.25 part, 0.3 part of surfactant, 0.3 part of synergist, 100 parts of deionized water.
The synergist is by citric acid, cinnamic acid, salicylic acid in mass ratio 1:1:1 is uniformly mixed to obtain.
The surfactant is pressed by Dodecyl Polyglucosides, Plantacare 818, n- octyl group-β-D- glucopyranosides Mass ratio 1:1:1 is uniformly mixed to obtain.
It is prepared by nano-silver water solution:0.32g silver nitrates are added in 10mL deionized waters solution A is made;By 0.005g Sodium carboxymethylcellulose and 0.005g sodium cellulose glycolates be added in 20mL deionized waters, rotating speed 200r/min stirring 30min dissolves, and adjusts pH value 8, solution B is made;Take solution A 0.1mL to be added in solution B, be placed in water-bath and be heated to 60 ℃;After when stirring reaction 4 is small, nano-silver water solution is obtained, obtained nano-Ag particles average grain diameter is less than 100 nanometers, nanometer The mass concentration of nano silver is 101 μ g/mL in silver-colored aqueous solution.
Decanoin, sodium carboxymethylcellulose, nano-silver water solution, surfactant, synergist are added successively It is uniformly mixed in deionized water, obtains antiseptic.Above-mentioned antiseptic is sprayed to paper diaper (is had using Shenzhen cotton Time Technology The Serial No. 800-001553 of limit company offer, the cotton urine pants that specification is S52 pieces) top layer, antiseptic fountain height is 200g/ m2, obtain the diaper of embodiment 1.
Embodiment 2
It is substantially the same manner as Example 1, differ only in:The synergist is by cinnamic acid, salicylic acid in mass ratio 1:1 It is uniformly mixed to obtain.
Embodiment 3
It is substantially the same manner as Example 1, differ only in:The synergist is by citric acid, salicylic acid in mass ratio 1:1 It is uniformly mixed to obtain.
Embodiment 4
It is substantially the same manner as Example 1, differ only in:The synergist is by citric acid, cinnamic acid in mass ratio 1:1 It is uniformly mixed to obtain.
Embodiment 5
It is substantially the same manner as Example 1, differ only in:The surfactant by Plantacare 818, n- octyl groups-β- D- glucopyranosides in mass ratio 1:1 is uniformly mixed to obtain.
Embodiment 6
It is substantially the same manner as Example 1, differ only in:The surfactant is pungent by Dodecyl Polyglucosides, n- Base-β-D- glucopyranosides in mass ratio 1:1 is uniformly mixed to obtain.
Embodiment 7
It is substantially the same manner as Example 1, differ only in:The surfactant is by Dodecyl Polyglucosides, decyl Glucoside in mass ratio 1:1 is uniformly mixed to obtain.
Test case 1
Reference《National Standard of the People's Republic of China GB15979-1995, Disposable Sanitary Accessory sanitary standard》, Diaper made from embodiment 1-7 is detected to the bacteriostasis property of following three kinds of microorganisms.
The microorganism tested:Escherichia coli (Escherichia coli) AS.1.90;Staphylococcus aureus (Staphylococcus aureus)AS.1.89;Candida albicans (Candida albicance) AS.2.2086.
Diaper made from embodiment 1-7 is after ultraviolet irradiation 1.5min sterilizations, in sanitary napkin top layer even spread large intestine Bacillus 1.0 × 105CFU/ pieces, staphylococcus aureus 1.0 × 105CFU/ pieces, staphylococcus aureus 1.0 × 105CFU/ pieces, Effect tests every sanitary napkin bacterial content after 30 minutes, and concrete outcome is shown in Table 1.
Table 1:Sanitary napkin bacteriostasis property result list position:CFU/ pieces
Escherichia coli Staphylococcus aureus Candida albicans
Embodiment 1 0 0 0
Embodiment 2 3.7×103 3.8×103 0.8×104
Embodiment 3 3.9×103 4.1×103 1.1×104
Embodiment 4 3.5×103 3.9×103 0.9×104
Embodiment 5 2.3×103 3.2×103 1.5×104
Embodiment 6 2.1×103 3.0×103 1.8×104
Embodiment 7 2.4×103 3.3×103 1.7×104
Comparing embodiment 1 and embodiment 2-4, embodiment 1 (citric acid, cinnamic acid, salicylic acid compounding) bacteriostasis property are obvious Better than embodiment 2-4 (any two kinds of compoundings in citric acid, cinnamic acid, salicylic acid);Comparing embodiment 1 and embodiment 5-7, implements Example 1 (Dodecyl Polyglucosides, Plantacare 818, n- octyl group-β-D- glucopyranosides compounding) bacteriostasis property is substantially better than reality Apply a 5-7 (the two any compounding in Dodecyl Polyglucosides, Plantacare 818, n- octyl group-β-D- glucopyranosides).

Claims (9)

1. a kind of diaper, including top layer, the top layer is sprayed with antiseptic, the antiseptic by following weight parts raw material Composition:0.5-1.5 parts of decanoin, 0.5-3.5 parts of sodium carboxymethylcellulose, 0.05-0.5 parts of nano-silver water solution, table Activating agent 0.1-0.5 parts of face, 0.1-0.5 parts of synergist, 95-105 parts of water.
2. diaper according to claim 1, it is characterised in that:The synergist is citric acid, cinnamic acid, salicylic acid Middle one or more mixture.
3. diaper according to claim 2, it is characterised in that:The synergist is by citric acid, cinnamic acid, salicylic acid Mix, the citric acid, cinnamic acid, salicylic mass ratio are(1-3):(1-3):(1-3).
4. diaper according to any one of claim 1-3, it is characterised in that:The surfactant is dodecane One or more mixture in base glucoside, Plantacare 818, n- octyl group-β-D- glucopyranosides.
5. diaper according to claim 4, it is characterised in that:The surfactant by Dodecyl Polyglucosides, Plantacare 818, n- octyl group-β-D- glucopyranosides mix, and the Dodecyl Polyglucosides, Plantacare 818, n- are pungent The mass ratio of base-β-D- glucopyranosides is(1-3):(1-3):(1-3).
6. according to the diaper any one of claim 1-5, it is characterised in that:The fountain height of antiseptic in the top layer For 100-500g/m2
7. according to the diaper any one of claim 1-5, it is characterised in that:Nano silver in the nano-silver water solution Mass concentration be 80-120 μ g/mL.
8. according to the diaper any one of claim 1-5, it is characterised in that:The material on the top layer is cotton.
9. according to the preparation method of diaper any one of claim 1-8, it is characterised in that:Antiseptic is uniformly sprayed To obtain the final product in paper diaper surface layer;
The antiseptic is made of the raw material of following weight parts:0.5-1.5 parts of decanoin, sodium carboxymethylcellulose 0.5- 3.5 parts, 0.05-0.5 parts of nano-silver water solution, 0.1-0.5 parts of surfactant, 0.1-0.5 parts of synergist, 95-105 parts of water.
CN201711248102.5A 2017-12-01 2017-12-01 diaper and preparation method thereof Pending CN107929791A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116785396A (en) * 2023-05-19 2023-09-22 云南清逸堂实业有限公司 Sanitary towel thermo-sensitive preparation for relieving dysmenorrhea

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2774443Y (en) * 2005-03-29 2006-04-26 程志新 Santiary protective pad of fragrance agents
US20140213764A1 (en) * 2012-06-08 2014-07-31 U.S. Army Research Laboratory Attn: Rdrl-Loc-I Nanocellulose foam containing active ingredients
CN105288713A (en) * 2015-11-12 2016-02-03 上海韬鸿化工科技有限公司 Bacteriostasis sanitary napkin
CN107233606A (en) * 2017-05-31 2017-10-10 苏州蔻美新材料有限公司 A kind of degerming panty liner of skin care

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2774443Y (en) * 2005-03-29 2006-04-26 程志新 Santiary protective pad of fragrance agents
US20140213764A1 (en) * 2012-06-08 2014-07-31 U.S. Army Research Laboratory Attn: Rdrl-Loc-I Nanocellulose foam containing active ingredients
CN105288713A (en) * 2015-11-12 2016-02-03 上海韬鸿化工科技有限公司 Bacteriostasis sanitary napkin
CN107233606A (en) * 2017-05-31 2017-10-10 苏州蔻美新材料有限公司 A kind of degerming panty liner of skin care

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116785396A (en) * 2023-05-19 2023-09-22 云南清逸堂实业有限公司 Sanitary towel thermo-sensitive preparation for relieving dysmenorrhea

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