CN103006923B - Chinese medicinal liquid band-aid and preparation method - Google Patents
Chinese medicinal liquid band-aid and preparation method Download PDFInfo
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- CN103006923B CN103006923B CN201210573882.1A CN201210573882A CN103006923B CN 103006923 B CN103006923 B CN 103006923B CN 201210573882 A CN201210573882 A CN 201210573882A CN 103006923 B CN103006923 B CN 103006923B
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Abstract
The invention discloses a Chinese medicinal liquid band-aid, and belongs to the technical field of medical care. The band-aid is characterized by comprising the following components in parts by weight: 1 to 15 parts of clover extract, 1 to 10 parts of chitosan, 1 to 25 parts of ethanol, 0.5 to 2 parts of glycerol, 0.5 to 3 parts of hydrogen peroxide, 0.5 to 5 parts of menthol, 1 to 30 purified water, and pharmaceutical grade azone accounting for 0.02 to 2.0 percent of the total amount. The Chinese medicinal liquid band-aid is convenient and easy to use, is not limited by wounds or positions, can be quickly formed into a film after being applied, can be easily permeated and absorbed, has small stimulation to skin of a human body, does not have allergic reaction and drug resistance, and can be used for promoting muscle tissue repair and regeneration and protecting and promoting wound healing to shorten the healing time and effectively solve the problems of wound infection and the like; and the main components of antibacterial and film forming materials of the band-aid are easily degradable and easily absorbable biomaterials, have excellent biocompatibility, can be automatically degraded, and is safe and environment-friendly.
Description
Technical field
The invention belongs to field of medical technology, be specifically related to a kind of Chinese medicinal liquor adhesive bandage and preparation method.
Background technology
Radix Apioris Fortunei (Radix Lespedezae Buergeri)
tetrastigma hemsleyanum,sweet in the mouth, cool in nature, is vitaceae, has another name called gold thread hoist, stone mouse, Radix Tetrastigmatis Hemsleyani, silk thread and hangs Jin Zhong.Radix Apioris Fortunei (Radix Lespedezae Buergeri) extract mainly contains flavonoid and flavonoid glycoside, polysaccharide, steroid, cupreol, the ingredients such as kaempferol, triterpenes, alkaloid, there is very strong promotion leukocyte and gulp down the function of having a liking for antibacterial, there are the effects such as refreshing and detoxicating, dispelling pathogenic wind and eliminating phlegm, antiviral, raising immunity, clinical in diseases such as upper respiratory tract infection, infantile pneumonia, hyperpyrexia convulsion, stomatitis, sore swollen toxin, venoms, be used in the recent period prevention and adjuvant therapy of tumors, hepatitis etc., there is clinical application widely.
Radix Apioris Fortunei (Radix Lespedezae Buergeri) is enjoyed the good reputation of bouvardin, and China's application Radix Apioris Fortunei (Radix Lespedezae Buergeri) among the people is treated the with a long history of disease, and the underground avette tuber of fresh Radix Apioris Fortunei (Radix Lespedezae Buergeri) is mashed external application, is used for the treatment of wound and innominate toxic swelling; Levigation after fresh Radix Apioris Fortunei (Radix Lespedezae Buergeri) tuber lyophilisation, is used for wound, gets appropriate Radix Apioris Fortunei (Radix Lespedezae Buergeri) dry powder and is spread on affected part, additional wrapping, can hemostasis and anti-inflammation, b referred to as a kind of pure natural adhesive bandage, but have the following disadvantages: preserve and use inconvenience, medicated powder is easily scattered and wastes valuable ingredient of Chinese medicine; Cannot apply ointment or plaster to the wound of privileged sites; Wound can not separate completely with the external world, easily causes wound to infect because antibacterial, dust or water immerse.
Summary of the invention
The object of this invention is to provide a kind of Chinese medicinal liquor adhesive bandage and preparation method that Radix Apioris Fortunei (Radix Lespedezae Buergeri) is raw material of utilizing.
Described a kind of Chinese medicinal liquor adhesive bandage, is characterized in that containing following component and ratio of weight and number thereof:
Radix Apioris Fortunei (Radix Lespedezae Buergeri) extract 1-15
Chitosan 1-10
Ethanol 1-25
Glycerol 0.5-2
Hydrogen peroxide 0.5-3
Mentholum 0.5-5
Purified water 1-30
The 0.02-2.0% of pharmaceutical grade azone total amount.
Described a kind of Chinese medicinal liquor adhesive bandage, is characterized in that containing following component and ratio of weight and number thereof, makes smear type Chinese medicinal liquor adhesive bandage:
Radix Apioris Fortunei (Radix Lespedezae Buergeri) extract 3-10
Chitosan 1.5
Ethanol 25
Glycerol 1
Hydrogen peroxide 0.5
Mentholum 4
Purified water 6
0.5% of pharmaceutical grade azone total amount.
Described a kind of Chinese medicinal liquor adhesive bandage, is characterized in that containing following component and ratio of weight and number, makes aerosol type Chinese medicinal liquor adhesive bandage:
Radix Apioris Fortunei (Radix Lespedezae Buergeri) extract 1-3
Chitosan 1.5
Ethanol 10
Glycerol 0.5
Hydrogen peroxide 0.5
Mentholum 3
Purified water 30
0.5% of pharmaceutical grade azone total amount.
Described a kind of Chinese medicinal liquor adhesive bandage, is characterized in that described Radix Apioris Fortunei (Radix Lespedezae Buergeri) extract adopts following methods preparation:
1) after the washing of Radix Apioris Fortunei (Radix Lespedezae Buergeri) tuber, soak 3～5 minutes with Eusol, then drench Xian with drinking water clean, dry;
2) by the Radix Apioris Fortunei (Radix Lespedezae Buergeri) tuber crushing and beating of drying, serosity is put into microwave extracting tank, adds the purified water of equivalent to stir, and opens the extraction of microwave extracting tank and within 3-5 minute, filters to obtain extract;
3) extract is heated to 38-42 ℃, processes 6～8 hours by α-amylase, completely the starch in enzymolysis solution obtains solution after enzymolysis;
4) by solution after enzymolysis through macroporous resin adsorption, use 50% ethanol elution, after eluent filters, be drying to obtain three Folium Isatidis extract dry powder with pressure type atomizing dryer, it is 5000kpa that atomization drying temperature is controlled at 45-50 ℃, atomizing pressure.
Described a kind of Chinese medicinal liquor adhesive bandage, is characterized in that described ethanol is anhydrous alcohol for medical use or 95% ethanol.
Described a kind of Chinese medicinal liquor adhesive bandage, is characterized in that also containing the EGCG of 1-3 weight portion.
Described a kind of Chinese medicinal liquor adhesive bandage, is characterized in that also containing the EGCG of 2 weight portions.
The preparation method of described a kind of Chinese medicinal liquor adhesive bandage, is characterized in that comprising the following steps:
1) press recipe quantity and prepare raw material, purified water is poured in preparation pot and is heated to boiling, add chitosan to be stirred to after being cooled to 88-92 ℃ and dissolve completely, then add glycerol to be uniformly mixed, regulate pH value 3.5-5.5, continue to stir 30 minutes, obtain solution A, be cooled to room temperature for subsequent use;
2) Radix Apioris Fortunei (Radix Lespedezae Buergeri) extract is added in alcoholic solution under room temperature stirring and dissolving complete, obtain solution B;
3) solution B is joined in solution A, mix homogeneously, adds Mentholum, hydrogen peroxide, pharmaceutical grade azone while stirring, as contained EGCG in formula, adds together, is uniformly mixed, and obtains Chinese medicinal liquor adhesive bandage.
That chitosan in above-mentioned formula (D-glucosamine) has is nontoxic, biodegradable, good biocompatibility, have good antibacterial activity, also has good film property.
In above-mentioned formula, glycerol, as medicine film wetting agent, makes antibacterial film softness, is close to affected part, keeps not dry and cracked coming off; Use biology to refine glycerol except moisturizing, humectation effect, also there is the special efficacy such as high activity, antioxidation, better effects if.
In above-mentioned formula, hydrogen peroxide is porogen, and hydrogen peroxide disproportionation releasing oxygen and make antibacterial film pore ventilative adds that dismutation reaction can heat release, can accelerate antibacterial film curing rate, and hydrogen peroxide also has sterilization.
The chemical name of above-mentioned formula Chinese medicine level azone: 1-orthododecyl nitrogen heterocyclo heptane-2-ketone, it is a new and effective safety non-toxic Percutaneous absorption enhancer, can increase effective ingredient biological activity and effect, azone itself also has antiviral and bacteriostasis.
In above-mentioned formula, Mentholum Chang Zuowei odorant uses, and acts on skin or mucosa, has refrigerant itching-relieving action, produces comfort.
Radix Apioris Fortunei (Radix Lespedezae Buergeri) extract has antiinflammatory, bactericidal action, and the disinfection sanitizers such as alternative nanometer silver, povidone iodine are prepared liquid adhesive bandage.Utilize Radix Apioris Fortunei (Radix Lespedezae Buergeri) extract biological antibiotic mechanism, can isolate, pathogenic microbe killing (comprising antibacterial, fungus and virus etc.), possess the tissue repair of promotion and regeneration, protection and wound healing, shorten healing time.
The Chinese medicinal liquor adhesive bandage that above-mentioned formula is made, it can be smear type, also can be aerosol type, all take Radix Apioris Fortunei (Radix Lespedezae Buergeri) extract as main material, add Sales polysaccharide, glycerol, hydrogen peroxide, ethanol, Mentholum, purified water etc. are prepared from, it is easy to use, be not subject to the restriction of wound and lump shape and present position, energy fast filming after coating, do not affect outward appearance and not limited by the activity of health coating position, overcome the shortcoming of direct use Radix Apioris Fortunei (Radix Lespedezae Buergeri) dry powder, easily osmotic absorption, give full play to precious Chinese medicine therapeutical effect, stimulate little to human body skin, not sensitization, avirulence, can not produce drug resistance and pollution problem, can effectively protect from infection, play hemostasis, analgesia, sterilization, the effects such as detumescence and raising body's immunity.
The EGCG(epigallocatechin gallate (EGCG) adding in above-mentioned formula) be preservative, skin protectant, formula adds EGCG and can improve effect product sterilization skin-care effect.
That the present invention has is easy to use, be not subject to the restriction of wound and present position, can fast filming after coating, easily osmotic absorption, to human body skin stimulate little, without anaphylaxis and drug resistance; Promote muscular tissue reparation and regeneration, protection and wound healing, shorten healing time, effectively prevents the problems such as wound infection; Its antibacterial and main component filmogen be easily degraded, easy organism-absorbing material, and biocompatibility is good, can degrade voluntarily, and safety and environmental protection.
The specific embodiment
The present invention is described in further detail below in conjunction with embodiment.
The preparation of Radix Apioris Fortunei (Radix Lespedezae Buergeri) extract: after fresh Radix Apioris Fortunei (Radix Lespedezae Buergeri) tuber water is cleaned up, with the bleaching fluid immersion 3-5 minute of germicidal solution 0.05%, then use drinking water drip washing clean, dry; By the Radix Apioris Fortunei (Radix Lespedezae Buergeri) tuber crushing and beating of drying, serosity is put into microwave extracting tank, adds the purified water of equivalent to stir, and opens the extraction of microwave extracting tank and within 3-5 minute, filters to obtain extract, and the microwave frequency that microwave tank uses is 2450 MHz; Extract is heated to 38-42 ℃, processes 6～8 hours by α-amylase, completely the starch in enzymolysis solution obtains solution after enzymolysis, and heating is beneficial to oozing out of effective ingredient; Solution after enzymolysis, through macroporous resin adsorption, is used to 50% ethanol elution, dry under temperature 45-50 ℃, the condition of atomizing pressure 5000kpa with pressure type atomizing dryer after eluent filters, obtain three Folium Isatidis extract dry powder, for subsequent use.
Embodiment 1
Weight of material part
radix Apioris Fortunei (Radix Lespedezae Buergeri) extract 10
Chitosan 1.5
Dehydrated alcohol 25
Glycerol 1
Hydrogen peroxide 0.5
Mentholum 4
Purified water 6
0.5% of pharmaceutical grade azone total amount
Wherein the supplementary material such as chitosan, ethanol, glycerol, hydrogen peroxide, Mentholum is pharmaceutical grade, during without medicinal rank, requires to meet food grade quality standard.
Preparation method is as follows:
1) press recipe quantity and prepare raw material, purified water is poured in preparation pot and is heated to boiling, add chitosan to be stirred to after being cooled to 88-92 ℃ and dissolve completely, then add glycerol to be uniformly mixed, regulate pH value 3.5-5.5, continue to stir 30 minutes, obtain solution A, be cooled to room temperature for subsequent use;
2) Radix Apioris Fortunei (Radix Lespedezae Buergeri) extract is added in ethanol solution under room temperature stirring and dissolving complete, obtain solution B;
3) solution B is joined in solution A, mix homogeneously, adds Mentholum, hydrogen peroxide, pharmaceutical grade azone while stirring, is uniformly mixed, and obtains smear type Chinese medicinal liquor adhesive bandage.
In this formula, ethanol content is higher, and drying and forming-film speed is fast, but zest is large, is applicable to the repellent antipruritic without the various sore swollen toxins of wound.
Embodiment 2
Weight of material part
Radix Apioris Fortunei (Radix Lespedezae Buergeri) extract 3
Chitosan 1.5
95% ethanol 10
Glycerol 0.5
Hydrogen peroxide 0.5
Mentholum 3
Purified water 30
0.5% of pharmaceutical grade azone total amount
Wherein the supplementary material such as chitosan, ethanol, glycerol, hydrogen peroxide, Mentholum is pharmaceutical grade, during without medicinal rank, requires to meet food grade quality standard.
Preparation method is with reference to embodiment 1.Aerosol type Chinese medicinal liquor adhesive bandage prepared by this formula, ethanol content is low, and essentially no zest is applicable to the impaired disease of the mucosa such as anti-inflammation and sterilization and oral ulcer of wound.
Embodiment 3
Weight of material part
Radix Apioris Fortunei (Radix Lespedezae Buergeri) extract 3
Chitosan 1.5
Dehydrated alcohol 25
Glycerol 1
Hydrogen peroxide 0.5
Mentholum 4
EGCG 2
Purified water 6
0.5% of pharmaceutical grade azone total amount
Preparation method is as follows:
1) press recipe quantity and prepare raw material, purified water is poured in preparation pot and is heated to boiling, add chitosan to be stirred to after being cooled to 88-92 ℃ and dissolve completely, then add glycerol to be uniformly mixed, regulate pH value 3.5-5.5, continue to stir 30 minutes, obtain solution A, be cooled to room temperature for subsequent use;
2) Radix Apioris Fortunei (Radix Lespedezae Buergeri) extract is added in ethanol solution under room temperature stirring and dissolving complete, obtain solution B;
3) solution B is joined in solution A, mix homogeneously, adds Mentholum, hydrogen peroxide, EGCG, pharmaceutical grade azone while stirring, is uniformly mixed, and obtains smear type Chinese medicinal liquor adhesive bandage.
Embodiment 4
Weight of material part
Radix Apioris Fortunei (Radix Lespedezae Buergeri) extract 1
Chitosan 1.5
95% ethanol 10
Glycerol 0.5
Hydrogen peroxide 0.5
Mentholum 3
EGCG 2
Purified water 30
0.5% of pharmaceutical grade azone total amount
Preparation method, with reference to embodiment 3, can prepare aerosol type Chinese medicinal liquor adhesive bandage.
Claims (7)
1. a Chinese medicinal liquor adhesive bandage, is characterized in that containing following component and ratio of weight and number thereof:
Radix Apioris Fortunei (Radix Lespedezae Buergeri) extract 1-15
Chitosan 1-10
Ethanol 1-25
Glycerol 0.5-2
Hydrogen peroxide 0.5-3
Mentholum 0.5-5
Purified water 1-30
The 0.02-2.0% of pharmaceutical grade azone total amount
Described Radix Apioris Fortunei (Radix Lespedezae Buergeri) extract adopts following methods preparation:
1) after the washing of Radix Apioris Fortunei (Radix Lespedezae Buergeri) tuber, soak 3～5 minutes with Eusol, then drench Xian with drinking water clean, dry;
2) by the Radix Apioris Fortunei (Radix Lespedezae Buergeri) tuber crushing and beating of drying, serosity is put into microwave extracting tank, adds the purified water of equivalent to stir, and opens the extraction of microwave extracting tank and within 3-5 minute, filters to obtain extract;
3) extract is heated to 38-42 ℃, processes 6～8 hours by α-amylase, completely the starch in enzymolysis solution obtains solution after enzymolysis;
4) by solution after enzymolysis through macroporous resin adsorption, use 50% ethanol elution, after eluent filters, be drying to obtain three Folium Isatidis extract dry powder with pressure type atomizing dryer, it is 5000kpa that atomization drying temperature is controlled at 45-50 ℃, atomizing pressure.
2. a kind of Chinese medicinal liquor adhesive bandage as claimed in claim 1, is characterized in that containing following component and ratio of weight and number thereof, makes smear type Chinese medicinal liquor adhesive bandage:
Radix Apioris Fortunei (Radix Lespedezae Buergeri) extract 3-10
Chitosan 1.5
Ethanol 25
Glycerol 1
Hydrogen peroxide 0.5
Mentholum 4
Purified water 6
0.5% of pharmaceutical grade azone total amount.
3. a kind of Chinese medicinal liquor adhesive bandage as claimed in claim 1, is characterized in that containing following component and ratio of weight and number, makes aerosol type Chinese medicinal liquor adhesive bandage:
Radix Apioris Fortunei (Radix Lespedezae Buergeri) extract 1-3
Chitosan 1.5
Ethanol 10
Glycerol 0.5
Hydrogen peroxide 0.5
Mentholum 3
Purified water 30
0.5% of pharmaceutical grade azone total amount.
4. a kind of Chinese medicinal liquor adhesive bandage as described in claim 1 or 2 or 3, is characterized in that described ethanol is anhydrous alcohol for medical use or 95% ethanol.
5. a kind of Chinese medicinal liquor adhesive bandage as claimed in claim 1, is characterized in that also containing the EGCG of 1-3 weight portion.
6. a kind of Chinese medicinal liquor adhesive bandage as claimed in claim 2 or claim 3, is characterized in that also containing the EGCG of 2 weight portions.
7. the preparation method of a kind of Chinese medicinal liquor adhesive bandage as claimed in claim 1, is characterized in that comprising the following steps:
1) press recipe quantity and prepare raw material, purified water is poured in preparation pot and is heated to boiling, add chitosan to be stirred to after being cooled to 88-92 ℃ and dissolve completely, then add glycerol to be uniformly mixed, regulate pH value 3.5-5.5, continue to stir 30 minutes, obtain solution A, be cooled to room temperature for subsequent use;
2) Radix Apioris Fortunei (Radix Lespedezae Buergeri) extract is added in alcoholic solution under room temperature stirring and dissolving complete, obtain solution B;
3) solution B is joined in solution A, mix homogeneously, adds Mentholum, hydrogen peroxide, pharmaceutical grade azone while stirring, as contained EGCG in formula, adds together, is uniformly mixed, and obtains Chinese medicinal liquor adhesive bandage.
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Cited By (3)
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| US20150374641A1 (en) * | 2013-02-13 | 2015-12-31 | Dong-A Pharmaceutical Co., Ltd | Film-forming pharmaceutical composition for wound healing and method for preparing the same |
| CN107233617A (en) * | 2017-06-05 | 2017-10-10 | 浙江工业大学 | A kind of wound dressing of liquid chitosan and its preparation and application |
| CN107468904A (en) * | 2017-08-24 | 2017-12-15 | 浙江医药高等专科学校 | Liquid bandage and preparation method thereof |
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