CN107916190A - A kind of Dracocephalum moldavica perfumed soap and its preparation method and application - Google Patents
A kind of Dracocephalum moldavica perfumed soap and its preparation method and application Download PDFInfo
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- CN107916190A CN107916190A CN201711228102.9A CN201711228102A CN107916190A CN 107916190 A CN107916190 A CN 107916190A CN 201711228102 A CN201711228102 A CN 201711228102A CN 107916190 A CN107916190 A CN 107916190A
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- Prior art keywords
- moldavica
- perfumed soap
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- dracocephalum moldavica
- dracocephalum
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
- C11D1/146—Sulfuric acid esters
Abstract
The present invention provides a kind of Dracocephalum moldavica perfumed soap and its preparation method and application, belong to perfumed soap technical field.The Dracocephalum moldavica perfumed soap, by being made for the raw material including following parts by weight：5~6 parts of moldavica dragonhead extractive, 3~5 parts of olive oil, 1~3 part of coconut oil, 1~3 part of palm oil, 8~9 parts of sodium hydroxide, 2~3 parts of lauryl sodium sulfate, 0.2~1 part of citric acid, 0.25~0.42 part of sodium chloride, 60~62.5 parts of water, 1~3 part of rosin acid；The preparation method of the moldavica dragonhead extractive, Dracocephalum moldavica powder is mixed with 65%~75% ethanol solution, immersion, obtains immersion feed liquid；The immersion feed liquid is ultrasonically treated；It is 1 by the volume ratio of obtained ethanol extract and water:2~4 mixing；Obtained mixed liquor is subjected to 13~17min of rotary evaporation under the conditions of 60~80 DEG C, obtains moldavica dragonhead extractive.Application of the Dracocephalum moldavica perfumed soap in bacteriostatic skin-care.
Description
Technical field
The invention belongs to perfumed soap technical field, and in particular to a kind of Dracocephalum moldavica perfumed soap and its preparation method and application.
Background technology
Perfumed soap is a kind of one of the most common and widely used articles for washing familiar to people.With green consumption tide
The influence of stream, and from the point of view of the double safety of human body and environment, people increasingly tend to use pure natural perfumed soap.To perfume (or spice)
The requirement of soap is in addition to clean cleaning function, it is often more important that there are the appearance of beauty, pleasant fragrance, and can bacteriostatic skin-care
It is and without side-effects.
Containing activating agent, preservative, foaming agent, fluorescer etc. in traditional perfumed soap, use is not gentle enough, sterilizing ability
Not strong, human body long-time service can produce larger stimulation to skin, and peculiar smell is larger.Chemical composition after use at the same time needs certain
Time could decompose, certain injury can be caused to environment.Pure natural perfumed soap is then completely absent the shortcomings that above, and with
The propulsion of national " modernization of Chinese medicine and industrialization development " action, the development and utilization to Chinese herbal medicine are being grown rapidly.But
Determined since the natural component extracting method in Chinese herb medicine is more difficult and the factors such as yield is low, cause such perfumed soap exploitation and
Develop barely satisfactory.
Dracocephalum moldavica (Dracocephalum moldavicaL.), alias rub eye, mountain mint, Lan Qiuhua, teosinte, perfume (or spice)
Beggar etc..Its quality standard record respectively in Inner Mongol mongolian medicine standard, the Sanitation Ministry medicine standard dimension medicine fascicle, also once recorded in
Version Chinese Pharmacopoeia in 1977, Chun Xing sections green grass or young crops Cymbidium annual herb plant, medicinal part are ground herb, are distributed mainly on China
North China, northeast, particularly northwest China area, the Inner Mongol and Xinjiang, the entitled Bi Yanggu of Mongolia.Dracocephalum moldavica, which has, alleviates the heart
Angina, improve myocardial ischemia, reduce the effect of heart tonifying and brain strengthening such as blood viscosity and platelet aggregation rate.It is fragrant in addition to as Chinese herbal medicine
Blue or green orchid is the important source material for preparing lemonene system spices because containing substantial amounts of volatile oil.In addition, the tender cauline leaf of Dracocephalum moldavica can be made
Eaten for special vegetable, dry cauline leaf and seed can make tea, flavoring or make spices.The multifunctional medical that Dracocephalum moldavica is contained with it
Health-care effect and the fragrance to show unique characteristics become the natural medicinal plant resource and virtue of a kind of great exploitation potential and national characters
Fragrant plant resources.
The content of the invention
In view of this, it is an object of the invention to provide a kind of Dracocephalum moldavica perfumed soap and its preparation method and application, the perfume (or spice)
Blue or green orchid perfumed soap has effects that obvious antibacterial and whitening and skin-protecting.
In order to realize foregoing invention purpose, the present invention provides following technical scheme：
The present invention provides a kind of Dracocephalum moldavica perfumed soap, by being made for the raw material including following parts by weight：Moldavica dragonhead extractive 5
~6 parts, 3~5 parts of olive oil, 1~3 part of coconut oil, 1~3 part of palm oil, 8~9 parts of sodium hydroxide, lauryl sodium sulfate 2~
3 parts, 0.2~1 part of citric acid, 0.25~0.42 part of sodium chloride, 60~62.5 parts of water, 1~3 part of rosin acid, 2~4 parts of propolis and
1~3 part of starch；
The preparation method of the moldavica dragonhead extractive, comprises the following steps：
1) Dracocephalum moldavica powder is mixed with the ethanol solution that volumetric concentration is 65%~75%, soaks 10~14h, soaked
Foam material liquid；The quality of the Dracocephalum moldavica powder and volumes of aqueous ethanol ratio are 1g：35~45mL；
2) the immersion feed liquid 25~35min of ultrasonic extraction that will be obtained in the step 1), obtained ethanol extract；
3) it is 1 by the ethanol extract and the volume ratio of water that are obtained in the step 2):2~4 mixing, obtain mixed liquor；
4) mixed liquor obtained in the step 3) is subjected to 13~17min of rotary evaporation under the conditions of 60~80 DEG C, obtained
To moldavica dragonhead extractive.
Preferably, the particle diameter of the Dracocephalum moldavica powder is 180~220 mesh.
Preferably, the volumetric concentration of the ethanol solution is 70%.
Preferably, the condition of supersound process：Supersonic frequency is 35~45KHz, and ultrasonic power is 90~110W, ultrasonic time
For 25~35min, ultrasonic temperature is 30~45 DEG C, and for ultrasonic extraction into between-line spacing ultrasound, ultrasonic interval time is 30~60s.
Preferably, by weight, raw material further includes 8~12 parts of lecithin, 3~5 parts of sorbitol anhydride fatty acid fat.
Preferably, by weight, raw material further includes 1~3 part of 2~4 parts of propolis and starch.
The present invention provides the preparation method of the Dracocephalum moldavica perfumed soap, comprise the following steps：
A, by olive oil, coconut oil and palm oil be mixed, obtained mixture be heated to 40~48 DEG C keep 25~
35min, obtains miscella；
B, sodium hydroxide and water are mixed, obtain aqueous slkali；
C, the aqueous slkali and rosin acid that are obtained in the step B are mixed, stirs 5min, obtain lotion；
D, by the lotion obtained in the miscella obtained in the step A and the step C carry out mixing 8~
12min, obtains soap lye；
E, Dracocephalum moldavica water extract, lauryl sodium sulfate, chlorination are sequentially added in the soap lye obtained into the step D
Sodium, citric acid, are mixed, obtain soap base；
F, by the soap base injection mould in the step E, seal, by the mould after sealing in 25~30 DEG C of ventilated environments
1~2h of middle placement, then 32~35 DEG C of 1~2h of placement are warming up to, after removing mould, obtain Dracocephalum moldavica perfumed soap；
There is no time sequencing limitation between the step A and step B~C.
Preferably, the temperature heated in the step A is 45 DEG C.
Preferably, the speed stirred in described step A, B, C, D and E stands alone as 45~60rpm.
Preferably, when raw material further includes lecithin and sorbitol anhydride fatty acid fat, by the step C by lecithin
Fat, sorbitol anhydride fatty acid fat are mixed with aqueous slkali at the same time with rosin acid, obtain lotion；When raw material further includes lecithin, mountain
When pears sugar alcohol acid anhydride fatty acid ester, propolis and starch, by the step C by lecithin, sorbitol anhydride fatty acid fat and rosin
Acid is mixed with aqueous slkali at the same time, obtains mixture；The mixture is mixed with propolis, starch again, obtains lotion.
The present invention provides Dracocephalum moldavica perfumed soap answering in bacteriostatic skin-care prepared by the Dracocephalum moldavica perfumed soap or the method
With.
The present invention provides a kind of Dracocephalum moldavica perfumed soap, mainly using olive oil, coconut oil, palm oil and sodium hydroxide it
Between react to each other, form soap base, there is the effect of sterilization and nourishing to skin with the use of rosin acid, while in moldavica dragonhead extractive
Flavone compound itself due to containing active material, be conducive to remove skin in free radical, promote skin it is new old
Metabolism, reduce pigmentation, whitening and moistening skin and other effects, and safe, without side-effects.
Further, the present invention provides a kind of Dracocephalum moldavica perfumed soap, with the use of lecithin and sorbitol anhydride fatty acid
Fat, soap scum is formed after effectively avoiding use；In addition, also added propolis and starch component in raw material, have to perfumed soap shaping
Good effect.
Brief description of the drawings
Fig. 1 is rutin solution standard curve in embodiment 4；
Fig. 2 is Dracocephalum moldavica perfumed soap appearance picture prepared by the present invention.
Embodiment
The present invention provides a kind of Dracocephalum moldavica perfumed soap, by being made for the raw material including following parts by weight：Moldavica dragonhead extractive 5
~6 parts, 3~5 parts of olive oil, 1~3 part of coconut oil, 1~3 part of palm oil, 8~9 parts of sodium hydroxide, lauryl sodium sulfate 2~
3 parts, 0.2~1 part of citric acid, 0.25~0.42 part of sodium chloride, 60~62.5 parts of water, 1~3 part of rosin acid.
The raw material of Dracocephalum moldavica perfumed soap provided by the invention includes moldavica dragonhead extractive.By weight, the Dracocephalum moldavica carries
It is 5~6 parts to take thing, is preferably 5.5 parts.
In the present invention, the preparation method of the moldavica dragonhead extractive, comprises the following steps：
1) it is 65%~75% ethanol solution by Dracocephalum moldavica powder and volumetric concentration, soaks 10~14h, soaked
Liquid；The quality of the Dracocephalum moldavica powder and volumes of aqueous ethanol ratio are 1g：35~45mL；
2) soak obtained in the step 1) is ultrasonically treated 25~35min, the soak of obtained supersound process；
3) it is 1 by the volume ratio for being ultrasonically treated soak and water obtained in the step 2):2~4 mixing, are mixed
Liquid；
4) mixed liquor obtained in the step 3) is subjected to 13~17min of rotary evaporation under the conditions of 60~80 DEG C, obtained
To moldavica dragonhead extractive.
Dracocephalum moldavica powder and volumetric concentration are 65%~75% ethanol solution by the present invention, are soaked 10~14h, are soaked
Steep liquid；The quality of the Dracocephalum moldavica powder and volumes of aqueous ethanol ratio are 1g：35~45mL.
In the present invention, the Dracocephalum moldavica powder is gathered by Dracocephalum moldavica plant, removes root, is cleaned, is dried in the shade, crushing is prepared.
In an embodiment of the present invention, the Dracocephalum moldavica plant collecting location is preferably Baotou Guyang County；It can also use
Commercial goods.In the present invention, the temperature dried in the shade is preferably 20~30 DEG C, more preferably 25 DEG C.The present invention is to the powder
Broken method is not particularly limited, using breaking method well-known to those skilled in the art.The Dracocephalum moldavica powder
Particle diameter is preferably 180~220 mesh, more preferably 200 mesh.
In the present invention, the volumetric concentration of the ethanol solution is preferably 70%.The solvent of ethanol solution is water.The immersion
Time be preferably 12~13h.The temperature of immersion is preferably 20~28 DEG C, more preferably 25 DEG C.The matter of the Dracocephalum moldavica powder
Amount is with volumes of aqueous ethanol than being preferably 1g：40mL.
Obtained soak, it is of the invention by 25~35min of the soak ultrasonic extraction, the immersion of obtained supersound process
Liquid.
In the present invention, the condition of supersound process preferably includes following parameter：Supersonic frequency is 35~45KHz, ultrasonic power
For 90~110W, ultrasonic time is 25~35min, and ultrasonic temperature is 30~45 DEG C, and ultrasonic interval time is 30~60s.It is super
The time of sonication is preferably 30min.The present invention is not particularly limited the supersound process with instrument, using art technology
Supersound process instrument known to personnel.In the embodiment of the present invention, the supersound process is B2500S-MT types with instrument
Number, it must can believe ultrasonic Co., Ltd purchased from Shanghai.
The volume ratio of the supersound process soak and water is 1 by obtained supersound process soak, the present invention:2~4 is mixed
Close, obtain mixed liquor.
In the present invention, the soak and the volume ratio of water of being ultrasonically treated is preferably 1:3.
In the present invention, water is preferably distilled water.After ethanol extraction, the purpose that adds water be by active material preferably and soap
Base merges.
After obtained mixed liquor, the present invention mixed liquor is carried out under the conditions of 60~80 DEG C rotary evaporation 13~
17min, obtains moldavica dragonhead extractive.
The present invention is not particularly limited the mode of the rotary evaporation, using rotation well-known to those skilled in the art
The scheme of evaporation.The temperature of the rotary evaporation is preferably 70 DEG C.The time of the rotary evaporation is preferably 14~16 DEG C,
More preferably 15 DEG C.The rotary evaporation is conducive to remove the ethanol in mixed liquor.
In the present invention, the general flavone containing 0.6~1mg/mL in the moldavica dragonhead extractive prepared using the above scheme.It is based on
The characteristic that flavone compound itself has, has numerous pharmacotoxicological effect and removes free radical in skin, promotes skin
Metabolism, reduce pigmentation, moisturizing and other effects, along with large area exists in plant kingdom, so in extraction Dracocephalum moldavica
Flavones ingredient be applied in the preparation of perfumed soap, the performance to perfumed soap whitening and skin-protecting effect plays an important role.At the same time based on upper
Technical solution is stated, the present invention provides a kind of method that general flavone is extracted from Dracocephalum moldavica, this method step is easy, and extraction is fast
Speed, and high concentration general flavone can be extracted.
The raw material of Dracocephalum moldavica perfumed soap provided by the invention includes olive oil.By weight, the olive oil is 3~5 parts,
Preferably 4 parts.The present invention is not particularly limited the source of the olive oil, using olive well-known to those skilled in the art
The source of oil.In the embodiment of the present invention, the olive oil is purchased from Tianjin Kai Tong chemical reagent Co., Ltd.
The raw material of Dracocephalum moldavica perfumed soap provided by the invention includes coconut oil.By weight, the coconut oil is 1~3 part,
Preferably 2 parts.The present invention is not particularly limited the source of the coconut oil, using coconut well-known to those skilled in the art
The source of oil.In the embodiment of the present invention, the coconut oil is purchased from Tianjin Kai Tong chemical reagent Co., Ltd.
The raw material of Dracocephalum moldavica perfumed soap provided by the invention includes palm oil.By weight, the palm oil is 1~3 part,
Preferably 2 parts.The present invention is not particularly limited the source of the palm oil, using palm well-known to those skilled in the art
The source of oil.In the embodiment of the present invention, the palm oil is purchased from Tianjin Kai Tong chemical reagent Co., Ltd.
In the present invention, the effect of olive oil, coconut oil and palm oil is to provide higher fatty acids for saponification.
The raw material of Dracocephalum moldavica perfumed soap provided by the invention includes sodium hydroxide.By weight, the sodium hydroxide for 8~
9 parts, be preferably 8.5 parts.The present invention is not particularly limited the source of the sodium hydroxide, ripe using those skilled in the art institute
The source for the sodium hydroxide known.In the embodiment of the present invention, the sodium hydroxide is limited purchased from the triumphant logical chemical reagent in Tianjin
Company.In the present invention, the effect of the sodium hydroxide is to provide alkaline solution for saponification.
The raw material of Dracocephalum moldavica perfumed soap provided by the invention includes lauryl sodium sulfate.By weight, the dodecane
Base sodium sulphate is 2~3 parts, is preferably 2.5 parts.The present invention is not particularly limited the source of the lauryl sodium sulfate, adopts
With the source of lauryl sodium sulfate well-known to those skilled in the art.In the embodiment of the present invention, the dodecyl
Sodium sulphate is purchased from Tianjin Kai Tong chemical reagent Co., Ltd.In the present invention, the effect of the lauryl sodium sulfate is decontamination
The effect of agent.
The raw material of Dracocephalum moldavica perfumed soap provided by the invention includes citric acid.By weight, the citric acid is 0.2~1
Part, it is preferably 0.4~0.8 part, is most preferably 0.6 part.The present invention is not particularly limited the source of the citric acid, using this
The source of citric acid known to field technology personnel.In the embodiment of the present invention, the citric acid is triumphant logical purchased from Tianjin
Chemical reagent Co., Ltd.In the present invention, the citric acid belongs to one kind of tartaric acid, is a kind of good moisturizer.
The raw material of Dracocephalum moldavica perfumed soap provided by the invention includes sodium chloride.By weight, the sodium chloride for 0.25~
0.42 part, be preferably 0.3~0.4 part, more preferably 0.35 part.The present invention is not particularly limited the source of the sodium chloride,
Using the source of sodium chloride well-known to those skilled in the art.In the embodiment of the present invention, the sodium chloride is purchased from Tianjin
Kai Tong chemical reagent Co., Ltd of city.In the present invention, the effect of the sodium chloride is to saltout.
The raw material of Dracocephalum moldavica perfumed soap provided by the invention includes water.By weight, the water is 60~62.5 parts, preferably
For 61 parts.The present invention is not particularly limited the source of the water, and the source using water well-known to those skilled in the art is
Can.The water is preferably distilled water.In the present invention, the effect of the water is to prepare the effect of lotion.
The raw material of Dracocephalum moldavica perfumed soap provided by the invention includes rosin acid.By weight, the rosin acid is 1~3 part,
Preferably 2 parts.The present invention is not particularly limited the source of the rosin acid, using rosin well-known to those skilled in the art
The source of acid.In the embodiment of the present invention, the rosin acid is purchased from Tianjin Kai Tong chemical reagent Co., Ltd.The present invention
In, the rosin acid has stronger antibacterial action.
The raw material of Dracocephalum moldavica perfumed soap provided by the invention preferably further includes lecithin.By weight, the lecithin is 8
~12 parts, be preferably 10 parts.The present invention is not particularly limited the source of the lecithin, ripe using those skilled in the art institute
The source for the lecithin known.In the embodiment of the present invention, the lecithin is purchased from Tianjin Kai Tong chemical reagent Co., Ltd.
The raw material of Dracocephalum moldavica perfumed soap provided by the invention preferably further includes sorbitol anhydride fatty acid fat.By weight,
The sorbitol anhydride fatty acid fat is 3~5 parts, is preferably 4 parts.Source of the present invention to the sorbitol anhydride fatty acid fat
It is not particularly limited, using the source of sorbitol anhydride fatty acid fat well-known to those skilled in the art.It is of the invention real
Apply in example, the sorbitol anhydride fatty acid fat is purchased from Tianjin Kai Tong chemical reagent Co., Ltd.
In the present invention, lecithin and the sorbitol anhydride fatty acid fat is added as amphoteric surfactant raw material,
Can be to avoid forming soap scum after use.Two big shortcomings of soaps are that low-temperature solubility is small and resistance to hard water is poor, amphoteric surface
Activating agent can reduce its KP temperature, improve its low-temperature water-soluble as hydrotropic agent.In addition, amphoteric surfactant is also
It can prevent soaps from forming soap scum suspended matter in hard water.For the structure of surfactant similar to a matchstick, match end is exactly parent
Water end (W.E.), splint are exactly that greasy dirt intramolecule, similar compatibility are inserted into hydrophobic end hydrophobic ends；Water-wet side is formed with water molecules
Micella group, in this way, pass through mechanical friction campaign again, just comes greasy dirt molecule is loose, draws in water, so as to reach puffing, molten
Solution, diffusion, the purpose of washing greasy dirt.Lecithin and sorbitol anhydride fatty acid fat are all pure natural surfactants, with synthesis
Surfactant compare, the surface-active such as its cleaning strength, dispersion force, emulsifying ability, foaming power is smaller, but toxicity is low, biology drop
Solution property is good.
The raw material of Dracocephalum moldavica perfumed soap provided by the invention preferably further includes propolis.By weight, the propolis is 2~4
Part, it is preferably 3 parts.The present invention is not particularly limited the source of the propolis, using bee well-known to those skilled in the art
The source of glue.In the embodiment of the present invention, the propolis is purchased from Tianjin Kai Tong chemical reagent Co., Ltd.In the present invention,
The propolis, has antibacterial action, can suppress to kill various bacteria, can also promote and biological human body protective capacities, improvement blood follow
Ring, promote granulation growth, accelerating wound healing, and has the function of moist, antipruritic, deodorization, sun-proof etc., while the addition of propolis,
Have the function that to perfumed soap shaping good.
The raw material of Dracocephalum moldavica perfumed soap provided by the invention preferably further includes starch.By weight, the starch is 1~3
Part, it is preferably 2 parts.The present invention is not particularly limited the source of the starch, using shallow lake well-known to those skilled in the art
The source of powder.In the embodiment of the present invention, the starch is purchased from Tianjin Kai Tong chemical reagent Co., Ltd.In the present invention,
Starch has the function that perfumed soap shaping good.
The present invention provides the preparation method of the Dracocephalum moldavica perfumed soap, comprise the following steps：
A, by olive oil, coconut oil and palm oil be mixed, obtained mixture be heated to 40~48 DEG C keep 25~
35min, obtains miscella；
B, sodium hydroxide and water are mixed, obtain aqueous slkali；
C, the aqueous slkali and rosin acid that are obtained in the step B are mixed, stirs 5min, obtain lotion；
D, by the lotion obtained in the miscella obtained in the step A and the step C carry out mixing 8~
12min, obtains soap lye；
E, Dracocephalum moldavica water extract, lauryl sodium sulfate, chlorination are sequentially added in the soap lye obtained into the step D
Sodium, citric acid, are mixed, obtain soap base；
F, by the soap base injection mould in the step E, seal, by the mould after sealing in 25~30 DEG C of ventilated environments
1~2h of middle placement, then 32~35 DEG C of 1~2h of placement are warming up to, after removing mould, obtain Dracocephalum moldavica perfumed soap；
There is no time sequencing limitation between the step A and step B~C.
Olive oil, coconut oil and palm oil are mixed the present invention, and obtained mixture is heated to 40~48 DEG C of holdings
25~35min, obtains miscella.
In the present invention, the rotating speed of the mixing is preferably 45~60rpm, more preferably 50~58rpm, is most preferably
55rpm.The temperature of the heating is preferably 45 DEG C.The time of the heating is preferably 30min.
Sodium hydroxide and water are mixed the present invention, obtain aqueous slkali.The rotating speed of the mixing is preferably 45~
60rpm, more preferably 50~58rpm.The container that the sodium hydroxide uses when being mixed with water is preferably resistance to alkali container.It is described resistance to
Alkali container is preferably open-top receptacle, even if releasing amount of heat discharge during to mix.
After obtained aqueous slkali, 5min is mixed in the aqueous slkali and rosin acid by the present invention, obtains lotion.
In the present invention, the rotating speed of the mixing is preferably 45~60rpm, more preferably 50~58rpm, is most preferably
55rpm。
After obtained miscella and lotion, the present invention by the miscella and the lotion carry out mixing 8~
12min, obtains soap lye.In the present invention, the rotating speed of the mixing is preferably 45~60rpm, more preferably 50~58rpm,
Most preferably 55rpm.The time of the mixing is preferably 10min.
In the present invention, when raw material further includes lecithin and sorbitol anhydride fatty acid fat, by the step C by lecithin
Fat, sorbitol anhydride fatty acid fat are mixed with aqueous slkali at the same time with rosin acid, obtain lotion；When raw material further includes lecithin, mountain
When pears sugar alcohol acid anhydride fatty acid ester, propolis and starch, by the step C by lecithin, sorbitol anhydride fatty acid fat and rosin
Acid is mixed with aqueous slkali at the same time, obtains mixture；The mixture is mixed with propolis, starch again, obtains lotion.
After obtaining soap lye, the present invention sequentially adds moldavica dragonhead extractive, lauryl sodium sulfate, chlorination into the soap lye
Sodium, citric acid, are mixed, obtain soap base.In the present invention, a kind of raw material is preferably often added, carries out mixed once stirring.
In the present invention, the speed of the mixing is 45~60rpm, more preferably 50~58rpm, is most preferably
55rpm。
After obtaining soap base, the present invention injects the soap base in mould, sealing, and the mould after sealing is logical at 25~30 DEG C
1~2h is placed in wind environment, then is warming up to 32~35 DEG C of 1~2h of placement, after removing mould, obtains Dracocephalum moldavica perfumed soap.
In the present invention, the method for the injection mould is not particularly limited, using note well-known to those skilled in the art
Enter the scheme of mould.The ventilated environment, which is placed with, to be beneficial to make soap base drying and moulding.The purpose of 32~35 DEG C of placements makes soap
Base consolidates shaping.
The present invention provides Dracocephalum moldavica perfumed soap answering in bacteriostatic skin-care prepared by the Dracocephalum moldavica perfumed soap or the method
With.
A kind of Dracocephalum moldavica perfumed soap provided by the invention and its preparation method and application is carried out with reference to embodiment detailed
Explanation, but they cannot be interpreted as limiting the scope of the present invention.
Embodiment 1
Moldavica dragonhead extractive preparation method
Dracocephalum moldavica plant is adopted to obtain in Baotou Guyang County, the plant adopted back is removed into root, net soil is trembled, is placed on interior
Naturally dry in the shade.Dracocephalum moldavica plant after drying in the shade smashs into powder to pieces with pulverizer, crosses the sieve of 200 mesh, obtains Dracocephalum moldavica fine powder,
Its is closed, and cool place preserves.
By the ethanol that Dracocephalum moldavica powder and volumetric concentration are 70%, by 1：40 solid-liquid ratio, is surpassed after soaking 12h with Ultrasound Instrument
Sound oscillation 30min, obtained medicinal extract.Medicinal extract and water are pressed 1 again:3 ratio is mixed, and is rotatably evaporated with the conditions of 70 DEG C
Instrument handles 15min, and vaporized alcohol is fallen, it is stand-by to obtain moldavica dragonhead extractive.
Embodiment 2
Moldavica dragonhead extractive preparation method
Dracocephalum moldavica plant is adopted to obtain in Baotou Guyang County, the plant adopted back is removed into root, net soil is trembled, is placed on interior
Naturally dry in the shade.Dracocephalum moldavica plant after drying in the shade smashs into powder to pieces with pulverizer, crosses the sieve of 220 mesh, obtains Dracocephalum moldavica fine powder,
Its is closed, and cool place preserves.
By the ethanol that Dracocephalum moldavica powder and volumetric concentration are 75%, by 1：35 solid-liquid ratio, is surpassed after soaking 14h with Ultrasound Instrument
Sound oscillation 35min, obtained medicinal extract.Medicinal extract and water are pressed 1 again:4 ratio is mixed, and is rotatably evaporated with the conditions of 75 DEG C
Instrument handles 13min, and vaporized alcohol is fallen, it is stand-by to obtain moldavica dragonhead extractive.
Embodiment 3
Moldavica dragonhead extractive preparation method
Dracocephalum moldavica plant is adopted to obtain in Baotou Guyang County, the plant adopted back is removed into root, net soil is trembled, is placed on interior
Naturally dry in the shade.Dracocephalum moldavica plant after drying in the shade smashs into powder to pieces with pulverizer, crosses the sieve of 180 mesh, obtains Dracocephalum moldavica fine powder,
Its is closed, and cool place preserves.
By the ethanol that Dracocephalum moldavica powder and volumetric concentration are 65%, by 1：35 solid-liquid ratio, is surpassed after soaking 10h with Ultrasound Instrument
Sound oscillation 25min, obtained medicinal extract.Medicinal extract and water are pressed 1 again:2 ratio is mixed, and is rotatably evaporated with the conditions of 65 DEG C
Instrument handles 17min, and vaporized alcohol is fallen, it is stand-by to obtain moldavica dragonhead extractive.
Comparative example 1
Moldavica dragonhead extractive is prepared using the preparation method of embodiment 1, difference is, uses volumetric concentration as 30%
Ethanol solution extracted.
Embodiment 4
Moldavica dragonhead extractive is detected using microplate reader.
Take liquid-transfering gun, draw the Dracocephalum moldavica sample solution that 5 μ L embodiments 1~3 are prepared respectively, click and enter the point in 96 holes
In model, detection is using straight alcohol as control group every time.Every kind of sample is clicked and entered in each perpendicular row, can once detect 11, by point
The good point template of sample is put into microplate reader inspection groove, can inputted setting wavelength 510nm in computer, is being set as that flavonoids detects,
A new file is established in microplate reader, every group of data carry out typing.
Microplate reader detects Dracocephalum moldavica sample solution, and every group of sample is surveyed 8 times, and average value is calculated with WPS forms.
Using rutin standard items as positive control, calculated according to the standard curve of positive control total in Dracocephalum moldavica sample solution
The concentration of flavones.Rutin standard solution concentration and the relation of general flavone content are shown in Table 1.
The relation of 1 rutin standard solution of table and general flavone content
According to the data in table 1, abscissa is arranged to the general flavone content M in rutin standard solution, and ordinate is corresponding
The A determined, draws the standard curve such as Fig. 1, can therefrom obtain its normal equation A=0.954M-0.0098, R2=
0.9941。
The absorption value of 2 wavelength 510nm Dracocephalum moldavica product to be tested solution of table
According to A=0.954M-0.0098
Then MSample to be tested=(A+0.0098)/0.954
According to the data of table 2, A is obtained；Bring obtained A into above formulas, can obtain in embodiment 1~3 and comparative example 1, it is total yellow
The concentration M of ketoneSample to be testedRespectively 9.14mg, 10.10mg, 9.11mg, 8.00mg.
Embodiment 5
It is spare to weigh following component quality：Moldavica dragonhead extractive 5kg prepared by embodiment 1, olive oil 5kg, coconut oil
1kg, palm oil 3kg, sodium hydroxide 8kg, lauryl sodium sulfate 3kg, citric acid 0.2kg, sodium chloride 0.42kg, water 60kg,
Rosin acid 3kg.
Weight according to above-mentioned raw materials carries out preparing perfumed soap：
(1) olive oil, coconut oil and palm oil of above-mentioned quality are put into container together and are heated, holding temperature is
40 DEG C, 30min is stirred with 60rpm speed, it is spare to obtain miscella.
(2) take the water of the parts by weight to be placed in container, sodium hydroxide is added to the water, while used with alkaline-resisting blender
60rpm speed stirs, and reacts to obtain aqueous slkali A.
(3) lecithin, sorbitol anhydride fatty acid fat, rosin acid stirring 5min are added while stirring into the lye again,
Propolis and starch are added, is stirred evenly with 60rpm speed, obtains lotion B.
(4) miscella is poured into the container equipped with lotion B, while is stirred with alkaline-resisting blender 60rpm speed, directly
Mixture surface energy in container marks complete 8 word, you can the soap lye is made.
(5) raw material mixes：The Dracocephalum moldavica water extract that will have been produced, is slowly added into thick soap lye, uses glass bar
Stirred evenly with 60rpm speed, then will dissolve lauryl sodium sulfate with minor amount of water adds in soap lye, is stirred with 60rpm speed
The additives such as sodium chloride, citric acid are continuously added after mixing uniformly.
(6) it is molded:The lotion obtained in step is poured into mould, then mould is covered with paper membrane, mould is ready to,
The soap base being stirred injection wherein, then with paper membrane covers mould, 1h is placed in temperature is 25 DEG C of fume hoods, then 32
DEG C incubator in place 1h, wait it solidify after, be drawn off, be placed on ventilation, avoid exposure in sunshine, that is, be molded.
Embodiment 6
It is spare to weigh following component quality：Moldavica dragonhead extractive 6kg prepared by embodiment 2, olive oil 3kg, coconut oil
3kg, palm oil 1kg, sodium hydroxide 9kg, lauryl sodium sulfate 2kg, citric acid 1kg, sodium chloride 0.25kg, water 62.5kg,
Rosin acid 1kg.
Obtained according to the following steps：
(1) olive oil, coconut oil and palm oil of above-mentioned quality are put into container together and are heated, holding temperature is
48 DEG C, 30min is stirred with 45rpm speed, it is spare to obtain miscella.
(2) take the water of the parts by weight to be placed in container, sodium hydroxide be added to the water, at the same with alkaline-resisting blender with
45rpm speed stirs, and reacts to obtain aqueous slkali A.
(3) lecithin, sorbitol anhydride fatty acid fat, rosin acid stirring 5min are added while stirring into the lye again,
Propolis and starch are added, is stirred evenly with 45rpm speed, obtains lotion B.
(4) miscella is poured into the container equipped with lotion B, while is stirred with alkaline-resisting blender with 45rpm speed, directly
Mixture surface energy in container marks complete 8 word, you can the soap lye is made.
(5) raw material mixes：The Dracocephalum moldavica water extract that will have been produced, is slowly added into thick soap lye, uses glass bar
Stir evenly, then will dissolve lauryl sodium sulfate with minor amount of water adds in soap lye, continues after being stirred evenly with 45rpm speed
Add the additives such as sodium chloride, citric acid.
(6) it is molded:The lotion obtained in step is poured into mould, then mould is covered with paper membrane,
Mould is ready to, the soap base being stirred injection wherein, then with paper membrane covers mould, it is logical for 30 DEG C in temperature
1h is placed in wind cupboard, then places 1h in 35 DEG C of incubator, after waiting it to solidify, is drawn off, is placed on ventilation, avoid sunlight
Exposure, that is, be molded.
Embodiment 7
It is spare to weigh following component quality：Moldavica dragonhead extractive 5.5kg prepared by embodiment 3, olive oil 4kg, coconut oil
2kg, palm oil 2kg, sodium hydroxide 8.5kg, lauryl sodium sulfate 2.5kg, citric acid 0.6kg, sodium chloride 0.35kg, water
61kg, rosin acid 2kg.
Obtained according to the following steps：
(1) olive oil, coconut oil and palm oil are put into container together and are heated, it is 5 DEG C to keep temperature, is used
55rpm speed stirs 30min, and it is spare to obtain miscella.
(2) take the water of the parts by weight to be placed in container, sodium hydroxide is added to the water, while used with alkaline-resisting blender
55rpm speed stirs, and reacts to obtain aqueous slkali A.
(3) lecithin, sorbitol anhydride fatty acid fat, rosin acid 55rpm speed are added while stirring into the lye again
Degree stirring 5min, adds propolis and starch, is stirred evenly with 55rpm speed, obtain lotion B.
(4) miscella is poured into the container equipped with lotion B, while is quickly stirred with alkaline-resisting blender, until container
Interior mixture surface energy marks complete 8 word, you can the soap lye is made.
(5) raw material mixes：The Dracocephalum moldavica water extract that will have been produced, is slowly added into thick soap lye, uses glass bar
Stirred evenly with 55rpm speed, then will dissolve lauryl sodium sulfate with minor amount of water adds in soap lye, is stirred with 55rpm speed
The additives such as sodium chloride, citric acid are continuously added after mixing uniformly.
(6) it is molded:The lotion obtained in step is poured into mould, then mould is covered with paper membrane,
Mould is ready to, the soap base being stirred injection wherein, then with paper membrane covers mould, it is logical for 28 DEG C in temperature
1h is placed in wind cupboard, then places 1h in 33 DEG C of incubator, after waiting it to solidify, is drawn off, is placed on ventilation, avoid sunlight
Exposure, that is, be molded.
Comparative example 2
Perfumed soap is prepared using the scheme of embodiment 1, difference is that raw material includes moldavica dragonhead extractive, but increases olive oil
Quality, the dosage of olive oil is improved the 90% of raw material dosage.
Comparative example 3
Perfumed soap is prepared using the scheme of embodiment 2, difference is not include rosin acid in raw material, while increases increase olive oil
Quality, the dosage of olive oil is improved the 90% of raw material dosage.
Embodiment 8
The perfumed soap that embodiment 1 and comparative example 2 are made, is dissolved in a times water for perfumed soap quality, and perfumed soap liquid is made.It is qualified to select afterwards
Spot examination device, with closed patch experiment method, tested material about 0.020mL-0.025mL drops are tried in device in spot, external application is special
Adhesive tape is covered on subject back, 0.5 it is small when after remove tested material, see respectively after removing 0.5,6,12,24 it is small when dermoreaction,
Result of the test display experiment perfumed soap used has slight adverse reaction after not adding moldavica dragonhead extractive, and skin is dark yellow.It is therefore fragrant
The effect of blue or green orchid extract is participation thing important in the perfumed soap, reduces stimulation and whitening and skin-protecting.
Embodiment 9
Embodiment 2 has been lacked into rosin acid compared with the perfumed soap that comparative example 3 makes, after discovery is finished, and some joints
The dirt at place is not easy to remove, i.e., detergency have dropped.
It is that Bacteria Indicators carry out bacteriostatic test with natural bacteria on hand using agar plate method.Perfumed soap is placed in mortar
Powder is pounded, 0.30g powder is accurately weighed and is dissolved in distilled water and be settled to 10mL, 0.4 μm of membrane filtration of via hole diameter is degerming, system
It is standby into sterile perfumed soap aqueous solution.The perfumed soap aqueous solution is taken to be mixed into 50 DEG C or so the ordinary nutrient agar culture mediums melted of cooling
(medium component：Beef extract 3g, peptone 10g, NaCl 5g, water 1000mL, is adjusted to pH7.0~7.2), concentration reaches volume
Fraction 2%.The control medium for being not added with perfumed soap aqueous solution is made at the same time.After its solidification, sample solution is bedewed with sterile cotton swab
Smear people's palmar side and be inoculated into experimental group and control group culture medium flat plate surface to be infected with natural bacteria, then with semar technique.It is placed in 37
Result is observed after cultivating 24h in DEG C constant incubator.Detect 3 times altogether.Result judgement is substantially few with bacterial population on experimental group tablet
In control group, that is, represent that the perfumed soap has bacteriostasis.It is basically identical through 3 batches repetition experimental results, show that its antibacterial is imitated
Fruit is stablized.
Therefore rosin acid is also participation thing important in the perfumed soap, rosin acid cooperates with performance antibacterial together with moldavica dragonhead extractive
Effect.
Embodiment 10
Perfumed soap is prepared using the scheme of embodiment 3, difference part is that increase lecithin 10kg, sorbitan esters of fatty
Sour fat 4kg, propolis 3kg and starch 2kg, when preparation, add entrance with rosin acid together, are obtained according to the following steps：
(1) olive oil, coconut oil and palm oil are put into container together and are heated, it is 5 DEG C to keep temperature, is used
55rpm speed stirs 30min, and it is spare to obtain miscella.
(2) take the water of the parts by weight to be placed in container, sodium hydroxide is added to the water, while used with alkaline-resisting blender
55rpm speed stirs, and reacts to obtain aqueous slkali A.
(3) the liquor-saturated fat vinegar 55rpm speed stirring of lecithin, D-sorbite is added while stirring into the lye again
5min, adds propolis and starch, is stirred evenly with 55rpm speed, obtains lotion B.
(4) miscella is poured into the container equipped with lotion B, while is quickly stirred with alkaline-resisting blender, until container
Interior mixture surface energy marks complete 8 word, you can the soap lye is made.
(5) raw material mixes：The Dracocephalum moldavica water extract that will have been produced, is slowly added into thick soap lye, uses glass bar
Stirred evenly with 55rpm speed, then will dissolve lauryl sodium sulfate with minor amount of water adds in soap lye, is stirred with 55rpm speed
The additives such as sodium chloride, citric acid are continuously added after mixing uniformly.
(6) it is molded:The lotion obtained in step is poured into mould, then mould is covered with paper membrane, mould is ready to,
By the soap base being stirred injection wherein, then with paper membrane mould is covered, places one hour in temperature is 25 DEG C of fume hood, then
Placed one hour in 32 DEG C of incubator, after waiting it to solidify, be drawn off, be placed on ventilation, avoid exposure in sunshine, that is, be molded.
As shown in Figure 2.
The above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, various improvements and modifications may be made without departing from the principle of the present invention, these improvements and modifications also should
It is considered as protection scope of the present invention.
Claims (10)
1. a kind of Dracocephalum moldavica perfumed soap, is made of the raw material including following parts by weight：5~6 parts of moldavica dragonhead extractive, olive oil 3~5
Part, 1~3 part of coconut oil, 1~3 part of palm oil, 8~9 parts of sodium hydroxide, 2~3 parts of lauryl sodium sulfate, citric acid 0.2~1
Part, 0.25~0.42 part of sodium chloride, 60~62.5 parts of water, 1~3 part of rosin acid；
The preparation method of the moldavica dragonhead extractive, comprises the following steps：
1) Dracocephalum moldavica powder is mixed with the ethanol solution that volumetric concentration is 65%~75%, soaks 10~14h, obtain immersion material
Liquid；The quality of the Dracocephalum moldavica powder and volumes of aqueous ethanol ratio are 1g：35~45mL；
2) the immersion feed liquid 25~35min of ultrasonic extraction that will be obtained in the step 1), obtains ethanol extract；
3) it is 1 by the ethanol extract and the volume ratio of water that are obtained in the step 2):2~4 mixing, obtain mixed liquor；
4) mixed liquor obtained in the step 3) is subjected to 14~17min of rotary evaporation under the conditions of 60~80 DEG C, obtains perfume (or spice)
Blue or green orchid extract.
2. Dracocephalum moldavica perfumed soap according to claim 1, it is characterised in that the particle diameter of the Dracocephalum moldavica powder is 180~220
Mesh.
3. Dracocephalum moldavica perfumed soap according to claim 1, it is characterised in that the condition of supersound process：Supersonic frequency for 35~
45KHz, ultrasonic power are 90~110W, and ultrasonic time is 25~35min, and ultrasonic temperature is 30~45 DEG C, at the ultrasound
Manage and be ultrasonically treated for interval, ultrasonic interval time is 30~60s.
4. the Dracocephalum moldavica perfumed soap according to claims 1 to 3 any one, by weight, raw material further include lecithin 8~
12 parts, 3~5 parts of sorbitol anhydride fatty acid fat.
5. Dracocephalum moldavica perfumed soap according to claim 4, by weight, raw material further include 2~4 parts of propolis and starch 1~3
Part.
6. the preparation method of Dracocephalum moldavica perfumed soap described in claims 1 to 3 any one, it is characterised in that comprise the following steps：
A, by olive oil, coconut oil and palm oil be mixed, obtained mixture be heated to 40~48 DEG C keep 25~
35min, obtains miscella；
B, sodium hydroxide and water are mixed, obtain aqueous slkali；
C, the aqueous slkali and rosin acid that are obtained in the step B are mixed, stirs 5min, obtain lotion；
D, the lotion obtained in the miscella obtained in the step A and the step C is subjected to 8~12min of mixing, obtained
To soap lye；
E, Dracocephalum moldavica water extract, lauryl sodium sulfate, sodium chloride, lemon are sequentially added in the soap lye obtained into the step D
Lemon acid, is mixed, obtains soap base；
F, by the soap base injection mould in the step E, sealing, the mould after sealing is put in 25~30 DEG C of ventilated environments
1~2h is put, then is warming up to 32~35 DEG C of 1~2h of placement, after removing mould, obtains Dracocephalum moldavica perfumed soap；
There is no time sequencing limitation between the step A and step B~C.
7. preparation method according to claim 6, it is characterised in that the temperature heated in the step A is 45 DEG C.
8. preparation method according to claim 6, it is characterised in that the speed stirred in described step A, B, C, D and E is independent
For 45~60rpm.
9. according to preparation method described in claim 6~8 any one, it is characterised in that when raw material further includes lecithin and mountain
During pears sugar alcohol acid anhydride fatty acid ester, by the step C by lecithin, sorbitol anhydride fatty acid fat and rosin acid at the same time and alkali soluble
Liquid mixes, and obtains lotion；When raw material further includes lecithin, sorbitol anhydride fatty acid fat, propolis and starch, by the step
Lecithin, sorbitol anhydride fatty acid fat are mixed with aqueous slkali at the same time with rosin acid in C, obtain mixture；By the mixing
Thing is mixed with propolis, starch again, obtains lotion.
10. prepared by Dracocephalum moldavica perfumed soap described in Claims 1 to 5 any one or claim 6~9 any one the method
Application of the Dracocephalum moldavica perfumed soap in bacteriostatic skin-care.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108403531A (en) * | 2018-05-30 | 2018-08-17 | 曾亿格 | Purposes of the moldavica dragonhead extractive in preparing whitening cosmetics |
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