CN107904134A - A kind of preparation method of bee honey health-care vinegar - Google Patents

A kind of preparation method of bee honey health-care vinegar Download PDF

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CN107904134A
CN107904134A CN201810057888.0A CN201810057888A CN107904134A CN 107904134 A CN107904134 A CN 107904134A CN 201810057888 A CN201810057888 A CN 201810057888A CN 107904134 A CN107904134 A CN 107904134A
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王耀斌
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Shaanxi Yangling Shanxi Agricultural Development Co Ltd
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    • C12JVINEGAR; PREPARATION OR PURIFICATION THEREOF
    • C12J1/00Vinegar; Preparation or purification thereof
    • C12J1/04Vinegar; Preparation or purification thereof from alcohol
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/48Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/48Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
    • A61K36/481Astragalus (milkvetch)
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K36/53Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/85Verbenaceae (Verbena family)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/88Liliopsida (monocotyledons)

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Abstract

The present invention provides a kind of preparation method of bee honey health-care vinegar, and invention formula is made of honey, wheat and glutinous rice slurries and middle medicinal herbs extracting solution, and bee honey health-care vinegar is obtained by Raw material processing, alcoholic fermentation and acetic fermentation process;In formula, honey, wheat, the processing technology of glutinous rice and herbal raw material carry out at low temperature, effectively maintain the original nutritional ingredient of raw material;In inventive formulation, grasswort and water hyacinth component are added, makes gained bee honey health-care vinegar have the function of to promote gastrointestinal disturbances;The addition of crafty son's leaf, disappear certainly Rong and Chinese milk vetch makes it have the effect of promoting blood circulation and removing blood stasis at the same time;In addition, using honey as main component in formula, while wheat and glutinous rice slurries are added, solving vinegar generally has irritation tart flavour, excessively edible rear stomach has the problem of cusalgia sense of discomfort, and makes fragrant and sweet taste and wheat perfume and rice perfume (or spice) fragrance of the gained health-care vinegar with honey.

Description

A kind of preparation method of bee honey health-care vinegar
Technical field
The invention belongs to health-care vinegar technical field, and in particular to a kind of preparation method of bee honey health-care vinegar.
Background technology
Honey is a kind of sticky, transparent or semitransparent colloidal liquid, mainly contains glucose, fructose, sucrose and wheat Bud sugar, is a kind of full of nutrition also containing materials such as micro amino acids, vitamin, enzyme, yeast, pollen grain and waxes Natural nourishing product.Vinegar is with a kind of tart flavour flavor enhancement, the use of rice or sorghum be mainly raw material in traditional wine vinegar technique, passes through Cross appropriate fermentation make containing carbohydrate as sugar, Starch Conversion be alcohol and carbon dioxide, alcohol is again by acetic acid bacteria Effect is combined with oxygen in air generates acetic acid and water.The main component of vinegar is acetic acid and organic acid, and acetic acid is conducive to sugar and fat Fat is fully converted into energy, prevents body fat from excessively accumulating, and can also soften the cholesterol level in blood vessel, reduction blood; Organic acid be then conducive to maintain human internal environment's acid-base value balance and stabilization, enable it is various metabolism and physiological function normally into OK.
Fermented type vinegar on the market generally uses single grain to make vinegar for raw material at present.During the fermentation, in raw material Organic nutrient substance easily aoxidized, make gained vinegar it is with single nutrient component;And nutritional ingredient can be also produced while be reduced Undesirable color and luster and smell, such as the exacerbation of vinegar color and with irritant tart flavour, this can influence product quality and eating mouth feel, nothing Method meets the market demand.
The content of the invention
The invention is intended to for above-mentioned existing issue, there is provided and it is a kind of full of nutrition, have and promote gastrointestinal disturbances and promoting blood circulationization Stasis of blood function, can solve the problems, such as the preparation method of the bee honey health-care vinegar of the irritant tart flavour of vinegar band.
To reach above-mentioned purpose, technical solution of the present invention is as follows:
A kind of preparation method of bee honey health-care vinegar, it is characterised in that:Comprise the following steps:
(1)By honey 1 ~ 2h of heating stirring, temperature control crosses 40 ~ 60 mesh at 35 ~ 50 DEG C, removes impurity;
(2)By step(1)Gained honey presses 1g with pure water:5mL~1g:The ratio mixing of 10mL, is heated, temperature after stirring evenly At 65 ± 2 DEG C, heating time is 1.5 ~ 3h for degree control;200 ~ 300 mesh sieves are crossed after the completion of heating, obtain pure honey liquid;
(3)Wheat and glutinous rice are taken, by 1:After 2 mass ratio mixing wash clean, by 1g:The ratio of 5mL adds water to be beaten, excessively 100 ~ 150 mesh sieves, obtain the mixed serum of wheat and glutinous rice, are placed in 3 ~ 6 DEG C of refrigerating chamber lucifuges and seal up for safekeeping;
(4)The young leaf of grasswort, thief, disappear certainly Rong, Chinese milk vetch, bitter fleabane, water hyacinth and rabdosia lophanthide is taken to clean up, with the second that concentration is 2% Alcoholic solution presses 1g:10mL ratio mixing, agitating and heating, heating-up temperature be 65 ~ 80 DEG C, heating time is 2 ~ 3h, after carried out Filter;Gained filtrate is concentrated into postcooling, it is 20% ~ 25% to control concentrate water content;
(5)Alcoholic fermentation:
By step(3)Gained wheat and glutinous rice mixed serum and step(2)Gained pure honey liquid presses 5:7 volume ratio mixing Zymotic fluid is obtained, by adding water management zymotic fluid sugar content between 20% ~ 35%, sterilize 25 ~ 30min at 90 DEG C, adds after cooling Enter mass concentration for 3% acetum, between the pH to 4 ~ 6 for adjusting zymotic fluid;
(6)By step(5)Gained zymotic fluid is placed in fermentation tank, is by solid-liquid ratio(2~6)g:The ratio of 10L adds grape wine and lives Property dry ferment after seal, temperature control is taken out at 20 ± 2 DEG C after continuously fermenting 5 ~ 7 days, cross 50 ~ 70 mesh sieves, obtain alcoholic fermentation Liquid;
(7)Acetic fermentation:
By step(4)Chinese herbal medicine concentrate and step obtained by gained(6)Gained alcohol fermentation liquid is according to 5:8 volume ratio mixes Zymotic fluid, by zymotic fluid:The volume ratio of acetic acid bacteria solution is 10:2~10:5 ratio adds the acetic acid bacteria that mass concentration is 80% Solution, stirs evenly, and is placed in fermentation tank and seals, and at 32 ± 1 DEG C, acetic acid fermentation liquid after continuously fermenting 4 ~ 6 days, is pressed temperature control Acetic acid fermentation liquid:The volume ratio of NaCl solution is 1:8 ratio adds the NaCl solution that mass concentration is 15%;
Wherein, the step(7)In acetic acid bacteria solution be solution that acetic acid bacteria is prepared after activation culture, acetic acid bacteria activation Method uses the prior art;
(8)By step(7)Gained acetic acid fermentation liquid crosses 80 ~ 120 mesh sieves, adds PVPP slurries and chitosan slurries, wherein, acetic acid Zymotic fluid:PVPP slurries:The mass ratio of chitosan slurries is 100: 6~12 :5, after standing 15 ~ 20h, cross 200-300 Mesh sieve, obtains acetic fermentation clarified solution, sterilizes at 80 ~ 95 DEG C, filling, obtains bee honey health-care vinegar finished product;
Wherein, the step(8)In PVPP be crosslinked polyvinylpyrrolidone, also known as crospovidone, in the present invention by Used as fining agent.
Preferably, the step(4)In, medicinal herb components weigh by weight, are respectively:30 ~ 70 parts of grasswort, thief son's leaf 20 ~ 65 parts, disappear 35 ~ 75 parts of Rong certainly, 32 ~ 70 parts of Chinese milk vetch, 15 ~ 49 parts of bitter fleabane, 10 ~ 22 parts of water hyacinth, 23 ~ 45 parts of rabdosia lophanthide.
Preferably, the step(4)In, medicinal herb components weigh by weight, are respectively:45 parts of grasswort, thief son's leaf 32 Part, disappear 43 parts of Rong certainly, 51 parts of Chinese milk vetch, 34 parts of bitter fleabane, 18 parts of water hyacinth, 35 parts of rabdosia lophanthide.
Preferably, the step(8)In, the preparation method of PVPP slurries is:PVPP presses 1g with deoxidized water:The ratio of 1.2mL Example mixing, stands 0.8 ~ 1h, after stirring evenly to obtain the final product;The preparation method of chitosan slurries is:Chitosan presses 1g with pure water: The ratio mixing of 2mL, stirs evenly, after 3 ~ 5h of standing to obtain the final product.
The present invention has the following advantages:
(1)In inventive formulation, grasswort and water hyacinth component are added, makes gained bee honey health-care vinegar that there is the work(for promoting gastrointestinal disturbances Energy;The addition of crafty son's leaf, disappear certainly Rong and Chinese milk vetch makes it have the effect of promoting blood circulation and removing blood stasis at the same time;In addition, formula in using honey as Main component, while wheat and glutinous rice slurries are added, solving vinegar generally has irritation tart flavour, and excessive edible rear stomach has The problem of cusalgia sense of discomfort, and make fragrant and sweet taste and wheat of the gained health-care vinegar with honey fragrant and rice perfume (or spice) fragrance;
(2)Technical solution of the present invention carries out at low temperature, not only ensure that the original nutritional ingredient of honey is not destroyed, but also Contain natural anti-oxidation component in honey so that during health-care vinegar is prepared, do not adding any preservative or antioxidant While also can guarantee that the Organic nutrient wherein contained is not oxidized, ensure that product color is delicious, and extend storage period; In addition, medicinal herb components are extracted using the ethanol solution of low concentration, heating is stirred continuously in extraction process, not only ensure that Chinese medicine Active ingredient can effectively be dissolved, and is stirred continuously in heating process, make containing alcohol component constantly volatilization totally, protect Demonstrate,prove in gained extracting solution and be free of ethanol liquid, avoided bringing to human body potentially hazardous;Gained bee honey health-care vinegar battalion of the invention Support and enrich, vinegar can be used as also to be eaten for a long time as health-care vinegar.
Embodiment
With reference to specific embodiment, technical scheme is further illustrated.
Embodiment 1
A kind of preparation method of bee honey health-care vinegar, comprises the following steps:
(1)By honey 1 ~ 2h of heating stirring, temperature control crosses 60 mesh at 50 DEG C, removes impurity;
(2)By step(1)Gained honey presses 1g with pure water:The ratio mixing of 5mL, is heated, temperature control exists after stirring evenly 65 ± 2 DEG C, heating time 1.5h;200 mesh sieves are crossed after the completion of heating, obtain pure honey liquid;
(3)Wheat and glutinous rice are taken, by 1:After 2 mass ratio mixing wash clean, by 1g:The ratio of 5mL adds water to be beaten, and crosses 100 mesh Sieve, obtains the mixed serum of wheat and glutinous rice, is placed in 3 ~ 6 DEG C of refrigerating chamber lucifuges and seals up for safekeeping;
(4)Weigh respectively by weight:30 parts of grasswort, 20 parts of leaf of thief son, disappear 35 parts of Rong certainly, 32 parts of Chinese milk vetch, 15 parts of bitter fleabane, phoenix Eye is 10 parts blue, and 23 parts of rabdosia lophanthide, cleans up after mixing, and 1g is pressed for 2% ethanol solution with concentration:The ratio mixing of 10mL, is stirred Mix heating, heating-up temperature is 65 DEG C, heating time 2h, after filtered;Gained filtrate is concentrated into postcooling, controls concentrate Water content is 20% ~ 25%;
(5)By step(3)Gained wheat and glutinous rice mixed serum and step(2)Gained pure honey liquid presses 5:7 volume ratio Zymotic fluid is mixed to obtain, sterilize 25min at 90 DEG C between 20% ~ 35% by adding water management zymotic fluid sugar content, adds after cooling Enter mass concentration for 3% acetum, between the pH to 4 ~ 6 for adjusting zymotic fluid;
(6)By step(5)Gained zymotic fluid is placed in fermentation tank, is 2g by solid-liquid ratio:It is dry that the ratio of 10L adds grape wine activity Sealed after yeast, temperature control is taken out at 20 ± 2 DEG C after continuously fermenting 5 ~ 7 days, crosses 50 mesh sieves, obtains alcohol fermentation liquid;
(7)By step(4)Chinese herbal medicine concentrate and step obtained by gained(6)Gained alcohol fermentation liquid is according to 5:8 volume ratio is mixed Zymotic fluid is closed to obtain, by zymotic fluid:The volume ratio of acetic acid bacteria solution is 10:The acetic acid that 2 ratio addition mass concentration is 80% Bacterium solution, stirs evenly, and is placed in fermentation tank and seals, and temperature control is at 32 ± 1 DEG C, acetic acid fermentation liquid after continuously fermenting 4 ~ 6 days, By acetic acid fermentation liquid:The volume ratio of NaCl solution is 1:8 ratio adds the NaCl solution that mass concentration is 15%;
Wherein, the step(7)The activation method of middle acetic acid bacteria is:
A. storage medium is prepared:Following component is weighed respectively:Glucose 5g, yeast extract 5g, CaCO310g, agar 10g, adds Enter 500mL distilled water, stirring sterilizes to after dissolving, and sterilising temp is 95 ~ 100 DEG C, sterilization time 15min;70 DEG C after sterilizing 3 ~ 4 drop ethanol solutions are added dropwise;
B. activation medium is prepared:Following component is weighed respectively:Glucose 5g, yeast extract 5g, add 500mL distilled water, stirring Sterilize after to dissolving, sterilising temp is 95 ~ 100 DEG C, sterilization time 15min;70 DEG C plus 40mL of absolute ethyl alcohol is molten after sterilizing Liquid;
C. acetic acid bacteria strain activates:Acetic acid bacteria preservation of bacteria strain carries out slant activation, activation temperature 32 first on storage medium DEG C, soak time 24h, after be transferred in acetic acid bacteria activation medium, carry out shaking table culture, 32 DEG C of cultivation temperature, incubation time 24h, shaking speed are set as 220r/min;
D. acetic acid bacterium solution obtained by step c and distilled water are pressed 4:5 volume ratio mixing, is prepared the vinegar that mass concentration is 80% Sour bacterium solution;
(8)By step(7)Gained acetic acid fermentation liquid crosses 80 mesh sieves, and 6% PVPP slurries and 5% chitosan are added by its volume ratio Slurries;After standing 15 ~ 20h, 200-300 mesh sieves are crossed, acetic fermentation clarified solution is obtained, sterilizes at 80 ~ 95 DEG C, it is filling, obtain bee Sweet health-care vinegar finished product;
Wherein, the preparation method of the PVPP slurries is:PVPP presses 1g with deoxidized water:The ratio mixing of 1.2mL, after stirring evenly Stand 0.8 ~ 1h, to obtain the final product;The preparation method of chitosan slurries is:Chitosan presses 1g with pure water:The ratio mixing of 2mL, stirring Uniformly, after 3 ~ 5h of standing to obtain the final product.
Embodiment 2
A kind of preparation method of bee honey health-care vinegar, comprises the following steps:
(1)By honey 1 ~ 2h of heating stirring, temperature control crosses 40 mesh at 35 DEG C, removes impurity;
(2)By step(1)Gained honey presses 1g with pure water:The ratio mixing of 10mL, is heated, temperature control exists after stirring evenly 65 ± 2 DEG C, heating time 3h;300 mesh sieves are crossed after the completion of heating, obtain pure honey liquid;
(3)Wheat and glutinous rice are taken, by 1:After 2 mass ratio mixing wash clean, by 1g:The ratio of 5mL adds water to be beaten, and crosses 150 mesh Sieve, obtains the mixed serum of wheat and glutinous rice, is placed in 3 ~ 6 DEG C of refrigerating chamber lucifuges and seals up for safekeeping;
(4)Weigh respectively by weight:70 parts of grasswort, 65 parts of leaf of thief son, disappear 75 parts of Rong certainly, 70 parts of Chinese milk vetch, 49 parts of bitter fleabane, phoenix Eye is 22 parts blue, 45 parts of rabdosia lophanthide, is uniformly mixed, cleans up, and 1g is pressed for 2% ethanol solution with concentration:The ratio of 10mL is mixed Close, agitating and heating, heating-up temperature be 80 DEG C, heating time is 2 ~ 3h, after filtered;Gained filtrate is concentrated into postcooling, control Concentrate water content processed is 20% ~ 25%;
(5)By step(3)Gained wheat and glutinous rice mixed serum and step(2)Gained pure honey liquid presses 5:7 volume ratio Zymotic fluid is mixed to obtain, sterilize 30min at 90 DEG C between 20% ~ 35% by adding water management zymotic fluid sugar content, adds after cooling Enter mass concentration for 3% acetum, between the pH to 4 ~ 6 for adjusting zymotic fluid;
(6)By step(5)Gained zymotic fluid is placed in fermentation tank, is 6g by solid-liquid ratio:It is dry that the ratio of 10L adds grape wine activity Sealed after yeast, temperature control is taken out at 20 ± 2 DEG C after continuously fermenting 5 ~ 7 days, crosses 70 mesh sieves, obtains alcohol fermentation liquid;
(7)By step(4)Chinese herbal medicine concentrate and step obtained by gained(6)Gained alcohol fermentation liquid is according to 5:8 volume ratio is mixed Zymotic fluid is closed to obtain, by zymotic fluid:The volume ratio of acetic acid bacteria solution is 10:The acetic acid that 5 ratio addition mass concentration is 80% Bacterium solution, stirs evenly, and is placed in fermentation tank and seals, and temperature control is at 32 ± 1 DEG C, acetic acid fermentation liquid after continuously fermenting 4 ~ 6 days, By acetic acid fermentation liquid:The volume ratio of NaCl solution is 1:8 ratio adds the NaCl solution that mass concentration is 15%;
(8)By step(7)Gained acetic acid fermentation liquid crosses 80 ~ 120 mesh sieves, and 12% PVPP slurries and 5% are added by its volume ratio Chitosan slurries;After standing 20h, 300 mesh sieves are crossed, acetic fermentation clarified solution is obtained, sterilizes at 80 ~ 95 DEG C, it is filling, obtain honey Health-care vinegar finished product;
Wherein, the preparation method of PVPP slurries is:PVPP presses 1g with deoxidized water:The ratio mixing of 1.2mL, stirs evenly rear quiet Set to 0 .8 ~ 1h, to obtain the final product;The preparation method of chitosan slurries is:Chitosan presses 1g with pure water:The ratio mixing of 2mL, stirring are equal It is even, to obtain the final product after standing 5h.
Embodiment 3
A kind of preparation method of bee honey health-care vinegar, comprises the following steps:
(1)By honey 1 ~ 2h of heating stirring, temperature control crosses 60 mesh at 45 DEG C, removes impurity;
(2)By step(1)Gained honey presses 1g with pure water:The ratio mixing of 8mL, is heated, temperature control exists after stirring evenly 65 ± 2 DEG C, heating time 3h;300 mesh sieves are crossed after the completion of heating, obtain pure honey liquid;
(3)Wheat and glutinous rice are taken, by 1:After 2 mass ratio mixing wash clean, by 1g:The ratio of 5mL adds water to be beaten, and crosses 150 mesh Sieve, obtains the mixed serum of wheat and glutinous rice, is placed in 3 ~ 6 DEG C of refrigerating chamber lucifuges and seals up for safekeeping;
(4)Weigh respectively by weight:45 parts of grasswort, 32 parts of leaf of thief son, disappear 43 parts of Rong certainly, 51 parts of Chinese milk vetch, 34 parts of bitter fleabane, phoenix Eye is 18 parts blue, 35 parts of rabdosia lophanthide, is uniformly mixed, cleans up, and 1g is pressed for 2% ethanol solution with concentration:The ratio of 10mL is mixed Close, agitating and heating, heating-up temperature be 78 DEG C, heating time is 2 ~ 3h, after filtered;Gained filtrate is concentrated into postcooling, control Concentrate water content processed is 20% ~ 25%;
(5)By step(3)Gained wheat and glutinous rice mixed serum and step(2)Gained pure honey liquid presses 5:7 volume ratio Zymotic fluid is mixed to obtain, sterilize 30min at 90 DEG C between 20% ~ 35% by adding water management zymotic fluid sugar content, adds after cooling Enter mass concentration for 3% acetum, between the pH to 4 ~ 6 for adjusting zymotic fluid;
(6)By step(5)Gained zymotic fluid is placed in fermentation tank, is 4g by solid-liquid ratio:It is dry that the ratio of 10L adds grape wine activity Sealed after yeast, temperature control is taken out at 20 ± 2 DEG C after continuously fermenting 5 ~ 7 days, crosses 70 mesh sieves, obtains alcohol fermentation liquid;
(7)By step(4)Chinese herbal medicine concentrate and step obtained by gained(6)Gained alcohol fermentation liquid is according to 5:8 volume ratio is mixed Zymotic fluid is closed to obtain, by zymotic fluid:The volume ratio of acetic acid bacteria solution is 10:The acetic acid that 3 ratio addition mass concentration is 80% Bacterium solution, stirs evenly, and is placed in fermentation tank and seals, and temperature control is at 32 ± 1 DEG C, acetic acid fermentation liquid after continuously fermenting 4 ~ 6 days, By acetic acid fermentation liquid:The volume ratio of NaCl solution is 1:8 ratio adds the NaCl solution that mass concentration is 15%;
(8)By step(7)Gained acetic acid fermentation liquid crosses 80 ~ 120 mesh sieves, and 8% PVPP slurries and 5% shell are added by its volume ratio Glycan slurries;After standing 18h, 300 mesh sieves are crossed, acetic fermentation clarified solution is obtained, sterilizes at 80 ~ 95 DEG C, it is filling, obtain honey guarantor Strong vinegar finished product;
Wherein, the preparation method of the PVPP slurries is:PVPP presses 1g with deoxidized water:The ratio mixing of 1.2mL, after stirring evenly Stand 0.8 ~ 1h, to obtain the final product;The preparation method of chitosan slurries is:Chitosan presses 1g with pure water:The ratio mixing of 2mL, stirring Uniformly, after standing 5h to obtain the final product.
The functional evaluation of bee honey health-care vinegar is tested
Control group 1:Bee honey health-care vinegar, preparation method are:Grasswort and water hyacinth are not contained in Chinese herbal medicine formula, remaining component and its Preparation method is the same as embodiment 1;
Control group 2:Bee honey health-care vinegar, preparation method are:Crafty young leaf is not contained in Chinese herbal medicine formula, disappear Rong and Chinese milk vetch certainly, its Remaining component and preparation method thereof is the same as embodiment 1;
Experimental group:Embodiment 1 prepares gained bee honey health-care vinegar.
(1)Zoopery:
Choose Kun Ming mice 30,20 ~ 23g of weight, laboratory bring up 2 days, to adapt to surrounding environment, after be randomly divided into 3 groups, every group 10;
A groups:Blank group, gavage physiological saline, each 2mL, 1 time a day;
B groups:The bee honey health-care vinegar of gavage control group 1, concentration 15%, each 10mL, one time a day;
C groups:The bee honey health-care vinegar of gavage experimental group, concentration 15%, each 10mL, one time a day;
Continuous processing 7 days.The 8th day gastric infusion as stated above is tested, whole mouse are filled with carbon powder mixing suspension after 15min Stomach, given low for 0.1mL/ only, after gavage 30min, put to death, location survey mouse small intestine total length of cutting open the belly, i.e., by whole short necks of mouse Duodenum end to caecum end, measures carbon dust advance distance and calculates propulsion rate;
Carbon dust propulsion rate=carbon dust advance distance(cm)/ total small intestinal length(cm)×100%
Experimental result is as shown in table 1:
Note:Compared with blank group*P 0.05, compared with the control group#P˂0.05
From data in table 1, compared with A groups, B group carbon dust propulsion rates are relatively low(P˂0.05);Compared with B groups, C groups carbon dust promotes Rate significantly improves, and difference has statistical significance(P˂0.05), and close to A group propulsion rates.Therefore can obtain, in inventive formulation, Grasswort and water hyacinth are the key components for promoting enterogastric peristalsis.Promote body stomach compacted so present invention gained health-care vinegar has It is dynamic, improve the function of gastrointestinal disturbances, can solve the problems, such as body constipation;
(2)Fresh animal blood is taken, is put in and condenses at room temperature, stripping and slicing after condensation, ensures that clot volume is identical.Gained clot is random It is divided into 3 groups, every group of clot quantity is consistent, is placed in container;
A groups:The mixed proportion of blank group, addition pure water, clot and pure water is 1g:10mL;
B groups:The bee honey health-care vinegar of control group 2 is added, concentration 50%, clot and its mixed proportion are 1g:10mL;
C groups:The bee honey health-care vinegar of experimental group is added, concentration 50%, clot and its mixed proportion are 1g:10mL;
Tri- groups of test specimens of A, B, C are placed in shaking table culture, simulate human body environment, by temperature control at 36.8 ± 0.1 DEG C, into Row shaking table culture.Experiment is carried out continuously 5 days, is observed and is recorded clot dissolution situation, the results are shown in Table 2:
From phenomenon in table 2, for C groups compared with B groups, it is notable to dissolve the function of clot, therefore, in inventive formulation, thief son's leaf, From Rong is disappeared and three taste traditional Chinese medicine ingredients of Chinese milk vetch are key components promoting blood circulation and removing blood stasis, also explanation present invention gained bee honey health-care vinegar has The effect of promoting blood circulation and removing blood stasis.
Bee honey health-care vinegar nutrient component determining
Control group:Commercially available Shanxi mature vinegar;
Experimental group:Embodiment 1 prepares gained bee honey health-care vinegar;
The nutritional ingredient of measure is respectively:Amino acid, electrolytes and minerals;
Measurement result is as shown in table 3:
From data in table 3, the bee honey health-care vinegar nutritional ingredient prepared by the present invention contains apparently higher than commercially available Shaanxi mature vinegar Have, this component contained in being not only formulated with invention and its configuration proportion are related, and preparation process condition is also critically important factor. Therefore, present invention gained bee honey health-care fruit vinegar is full of nutrition, overcomes the problem of vinegar obtained by traditional handicraft is with single nutrient component.

Claims (4)

  1. A kind of 1. preparation method of bee honey health-care vinegar, it is characterised in that:Comprise the following steps:
    (1)By honey 1 ~ 2h of heating stirring, temperature control crosses 40 ~ 60 mesh at 35 ~ 50 DEG C, removes impurity;
    (2)By step(1)Gained honey presses 1g with pure water:5mL~1g:The ratio mixing of 10mL, is heated, temperature after stirring evenly At 65 ± 2 DEG C, heating time is 1.5 ~ 3h for degree control;200 ~ 300 mesh sieves are crossed after the completion of heating, obtain pure honey liquid;
    (3)Wheat and glutinous rice are taken, by 1:After 2 mass ratio mixing wash clean, by 1g:The ratio of 5mL adds water to be beaten, excessively 100 ~ 150 mesh sieves, obtain the mixed serum of wheat and glutinous rice, are placed in 3 ~ 6 DEG C of refrigerating chamber lucifuges and seal up for safekeeping;
    (4)The young leaf of grasswort, thief, disappear certainly Rong, Chinese milk vetch, bitter fleabane, water hyacinth and rabdosia lophanthide is taken to clean up, with the second that concentration is 2% Alcoholic solution presses 1g:10mL ratio mixing, agitating and heating, heating-up temperature be 65 ~ 80 DEG C, heating time is 2 ~ 3h, after carried out Filter;Gained filtrate is concentrated into postcooling, it is 20% ~ 25% to control concentrate water content;
    (5)Alcoholic fermentation:
    By step(3)Gained wheat and glutinous rice mixed serum and step(2)Gained pure honey liquid presses 5:7 volume ratio mixing Zymotic fluid is obtained, by adding water management zymotic fluid sugar content between 20% ~ 35%, sterilize 25 ~ 30min at 90 DEG C, adds after cooling Enter mass concentration for 3% acetum, between the pH to 4 ~ 6 for adjusting zymotic fluid;
    (6)By step(5)Gained zymotic fluid is placed in fermentation tank, is by solid-liquid ratio(2~6)g :The ratio of 10L adds grape wine Sealed after active dry yeast, temperature control is taken out at 20 ± 2 DEG C after continuously fermenting 5 ~ 7 days, crosses 50 ~ 70 mesh sieves, obtains alcoholic fermentation Liquid;
    (7)Acetic fermentation:
    By step(4)Chinese herbal medicine concentrate and step obtained by gained(6)Gained alcohol fermentation liquid is according to 5:8 volume ratio mixes Zymotic fluid, by zymotic fluid:The volume ratio of acetic acid bacteria solution is 10:2~10:5 ratio adds the acetic acid that mass concentration is 80% Bacterium solution, stirs evenly, and is placed in fermentation tank and seals, and temperature control is at 32 ± 1 DEG C, acetic acid fermentation liquid after continuously fermenting 4 ~ 6 days, By acetic acid fermentation liquid:The volume ratio of NaCl solution is 1:8 ratio adds the NaCl solution that mass concentration is 15%;
    (8)By step(7)Gained acetic acid fermentation liquid crosses 80 ~ 120 mesh sieves, adds PVPP slurries and chitosan slurries, wherein, acetic acid Zymotic fluid:PVPP slurries:The mass ratio of chitosan slurries is 100:(6~12 ):5, after standing 15 ~ 20h, cross 200- 300 mesh sieves, obtain acetic fermentation clarified solution, sterilize at 80 ~ 95 DEG C, filling, obtain bee honey health-care vinegar finished product.
  2. 2. the preparation method of bee honey health-care vinegar according to claim 1, it is characterised in that:The step(4)In, Chinese herbal medicine Component weighs by weight, is respectively:30 ~ 70 parts of grasswort, 20 ~ 65 parts of leaf of thief son, disappear 35 ~ 75 parts of Rong certainly, Chinese milk vetch 32 ~ 70 Part, 15 ~ 49 parts of bitter fleabane, 10 ~ 22 parts of water hyacinth, 23 ~ 45 parts of rabdosia lophanthide.
  3. 3. the preparation method of bee honey health-care vinegar according to claim 1, it is characterised in that:The step(4)In, Chinese herbal medicine Component weighs by weight, is respectively:45 parts of grasswort, 32 parts of leaf of thief son, disappear 43 parts of Rong certainly, 51 parts of Chinese milk vetch, 34 parts of bitter fleabane, phoenix Eye is 18 parts blue, 35 parts of rabdosia lophanthide.
  4. 4. the preparation method of bee honey health-care vinegar according to claim 1 or 2, it is characterised in that:The step(8)In, The preparation method of PVPP slurries is:PVPP presses 1g with deoxidized water:The ratio mixing of 1.2mL, stands 0.8 ~ 1h, i.e., after stirring evenly ;The preparation method of chitosan slurries is:Chitosan presses 1g with pure water:The ratio mixing of 2mL, stirs evenly, stands 3 ~ 5h Afterwards to obtain the final product.
CN201810057888.0A 2018-01-22 2018-01-22 A kind of preparation method of bee honey health-care vinegar Pending CN107904134A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111304044A (en) * 2020-03-31 2020-06-19 白山蜂收蜂制品科技开发有限公司 A nanometer selenium-rich Chinese herbal medicine and Mel fermented health wine and vinegar, and its preparation method and drinking method

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1763169A (en) * 2005-09-30 2006-04-26 孙士尧 Brewing of honey vinegar and nutritious healthy vinegar and method for making vinegar drink
CN102199519A (en) * 2011-03-18 2011-09-28 弓正田 Medicinal vinegar and method for preparing the same
CN102337198A (en) * 2011-10-22 2012-02-01 王姗思 Health care fruit vinegar
CN103205356A (en) * 2013-04-18 2013-07-17 魏巍 Astragalus sinicus vinegar
CN103421671A (en) * 2013-09-09 2013-12-04 张凤平 Method for producing privet vinegar
KR101591708B1 (en) * 2014-08-25 2016-02-04 강주원 The natural brewing vinegarmade use beauveria sp, and its producing method
CN105524822A (en) * 2015-12-28 2016-04-27 贵州赤水黔老翁晒醋有限公司 Rosa roxbunghii honey sun vinegar preparation technology

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1763169A (en) * 2005-09-30 2006-04-26 孙士尧 Brewing of honey vinegar and nutritious healthy vinegar and method for making vinegar drink
CN102199519A (en) * 2011-03-18 2011-09-28 弓正田 Medicinal vinegar and method for preparing the same
CN102337198A (en) * 2011-10-22 2012-02-01 王姗思 Health care fruit vinegar
CN103205356A (en) * 2013-04-18 2013-07-17 魏巍 Astragalus sinicus vinegar
CN103421671A (en) * 2013-09-09 2013-12-04 张凤平 Method for producing privet vinegar
KR101591708B1 (en) * 2014-08-25 2016-02-04 강주원 The natural brewing vinegarmade use beauveria sp, and its producing method
CN105524822A (en) * 2015-12-28 2016-04-27 贵州赤水黔老翁晒醋有限公司 Rosa roxbunghii honey sun vinegar preparation technology

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
徐清萍: "《食醋生产技术问答》", 31 May 2011, 北京:中国纺织出版社 *
方亮: "《药剂学》", 31 March 2016, 北京:中国医药科技出版社 *
顾健: "《中国藏药:汉藏对照》", 31 October 2016, 北京:民族出版社 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111304044A (en) * 2020-03-31 2020-06-19 白山蜂收蜂制品科技开发有限公司 A nanometer selenium-rich Chinese herbal medicine and Mel fermented health wine and vinegar, and its preparation method and drinking method

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Application publication date: 20180413