CN109892500A - A kind of method of lycium ruthenicum juicing - Google Patents
A kind of method of lycium ruthenicum juicing Download PDFInfo
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- CN109892500A CN109892500A CN201910271842.3A CN201910271842A CN109892500A CN 109892500 A CN109892500 A CN 109892500A CN 201910271842 A CN201910271842 A CN 201910271842A CN 109892500 A CN109892500 A CN 109892500A
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- lycium ruthenicum
- black
- wolfberry juice
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Abstract
This application discloses a kind of methods of lycium ruthenicum juicing, comprising the following steps: lycium ruthenicum fresh fruit is removed the medlar fresh fruit surface irregularities by pure water spray with the NaCl aqueous solution pressure pulse cleaning of 10%-15% by S1;S2 air-dries the lycium ruthenicum fresh fruit, removes epidermis moisture content, and freeze preservation is delivered to crusher removal carpopodium when then processing black wolfberry juice, is pumped to beater separation skin seed;S3, the feed liquid isolated are added VC and carry out antioxidation and color-protecting;S4 under conditions of high-pressure homogeneous 25-30MPa pressure, keeps black fruit fructus lycii juice cell wall broken.The present invention is obtained under certain acidity by many experiments, improve heating temperature of the black wolfberry juice in the case where keeping active situation, effectively black wolfberry juice can be sterilized, improve the shelf-life of black wolfberry juice, it ensure that nutrient in black wolfberry juice simultaneously, guarantee the color value stability of black wolfberry juice and the content of anthocyanidin, bacterium can be killed by demonstrating black wolfberry juice in 62-65 degree.
Description
Technical field
The present invention relates to a kind of methods that juice technical field more particularly to lycium ruthenicum are squeezed the juice.
Background technique
The effect of lycium ruthenicum, Tibetan medicine claim " other Ma ", and traditional medicine is about lycium ruthenicum discuss lycium ruthenicum be suitable for soreness and weakness of waist and knees,
It the symptoms such as has a dizzy spell, is bleary-eyed, Tibetan medicine and pharmacology classical " curing in western part four ", " Jingzhubencao " etc. record lycium ruthenicum and cure mainly heart heat
Disease, heart disease, irregular menstruation, menopause etc.." Uygur medicine will " is recorded, and Uygur doctor often uses lycium ruthenicum fruit and root skin to treat
Urethral calculus, Xian scabies, gingiva bleeding gingival hemorrhage etc., civil to be used as strengthening by means of tonics, improving eyesight and hypotensor, the sweet in flavor and neutral in nature of lycium ruthenicum is existing
Generation science also has a large amount of research to have shown that, it being capable of nourishing liver and kidney, benefiting shrewd head and blood-nourishing, the immunity for enhancing people.In addition,
Lycium ruthenicum can liver protection, it is hypoglycemic, softening blood vessel, reduce blood in cholesterol, triglyceride levels, to fatty liver and glycosuria
Patient has certain curative effect.It is proved according to clinical medicine, lycium ruthenicum can also treat chronic renal failure.Lycium ruthenicum can with beauty,
Natural anti-oxidation effect is best.The anthocyanidin being rich in lycium ruthenicum is natural sunlight overcover, can effectively prevent ultraviolet light
Damage to skin.And the procyanidine in lycium ruthenicum can effectively clear the accumulation and precipitating of skin harmful substance free radical,
Delaying human body cell ageing protects collagen, makes skin fresh and alive flexible, keeps younger state, reduces wrinkle, delays to decline
Always.
Therefore, black fruit fructus lycii magma is a kind of good natural food materials of healthcare function, due to lycium ruthenicum fresh fruit it is fresh-keeping when
Between it is short, currently, lycium ruthenicum beverage mostly uses greatly the form that fruit juice is made in lycium ruthenicum to be added in other food materials, eaten for people
With.But during lycium ruthenicum is processed into fruit juice, due to the effect aoxidized in air, tends to occur aoxidize, cause nutrient
The loss of ingredient, and the holding time of black wolfberry juice is short, extends the shelf life and has to sterilize, since lycium ruthenicum magma is rich in flower
Green element, to very temperature sensitive, excessively high sterilization temperature can make the nutriment in lycium ruthenicum lose activity, and it is further contemplated that protecting
Matter phase problem, obtain it is a kind of can extend the shelf life and prevent lycium ruthenicum magma from losing activity, the technology of not brown stain is sent out
It is bright particularly important, for this purpose, we have proposed a kind of methods of lycium ruthenicum juicing.
Summary of the invention
This application provides a kind of method of lycium ruthenicum juicing, solve during lycium ruthenicum is processed into fruit juice, due to
The problem of effect aoxidized in air tends to occur aoxidize, and color value variation causes the loss of nutrient compositions.
This application provides a kind of methods of lycium ruthenicum juicing, comprising the following steps:
Lycium ruthenicum fresh fruit is removed institute by pure water spray with the NaCl aqueous solution pressure pulse cleaning of 10%-15% by S1
State medlar fresh fruit surface irregularities;
S2 air-dries the lycium ruthenicum fresh fruit, removes epidermis moisture content, and freeze preservation conveys when then processing black wolfberry juice
Carpopodium is removed to crusher, is pumped to beater separation skin seed;
S3, the feed liquid isolated are added VC and carry out antioxidation and color-protecting;
S4 under conditions of high-pressure homogeneous 25-30MPa pressure, keeps black fruit fructus lycii juice cell wall broken, passes through accurate filter
Filtering;
S5, the malic acid for adding 0.3% keep pH value to be less than or equal to 4.1, obtain black wolfberry juice simultaneously by supercentrifuge
Carry out light transmittance test;
S6 is packed by bottle placer;
S7, will be filling after black wolfberry juice by 62 DEG C -65 DEG C of temperature, sterilize 30min-40min.
Preferably, the revolving speed of the supercentrifuge is 4700 revs/min.
Preferably, the PH is 4.2.
Preferably, the filter mesh diameter of the beater is 0.5-0.6mm.
Preferably, described to be packaged as vial or flexible package.
Preferably, the concentration of the VC is 0.3%g/L.
Preferably, the optical source wavelength of the transmitance is 620mm, and light transmittance is less than or equal to 30%, and color value is stablized.
From the above technical scheme, this application provides make black with the NaCl aqueous solution pressure pulse cleaning of 10%-15%
Medlar fresh fruit obtains sufficient soaking and washing, to reach comprehensive thorough cleaning effect, then removes surface with pure water spray
Sundries air-dries lycium ruthenicum fresh fruit, removes epidermis moisture content, is delivered to crusher removal carpopodium, is pumped to beater separation skin seed,
Fresh black wolfberry juice is conveniently obtained, the VC that 0.3%g/L is added in the feed liquid isolated carries out antioxidation and color-protecting, improves lycium ruthenicum fresh fruit
The inoxidizability during stoste is produced, prevents from will appear brown stain situation in production process, high-pressure homogeneous 25-30MPa pressure
Under the conditions of, keep black fruit fructus lycii juice cell wall broken, then again by accurate filter, can obtain more limpid and be easier to be inhaled
The wolfberry juice of receipts, the malic acid for adding 0.3% keep PH4.1-4.2, keep the stability of black wolfberry juice, in this section, both
The stability for being able to maintain black wolfberry juice can improve the thermal stability of black wolfberry juice again, when black wolfberry juice during sterilization not
It is devitalized, the black wolfberry juice of light transmittance≤30% (620mm wavelength) is obtained by supercentrifuge, improves the matter of black wolfberry juice
Amount is grouted into 30ml, 50ml, 30ml flexible package sealing, 62 DEG C of -65 DEG C, PH4,1-4.2 energy of sterilization temperature of lycium ruthenicum magma
The bacterium in lycium ruthenicum magma is enough inactivated, and colour-fast, the black wolfberry juice of long shelf-life and nutritional ingredient non-inactivation is made.
The beneficial effects of the present invention are: being obtained under certain acidity by many experiments, improves black wolfberry juice and keeping
Heating temperature in active situation can effectively sterilize black wolfberry juice, improve the shelf-life of black wolfberry juice, simultaneously
It ensure that nutrient in black wolfberry juice, guarantee the color value stability of black wolfberry juice and the content of anthocyanidin, demonstrate lycium ruthenicum
Juice can kill bacterium in 62-65 degree, and the product faint scent of production is swung, and quiet, purple is dense refined, and the exclusive flavor with lycium ruthenicum is dissolved in
Water, mellow in taste, polysaccharides content ﹥ 1.8mg/L, have it is anti-oxidant, build up health, be antifatigue, protection skin elasticity, delay
The miscellaneous function of aging improves the commodity value of lycium ruthenicum, facilitates the development of lycium ruthenicum planting industry, increases local economy
Development level.
Detailed description of the invention
In order to illustrate more clearly of the technical solution of the application, attached drawing needed in case study on implementation will be made below
Simply introduce, it should be apparent that, for those of ordinary skills, in the premise of not making the creative labor property
Under, it is also possible to obtain other drawings based on these drawings.
Fig. 1 is that the oxidation of VC additive under the 620nm wavelength in a kind of method of lycium ruthenicum juicing proposed by the present invention becomes
Spirogram;
Fig. 2 is influence of the temperature to lycium ruthenicum magma color value in a kind of method of lycium ruthenicum juicing proposed by the present invention
Figure.
Specific embodiment
In order to make those skilled in the art better understand the technical solutions in the application, below in conjunction with attached drawing, it is right
Technical solution in the embodiment of the present application is clearly and completely described.
Referring to Fig. 1-2, a kind of method of lycium ruthenicum juicing, comprising the following steps:
S1, by lycium ruthenicum fresh fruit, with the NaCl aqueous solution pressure pulse cleaning of 10%-15%, pressure pulse cleaning has good clear
Effect is washed, NaCl, which is added, can be good at removing the dissolved organic matter on lycium ruthenicum surface, guarantee following process black wolfberry juice
Quality removes medlar fresh fruit surface irregularities by pure water spray;
S2 air-dries lycium ruthenicum fresh fruit, removes epidermis moisture content, and freeze preservation is delivered to brokenly when then processing black wolfberry juice
Broken machine removes carpopodium, is pumped to beater separation skin seed, extracts the Normal juice in lycium ruthenicum, the filter mesh diameter of beater is
0.5-0.6mm;
S3, the lycium ruthenicum Normal juice isolated are added VC and carry out antioxidation and color-protecting, since lycium ruthenicum is rich in anthocyanidin, easily oxygen
Change, brown stain, colour fading are added VC to feed liquid and carry out antioxidation and color-protecting, and the concentration of VC is 0.3%g/L, guarantees black fruit fructus lycii juice color value
Storage rate;
Color value method for measuring is 722 spectrophotometric curve measuring methods;
By the clarification black fruit fructus lycii juice of 100ml under certain temperature environment, taking part stoste to be put into depth is 1cm cuvette
In, light absorption value is measured under 620nm wavelength, the formula for calculating light absorption value is as follows:
A is light absorption value in formula, and W is sample quality ml;
The formula for calculating storage rate is as follows: storage rate (%)=A/A0 × 100, in formula: for treated, light absorption value A0 is A
Light absorption value before processing.
The design scheme of Vc: antioxidation;
The magma for taking 100ml first filters in laboratory by 300 mesh filter cloths;
15 25ml cuvettes are taken, are divided into 5 groups, the black of 20ml difference VC amount is added in every group of 3 Duplicate Samples, each cuvette
Fruit fructus lycii stoste, static 30min-60min measure its light absorption value, black fruit fructus lycii juice color value storage rate are calculated, as black fruit Chinese holly
For Qi stoste to the parameter that the analysis of VC rear stability is added, data are described in Fig. 1;
Under under 620nm wavelength situation, normal temperature environment, by the variable of different Vc, light transmittance is tested, light transmittance is higher, card
Its bright oxidisability is weak;
Brown stain, can all occur in process of production in inoxidizability during same batch lycium ruthenicum fresh fruit production stoste
Journey, oxidation resistant optimum addition add color stability after the Vc of 0.3%g/L as can be seen from Figure 1;
S4 under conditions of high-pressure homogeneous 25-30MPa pressure, keeps black fruit fructus lycii juice cell wall broken, energy after cell wall is broken
Enough make the nutrient of black wolfberry juice be easier to be absorbed, filtered by accurate filter, filters biggish lycium ruthenicum tissue, obtain
Obtain finer black wolfberry juice;
S5, the malic acid for adding 0.3% keep pH value to be less than or equal to 4.1, obtain black wolfberry juice simultaneously by supercentrifuge
Light transmittance test is carried out, the optical source wavelength of transmitance is 620mm, and light transmittance is less than or equal to 30%, and color value is stablized, supercentrifuge
Revolving speed be 4700 revs/min;
Light absorption value of the different PH to black fruit fructus lycii stoste, the influence of storage rate;
Take 15 25ml cuvettes, be divided into 5 groups, every 3 groups are 1 Duplicate Samples, every 3 cuvettes be added pH value be 4.3,
4.2,4.1,4.0,3.9 black fruit fructus lycii stoste places 1 day, 2 days, 3 days, 4 days, 5 days in identical temperature environment, observes its color value
Variation;
First day
PH | Color value | Absorptance | Remarks |
4.3 | 35 | 74.3 | |
4.2 | 33 | 78.8 | |
4.1 | 30 | 86.7 | |
4.0 | 30 | 86.7 | |
3.9 | 30 | 86.7 |
Second day
PH | Color value | Absorptance | Remarks |
4.3 | 35 | 74.3 | |
4.2 | 33 | 78.8 | |
4.1 | 30 | 86.7 | |
4.0 | 30 | 86.7 | |
3.9 | 30 | 86.7 |
Third day
PH | Color value | Absorptance | Remarks |
4.3 | 36 | 72.2 | |
4.2 | 34 | 76.4 | |
4.1 | 30 | 86.7 | |
4.0 | 30 | 86.7 | |
3.9 | 30 | 86.7 |
4th day
PH | Color value | Absorptance | Remarks |
4.3 | 36.5 | 71.2 | |
4.2 | 34 | 76.4 | |
4.1 | 30 | 86.7 | |
4.0 | 30 | 86.7 | |
3.9 | 30 | 86.7 |
5th day
PH | Color value | Absorptance | Remarks |
4.3 | 37 | 70.2 | |
4.2 | 35 | 74.2 | |
4.1 | 30 | 86.7 | |
4.0 | 30 | 86.7 | |
3.9 | 30 | 86.7 |
The situation of change and storage rate of its difference PH color value from 5 days time
PH | Light absorption value | Storage rate | Remarks |
4.3 | 35 | 74.3 | |
4.2 | 33 | 78.8 | |
4.1 | 30 | 86.7 | |
4.0 | 30 | 86.7 | |
3.9 | 30 | 86.7 |
From upper table analysis pH value, black fruit fructus lycii magma is more stable below 4.1.
S6 is packed by bottle placer, is packaged as vial or flexible package, is conducive to transport and sterilization preservation;
S7 will be filling after black wolfberry juice by 62 DEG C -65 DEG C of temperature, sterilize 30min-40min;
Temperature measures black fruit fructus lycii magma stability influence
15 25ml cuvettes are taken, are divided into 5 groups, every group of 3 Duplicate Samples, it is former that 20ml black fruit fructus lycii is added in each cuvette
Liquid is placed in 30,35,40,45,50,55,60,65 DEG C of thermostat water baths, stands heating;The light absorption value of each temperature section is measured,
Black fruit fructus lycii juice color value storage rate is calculated, as black fruit fructus lycii stoste to the parameter of thermal stability analysis, as shown in Figure 2;
Temperature DEG C | Light absorption value | Storage rate | Remarks |
30 | 30 | 86.7 | |
35 | 30 | 86.7 | |
40 | 30 | 86.7 | |
50 | 30 | 86.7 | |
55 | 30 | 86.7 | |
60 | 35 | 74.2 | |
65 | 40 | 65.0 | |
70 | 43 | 60.4 |
The influence of black fruit fructus lycii magma light transmittance in temperature environment
By humid test at 55 DEG C hereinafter, black fruit fructus lycii juice light transmittance is constant, it was demonstrated that it is particularly stable, if it exceeds 55 DEG C
Then light transmittance changes very greatly, it was demonstrated that black fruit fructus lycii juice loses very temperature sensitive, activity, and antioxidation gradually weakens;
Since lycium ruthenicum magma is rich in anthocyanidin, very temperature sensitive is changed over time in 55 DEG C of temperatures above, by
Gradient color, black fruit fructus lycii magma color value increase.The problem of shelf-life must be taken into consideration in lycium ruthenicum magma extends the shelf life and has to kill
Bacterium, then the killing bacterium environment of lycium ruthenicum magma in 62 DEG C -65 DEG C can killing activity, occur as soon as contradictory problems, black fruit
Fructus lycii magma can also lose activity in 55 DEG C of temperatures above, and it is further contemplated that shelf-life problem, is tested after study, guarantor can be extended
The matter phase prevents lycium ruthenicum magma from losing activity again, the technology of not brown stain is invented;
Due to being the key point of its shelf-life of black fruit fructus lycii stoste production black fruit fructus lycii stoste, pass through the black fruit Chinese holly of many experiments
Qi stoste is all very sensitive under different temperatures and pH value situation, due to considering the shelf-life of black fruit fructus lycii stoste, explores first
Black fruit fructus lycii stoste is in the variation of temperature (50,55,60,62,65,68,70,72 degree of bacteria inactivations) pH value and black fruit fructus lycii juice
Stability;
Temperature DEG C | 50 | 55 | 60 | 62 | 65 | 68 | 70 | 72 |
Survival probability of bacteria | 1000 | 100 | 100 | 0 | 0 | 0 | 0 | 0 |
PH value | 4.1 | 4.1 | 4.1 | 4.1 | 4.1 | 4.1 | 4.1 | 4.1 |
Light absorption value | 30 | 30 | 30 | 30 | 31 | 33 | 33.5 | 40 |
It summarizes temperature and is kept for 62 DEG C -65 DEG C, sterilize 30min-40min, can inactivate and inhale bacterium, 65 DEG C or more light absorption values
Variation is big, and pH value is adjusted 4.2, and the black fruit fructus lycii magma most stable shelf-life meets fruit-vegetable juice beverage requirement.
The present invention explores a set of black fruit fructus lycii juice since lycium ruthenicum liquid is very sensitive to temperature by up to a hundred tests
In the process technology scheme that some temperature environment least changes colour, reliable foundation is provided for sterilized environment.
From the above technical scheme, with the NaCl aqueous solution pressure pulse cleaning of 10%-15%, obtain lycium ruthenicum fresh fruit
Sufficient soaking and washing to reach comprehensive thorough cleaning effect, then removes surface irregularities with pure water spray, by lycium ruthenicum
Fresh fruit air-dries, and removes epidermis moisture content, is delivered to crusher removal carpopodium, is pumped to beater separation skin seed, conveniently obtains fresh black
Wolfberry juice, the VC that 0.3%g/L is added in the feed liquid isolated carry out antioxidation and color-protecting, improve lycium ruthenicum fresh fruit and produce stoste process
In inoxidizability, prevent from will appear brown stain situation in production process, under conditions of high-pressure homogeneous 25-30MPa pressure, make black fruit
Wolfberry juice cell wall is broken, then again by accurate filter, can obtain more limpid and be easier to absorbed wolfberry juice, add
Add 0.3% malic acid to keep PH4.1-4.2, keeps the stability of black wolfberry juice, in this section, be both able to maintain black wolfberry juice
Stability can improve the thermal stability of black wolfberry juice again, when black wolfberry juice in non-inactivation during sterilization, through excessively high
Fast centrifuge obtains the black wolfberry juice of light transmittance≤30% (620mm wavelength), improves the quality of black wolfberry juice, be grouted into 30ml,
50ml, 30ml flexible package sealing, 62 DEG C -65 DEG C, PH4,1-4.2 of sterilization temperature of lycium ruthenicum magma can inactivate lycium ruthenicum original
Bacterium in slurry, and it is colour-fast, the black wolfberry juice of long shelf-life and nutritional ingredient non-inactivation is made.
Those skilled in the art will readily occur to its of the application after considering specification and practicing application disclosed herein
Its embodiment.This application is intended to cover any variations, uses, or adaptations of the application, these modifications, purposes or
Person's adaptive change follows the general principle of the application and including the undocumented common knowledge in the art of the application
Or conventional techniques.The description and examples are only to be considered as illustrative, and the true scope of the application is pointed out by claim.
It should be understood that the application is not limited to the precise structure that has been described above and shown in the drawings, and
And various modifications and changes may be made without departing from the scope thereof.Above-described the application embodiment is not constituted to this Shen
Please protection scope restriction.
Claims (7)
1. a kind of method of lycium ruthenicum juicing, which comprises the following steps:
Lycium ruthenicum fresh fruit is removed the Chinese holly by pure water spray with the NaCl aqueous solution pressure pulse cleaning of 10%-15% by S1
Qi fresh fruit surface irregularities;
S2 air-dries the lycium ruthenicum fresh fruit, removes epidermis moisture content, and freeze preservation is delivered to brokenly when then processing black wolfberry juice
Broken machine removes carpopodium, is pumped to beater separation skin seed;
S3, the feed liquid isolated are added VC and carry out antioxidation and color-protecting;
S4 under conditions of high-pressure homogeneous 25-30MPa pressure, keeps black fruit fructus lycii juice cell wall broken, passes through accurate filter mistake
Filter;
S5, the malic acid for adding 0.3% keep pH value to be less than or equal to 4.1, obtain black wolfberry juice by supercentrifuge and carry out
Light transmittance test;
S6 is packed by bottle placer;
S7, will be filling after black wolfberry juice by 62 DEG C -65 DEG C of temperature, sterilize 30min-40min.
2. a kind of method of lycium ruthenicum juicing according to claim 1, which is characterized in that the revolving speed of the supercentrifuge
It is 4700 revs/min.
3. a kind of method of lycium ruthenicum juicing according to claim 1, which is characterized in that the PH is 4.2.
4. a kind of method of lycium ruthenicum juicing according to claim 1, which is characterized in that the filter mesh of the beater
Diameter is 0.5-0.6mm.
5. a kind of method of lycium ruthenicum juicing according to claim 1, which is characterized in that described to be packaged as vial or soft
Packaging.
6. a kind of method of lycium ruthenicum juicing according to claim 1, which is characterized in that the concentration of the VC is 0.3%
g/L。
7. a kind of method of lycium ruthenicum juicing according to claim 1, which is characterized in that the optical source wavelength of the transmitance
For 620mm, light transmittance is less than or equal to 30%, and color value is stablized.
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CN110522031A (en) * | 2019-09-27 | 2019-12-03 | 宁夏菊花台枸杞生物科技有限公司 | A kind of full fructus lycii magma oral liquor |
CN112106948A (en) * | 2020-08-28 | 2020-12-22 | 宁夏杞乡生物食品工程有限公司 | Preparation method of cistanche primary pulp |
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CN110522031A (en) * | 2019-09-27 | 2019-12-03 | 宁夏菊花台枸杞生物科技有限公司 | A kind of full fructus lycii magma oral liquor |
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Application publication date: 20190618 |