CN1078808C - Plant pesticide - Google Patents
Plant pesticide Download PDFInfo
- Publication number
- CN1078808C CN1078808C CN96115603A CN96115603A CN1078808C CN 1078808 C CN1078808 C CN 1078808C CN 96115603 A CN96115603 A CN 96115603A CN 96115603 A CN96115603 A CN 96115603A CN 1078808 C CN1078808 C CN 1078808C
- Authority
- CN
- China
- Prior art keywords
- ethanol
- soak
- natural plants
- solvent
- select
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The present invention provides plant insecticide and a manufacturing method thereof. The plant insecticide comprises natural plants, such as nuxvomica, croton, bitter apricot seed, Chinese honeylocust fruit, white pepper, fructus hordei germinatus, etc., active ingredients are soaked out through volatile solvent, such as methanol and ethanol, or the mixed liquor of the volatile solvent and chloroform, and the plant insecticide is formed by mixing the active ingredients. The plant insecticide has strong lethality for crop or plant pests, and has no harm for people, livestock, poultry, fishes, etc.; the disease resistance of plants and crops can be enhanced, and the present invention has the advantages of low cost and no pollution in the process of production.
Description
The invention provides vegetative insecticide and preparation method thereof and using method, belong to technical field of pesticide.
Existing chemical pesticide is because its hypertoxicity, in use often because of operating incorrect cause people, animal, fowl poisoning, and easily on crop, leave residual hazard, cause secondary pollution, environment also there is very big adverse effect, particularly use through the normal phase, make some plant insects produce pesticide resistance, insecticidal effect is also more and more lower.
Purpose of the present invention just provides insecticide and manufacture method and the purposes that a kind of plant is made, and environmentally safe has stronger insecticidal effect, does not stay residual hazard, and harmless to people, animal, fowl, and production process does not have contamination hazard to human body and environment yet.
The object of the present invention is achieved like this:
1. select the natural plants dry product that comprises vomiting nut, crotons, semen armeniacae amarae, Chinese honey locust, white pepper, fructus hordei germinatus for use, pulverize stand-by;
2. select for use volatile solvent soln to make solvent, above-mentioned steps each dry product in is 1. soaked in sealing respectively, and the weight ratio of dry product and solvent is 1: (2-3).Volatile solvent comprises the ethanol of 75% ethanol, methyl alcohol, 95% ethanol or 95% and the mixed liquor that chloroform is made by 1: 3 volume ratio.Each natural plants adopts any immersion in above-mentioned four kinds of solvents, and wherein, the solvent of white pepper, fructus hordei germinatus is preferably selected 95% ethanol for use; The immersion solvent of Chinese honey locust is preferably selected 75% ethanol or methyl alcohol for use; Vomiting nut, crotons, amygdalate immersion solvent are preferably selected 95% ethanol or 95% ethanol and chloroform mixed liquor for use;
3. sealing soak time is 2-15 days.Can be shaken in the immersion process, be soaked effect to strengthen;
4. the soak after 3. step being soaked takes out clear liquid through precipitation behind the filter residue, selects for use wherein at least three kinds to soak clear liquids and press tabulation 1 listed combination and volume parts ratio, and the immersion clear liquid of selecting for use is mixed, and makes vegetable insecticide.
Table 1
The combination sequence number | The vomiting nut soak | The crotons soak | The semen armeniacae amarae soak | The Chinese honey locust soak | The white pepper soak | The fructus hordei germinatus soak |
A | 3-5 | 2-4 | 1.5-2.5 | 0.5-1.5 | 0.3-0.8 | 0.3-1 |
B | 3-5 | 2.5-3.5 | 1.5-2.5 | 0.5-1.5 | 0.3-0.8 | |
C | 3-5 | 2-4 | 1.5-2.8 | 0.5-1.5 | 0.3-0.8 | |
D | 3-5 | 2-4 | 1.5-2.8 | 0.5-1.5 | 0.3-0.8 | |
E | 4-6 | 2-4 | 1.5-2.8 | 0.3-0.8 | ||
F | 4-6 | 2-4 | 1-3 | |||
G | 4-6 | 2-4 | 1-3 |
The vegetable insecticide of the present invention that said method is made should seal preservation in the cool.During use, with clear water dilution 500-1500 doubly, preferably dilute 500-1000 doubly, be used for crops or plant-spraying.Muddiness may occur in the preservation process, through shaking muddy can the disappearance, muddiness or small amount of precipitate occurring does not influence use, and precipitation mainly is because of filter residue does not thoroughly form, and the filtering precipitation gets final product during use, in order to avoid stop up the instrument that sprays.
The desinsection of vegetable insecticide of the present invention is renderd a service, and is subjected to applying environment temperature effect that minor variations is arranged, and when temperature improved, desinsection is renderd a service to be increased, and can cross the variation among a small circle of diluted concentration and regulate when dilution.
Vegetable insecticide of the present invention also can add the emulsifier that is no more than vegetable insecticide total amount 5% and be used, and to strengthen spray effect, emulsifier is farming breast No. 500 or a dodecyl laruyl alcohol.
Vegetable insecticide of the present invention can extensively be applied to crops and plant and insect is had kill effect significantly.Active component content is low in this insecticide, and is all harmless to people, animal, fowl, fish through dilution more than 500 times when particularly spraying.Facts have proved the resistance against diseases that can also strengthen crops or plant after spraying.
Below be vegetable insecticide insecticidal test result of the present invention, reach and agricultural chemicals contrast and experiment such as phoxim, 1605, nuvacron, be test mean value 10-30 time.Vegetable insecticide, phoxim, 1605, nuvacron dilute 1000 times respectively in the experiment, and spraying imposes on crops or the plant.
Experimental result one: (33 ℃ of temperature)
Object is: 3-5 cotton bollworm in age, 4-5 cabbage caterpillar in age, and vegetable insecticide was knocked down insect in 25 minutes, and insect dead 75% in 3 hours.12 hours insects of nuvacron are dead 21%, 12 hours insects dead 25% of phoxim.
Experimental result two: (temperature 28-30 ℃)
Object is: 3-4 cotton bollworm in age, 4-5 cabbage caterpillar in age, stinkbug etc., and vegetable insecticide was knocked down insect in 36 minutes, and insect dead 50% in 3 hours.160512 hours insects dead 50% of agricultural chemicals.
Experimental result three: (32.5 ℃ of temperature)
Object is: 3-5 cotton bollworm in age, caterpillar, 3-5 cabbage caterpillar in age, and vegetable insecticide was knocked down insect in 20 minutes, and insect dead 95% in 4 hours.12 hours insects dead 20% of nuvacron.
Experimental result four: (33 ℃ of temperature)
Object is: 3-4 cotton bollworm in age, pink bollworm, 4-5 cabbage caterpillar in age, 3 hours insects dead 65% of vegetable insecticide.160512 hours insects dead 24% of agricultural chemicals.
Experimental result five: (31 ℃ of temperature)
Object is: 1-3 codling moth in age, 1-4 pear leaf worm, and vegetable insecticide was knocked down insect in 25 minutes, and insect dead 92.7% in 12 hours.
Experimental result six: (29 ℃ of temperature)
Object is: 1-3 codling moth in age, 1-4 pear leaf worm, and vegetable insecticide was knocked down insect in 36 minutes, and insect dead 67.2% in 12 hours.
Experimental result seven: (temperature 26-27 ℃)
Object is: stinkbug, cotton bollworm, and vegetable insecticide, stinkbug was knocked down in 40 minutes, 3 hours dead 50%; 4-5 cotton bollworm in age was knocked down in 27 minutes, 12 hours dead 53%; 2 ages, cotton instar was knocked down 12 hours dead 57% in 10 minutes.12 hours insects average dead 42% of phoxim.
Experimental result eight: (31 ℃ of temperature)
Object is: 3-5 bean worm in age, caterpillar, 3-5 cabbage caterpillar in age, and vegetable insecticide was knocked down insect in 20 minutes, and insect dead 95% in 4 hours.12 hours insects dead 20% of nuvacron.
Embodiment one
Select solvent and ratio for use and select for use soak and mixed proportion to see the following form:
Natural plants | Natural plants with select the weight of solvent ratio for use | Select soaking solution and portion rate for use | |||
95% ethanol | 95% ethanol and chloroform mixed liquor | Methyl alcohol | 75% ethanol | ||
Vomiting nut | 1∶2.5 | 4 | |||
Crotons | 1∶2.6 | 3 | |||
Semen armeniacae amarae | 1∶2.6 | 2 | |||
Chinese honey locust | 1∶2.6 | 1 | |||
White pepper | 1∶2.6 | 0.5 | |||
Fructus hordei germinatus | 1∶2.5 | 0.5 |
Be mixed and made into vegetable insecticide in listed natural plants soak and the ratio of selecting for use of this table.Be used for crops or plant through 1000 times of clear water dilutions.
Embodiment two
Select solvent and ratio for use and select for use soak and mixed proportion to see the following form:
Natural plants | Natural plants with select the weight of solvent ratio for use | Select soaking solution and portion rate for use | |||
95% ethanol | 95% ethanol and chloroform mixed liquor | Methyl alcohol | 75% ethanol | ||
Vomiting nut | 1∶2.5 | 4 | |||
Crotons | 1∶2.6 | 3 | |||
Semen armeniacae amarae | 1∶2.6 | 2 | |||
Chinese honey locust | 1∶2.6 | 1 | |||
White pepper | 1∶2.6 | 0.5 | |||
Fructus hordei germinatus | 1∶2.5 | 0.5 |
Be mixed and made into vegetable insecticide in listed natural plants soak and the ratio of selecting for use of this table.Be used for crops or plant through 1500 times of clear water dilutions.
Embodiment three
Select solvent and ratio for use and select for use soak and mixed proportion to see the following form:
Natural plants | Natural plants with select the weight of solvent ratio for use | Select soaking solution and portion rate for use | |||
95% ethanol | 95% ethanol and chloroform mixed liquor | Methyl alcohol | 75% ethanol | ||
Vomiting nut | 1∶2 | 3 | |||
Crotons | 1∶2 | 2 | |||
Semen armeniacae amarae | 1∶3 | 2.5 | |||
Chinese honey locust | 1∶2 | 0.5 | |||
White pepper | 1∶3 | 0.8 | |||
Fructus hordei germinatus | 1∶3 | 1 |
Be mixed and made into vegetable insecticide in listed natural plants soak and the ratio of selecting for use of this table.Be used for crops or plant through 500 times of clear water dilutions.
Embodiment four
Select solvent and ratio for use and select for use soak and mixed proportion to see the following form:
Natural plants | Natural plants with select the weight of solvent ratio for use | Select soaking solution and portion rate for use | |||
95% ethanol | 95% ethanol and chloroform mixed liquor | Methyl alcohol | 75% ethanol | ||
Vomiting nut | 1∶3 | 5 | |||
Crotons | 1∶3 | 4 | |||
Semen armeniacae amarae | 1∶2 | 1.5 | |||
Chinese honey locust | 1∶3 | 1.5 | |||
White pepper | 1∶2 | 0.3 | |||
Fructus hordei germinatus | 1∶3 | 1 |
Be mixed and made into vegetable insecticide in listed natural plants soak and the ratio of selecting for use of this table.Be used for crops or plant through 1000 times of clear water dilutions.
Embodiment five
Select solvent and ratio for use and select for use soak and mixed proportion to see the following form:
Natural plants | Natural plants with select the weight of solvent ratio for use | Select soaking solution and portion rate for use | |||
95% ethanol | 95% ethanol and chloroform mixed liquor | Methyl alcohol | 75% ethanol | ||
Vomiting nut | 1∶2.5 | 4 | |||
Crotons | 1∶2.6 | 3 | |||
Semen armeniacae amarae | 1∶2.6 | 2 | |||
Chinese honey locust | |||||
White pepper | 1∶2.6 | 1 | |||
Fructus hordei germinatus | 1∶2.5 | 0.5 |
Be mixed and made into vegetable insecticide in listed natural plants soak and the ratio of selecting for use of this table.Be used for crops or plant through 1000 times of clear water dilutions.
Embodiment six
Select solvent and ratio for use and select for use soak and mixed proportion to see the following form:
Natural plants | Natural plants with select the weight of solvent ratio for use | Select soaking solution and portion rate for use | |||
95% ethanol | 95% ethanol and chloroform mixed liquor | Methyl alcohol | 75% ethanol | ||
Vomiting nut | 1∶2.5 | 4 | |||
Crotons | 1∶2.6 | 3 | |||
Semen armeniacae amarae | 1∶2.6 | 2 | |||
Chinese honey locust | |||||
White pepper | 1∶2.6 | 1 | |||
Fructus hordei germinatus | 1∶2.5 | 0.5 |
Be mixed and made into vegetable insecticide in listed natural plants soak and the ratio of selecting for use of this table.Be used for crops or plant through 1000 times of clear water dilutions.
Embodiment seven
Select solvent and ratio for use and select for use soak and mixed proportion to see the following form:
Natural plants | Natural plants with select the weight of solvent ratio for use | Select soaking solution and portion rate for use | |||
95% ethanol | 95% ethanol and chloroform mixed liquor | Methyl alcohol | 75% ethanol | ||
Vomiting nut | 1∶2 | 3 | |||
Crotons | 1∶2 | 2.5 | |||
Semen armeniacae amarae | 1∶3 | 2.5 | |||
Chinese honey locust | |||||
White pepper | 1∶3 | 1.5 | |||
Fructus hordei germinatus | 1∶2 | 0.3 |
Be mixed and made into vegetable insecticide in listed natural plants soak and the ratio of selecting for use of this table.Be used for crops or plant through 1000 times of clear water dilutions.
Embodiment eight
Select solvent and ratio for use and select for use soak and mixed proportion to see the following form:
Natural plants | Natural plants with select the weight of solvent ratio for use | Select soaking solution and portion rate for use | |||
95% ethanol | 95% ethanol and chloroform mixed liquor | Methyl alcohol | 75% ethanol | ||
Vomiting nut | 1∶3 | 5 | |||
Crotons | 1∶3 | 3.5 | |||
Semen armeniacae amarae | 1∶2 | 1.5 | |||
Chinese honey locust | |||||
White pepper | 1∶2 | 0.5 | |||
Fructus hordei germinatus | 1∶3 | 0.8 |
Be mixed and made into vegetable insecticide in listed natural plants soak and the ratio of selecting for use of this table.Be used for crops or plant through 1000 times of clear water dilutions.
Embodiment nine
Select solvent and ratio for use and select for use soak and mixed proportion to see the following form:
Be mixed and made into vegetable insecticide in listed natural plants soak and the ratio of selecting for use of this table.Be used for crops or plant through 1000 times of clear water dilutions.
Natural plants | Natural plants with select the weight of solvent ratio for use | Select soaking solution and portion rate for use | |||
95% ethanol | 95% ethanol and chloroform mixed liquor | Methyl alcohol | 75% ethanol | ||
Vomiting nut | 1∶2.5 | 4 | |||
Crotons | |||||
Semen armeniacae amarae | 1∶2.6 | 3 | |||
Chinese honey locust | 1∶2.6 | 2 | |||
White pepper | 1∶2.6 | 1 | |||
Fructus hordei germinatus | 1∶2.5 | 0.5 |
Embodiment ten
Select solvent and ratio for use and select for use soak and mixed proportion to see the following form:
Natural plants | Natural plants with select the weight of solvent ratio for use | Select soaking solution and portion rate for use | |||
95% ethanol | 95% ethanol and chloroform mixed liquor | Methyl alcohol | 75% ethanol | ||
Vomiting nut | 1∶2 | 3 | |||
Crotons | |||||
Semen armeniacae amarae | 1∶2 | 2 | |||
Chinese honey locust | 1∶2 | 1.5 | |||
White pepper | 1∶2 | 0.5 | |||
Fructus hordei germinatus | 1∶2 | 0.3 |
Be mixed and made into vegetable insecticide in listed natural plants soak and the ratio of selecting for use of this table.Be used for crops or plant through 1000 times of clear water dilutions.
Embodiment 11
Select solvent and ratio for use and select for use soak and mixed proportion to see the following form:
Natural plants | It plant with select the weight of solvent ratio for use | Select soaking solution and portion rate for use | |||
95% ethanol | 95% ethanol and chloroform mixed liquor | Methyl alcohol | 75% ethanol | ||
Vomiting nut | 1∶3 | 5 | |||
Crotons | |||||
Semen armeniacae amarae | 1∶3 | 4 | |||
Chinese honey locust | 1∶3 | 2.8 | |||
White pepper | 1∶3 | 1.5 | |||
Fructus hordei germinatus | 1∶3 | 1 |
Be mixed and made into vegetable insecticide in listed natural plants soak and the ratio of selecting for use of this table.Be used for crops or plant through 1000 times of clear water dilutions.
Embodiment 12
Select solvent and ratio for use and select for use soak and mixed proportion to see the following form:
Natural plants | Natural plants with select the weight of solvent ratio for use | Select soaking solution and portion rate for use | |||
95% ethanol | 95% ethanol and chloroform mixed liquor | Methyl alcohol | 75% ethanol | ||
Vomiting nut | |||||
Crotons | 1∶2.6 | 4 | |||
Semen armeniacae amarae | 1∶2.6 | 3 | |||
Chinese honey locust | 1∶2.6 | 2 | |||
White pepper | 1∶2.6 | 1 | |||
Fructus hordei germinatus | 1∶2.5 | 0.5 |
Be mixed and made into vegetable insecticide in listed natural plants soak and the ratio of selecting for use of this table.Be used for crops or plant through 1000 times of clear water dilutions.
Embodiment 13
Select solvent and ratio for use and select for use soak and mixed proportion to see the following form:
Natural plants | Natural plants with select the weight of solvent ratio for use | Select soaking solution and portion rate for use | |||
95% ethanol | 95% ethanol and chloroform mixed liquor | Methyl alcohol | 75% ethanol | ||
Vomiting nut | |||||
Crotons | 1∶2 | 3 | |||
Semen armeniacae amarae | 1∶2 | 2 | |||
Chinese honey locust | 1∶2 | 1.5 | |||
White pepper | 1∶2 | 0.5 | |||
Fructus hordei germinatus | 1∶2 | 0.3 |
Be mixed and made into vegetable insecticide in listed natural plants soak and the ratio of selecting for use of this table.Be used for crops or plant through 1000 times of clear water dilutions.
Embodiment 14
Select solvent and ratio for use and select for use soak and mixed proportion to see the following form:
Natural plants | Natural plants with select the weight of solvent ratio for use | Select soaking solution and portion rate for use | |||
95% ethanol | 95% ethanol and chloroform mixed liquor | Methyl alcohol | 75% ethanol | ||
Vomiting nut | |||||
Crotons | 1∶3 | 5 | |||
Semen armeniacae amarae | 1∶3 | 4 | |||
Chinese honey locust | 1∶3 | 2.8 | |||
White pepper | 1∶3 | 1.5 | |||
Fructus hordei germinatus | 1∶3 | 1 |
Be mixed and made into vegetable insecticide in listed natural plants soak and the ratio of selecting for use of this table.Be used for crops or plant through 1000 times of clear water dilutions.
Embodiment 15
Select solvent and ratio for use and select for use soak and mixed proportion to see the following form:
Natural plants | Natural plants with select the weight of solvent ratio for use | Select soaking solution and portion rate for use | |||
95% ethanol | 95% ethanol and chloroform mixed liquor | Methyl alcohol | 75% ethanol | ||
Vomiting nut | |||||
Crotons | 1∶2.6 | 5 | |||
Semen armeniacae amarae | 1∶2.6 | 3 | |||
Chinese honey locust | 1∶2.6 | 2 | |||
White pepper | |||||
Fructus hordei germinatus | 1∶2.5 | 0.5 |
Be mixed and made into vegetable insecticide in listed natural plants soak and the ratio of selecting for use of this table.Be used for crops or plant through 1000 times of clear water dilutions.
Embodiment 16
Select solvent and ratio for use and select for use soak and mixed proportion to see the following form:
Natural plants | Natural plants with select the weight of solvent ratio for use | Select soaking solution and portion rate for use | |||
95% ethanol | 95% ethanol and chloroform mixed liquor | Methyl alcohol | 75% ethanol | ||
Vomiting nut | |||||
Crotons | 1∶2 | 4 | |||
Semen armeniacae amarae | 1∶2 | 2 | |||
Chinese honey locust | 1∶2 | 1.5 | |||
White pepper | |||||
Fructus hordei germinatus | 1∶2 | 0.3 |
Be mixed and made into vegetable insecticide in listed natural plants soak and the ratio of selecting for use of this table.Be used for crops or plant through 1000 times of clear water dilutions.
Embodiment 17
Select solvent and ratio for use and select for use soak and mixed proportion to see the following form:
Natural plants | Natural plants with select the weight of solvent ratio for use | Select soaking solution and portion rate for use | |||
95% ethanol | 95% ethanol and chloroform mixed liquor | Methyl alcohol | 75% ethanol | ||
Vomiting nut | |||||
Crotons | 1∶3 | 6 | |||
Semen armeniacae amarae | 1∶3 | 4 | |||
Chinese honey locust | 1∶3 | 2.8 | |||
White pepper | |||||
Fructus hordei germinatus | 1∶3 | 1 |
Be mixed and made into vegetable insecticide in listed natural plants soak and the ratio of selecting for use of this table.Be used for crops or plant through 1000 times of clear water dilutions.
Embodiment 18
Select solvent and ratio for use and select for use soak and mixed proportion to see the following form:
Natural plants | Natural plants with select the weight of solvent ratio for use | Select soaking solution and portion rate for use | |||
95% ethanol | 95% ethanol and chloroform mixed liquor | Methyl alcohol | 75% ethanol | ||
Vomiting nut | |||||
Crotons | 1∶2.6 | 5 | |||
Semen armeniacae amarae | 1∶2.6 | 3 | |||
Chinese honey locust | |||||
White pepper | 1∶2.6 | 2 | |||
Fructus hordei germinatus |
Be mixed and made into vegetable insecticide in listed natural plants soak and the ratio of selecting for use of this table.Be used for crops or plant through 1000 times of clear water dilutions.
Embodiment 19
Select solvent and ratio for use and select for use soak and mixed proportion to see the following form:
Natural plants | Natural plants with select the weight of solvent ratio for use | Select soaking solution and portion rate for use | |||
95% ethanol | 95% ethanol and chloroform mixed liquor | Methyl alcohol | 75% ethanol | ||
Vomiting nut | |||||
Crotons | 1∶2 | 4 | |||
Bitter apricot two | 1∶2 | 2 | |||
Chinese honey locust | |||||
White pepper | 1∶3 | 3 | |||
Fructus hordei germinatus |
Be mixed and made into vegetable insecticide in listed natural plants soak and the ratio of selecting for use of this table.Be used for crops or plant through 1000 times of clear water dilutions.
Embodiment 20
Select solvent and ratio for use and select for use soak and mixed proportion to see the following form:
Natural plants | Natural plants with select the weight of solvent ratio for use | Select soaking solution and portion rate for use | |||
95% ethanol | 95% ethanol and chloroform mixed liquor | Methyl alcohol | 75% ethanol | ||
Vomiting nut | |||||
Crotons | 1∶3 | 6 | |||
Semen armeniacae amarae | 1∶3 | 4 | |||
Chinese honey locust | |||||
White pepper | 1∶2 | 1 | |||
Fructus hordei germinatus |
Be mixed and made into vegetable insecticide in listed natural plants soak and the ratio of selecting for use of this table.Be used for crops or plant through 1000 times of clear water dilutions.
Embodiment 21
Select solvent and ratio for use and select for use soak and mixed proportion to see the following form:
Natural plants | Natural plants with select the weight of solvent ratio for use | Select soaking solution and portion rate for use | |||
95% ethanol | 95% ethanol and chloroform mixed liquor | Methyl alcohol | 75% ethanol | ||
Vomiting nut | |||||
Crotons | 1∶2.6 | 5 | |||
Semen armeniacae amarae | 1∶2.6 | 3 | |||
Chinese honey locust | 1∶2.6 | 2 | |||
White pepper | |||||
Fructus hordei germinatus |
Be mixed and made into vegetable insecticide in listed natural plants soak and the ratio of selecting for use of this table.Be used for crops or plant through 1000 times of clear water dilutions.
Embodiment 22
Select solvent and ratio for use and select for use soak and mixed proportion to see the following form:
Natural plants | Natural plants with select the weight of solvent ratio for use | Select soaking solution and portion rate for use | |||
95% ethanol | 95% ethanol and chloroform mixed liquor | Methyl alcohol | 75% ethanol | ||
Vomiting nut | |||||
Crotons | 1∶2 | 4 | |||
Semen armeniacae amarae | 1∶3 | 4 | |||
Chinese honey locust | 1∶2 | 3 | |||
White pepper | |||||
Fructus hordei germinatus |
Be mixed and made into vegetable insecticide in listed natural plants soak and the ratio of selecting for use of this table.Be used for crops or plant through 1000 times of clear water dilutions.
Embodiment 23
Select solvent and ratio for use and select for use soak and mixed proportion to see the following form:
Natural plants | Natural plants with select the weight of solvent ratio for use | Select soaking solution and portion rate for use | |||
95% ethanol | 95% ethanol and 95% mixed liquor | Methyl alcohol | 75% ethanol | ||
Vomiting nut | |||||
Crotons | 1∶3 | 6 | |||
Semen armeniacae amarae | 1∶2 | 2 | |||
Chinese honey locust | 1∶3 | 1 | |||
White pepper | |||||
Fructus hordei germinatus |
Be mixed and made into vegetable insecticide in listed natural plants soak and the ratio of selecting for use of this table.Be used for crops or plant through 1000 times of clear water dilutions.
Claims (5)
1, a vegetative insecticide, it is characterized in that: this vegetable insecticide is by vomiting nut, crotons, semen armeniacae amarae, Chinese honey locust, white pepper, six kinds of natural plants of fructus hordei germinatus, soak after the volatility soluble solvent soaks mixes composition respectively, wherein said natural plants is 1 with the weight ratio of soaking solvent: (2-3), volatile solvent is methyl alcohol or 75% ethanol or 95% ethanol or 95% ethanol and chloroform mixed liquor, and wherein the volume ratio of 95% ethanol and chloroform mixed liquor is 1: 3.
2, vegetable insecticide as claimed in claim 1 is characterized in that in each soak, and the solvent that immersion vomiting nut, crotons, semen armeniacae amarae are used is 95% ethanol or 95% ethanol and chloroform mixed liquor; The solvent that immersion white pepper, fructus hordei germinatus are used is 95% ethanol; The solvent that the immersion Chinese honey locust is used is 75% ethanol or methyl alcohol.
3, vegetable insecticide as claimed in claim 1 or 2, it is characterized in that: this vegetable insecticide is made up of vomiting nut, crotons, semen armeniacae amarae, Chinese honey locust, white pepper, six kinds of natural plants soaks of fructus hordei germinatus, and wherein the volume parts of each natural plants soak is than being the vomiting nut soak: crotons soak: semen armeniacae amarae soak: Chinese honey locust soak: white pepper soak: fructus hordei germinatus soak=(3-5): (2-4): (1.5-2.5): (0.5-1.5): (0.3-0.8): (0.3-1).
4, the preparation method of vegetable insecticide as claimed in claim 1, it is characterized in that: it is made up of following steps,
(1) vomiting nut, crotons, semen armeniacae amarae, Chinese honey locust, white pepper, six kinds of natural plants dry products of fructus hordei germinatus are pulverized stand-by;
(2) soak white pepper, fructus hordei germinatus respectively with 95% ethanolic solution, the weight ratio of the two dry powder and solvent is 1: (2-3); With the mixed liquor of 95% ethanol or 95% ethanol and chloroform, and ethanol is 1: 3 with chloroform volume parts ratio in the mixed liquor, soaks vomiting nut, crotons, semen armeniacae amarae respectively, and the weight ratio between three and the soaking solution is 1: (2-3); Soak Chinese honey locust with 75% ethanol or methanol solution, Chinese honey locust is 1 with used solution weight ratio: (2-3);
(3) the sealing soak time is 2-15 days, can be shaken in the immersion process, soaks effect to strengthen;
(4) the immersion clear liquid of getting process (3) by a certain percentage mixes and sealing, can form vegetable insecticide.
5, the using method of vegetable insecticide as claimed in claim 1 is characterized in that: this vegetable insecticide after 500-1500 times of clear water dilutions, is applied to crops or plant.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN96115603A CN1078808C (en) | 1996-01-04 | 1996-01-04 | Plant pesticide |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN96115603A CN1078808C (en) | 1996-01-04 | 1996-01-04 | Plant pesticide |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1153599A CN1153599A (en) | 1997-07-09 |
CN1078808C true CN1078808C (en) | 2002-02-06 |
Family
ID=5122836
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN96115603A Expired - Fee Related CN1078808C (en) | 1996-01-04 | 1996-01-04 | Plant pesticide |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN1078808C (en) |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103229786B (en) * | 2012-04-18 | 2014-07-09 | 湖北省文东农业发展有限公司 | Complex organic plant pesticide and preparation method thereof |
CN103385258A (en) * | 2013-08-13 | 2013-11-13 | 崇州市地龙海龙生物制品开发研究所 | Preparation method for environment-friendly insecticide |
CN104472600A (en) * | 2014-11-18 | 2015-04-01 | 罗翼 | Biological insecticide for Chinese cabbage and preparation method thereof |
CN104472602A (en) * | 2014-12-09 | 2015-04-01 | 刘晓 | Biological insecticide used for lettuces and preparation method thereof |
CN105230669A (en) * | 2015-09-18 | 2016-01-13 | 荣成复合材料有限公司 | Novel pesticide |
CN105145657A (en) * | 2015-09-18 | 2015-12-16 | 崇州市地龙海龙生物制品开发研究所 | Environment-friendly mosquito repellent preparing method |
CN105284965A (en) * | 2015-11-12 | 2016-02-03 | 刘均同 | High-efficient nontoxic green pesticide capable of preventing and killing pests and preparation method thereof |
CN106234460A (en) * | 2016-07-15 | 2016-12-21 | 广西顺帆投资有限公司 | A kind of insecticide and preparation method thereof |
CN106689229A (en) * | 2016-12-20 | 2017-05-24 | 郭海桥 | Botanical pesticide and preparation method thereof |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1064389A (en) * | 1991-03-02 | 1992-09-16 | 王杰民 | The preparation of kushenin vegetable insecticide and make usage |
-
1996
- 1996-01-04 CN CN96115603A patent/CN1078808C/en not_active Expired - Fee Related
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1064389A (en) * | 1991-03-02 | 1992-09-16 | 王杰民 | The preparation of kushenin vegetable insecticide and make usage |
Non-Patent Citations (1)
Title |
---|
中药大辞典 第1版 1986.6.1 江苏新医学院,上海科出版社 * |
Also Published As
Publication number | Publication date |
---|---|
CN1153599A (en) | 1997-07-09 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN1155314C (en) | Vegetative insecticidal germicidal agent | |
CN1663380A (en) | Matrine and capsaicin composite pesticide | |
CN1078808C (en) | Plant pesticide | |
CN1113605C (en) | Liquid insecticide as agricultural chemical prepared from natural plant and its preparing process | |
CN106386886A (en) | Environment-friendly pesticide for vegetables, melons and fruits and preparation method thereof | |
CN1134786A (en) | Multi-purpose, no-polution composite agricultural chemicals for plants and method for mfg. same | |
CN1926998A (en) | Vegetable oil insecticide and method of use thereof | |
CN1112106C (en) | Plant-type nimbin insecticide | |
CN104872216A (en) | Plant-source synergist and insect aerosol prepared by same | |
CN1209027C (en) | Pesticide without toxin and public nuisance and its production process | |
CN1317930A (en) | Insecticidal compsn. | |
CN1537432A (en) | Environmental protection type insecticide | |
CN1166295C (en) | Insecticide and acaricide composition containing abamectin | |
CN1317929A (en) | Product and method for improving avian health | |
CN114287450A (en) | Pesticide composition for preventing and treating sugarcane thrips | |
CN1158927C (en) | Prepn. of incense used as herbal mosquito repelling agent | |
CN1184891C (en) | Compound pure Chinese medicine agricultural fungicide | |
KR0148377B1 (en) | Exterminating method of noxious terrestrial and aquatic mollusca | |
CN111066827A (en) | Agent for attracting and killing termites and preparation method thereof | |
CN1059782C (en) | Chemical biological pesticide without public nuisance and its preparing method | |
US20110236589A1 (en) | Novel pest repellant and pesticide composition and method of use | |
CN1169443C (en) | Chlopyrifos and cyromazine pesticide composition | |
CN1557155A (en) | Multiple dispensing acaricide emulsifiable solution | |
CN103755471A (en) | Biogas slurry compound bactericide for preventing and treating leaf mold | |
CN109526990B (en) | Attractant for attracting feeding of red-belly squirrel and preparation method thereof |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
C19 | Lapse of patent right due to non-payment of the annual fee | ||
CF01 | Termination of patent right due to non-payment of annual fee |