CN107879677A - A kind of true mineral varnish of self demixing anti-soil and preparation method thereof - Google Patents
A kind of true mineral varnish of self demixing anti-soil and preparation method thereof Download PDFInfo
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- CN107879677A CN107879677A CN201711140059.0A CN201711140059A CN107879677A CN 107879677 A CN107879677 A CN 107879677A CN 201711140059 A CN201711140059 A CN 201711140059A CN 107879677 A CN107879677 A CN 107879677A
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- mineral varnish
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B26/00—Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
- C04B26/30—Compounds having one or more carbon-to-metal or carbon-to-silicon linkages ; Other silicon-containing organic compounds; Boron-organic compounds
- C04B26/32—Compounds having one or more carbon-to-metal or carbon-to-silicon linkages ; Other silicon-containing organic compounds; Boron-organic compounds containing silicon
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B26/00—Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
- C04B26/02—Macromolecular compounds
- C04B26/04—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C04B26/06—Acrylates
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
- C04B2111/00482—Coating or impregnation materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
- C04B2111/27—Water resistance, i.e. waterproof or water-repellent materials
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Paints Or Removers (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
Abstract
A kind of true mineral varnish of self demixing anti-soil and preparation method thereof, a kind of true mineral varnish of self demixing anti-soil is prepared by adding hydrophobic fiber in true mineral varnish formula system, its concrete component and part by weight are：Water 10 ~ 16.5%；Hydroxyethyl cellulose 0.1 ~ 0.2%；Defoamer 0.2 ~ 0.4%；Multifunctional assistant 0.1 ~ 0.2%；Wetting agent 0.1 ~ 0.15%；Bactericide 0.1 ~ 0.2%；True mineral varnish emulsion 12 ~ 25%；Coalescents 0.5 ~ 2%；Water-repelling agent 0 ~ 2%；Inorganic gel 0.2 ~ 0.4%；Hydrophobic fiber 3 ~ 5%；Color sand 55 ~ 71%.The true mineral varnish of self demixing anti-soil prepared by the present invention has obvious hydrophobicity, improves the contaminated resistance of coating, ensure that the service life of true mineral varnish and outward appearance are persistently beautiful；With obvious superiority of effectiveness, production cost is greatly reduced.
Description
Technical field
The invention belongs to architectural decoration coating material preparation field, and in particular to one kind prepares self demixing anti-soil using hydrophobic fiber
True mineral varnish and preparation method thereof.
Background technology
True mineral varnish product is gradually ripe by the technology such as Developing Extension, its production technology, construction application for many years.With tradition
Dry-hang stone compare, true mineral varnish have construct it is convenient, environment-protecting and non-poisonous, cost is relatively low, decorative effect is numerous excellent close to stone material etc.
Point, welcome by numerous owners and real estate merchant, its accounting in building coating is also improved increasingly, but the resistance to of true mineral varnish is stained with
Dirt be always in industry one be very difficult to solve the problems, such as, or as true mineral varnish continue development bottleneck.
In order to improve the application effect of product, each coatings enterprises develop the true mineral varnish auxiliary products of stain resistant one after another, such as develop
Special cover agent, the true mineral varnish of resistant etc..
Special cover agent improves the resistance to soiling of coating to a certain extent, but due to true mineral varnish rough surface, cover agent is not
It can uniformly brush, cause uneven lustre situation（In addition, holiday, connecing raft and also resulting in uneven lustre）Final effect is influenceed, and
The use of cover agent adds construction cost and construction risk.
The true mineral varnish product of resistant mainly has two kinds：A kind of scheme is using materials such as organosilicon, fluorine carbon emulsions so that true stone
Lacquer coat surface forms hydrophobic layer, is not easy adhesive dust；Another scheme is that photocatalyst material is added in formula system, is utilized
Degradation of the photocatalyst to organic matter so that the organic pollution for being attached to true mineral varnish surface is decomposed and gone with rain-out
Remove, two schemes all have the problem of material cost is higher, and downstream client is not easily accepted by typically, or loses the meaning being widely applied
Justice.
The content of the invention
The invention provides a kind of true mineral varnish of self demixing anti-soil and preparation method thereof, and it is resistance to which overcome current true mineral varnish product
The shortcomings that staiing effect difference, there is the advantages of superpower hydrophobic, contaminated resistance is good, so as to ensure that the decorative effect of true mineral varnish,
Extend its service life.In addition, the true mineral varnish of anti-soil and traditional true mineral varnish production construction technology in the present invention are basic
Identical, cost only slightly improves, and has and is widely applied value, suitable for the decoration on skin surface, has excellent resistance to
The true mineral varnish product of dirty performance, it is widely used in the decoration of exterior wall of the high-grade building such as hotel, villa, office building.
In order to achieve the above object, technical scheme proposed by the present invention is：Dredged by being added in true mineral varnish formula system
A kind of true mineral varnish of self demixing anti-soil is prepared in water cellulose.
A kind of true mineral varnish of self demixing anti-soil, concrete component and part by weight are：
Water：10~16.5%；
Hydroxyethyl cellulose：0.1~0.2%；
Defoamer：0.2~0.4%；
Multifunctional assistant：0.1~0.2%；
Wetting agent：0.1~0.15%；
Bactericide：0.1~0.2%；
True mineral varnish emulsion：12~25%；
Water-repelling agent：0~2%；
Coalescents：0.5~2%；
Inorganic gel：0.2~0.4%；
Hydrophobic fiber：3~5%；
Color sand：55~71%；
The hydroxyethyl cellulose such as EBS451, Aksu；
The true mineral varnish emulsion such as RS-9765, Ahmedabad are rich；TX-100, Tao Shi；
The defoamer is mineral oils product, primarily serves and eliminates caused bubble in true mineral varnish production process, and construction
During caused bubble.Such as Nuo Puke, NXZ；
The multifunctional assistant is alcamines product, for adjusting the pH value of formula system, while plays dispersion moistening effect.Such as
Angus, AMP-95；
The wetting agent is alkyl glymes product, and color stuffing surface is soaked, is easy to melting for the various materials of system
Close, soak substrate surface in work progress in addition, improve the adhesive force of product.Such as Clariant, LCN407；
The bactericide is the compound of OIT and formaldehyde, primarily serves in-can preservation bactericidal action, ensures that product exists
Quality in shelf-life is constant.Such as Sol HF；
The water-repelling agent is wax emulsion, and one layer of hydrophobic membrane is mainly established on true mineral varnish surface, and collaboration hydrophobic fiber plays lotus leaf and dredged
Water acts on, and can not add.The selection of wax emulsion, such as Ning Baidi, R/75；
The coalescents are alkoxide product, reduce the glass transition temperature of emulsion, promote mutually to merge between emulsion particle, are formed
Fine and close paint film.As safe, alcohol ester 12 is moistened in Jiangsu；
The inorganic gel is modified alta-mud, as the anti-settling agent of system, prevents sand and filler from occurring during storage
Precipitated and separated situation, the uniform and stable property of guarantee system.Such as Zhejiang Feng Hong, SMP-HV2, BASF ATTAGEL 40；
The hydrophobic fiber can be one or more combinations in artificial synthetic fiber, hydrophobically modified fiber, mainly in true stone
The micro emulsion lug structure that similar lotus leaf surface is established on surface is painted, to play lotus leaf hydrophobic effect.Such as Hangzhou high-tech, polypropylene fibre
Powder；The fertile China in Lianyun Harbour, hydrophobic glass powder；Hubei Feng Jiashan, modified wollastonite powder；
The color sand is 10-20 mesh, 20-40 mesh, 40-80 mesh or 80-120 mesh coloured silk sand；Wherein, the actual proportioning of color sand needs root
Depending on required color effects, while also to meet the related request of final national standard.Because if being all coarse sand, hole can compare
Greatly, covering power is bad, and dust and water enter coating easily by hole, cause various problems；If all it is fine sand, the matter of coating
Sympathetic unobvious, and fine sand oil absorption is big, and corresponding emulsion amount is with regard to big, and otherwise the hardness of coating and adhesive force do not reach state
Mark requires.
The present invention provides a kind of preparation method of the true mineral varnish of self demixing anti-soil, and specific preparation process is as follows：
1）Appropriate water is added in paint can, opens stirring, rotating speed is controlled at 600 ~ 800 revs/min；
2）The hydroxyethyl cellulose, defoamer, multifunctional assistant, wetting agent, bactericide, true mineral varnish breast are slowly added to successively
Liquid, water-repelling agent, coalescents, inorganic gel, keep rotating speed constant, stir 10 ~ 20 minutes, true mineral varnish glue is prepared, it is stand-by；
3）By step 2）Described in true mineral varnish glue be pumped into agitator tank, rotating speed control at 300 ~ 400 revs/min, then add described in
Color sand, added according to the fineness of color sand order, first refinement sand, rear overstriking sand, keep rotating speed to stir 10 ~ 20 minutes, then add
The hydrophobic fiber, keep rotating speed to stir 5 ~ 10 minutes, the true mineral varnish of self demixing anti-soil is made.
Operation principle：As shown in figure 1, in atomization process is sprayed, a part of hydrophobic fiber sweeps along spray by emulsion and sand
Metope is mapped to, another part then forms the different speeds of service, is pricked in dartlike weapon shape in coating, in the true mineral varnish coating of self demixing anti-soil
In drying process, hydrophobic fiber is because surface hydrophobic gradually migrates to coating surface, while viscosity liter when being dried by coating again
High drag effects so that migration velocity it is slack-off until stagnate, final hydrophobic fiber in " rice shoot state " heeling-in in the coating, shape
Into the micro emulsion lug structure similar to lotus leaf surface, super-hydrophobic effect can be achieved after fully drying to be coated.
The true mineral varnish of self demixing anti-soil, which is prepared, using hydrophobic fiber prepares the most main of true mineral varnish with lotus leaf water-repelling agent is used alone
The difference wanted is that it is to form coating of wax matter hydrophobic membrane in coating surface to prepare true mineral varnish using lotus leaf water-repelling agent, that is, film is dredged
Water, but wax material gradually can be failed in degraded by ultraviolet irradiation out of doors, hydrophobic performance maintains one or two years；And use hydrophobic
Fiber prepares the true mineral varnish of self demixing anti-soil, it is therefore an objective to and lotus leaf micro emulsion lug structure is built in coating surface, is that a kind of structure is hydrophobic, tool
There is permanently hydrophobic effect, service life length, be many decades.
The application method of the true mineral varnish of self demixing anti-soil is：Reasonable adjusting spraying equipment parameters in work progress,
The true mineral varnish of self demixing anti-soil is sprayed into coated thing surface.
The beneficial effects of the invention are as follows：
1）It is micro- that the true mineral varnish of self demixing anti-soil can form similar lotus leaf after the completion of construction, by fully maintenance in coating surface
Structure is seen, there is obvious hydrophobicity, improve the contaminated resistance of coating, the service life and outer light that ensure that true mineral varnish are held
It is beautiful long；
2）The true mineral varnish of anti-soil prepared by addition hydrophobic fiber is using the hydrophobic principle of structure, compared to directly addition water-repelling agent
It is longer using the hydrophobic principle of film, the former service life；
3）Realize same lotus leaf effect, the cost required for adding hydrophobic fiber be independent addition water-repelling agent cost 10% ~
25%, there is obvious superiority of effectiveness, greatly reduce production cost.
Brief description of the drawings
Fig. 1 is the true mineral varnish schematic diagram of self demixing anti-soil of the present invention.
Fig. 2 is that the coating of the true mineral varnish of self demixing anti-soil in the embodiment of the present invention 1 meets water design sketch.
Embodiment
Below in conjunction with the accompanying drawings and embodiment is described in further detail to the present invention, it should be appreciated that these embodiments
It is merely to illustrate the application of the present invention rather than the limitation present invention.
Embodiment one
Water 15.6%；Hydroxyethyl cellulose（ES451）0.15%；Defoamer（NXZ）0.3%；
Multifunctional assistant（AMP-95）0.15%；Wetting agent（LCN407）0.1%；
Bactericide（HF）0.15%；True mineral varnish emulsion（RS9765）12.5%；
Water-repelling agent（R/75）2%；Coalescents（Alcohol ester 12）0.65%；
Inorganic gel（SMP-HV2）0.4%；Hydrophobic fiber（Polypropylene fibre powder）3%；
Color sand 65%.
Specific preparation process is as follows：
1）Appropriate water is added in paint can, opens stirring, rotating speed is controlled at 600 revs/min；
2）Hydroxyethyl cellulose is slowly added to successively（ES451）, defoamer（NXZ）, multifunctional assistant（AMP-95）, wetting agent
（LCN407）, bactericide（HF）, true mineral varnish emulsion（RS9765）, water-repelling agent（R/75）, coalescents（Alcohol ester 12）, it is inorganic solidifying
Glue（SMP-HV2）, keep rotating speed constant, stir 18 minutes, true mineral varnish glue is prepared, it is stand-by；
3）By step 2）Described in true mineral varnish glue be pumped into agitator tank, rotating speed control at 320 revs/min, then add the coloured silk
Sand, added according to the fineness of color sand order, first refinement sand, rear overstriking sand, keep rotating speed to stir 18 minutes, then add described dredge
Water cellulose（Polypropylene fibre powder）, keep rotating speed to stir 8 minutes, the true mineral varnish of self demixing anti-soil be made.
Embodiment two
Water 10.4%；Hydroxyethyl cellulose（ES451）0.15%；Defoamer（NXZ）0.3%；
Multifunctional assistant（AMP-95）0.15%；Wetting agent（LCN407）0.1%；
Bactericide（HF）0.2%；True mineral varnish emulsion（RS9765）16%；
Water-repelling agent（R/75）0%；Coalescents（Alcohol ester 12）0.8%；
Inorganic gel（SMP-HV2）0.4%；Hydrophobic fiber（Hydrophobic glass powder）5%；
Color sand 66.5%.
Specific preparation process is as follows：
1）Appropriate water is added in paint can, opens stirring, rotating speed is controlled at 700 revs/min；
2）Hydroxyethyl cellulose is slowly added to successively（ES451）, defoamer（NXZ）, multifunctional assistant（AMP-95）, wetting agent
（LCN407）, bactericide（HF）, true mineral varnish emulsion（RS9765）, coalescents（Alcohol ester 12）, inorganic gel（SMP-HV2）,
Keep rotating speed constant, stir 15 minutes, true mineral varnish glue is prepared, it is stand-by；
3）By step 2）Described in true mineral varnish glue be pumped into agitator tank, rotating speed control at 350 revs/min, then add the coloured silk
Sand, added according to the fineness of color sand order, first refinement sand, rear overstriking sand, keep rotating speed to stir 15 minutes, then add described dredge
Water cellulose（Hydrophobic glass powder）, keep rotating speed to stir 6 minutes, the true mineral varnish of self demixing anti-soil be made.
Embodiment three
Water 11.8%；Hydroxyethyl cellulose（ES451）0.2%；Defoamer（NXZ）0.3%；
Multifunctional assistant（AMP-95）0.15%；Wetting agent（LCN407）0.1%；
Bactericide（HF）0.15%；True mineral varnish emulsion（TX100）23.5%；
Water-repelling agent（R/75）0%；Coalescents（Alcohol ester 12）1%；
Inorganic gel（ATTAGEL 40）0.3%；Hydrophobic fiber（Modified wollastonite powder）4.5%；
Color sand 58%.
Specific preparation process is as follows：
1）Appropriate water is added in paint can, opens stirring, rotating speed is controlled at 780 revs/min；
2）Hydroxyethyl cellulose is slowly added to successively（ES451）, defoamer（NXZ）, multifunctional assistant（AMP-95）, wetting agent
（LCN407）, bactericide（HF）, true mineral varnish emulsion（TX100）, coalescents（Alcohol ester 12）, inorganic gel（ATTAGEL
40）, keep rotating speed constant, stir 12 minutes, true mineral varnish glue is prepared, it is stand-by；
3）By step 2）Described in true mineral varnish glue be pumped into agitator tank, rotating speed control at 400 revs/min, then add the coloured silk
Sand, added according to the fineness of color sand order, first refinement sand, rear overstriking sand, keep rotating speed to stir 10 minutes, then add described dredge
Water cellulose（Modified wollastonite powder）, keep rotating speed to stir 6 minutes, the true mineral varnish of self demixing anti-soil be made.
As shown in Fig. 2, it is that the coating of the true mineral varnish of self demixing anti-soil in the embodiment of the present invention 1 meets water design sketch, is put in level
When putting and being disposed vertically, it can reach good hydrophobic effect.
The true mineral varnish of self demixing anti-soil prepared by the present invention has obvious hydrophobicity, improves the contaminated resistance of coating,
It ensure that service life and the outward appearance of true mineral varnish are persistently beautiful；With obvious superiority of effectiveness, production cost is greatly reduced.
Described above is only the better embodiment of the present invention, therefore all constructions according to described in present patent application scope,
The equivalent change or modification that feature and principle are done, is included in the range of present patent application.
Claims (4)
1. a kind of true mineral varnish of self demixing anti-soil, it is characterised in that concrete component and part by weight are：
Water 10 ~ 16.5%；Hydroxyethyl cellulose 0.1 ~ 0.2%；Defoamer 0.2 ~ 0.4%；
Multifunctional assistant 0.1 ~ 0.2%；Wetting agent 0.1 ~ 0.15%；Bactericide 0.1 ~ 0.2%；
True mineral varnish emulsion 12 ~ 25%；Coalescents 0.5 ~ 2%；Water-repelling agent 0 ~ 2%；
Inorganic gel 0.2 ~ 0.4%；Hydrophobic fiber 3 ~ 5%；Color sand 55 ~ 71%.
2. a kind of true mineral varnish of self demixing anti-soil according to claim 1, it is characterised in that the hydrophobic fiber is manually to close
Into the one or more combination in fiber, hydrophobically modified fiber, mainly the micro emulsion similar to lotus leaf surface is established on true mineral varnish surface
Lug structure, to play lotus leaf hydrophobic effect.
3. a kind of preparation method of the true mineral varnish of self demixing anti-soil, it is characterised in that specific preparation process is as follows：
1）Appropriate water is added in paint can, opens stirring, rotating speed is controlled at 600 ~ 800 revs/min；
2）The hydroxyethyl cellulose, defoamer, multifunctional assistant, wetting agent, bactericide, true mineral varnish breast are slowly added to successively
Liquid, coalescents, water-repelling agent, inorganic gel, keep rotating speed constant, stir 10 ~ 20 minutes, true mineral varnish glue is prepared, it is stand-by；
3）By step 2）Described in true mineral varnish glue be pumped into agitator tank, rotating speed control at 300 ~ 400 revs/min, then add described in
Color sand, added according to the fineness of color sand order, first refinement sand, rear overstriking sand, keep rotating speed to stir 10 ~ 20 minutes, then add
The hydrophobic fiber, keep rotating speed to stir 5 ~ 10 minutes, the true mineral varnish of self demixing anti-soil is made.
A kind of 4. preparation method of true mineral varnish of self demixing anti-soil according to claim 3, it is characterised in that：It is described to divide certainly
The color and granularity of the layer true mineral varnish of anti-soil can be adjusted by the color and proportion of thin natural colour sand and thick natural colour sand
Section.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711140059.0A CN107879677A (en) | 2017-11-16 | 2017-11-16 | A kind of true mineral varnish of self demixing anti-soil and preparation method thereof |
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| CN201711140059.0A CN107879677A (en) | 2017-11-16 | 2017-11-16 | A kind of true mineral varnish of self demixing anti-soil and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108948876A (en) * | 2018-07-10 | 2018-12-07 | 太仓市美航涂料有限公司 | A kind of preparation method of multi-functional actual granite imitation coating |
| CN108948922A (en) * | 2018-07-10 | 2018-12-07 | 太仓市美航涂料有限公司 | A kind of modified stone paint of surface anti-pollution |
| CN109135434A (en) * | 2018-07-10 | 2019-01-04 | 太仓市美航涂料有限公司 | A kind of multi-functional actual granite imitation coating |
| CN111470843A (en) * | 2020-04-07 | 2020-07-31 | 重庆市好迪涂料有限公司 | Lotus leaf-shaped real stone paint and preparation process thereof |
| CN111876040A (en) * | 2020-07-17 | 2020-11-03 | 中山市华图建筑材料有限公司 | Intelligent high-tech lotus leaf stone-like paint |
| CN115948086A (en) * | 2022-03-28 | 2023-04-11 | 上海涂固安高科技有限公司 | Multifunctional antifouling stone-like paint and application thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108948876A (en) * | 2018-07-10 | 2018-12-07 | 太仓市美航涂料有限公司 | A kind of preparation method of multi-functional actual granite imitation coating |
| CN108948922A (en) * | 2018-07-10 | 2018-12-07 | 太仓市美航涂料有限公司 | A kind of modified stone paint of surface anti-pollution |
| CN109135434A (en) * | 2018-07-10 | 2019-01-04 | 太仓市美航涂料有限公司 | A kind of multi-functional actual granite imitation coating |
| CN111470843A (en) * | 2020-04-07 | 2020-07-31 | 重庆市好迪涂料有限公司 | Lotus leaf-shaped real stone paint and preparation process thereof |
| CN111876040A (en) * | 2020-07-17 | 2020-11-03 | 中山市华图建筑材料有限公司 | Intelligent high-tech lotus leaf stone-like paint |
| CN115948086A (en) * | 2022-03-28 | 2023-04-11 | 上海涂固安高科技有限公司 | Multifunctional antifouling stone-like paint and application thereof |
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Application publication date: 20180406 |