CN107854404A - Sunlight screening skin-protecting product containing Gotu Kola P.E and preparation method thereof - Google Patents
Sunlight screening skin-protecting product containing Gotu Kola P.E and preparation method thereof Download PDFInfo
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- CN107854404A CN107854404A CN201711425032.6A CN201711425032A CN107854404A CN 107854404 A CN107854404 A CN 107854404A CN 201711425032 A CN201711425032 A CN 201711425032A CN 107854404 A CN107854404 A CN 107854404A
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- gotu kola
- protecting product
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- 244000146462 Centella asiatica Species 0.000 title claims abstract description 37
- 235000004032 Centella asiatica Nutrition 0.000 title claims abstract description 37
- 238000012216 screening Methods 0.000 title claims abstract description 24
- 238000002360 preparation method Methods 0.000 title claims description 13
- 239000000284 extract Substances 0.000 claims abstract description 67
- 238000000034 method Methods 0.000 claims abstract description 16
- 241000100289 Lonicera confusa Species 0.000 claims abstract description 15
- 239000002131 composite material Substances 0.000 claims abstract description 15
- 241000050051 Chelone glabra Species 0.000 claims abstract description 14
- 235000013311 vegetables Nutrition 0.000 claims abstract description 14
- HDTRYLNUVZCQOY-UHFFFAOYSA-N α-D-glucopyranosyl-α-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OC1C(O)C(O)C(O)C(CO)O1 HDTRYLNUVZCQOY-UHFFFAOYSA-N 0.000 claims abstract description 9
- FYGDTMLNYKFZSV-URKRLVJHSA-N (2s,3r,4s,5s,6r)-2-[(2r,4r,5r,6s)-4,5-dihydroxy-2-(hydroxymethyl)-6-[(2r,4r,5r,6s)-4,5,6-trihydroxy-2-(hydroxymethyl)oxan-3-yl]oxyoxan-3-yl]oxy-6-(hydroxymethyl)oxane-3,4,5-triol Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC1[C@@H](CO)O[C@@H](OC2[C@H](O[C@H](O)[C@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O FYGDTMLNYKFZSV-URKRLVJHSA-N 0.000 claims abstract description 9
- 229920002498 Beta-glucan Polymers 0.000 claims abstract description 9
- BIVBRWYINDPWKA-VLQRKCJKSA-L Glycyrrhizinate dipotassium Chemical compound [K+].[K+].O([C@@H]1[C@@H](O)[C@H](O)[C@H](O[C@@H]1O[C@H]1CC[C@]2(C)[C@H]3C(=O)C=C4[C@@H]5C[C@](C)(CC[C@@]5(CC[C@@]4(C)[C@]3(C)CC[C@H]2C1(C)C)C)C(O)=O)C([O-])=O)[C@@H]1O[C@H](C([O-])=O)[C@@H](O)[C@H](O)[C@H]1O BIVBRWYINDPWKA-VLQRKCJKSA-L 0.000 claims abstract description 9
- 235000006484 Paeonia officinalis Nutrition 0.000 claims abstract description 9
- HDTRYLNUVZCQOY-WSWWMNSNSA-N Trehalose Natural products O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-WSWWMNSNSA-N 0.000 claims abstract description 9
- 235000018936 Vitellaria paradoxa Nutrition 0.000 claims abstract description 9
- 241001135917 Vitellaria paradoxa Species 0.000 claims abstract description 9
- HDTRYLNUVZCQOY-LIZSDCNHSA-N alpha,alpha-trehalose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-LIZSDCNHSA-N 0.000 claims abstract description 9
- BMRWNKZVCUKKSR-UHFFFAOYSA-N butane-1,2-diol Chemical class CCC(O)CO BMRWNKZVCUKKSR-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229940101029 dipotassium glycyrrhizinate Drugs 0.000 claims abstract description 9
- 229930182478 glucoside Natural products 0.000 claims abstract description 9
- 150000008131 glucosides Chemical class 0.000 claims abstract description 9
- 229940119170 jojoba wax Drugs 0.000 claims abstract description 9
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229940057910 shea butter Drugs 0.000 claims abstract description 9
- 235000015112 vegetable and seed oil Nutrition 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 9
- ZAKOWWREFLAJOT-CEFNRUSXSA-N D-alpha-tocopherylacetate Chemical compound CC(=O)OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C ZAKOWWREFLAJOT-CEFNRUSXSA-N 0.000 claims abstract description 8
- CJZGTCYPCWQAJB-UHFFFAOYSA-L calcium stearate Chemical class [Ca+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O CJZGTCYPCWQAJB-UHFFFAOYSA-L 0.000 claims abstract description 8
- 229940082500 cetostearyl alcohol Drugs 0.000 claims abstract description 8
- 239000008367 deionised water Substances 0.000 claims abstract description 8
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 8
- 239000002994 raw material Substances 0.000 claims abstract description 8
- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 claims abstract description 8
- OULAJFUGPPVRBK-UHFFFAOYSA-N tetratriacontyl alcohol Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCO OULAJFUGPPVRBK-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229940042585 tocopherol acetate Drugs 0.000 claims abstract description 8
- WTVHAMTYZJGJLJ-UHFFFAOYSA-N (+)-(4S,8R)-8-epi-beta-bisabolol Natural products CC(C)=CCCC(C)C1(O)CCC(C)=CC1 WTVHAMTYZJGJLJ-UHFFFAOYSA-N 0.000 claims abstract description 7
- RGZSQWQPBWRIAQ-CABCVRRESA-N (-)-alpha-Bisabolol Chemical compound CC(C)=CCC[C@](C)(O)[C@H]1CCC(C)=CC1 RGZSQWQPBWRIAQ-CABCVRRESA-N 0.000 claims abstract description 7
- 229920002385 Sodium hyaluronate Polymers 0.000 claims abstract description 7
- RGZSQWQPBWRIAQ-LSDHHAIUSA-N alpha-Bisabolol Natural products CC(C)=CCC[C@@](C)(O)[C@@H]1CCC(C)=CC1 RGZSQWQPBWRIAQ-LSDHHAIUSA-N 0.000 claims abstract description 7
- 229940036350 bisabolol Drugs 0.000 claims abstract description 7
- HHGZABIIYIWLGA-UHFFFAOYSA-N bisabolol Natural products CC1CCC(C(C)(O)CCC=C(C)C)CC1 HHGZABIIYIWLGA-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229940010747 sodium hyaluronate Drugs 0.000 claims abstract description 7
- 229920001285 xanthan gum Polymers 0.000 claims abstract description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 41
- 238000000605 extraction Methods 0.000 claims description 29
- 239000000047 product Substances 0.000 claims description 28
- 238000010438 heat treatment Methods 0.000 claims description 15
- 239000000706 filtrate Substances 0.000 claims description 12
- 239000000843 powder Substances 0.000 claims description 12
- 238000010992 reflux Methods 0.000 claims description 12
- 238000007598 dipping method Methods 0.000 claims description 10
- 241000736199 Paeonia Species 0.000 claims description 8
- 239000000419 plant extract Substances 0.000 claims description 8
- 244000003416 Asparagus officinalis Species 0.000 claims description 6
- 235000005340 Asparagus officinalis Nutrition 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 241001570521 Lonicera periclymenum Species 0.000 claims description 5
- 238000001914 filtration Methods 0.000 claims description 5
- 241000167550 Centella Species 0.000 claims description 4
- 150000001875 compounds Chemical class 0.000 claims description 4
- 239000000463 material Substances 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 3
- 229940074410 trehalose Drugs 0.000 claims description 3
- 229940083957 1,2-butanediol Drugs 0.000 claims description 2
- 241000196324 Embryophyta Species 0.000 claims description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- 229940079593 drug Drugs 0.000 claims 1
- 239000003814 drug Substances 0.000 claims 1
- 229940100460 peg-100 stearate Drugs 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- 239000011734 sodium Substances 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 5
- 230000002195 synergetic effect Effects 0.000 abstract description 3
- 244000170916 Paeonia officinalis Species 0.000 abstract 1
- 230000000052 comparative effect Effects 0.000 description 13
- 239000000516 sunscreening agent Substances 0.000 description 11
- 239000002537 cosmetic Substances 0.000 description 9
- 238000012360 testing method Methods 0.000 description 9
- 230000000475 sunscreen effect Effects 0.000 description 8
- 239000007787 solid Substances 0.000 description 4
- MKYBYDHXWVHEJW-UHFFFAOYSA-N N-[1-oxo-1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propan-2-yl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(C(C)NC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 MKYBYDHXWVHEJW-UHFFFAOYSA-N 0.000 description 3
- 238000003556 assay Methods 0.000 description 3
- 230000004224 protection Effects 0.000 description 3
- 206010040880 Skin irritation Diseases 0.000 description 2
- 230000006750 UV protection Effects 0.000 description 2
- 230000001476 alcoholic effect Effects 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 235000013336 milk Nutrition 0.000 description 2
- 239000008267 milk Substances 0.000 description 2
- 210000004080 milk Anatomy 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 231100000475 skin irritation Toxicity 0.000 description 2
- 230000036556 skin irritation Effects 0.000 description 2
- 238000013112 stability test Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 244000020998 Acacia farnesiana Species 0.000 description 1
- 235000003074 Acacia farnesiana Nutrition 0.000 description 1
- 206010015150 Erythema Diseases 0.000 description 1
- 206010020751 Hypersensitivity Diseases 0.000 description 1
- 235000014676 Phragmites communis Nutrition 0.000 description 1
- JSXROLUNEDJZJE-UHFFFAOYSA-N acetic acid;phenol Chemical class CC(O)=O.OC1=CC=CC=C1 JSXROLUNEDJZJE-UHFFFAOYSA-N 0.000 description 1
- 208000026935 allergic disease Diseases 0.000 description 1
- 230000007815 allergy Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 229940081733 cetearyl alcohol Drugs 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 231100000321 erythema Toxicity 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
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- 238000005259 measurement Methods 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 230000005180 public health Effects 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 230000037072 sun protection Effects 0.000 description 1
- 239000006097 ultraviolet radiation absorber Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Dermatology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of sunlight screening skin-protecting product containing Gotu Kola P.E, it is made up of the raw material of following percentage by weight：Composite vegetables extractive 2 5%, peony seed oil 2 5%, hydrogenated jojoba oil 2 6%, shea butter 2 6%, 1,2 butanediols 1 3%, beta glucan 1 3%, cetostearyl alcohol 1 3%, the stearates 2 5% of PEG 100, trehalose 1 2%, saualane 0.5 1.5%, Sodium Hyaluronate 0.05 0.15%, xanthans 0.3 0.6%, tocopherol acetate 0.1 0.5%, dipotassium glycyrrhizinate 0.1 0.2%, bisabolol 0.2 0.4%, cetearyl glucoside 0.2 0.8%, surplus are deionized water.The composite vegetables extractive is made up of the extract of following parts by weight：10 20 parts of Gotu Kola P.E, 15 parts of Thallus Gracilariae extract, 13 parts of Lonicera confusa extract, 38 parts of Baical Skullcap root P.E, obvious synergistic function is served in terms of sun-proof skin care, achieves unexpected technique effect.
Description
Technical field
The present invention relates to daily cosmetics field, be specifically related to a kind of sunlight screening skin-protecting product containing Gotu Kola P.E and
Its preparation method.
Background technology
As people deepen continuously to ultraviolet protection importance and necessity understanding, the demand in sun care preparations market
Also it is being continuously increased, safe efficient, wide spectrum sunscreen product is increasingly becoming focus of concern.Sun-screening agent is sun-proof cosmetic
The key component of anti-sunlight function is played in product, sun-screening agent on the market is broadly divided into physical ultraviolet light screener and chemistry at present
The ultraviolet absorber of property.Physical sunscreen agent is to no skin irritation, but absorbability, the transparency and poor air permeability, anti-for preparing
Cosmetics are shone, product comfort has much room for improvement.Chemical sun has certain stimulation to skin, may cause sensitivity
The allergy and stimulate the reaction of skin, meanwhile, part chemical sun light resistance and photostability be not high, easily by light degradation, is used for
Sun care preparations is prepared, the safety and stability of product has much room for improvement.
Meanwhile as the development of plant extract technology, increasing plant extracts are applied in cosmetics, turning into
Effective both effectiveness composition in cosmetic.Though there is the diversified sun care preparations containing plant extracts at present, due to kind
Kind reason, its using effect is simultaneously not fully up to expectations, therefore, it is imperative to develop the significant cosmetics of new sun-proof function.
The content of the invention
In view of the deficienciess of the prior art, it is an object of the invention to provide the sun-proof skin care containing Gotu Kola P.E
Product, realized particular by following technical scheme：
Sunlight screening skin-protecting product containing Gotu Kola P.E, it is made up of the raw material of following percentage by weight：Composite vegetables extractive 2-
5%th, peony seed oil 2-5%, hydrogenated jojoba oil 2-6%, shea butter 2-6%, 1,2- butanediol 1-3%, beta glucan 1-
3%th, cetostearyl alcohol 1-3%, PEG-100 stearates 2-5%, trehalose 1-2%, saualane 0.5-1.5%, hyaluronic acid
Sodium 0.05-0.15%, xanthans 0.3-0.6%, tocopherol acetate 0.1-0.5%, dipotassium glycyrrhizinate 0.1-0.2%, opopanax
Alcohol 0.2-0.4%, cetearyl glucoside 0.2-0.8%, surplus are deionized water；The composite vegetables extractive is by as follows
The extract composition of parts by weight：Gotu Kola P.E 10-20 parts, Thallus Gracilariae extract 1-5 parts, Lonicera confusa extract 1-3 parts, Huang
A kind of reed mentioned in ancient books extract 3-8 parts.
Preferably, composite vegetables extractive is made up of the extract of following parts by weight：15 parts of Gotu Kola P.E, asparagus
3 parts of extract, 2 parts of Lonicera confusa extract, 5 parts of Baical Skullcap root P.E.
Preferably, the sunlight screening skin-protecting product containing Gotu Kola P.E, it is made up of the raw material of following percentage by weight：Compound plant
Thing extract 4%, peony seed oil 3%, hydrogenated jojoba oil 3%, shea butter 3%, 1,2- butanediols 2%, beta glucan
1%th, cetostearyl alcohol 2%, PEG-100 stearates 2%, trehalose 1%, saualane 0.5%, Sodium Hyaluronate 0.15%, Huang
Virgin rubber 0.5%, tocopherol acetate 0.1%, dipotassium glycyrrhizinate 0.1%, bisabolol 0.2%, cetearyl glucoside
0.5%th, surplus is deionized water；The composite vegetables extractive is made up of the extract of following parts by weight：Gotu Kola P.E 15
Part, 3 parts of Thallus Gracilariae extract, 2 parts of Lonicera confusa extract, 5 parts of Baical Skullcap root P.E.
Preferably, the Gotu Kola P.E, Thallus Gracilariae extract, Lonicera confusa extract and Baical Skullcap root P.E are by low
Concentration ethanol traditional extraction obtains after drying.
It is further preferred that the Gotu Kola P.E uses following extracting methods：Add 5 ~ 10 times after centella is crushed
The volume parts of amount are 10 ~ 30% alcohol solution dipping after 4 ~ 6 hours, heating and refluxing extraction 2 ~ 3 times, each extraction time is 1 ~
2h, merge extract solution, filter, be condensed into medicinal extract after the recovered ethanol of filtrate, be finally dried to powder.
It is further preferred that the Thallus Gracilariae extract uses following extracting methods：Add 5 ~ 10 times after asparagus is crushed
The volume parts of amount are 20 ~ 30% alcohol solution dipping after 4 ~ 6 hours, heating and refluxing extraction 2 ~ 3 times, each extraction time is 1 ~
2h, merge extract solution, filter, be condensed into medicinal extract after the recovered ethanol of filtrate, be finally dried to powder；
It is further preferred that the Lonicera confusa extract uses following extracting methods：After Honeysuckle flower is crushed plus 5 ~ 10 times amount
Volume parts are 10 ~ 20% alcohol solution dipping after 4 ~ 6 hours, and heating and refluxing extraction 2 ~ 3 times, each extraction time is 1 ~ 2h,
Merge extract solution, filter, be condensed into medicinal extract after the recovered ethanol of filtrate, be finally dried to powder.
It is further preferred that the Baical Skullcap root P.E uses following extracting methods：After radix scutellariae is crushed plus 5 ~ 10 times amount
Volume parts are 30 ~ 50% alcohol solution dipping after 4 ~ 6 hours, and heating and refluxing extraction 2 ~ 3 times, each extraction time is 1 ~ 2h,
Merge extract solution, filter, be condensed into medicinal extract after the recovered ethanol of filtrate, be finally dried to powder.
The preparation method of the sunlight screening skin-protecting product containing Gotu Kola P.E of the present invention, comprises the following steps：
（1）By peony seed oil, hydrogenated jojoba oil, shea butter, cetostearyl alcohol, PEG-100 stearates, saualane, Huang
Virgin rubber, tocopherol acetate, bisabolol, cetearyl glucoside mixing, are heated to 80-90 DEG C；
（2）Deionized water, 1,2- butanediols, beta glucan, trehalose, Sodium Hyaluronate and dipotassium glycyrrhizinate are mixed, heating
To 80-90 DEG C；
（3）By above-mentioned steps（1）With（2）The material mixing of gained, homogeneous；
（4）30-40 DEG C is cooled to, composite vegetables extractive is added, is uniformly mixed, is cooled to room temperature and can be prepared by described contain
There is the sunlight screening skin-protecting product of Gotu Kola P.E.
Compared with prior art, the beneficial effects of the present invention are：The sun-proof result of skin care item of the present invention is notable, by that will accumulate
Four kinds of careless extract, Thallus Gracilariae extract, Lonicera confusa extract and Baical Skullcap root P.E raw materials are avenged to obtain after compounding in specific proportions
Compound plant extract, obvious synergistic function is served in terms of sun-proof skin care, is achieved unexpected
Technique effect.Sunlight screening skin-protecting product of the present invention complies fully with country's promulgation《Cosmetics safety technical specification（Version in 2015）》In
Indices, to no skin irritation, securely and reliably.
Embodiment
The present invention is described in further detail with reference to embodiment.
Embodiment 1：
Sunlight screening skin-protecting product containing Gotu Kola P.E, it is made up of the raw material of following percentage by weight：Composite vegetables extractive
4%th, peony seed oil 3%, hydrogenated jojoba oil 3%, shea butter 3%, 1,2- butanediols 2%, beta glucan 1%, cetearyl alcohol
Alcohol 2%, PEG-100 stearates 2%, trehalose 1%, saualane 0.5%, Sodium Hyaluronate 0.15%, xanthans 0.5%, life
It is to go to educate phenol acetic acid esters 0.1%, dipotassium glycyrrhizinate 0.1%, bisabolol 0.2%, cetearyl glucoside 0.5%, surplus
Ionized water；The composite vegetables extractive is made up of the extract of following parts by weight：15 parts of Gotu Kola P.E, asparagus extraction
3 parts of thing, 2 parts of Lonicera confusa extract, 5 parts of Baical Skullcap root P.E.
The Gotu Kola P.E uses following extracting methods：After centella is crushed plus 10 times of volume parts measured are
After 10% alcohol solution dipping 5 hours, heating and refluxing extraction 2 times, each extraction time is 2h, merges extract solution, filtering, filtrate
Medicinal extract is condensed into after recovered ethanol, is finally dried to powder.
The Thallus Gracilariae extract uses following extracting methods：After asparagus is crushed plus 5 times of volume parts measured are
After 20% alcohol solution dipping 4 hours, heating and refluxing extraction 3 times, each extraction time is 1h, merges extract solution, filtering, filtrate
Medicinal extract is condensed into after recovered ethanol, is finally dried to powder；
The Lonicera confusa extract uses following extracting methods：After Honeysuckle flower is crushed plus 8 times of volume parts measured are 15% second
After alcoholic solution soaks 6 hours, heating and refluxing extraction 2 times, each extraction time is 2h, merges extract solution, is filtered, and filtrate is recovered
Medicinal extract is condensed into after ethanol, is finally dried to powder.
The Baical Skullcap root P.E uses following extracting methods：After radix scutellariae is crushed plus 10 times of volume parts measured are 50% second
After alcoholic solution soaks 6 hours, heating and refluxing extraction 3 times, each extraction time is 1h, merges extract solution, is filtered, and filtrate is recovered
Medicinal extract is condensed into after ethanol, is finally dried to powder.
The preparation method of the sunlight screening skin-protecting product containing Gotu Kola P.E, comprises the following steps：
（1）By peony seed oil, hydrogenated jojoba oil, shea butter, cetostearyl alcohol, PEG-100 stearates, saualane, Huang
Virgin rubber, tocopherol acetate, bisabolol, cetearyl glucoside mixing, are heated to 90 DEG C；
（2）Deionized water, 1,2- butanediols, beta glucan, trehalose, Sodium Hyaluronate and dipotassium glycyrrhizinate are mixed, heating
To 90 DEG C；
（3）By above-mentioned steps（1）With（2）The material mixing of gained, homogeneous；
（4）40 DEG C are cooled to, composite vegetables extractive is added, is uniformly mixed, is cooled to room temperature and can be prepared by described contain
The sunlight screening skin-protecting product of Gotu Kola P.E.
Comparative example 1 ~ 4：
By the weight for Gotu Kola P.E, Thallus Gracilariae extract, Lonicera confusa extract and the Baical Skullcap root P.E specified in table 1 below
Part dosage repeats the preparation method of embodiment 1, the preparation method and 1 complete phase of embodiment of each plant extracts in comparative example
Together, the species of other unlisted components and dosage are identical with embodiment 1, and it is different to respectively obtain plant extracts component
Skin care item.
Table 1
| Material name | Comparative example 1 | Comparative example 2 | Comparative example 3 | Comparative example 4 |
| Gotu Kola P.E | 15 parts | 15 parts | 15 parts | Nothing |
| Thallus Gracilariae extract | 3 parts | 3 parts | Nothing | 5 parts |
| Lonicera confusa extract | 7 parts | Nothing | 2 parts | 5 parts |
| Baical Skullcap root P.E | Nothing | 7 parts | 8 parts | 15 parts |
First, in order to verify the stability of embodiment 1, the skin care item obtained by comparative example 1-4 during storage and use, according to
GB/T 29665-2013, and GB/T 16497-2007 are referred to, the strict of high temperature and low tempertaure storage stability is carried out to skin care item
Test.
Test 1：3000 r·min-1Whether observation skin care item are layered after centrifugation 30min；
Test 2：48 DEG C of continuous constant temperature 20d, then recover room temperature and keep 8 more than h, whether observation skin care item have layering, separate out solid
Or other inhomogenous phenomenons；
Test 3：In -25 DEG C of continuous freezing 20d, then recover room temperature and keep more than 8h, whether observation skin care item have layering, precipitation solid
Body or other inhomogenous phenomenons；
Test 4：24h, which colds and heat succeed each other, under the conditions of 48 and -25 DEG C circulates 20d, then recovers room temperature and keep more than 8h, observes skin care milk
Whether there is layering, separate out solid or other inhomogenous phenomenons.
In above-mentioned test, if skin care item lead to without layering, precipitation solid or other heterogeneity phenomenons, stability test
Cross, otherwise do not pass through for stability test.
Through overtesting, the skin care item of embodiment 1 are all by above-mentioned several tests, and comparative example 1-4 skin care milk is not
Can be completely by above-mentioned several tests, this illustrates that the stability of sunlight screening skin-protecting product system of the present invention is high.
2nd, the SPF measure of containing sunscreen skincare emulsion of the present invention
Given the test agent is the embodiment of the present invention 1, sunlight screening skin-protecting product made from comparative example 1-4.With reference to the Ministry of Public Health《Cosmetics health is advised
Model》" sun care preparations SPF (spf value) assay method " and " sun care preparations long wave ultraviolet protection in (version in 2007)
The related request and assay method of index (PFA values) assay method " are carried out, and concrete outcome is shown in Table 2.
The SPF measurement result of table 2
| Group | Embodiment 1 | Comparative example 1 | Comparative example 2 | Comparative example 3 | Comparative example 4 |
| Spf value | 27 | 6 | 7 | 7 | 8 |
| PFA values | 9 | 2 | 3 | 2 | 3 |
| PA grades | PA+++ | PA+ | PA+ | PA+ | PA+ |
Remarks：
SPF SPF（Sun Protection Factor）It is to measure defence capability of the sunscreen productses to sunlight middle-ultraviolet lamp UVB
Detection index, show the height of the sun-proof efficiency that sun-proof articles can play.It is according to the minimum Erythema Dose of skin come
Determine.Rudimentary sunscreen productses SPF is SPF2 ~ 6, and middle rank is SPF6 ~ 8, and high sunscreen productses are then SPF8 ~ 12, and spf value exists
Product in the range of 12 ~ 30 then belongs to the high-strength or strong sunscreen productses of superelevation.
Ultraviolet light,long wave-protection index PFA（Protection Factor of UVA）Refer to the defence capability to UVA.Calculate
Formula is that PFA=the MPPD values of smearing sunscreen productses skin/does not smear the MPPD values of sunscreen productses skin.PFA values are higher, represent protection
Time is longer.
Sun-proof index PA（ProtectionUVA）It is that Japanese cosmetic industrial combination in 1996 can be announced " UVA prevents from imitating
Fruit determination method standard ", refer to preventing UVA significant degree index, be most wide adopted standard, defence effect in Japanese commodity
Fruit is divided into three-level, i.e. PA+, PA++, PA+++, adds PA++++ again within 2013.
It can be seen that compound plant extract of the present invention employs Gotu Kola P.E, Thallus Gracilariae extract, Lonicera confusa extract
Compounded in specific proportions with four kinds of raw materials of Baical Skullcap root P.E, obvious synergistic function is served in terms of sun-proof skin care, is taken
Obtained unexpected technique effect.
Above-described embodiment is only currently preferred case study on implementation, it is impossible to limits present invention model claimed with this
Enclose, any unsubstantiality and replacement that those skilled in the art is done on the basis of the present invention belongs to application claims
The scope of protection.
Claims (9)
1. the sunlight screening skin-protecting product containing Gotu Kola P.E, it is made up of the raw material of following percentage by weight：Composite vegetables extractive
2-5%, peony seed oil 2-5%, hydrogenated jojoba oil 2-6%, shea butter 2-6%, 1,2- butanediol 1-3%, beta glucan
1-3%, cetostearyl alcohol 1-3%, PEG-100 stearate 2-5%, trehalose 1-2%, saualane 0.5-1.5%, hyalomitome
Sour sodium 0.05-0.15%, xanthans 0.3-0.6%, tocopherol acetate 0.1-0.5%, dipotassium glycyrrhizinate 0.1-0.2%, red do not have
Medicine alcohol 0.2-0.4%, cetearyl glucoside 0.2-0.8%, surplus are deionized water；Characterized in that, the compound plant
Thing extract is made up of the extract of following parts by weight：Gotu Kola P.E 10-20 parts, Thallus Gracilariae extract 1-5 parts, Honeysuckle flower
Extract 1-3 parts, Baical Skullcap root P.E 3-8 parts.
2. the sunlight screening skin-protecting product according to claim 1 containing Gotu Kola P.E, it is characterised in that the composite plant
Extract is made up of the extract of following parts by weight：15 parts of Gotu Kola P.E, 3 parts of Thallus Gracilariae extract, Lonicera confusa extract 2
Part, 5 parts of Baical Skullcap root P.E.
3. the sunlight screening skin-protecting product according to claim 1 or 2 containing Gotu Kola P.E, it is characterised in that by following heavy
The raw material of amount percentage is made：Composite vegetables extractive 4%, peony seed oil 3%, hydrogenated jojoba oil 3%, shea butter 3%,
1,2- butanediols 2%, beta glucan 1%, cetostearyl alcohol 2%, PEG-100 stearates 2%, trehalose 1%, saualane
0.5%th, Sodium Hyaluronate 0.15%, xanthans 0.5%, tocopherol acetate 0.1%, dipotassium glycyrrhizinate 0.1%, bisabolol
0.2%th, cetearyl glucoside 0.5%, surplus are deionized water；Characterized in that, the composite vegetables extractive is by as follows
The extract composition of parts by weight：15 parts of Gotu Kola P.E, 3 parts of Thallus Gracilariae extract, 2 parts of Lonicera confusa extract, radix scutellariae extraction
5 parts of thing.
4. according to the sunlight screening skin-protecting product containing Gotu Kola P.E described in claim any one of 1-3, it is characterised in that described
Gotu Kola P.E, Thallus Gracilariae extract, Lonicera confusa extract and Baical Skullcap root P.E are done by low-concentration ethanol traditional extraction
Obtained after dry.
5. the sunlight screening skin-protecting product according to claim 4 containing Gotu Kola P.E, it is characterised in that the centella carries
Thing is taken to use following extracting methods：After centella is crushed plus 5 ~ 10 times of volume parts measured are 10 ~ 30% alcohol solution dippings 4
After ~ 6 hours, heating and refluxing extraction 2 ~ 3 times, each extraction time is 1 ~ 2h, merges extract solution, filtering, the recovered ethanol of filtrate
After be condensed into medicinal extract, be finally dried to powder.
6. the sunlight screening skin-protecting product according to claim 4 containing Gotu Kola P.E, it is characterised in that the asparagus carries
Thing is taken to use following extracting methods：After asparagus is crushed plus 5 ~ 10 times of volume parts measured are 20 ~ 30% alcohol solution dippings 4
After ~ 6 hours, heating and refluxing extraction 2 ~ 3 times, each extraction time is 1 ~ 2h, merges extract solution, filtering, the recovered ethanol of filtrate
After be condensed into medicinal extract, be finally dried to powder.
7. the sunlight screening skin-protecting product according to claim 4 containing Gotu Kola P.E, it is characterised in that the Honeysuckle flower carries
Thing is taken to use following extracting methods：After Honeysuckle flower is crushed plus 5 ~ 10 times of volume parts measured are 10 ~ 20% alcohol solution dippings 4
After ~ 6 hours, heating and refluxing extraction 2 ~ 3 times, each extraction time is 1 ~ 2h, merges extract solution, filtering, the recovered ethanol of filtrate
After be condensed into medicinal extract, be finally dried to powder.
8. the sunlight screening skin-protecting product according to claim 4 containing Gotu Kola P.E, it is characterised in that the radix scutellariae extraction
Thing uses following extracting methods：After radix scutellariae is crushed plus 5 ~ 10 times of volume parts measured are small for 30 ~ 50% alcohol solution dippings 4 ~ 6
Shi Hou, heating and refluxing extraction 2 ~ 3 times, each extraction time are 1 ~ 2h, merge extract solution, are filtered, dense after the recovered ethanol of filtrate
Shorten medicinal extract into, be finally dried to powder.
9. the preparation method of the sunlight screening skin-protecting product containing Gotu Kola P.E according to claim any one of 1-3, it is special
Sign is, comprises the following steps：
（1）By peony seed oil, hydrogenated jojoba oil, shea butter, cetostearyl alcohol, PEG-100 stearates, saualane, Huang
Virgin rubber, tocopherol acetate, bisabolol, cetearyl glucoside mixing, are heated to 80-90 DEG C；
（2）Deionized water, 1,2- butanediols, beta glucan, trehalose, Sodium Hyaluronate and dipotassium glycyrrhizinate are mixed, heating
To 80-90 DEG C；
（3）By above-mentioned steps（1）With（2）The material mixing of gained, homogeneous；
（4）30-40 DEG C is cooled to, composite vegetables extractive is added, is uniformly mixed, is cooled to room temperature and can be prepared by described contain
There is the sunlight screening skin-protecting product of Gotu Kola P.E.
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| CN201711425032.6A CN107854404B (en) | 2017-12-25 | 2017-12-25 | Sunscreen skin care product containing herba Centellae extract and its preparation method |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115252512A (en) * | 2022-09-29 | 2022-11-01 | 美尚(广州)化妆品股份有限公司 | Sunscreen composition and preparation method and application thereof |
| CN115475130A (en) * | 2022-10-26 | 2022-12-16 | 浙江兰树化妆品有限公司 | A method for preparing skin care product containing herba Centellae extract |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105380848A (en) * | 2015-11-25 | 2016-03-09 | 陕西艾美雅生物科技有限公司 | Composition, preparation method thereof, cosmetic containing composition and use method thereof |
| CN106420471A (en) * | 2016-10-31 | 2017-02-22 | 广东科玮生物技术股份有限公司 | Skin care product with sunscreen and sun repair functions and preparation method thereof |
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| CN105380848A (en) * | 2015-11-25 | 2016-03-09 | 陕西艾美雅生物科技有限公司 | Composition, preparation method thereof, cosmetic containing composition and use method thereof |
| CN106420471A (en) * | 2016-10-31 | 2017-02-22 | 广东科玮生物技术股份有限公司 | Skin care product with sunscreen and sun repair functions and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115252512A (en) * | 2022-09-29 | 2022-11-01 | 美尚(广州)化妆品股份有限公司 | Sunscreen composition and preparation method and application thereof |
| CN115252512B (en) * | 2022-09-29 | 2022-12-13 | 美尚(广州)化妆品股份有限公司 | Sunscreen composition and preparation method and application thereof |
| CN115475130A (en) * | 2022-10-26 | 2022-12-16 | 浙江兰树化妆品有限公司 | A method for preparing skin care product containing herba Centellae extract |
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| CN107854404B (en) | 2021-04-23 |
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