CN107815274A - A kind of sweetish cork paper and preparation method - Google Patents
A kind of sweetish cork paper and preparation method Download PDFInfo
- Publication number
- CN107815274A CN107815274A CN201710933222.2A CN201710933222A CN107815274A CN 107815274 A CN107815274 A CN 107815274A CN 201710933222 A CN201710933222 A CN 201710933222A CN 107815274 A CN107815274 A CN 107815274A
- Authority
- CN
- China
- Prior art keywords
- cigarette
- sweetish
- modifying agent
- paper
- cork paper
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/08—Macromolecular additives
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J121/00—Adhesives based on unspecified rubbers
- C09J121/02—Latex
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
Abstract
The present invention provides a kind of sweetish cork paper and preparation method, for cigarette filter, cigarette filter includes filter wire fasces, including outer layer forming paper, fill acetate silk in filter wire fasces both ends, acetate silk is bonded by adhesive and outer layer forming paper, and adhesive includes modifying agent and water-base cement, and modifying agent includes sweetener, glucono-delta-lactone, chitin chitosan emulsion.The present invention can increase the sense of flue gas sweet tea, improves flue gas mildness and improve pleasant impression, as long as the effect of significantly enhancing cigarette sweet sense can be reached on a small quantity by adding, and the material can be sprayed directly on tow and be prepared into cigarette filter tip, it is not involved in burning, avoids and result from the uncoordinated miscellaneous gas of tobacco this perfume because material participates in cigarette burning in itself.The low raw-material cost of the present invention simultaneously, preparation is simple, and it is applied to cigarette industry mature production technology, is had a wide range of applications in tobacco business.
Description
Technical field
The invention belongs to cigarette supplementary material technical field, and in particular to a kind of sweetish cork paper and preparation method.
Background technology
Sweet taste is generally liked for masses always, also in this way, sweet tea sense can lift the comfortableness of cigarette smoking on cigarette, by
Consumers.Researcher generally increases the sweet tea sense of cigarette smoke by tobacco perfuming feeding technique, but flavoring and casing can companion
Burnt with suction, often bring other miscellaneous tastes.Being sweetened in the auxiliary materials such as mouth rod also has research, and previous studies are mainly
Dispensing fluid sweetener, it is then added in the cork paper of mouth rod, overlapping glue, also has by being added in filter tow added with sweet tea
The cotton thread of taste agent reaches sweetening effect, is directly seen in report using the less of solid sweetener.
Important component of the filter stick as cigarette, to increasing flue gas concentration, cigarette perfume is enriched, lifts flue gas moisture feeling, is improved
Cigarette smoking quality plays vital effect.The cigarette filter rod used at present in industry has cellulose acetate filter rod, paper
Matter filter stick and polypropylene filter.Cellulose acetate filter rod is current most popular a kind of cigarette filter rod, and such filter stick is to flue gas
Grain phase component has certain intercepting efficiency, and larger negative effect will not be produced to cigarette odor-absorbing, but as cigarette industry is to volume
The continuous improvement of cigarette flavouring humectation requirement, simple cellulose acetate filter rod have been difficult to meet need of the cigarette industry to filter stick functionalization
Ask, and many functional powder body materials show excellent properties in terms of cigarette flavouring humectation, but produced by its solvent spinning
The limitation of technique, it is impossible to be directly carried in acetate fiber, can only in the production process that acetate fiber is prepared into filter stick with
The form of grain or line load is applied in filter stick, and the particle diameter of particle need to be typically controlled in 40-80 mesh, but above-mentioned application mode
The defects of functional material addition is limited, filter stick homogeneity is serious, production cost is high be present.Therefore, a kind of raw material sources are developed
Extensively, it is easy to a large amount of loads of function powder material, production cost is low and can effectively improve the new cigarette of cigarette smoking quality
Filter stick seems particularly urgent.
The content of the invention
【1】Technical problems to be solved
The technical problem to be solved in the present invention is to provide one kind can play increase flue gas it is sweet degree and comfortableness, cover it is miscellaneous
Gas etc. is acted on, and is not involved in burning, and the sweetish cork paper and preparation method of any negative effect will not be come to tobacco rolling belt.
【2】The technical scheme solved the problems, such as
The present invention provides a kind of sweetish cork paper, and for cigarette filter, the cigarette filter includes filter wire
Acetate silk is filled at fasces, including outer layer forming paper, the filter wire fasces both ends, and the acetate silk passes through glue
Stick bonds with the outer layer forming paper, and the adhesive includes modifying agent and water-base cement, and the modifying agent includes sweetener, Portugal
Grape saccharic acid-delta-lactone, chitin-chitosan emulsion, the weight ratio of each component are：Glucono-δ-lactone 18%~21%,
Sweetener 7.2%~9.8%, chitin-chitosan emulsion 60%~84%.
Above-mentioned sweetish cork paper, the sweetener be acesulfame potassium, steviol glycoside and Aspartame in one kind or
A variety of compositions.
Above-mentioned sweetish cork paper, the water-base cement include Aqueous Adhesives 18%~21%, deionized water 42%
~76%, organic amine 1%~10%, organic acid 1%~10%；The modifying agent and the water-base cement mixing and emulsifying shape at room temperature
Into mix emulsion fluid.
Above-mentioned sweetish cork paper, the organic amine are ethylenediamine, propane diamine, butanediamine, monoethanolamine, guanidine and diformazan
One or more in base biguanides；The organic acid is the one or more in acetic acid, propionic acid, citric acid and malic acid.
Technical problem solved by the invention can be realized using following technical scheme：A kind of sweetish cork paper
Preparation method, comprise the following steps：
Step A, after organic amine, organic acid and deionized water are mixed, under agitation, it is slowly dropped to water-based gluing
In agent, ultrasonic disperse 40-60min after stirring, water-base cement emulsion is obtained；Step B, by sweetener, gluconic acid-δ-interior
After ester mixes, it is added in chitin-chitosan emulsion, after stirring, obtains modifying agent；
Step C, the water-base cement emulsion obtained by step A is mixed with 2 DEG C/min heating with the modifying agent obtained by step B
Speed, 60 DEG C are warming up to by normal temperature, natural cooling, then produce adhesive after flowing back, centrifuging；
Step D, the adhesive is applied in outer layer forming paper using sizer.
The preparation method of above-mentioned sweetish cork paper, the step B include step B1, by chitin-chitosan breast
Liquid is heated up to 42 DEG C, and then stirring adds sweetener, mixing time 15-20min.
【3】Beneficial effect
This sweetish cork paper of the present invention and preparation method can increase the sense of flue gas sweet tea, improve flue gas mildness and change
Kind pleasant impression, if the effect that can reach significantly enhancing cigarette sweet sense on a small quantity is added, and also the material can be sprayed directly on
Cigarette filter tip is prepared on tow, is not involved in burning, avoids and results from tobacco this perfume because material participates in cigarette burning in itself
Uncoordinated miscellaneous gas.The low raw-material cost of the present invention simultaneously, preparation is simple, and it is applied to cigarette industry production work
Skill is ripe, is had a wide range of applications in tobacco business.
Brief description of the drawings
Fig. 1 is a kind of sweetish cork paper of the present invention and the structural representation of preparation method.
Embodiment
Below in conjunction with the accompanying drawings, the embodiment of the present invention is discussed in detail.
The present invention provides a kind of sweetish cork paper, and for cigarette filter, the cigarette filter includes filter wire
Acetate silk is filled at fasces, including outer layer forming paper, the filter wire fasces both ends, and the acetate silk passes through glue
Stick bonds with the outer layer forming paper, and the adhesive includes modifying agent and water-base cement, and the modifying agent includes sweetener, Portugal
Grape saccharic acid-delta-lactone, chitin-chitosan emulsion, the weight ratio of each component are：Glucono-δ-lactone 18%~21%,
Sweetener 7.2%~9.8%, chitin-chitosan emulsion 60%~84%.
Further, in a kind of preferred embodiment of sweetish cork paper of the present invention, the sweetener be acesulfame potassium,
One or more compositions in steviol glycoside and Aspartame.
Further, in a kind of preferred embodiment of sweetish cork paper of the present invention, the water-base cement includes water-based
Adhesive 18%~21%, deionized water 42%~76%, organic amine 1%~10%, organic acid 1%~10%；The modification
Mixing and emulsifying forms mix emulsion fluid at room temperature with the water-base cement for agent.
Further, in a kind of preferred embodiment of sweetish cork paper of the present invention, the organic amine be ethylenediamine,
One or more in propane diamine, butanediamine, monoethanolamine, guanidine and dimethylbiguanide；The organic acid is acetic acid, propionic acid, lemon
One or more in acid and malic acid.
Smoke panel test experiment：Certain brand cigarette of selection with mouth rod length identical with cigarette filter tip A, cigarette filter tip B and size
As control cigarette, mouth rod therein is the solid mouth rod for being stuffed entirely with filtering material.Then by cigarette filter tip A and cigarette filter tip
Cigarette A and cigarette B is respectively prepared in B, and wherein cigarette A and cigarette B tobacco material is identical with tobacco material in control cigarette, cigarette
A and cigarette B cigarette paper and tipping paper scantling is identical with control cigarette.Then respectively to cigarette A, cigarette B and
Control cigarette is smoked panel test, and extracts each sample by GB/T5606.1, sample moisture is adjusted according to GB/T16447 before smokeing panel test.According to
《Cigarette》GB5606.4-2005 Sensory Quality of Cigarette technical requirements table evaluates the improvement of aesthetic quality, the sense organ matter of cigarette product
Amount is generally included in gloss, fragrance, harmony, miscellaneous gas, excitant and wherein each index of six technical requirements of pleasant impression, is score value
More high organoleptic quality is better.
Cross specialty to smoke panel test technical staff's evaluation, unanimously think taking out using the cigarette of composite tip stick of addition solid sweetener
Harmony, fragrance etc. do not destroy during suction, do not have negative interaction to the suction quality of cigarette, and can slightly improve the comfortableness of suction.
Contrasted by evaluation effect, it is found that the sugariness of the cigarette flue gas using the composite tip stick added with granular sweetener shows
Increase is write, is shown by analysis of experimental data and Analyses Methods for Sensory Evaluation Results, mixing sweetener is more preferable than single sweetener effect, right
The sweetening effect of flue gas becomes apparent from.And acesulfame potassium, steviol glycoside, Aspartame are according to 1:4:The sweet tea prepared after the mixing of 15 ratios
Taste agent, score value highest of smokeing panel test, the sweet tea sense lifting of flue gas are most notable.
Refering to Fig. 1, a kind of preparation method of sweetish cork paper, comprise the following steps：
Step A, after organic amine, organic acid and deionized water are mixed, under agitation, it is slowly dropped to water-based gluing
In agent, ultrasonic disperse 40-60min after stirring, water-base cement emulsion is obtained；Step B, by sweetener, gluconic acid-δ-interior
After ester mixes, it is added in chitin-chitosan emulsion, after stirring, obtains modifying agent；
Step C, the water-base cement emulsion obtained by step A is mixed with 2 DEG C/min heating with the modifying agent obtained by step B
Speed, 60 DEG C are warming up to by normal temperature, natural cooling, then produce adhesive after flowing back, centrifuging；
Step D, the adhesive is applied in outer layer forming paper using sizer.
Further, it is described in a kind of preferred embodiment of the preparation method of sweetish cigarette filter of the present invention
Step B includes step B1, and chitin-chitosan emulsion is heated up into 42 DEG C, and then stirring adds sweetener, and mixing time is
15-20min。
This sweetish cork paper of the present invention and preparation method can increase the sense of flue gas sweet tea, improve flue gas mildness and change
Kind pleasant impression, if the effect that can reach significantly enhancing cigarette sweet sense on a small quantity is added, and also the material can be sprayed directly on
Cigarette filter tip is prepared on tow, is not involved in burning, avoids and results from tobacco this perfume because material participates in cigarette burning in itself
Uncoordinated miscellaneous gas.The low raw-material cost of the present invention simultaneously, preparation is simple, and it is applied to cigarette industry production work
Skill is ripe, is had a wide range of applications in tobacco business.
Described above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, without departing from the technical principles of the invention, some improvements and modifications can also be made, these improvements and modifications
Also it should be regarded as protection scope of the present invention.
Claims (6)
1. a kind of sweetish cork paper, for cigarette filter, the cigarette filter includes filter wire fasces, and its feature exists
In, including outer layer forming paper, the filter wire fasces both ends filling acetate silk, the acetate silk passes through gluing
Agent bonds with the outer layer forming paper, and the adhesive includes modifying agent and water-base cement, and the modifying agent includes sweetener, grape
Saccharic acid-delta-lactone, chitin-chitosan emulsion, the weight ratio of each component are：Glucono-δ-lactone 18%~21%, sweet tea
Taste agent 7.2%~9.8%, chitin-chitosan emulsion 60%~84%.
2. a kind of sweetish cork paper as claimed in claim 1, it is characterised in that the sweetener is acesulfame potassium, stevia rebaudianum
One or more compositions in glucosides and Aspartame.
3. a kind of sweetish cork paper as claimed in claim 1, it is characterised in that the water-base cement includes Aqueous Adhesives
18%~21%, deionized water 42%~76%, organic amine 1%~10%, organic acid 1%~10%；The modifying agent and institute
Stating water-base cement, mixing and emulsifying forms mix emulsion fluid at room temperature.
4. a kind of sweetish cork paper as claimed in claim 3, it is characterised in that the organic amine is ethylenediamine, the third two
One or more in amine, butanediamine, monoethanolamine, guanidine and dimethylbiguanide；The organic acid be acetic acid, propionic acid, citric acid and
One or more in malic acid.
5. a kind of preparation method of sweetish cork paper, it is characterised in that comprise the following steps：
Step A, after organic amine, organic acid and deionized water are mixed, under agitation, it is slowly dropped to Aqueous Adhesives
In, ultrasonic disperse 40-60min after stirring, obtain water-base cement emulsion；
Step B, after sweetener, glucono-δ-lactone are mixed, it is added in chitin-chitosan emulsion, stirs
Afterwards, modifying agent is obtained；
Step C, the water-base cement emulsion obtained by step A is mixed with the modifying agent obtained by step B to the heating speed with 2 DEG C/min
Degree, 60 DEG C are warming up to by normal temperature, natural cooling, then produce adhesive after flowing back, centrifuging；
Step D, the adhesive is applied in outer layer forming paper using sizer.
6. a kind of preparation method of sweetish cork paper as claimed in claim 5, it is characterised in that the step B includes
Step B1, chitin-chitosan emulsion is heated up to 42 DEG C, then stirring adds sweetener, mixing time 15-20min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710933222.2A CN107815274A (en) | 2017-10-10 | 2017-10-10 | A kind of sweetish cork paper and preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710933222.2A CN107815274A (en) | 2017-10-10 | 2017-10-10 | A kind of sweetish cork paper and preparation method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107815274A true CN107815274A (en) | 2018-03-20 |
Family
ID=61607848
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710933222.2A Pending CN107815274A (en) | 2017-10-10 | 2017-10-10 | A kind of sweetish cork paper and preparation method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107815274A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108977139A (en) * | 2018-07-05 | 2018-12-11 | 常州思宇知识产权运营有限公司 | A kind of preparation method of cigarette glue |
-
2017
- 2017-10-10 CN CN201710933222.2A patent/CN107815274A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108977139A (en) * | 2018-07-05 | 2018-12-11 | 常州思宇知识产权运营有限公司 | A kind of preparation method of cigarette glue |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104946390B (en) | A kind of processing method of electronics natural perfume for cigarette | |
| CN106281680A (en) | A kind of quick-fried pearl of Herba Menthae cigarette cool taste Mint Essence and preparation method and application | |
| CN103054180B (en) | Aromatized composite particle filter stick and production method thereof | |
| CN206062125U (en) | A kind of feature cigarette holder containing quick-fried pearl | |
| CN101836764B (en) | Natural plant extract microcapsule and cigarette filter tip containing same | |
| CN109820243A (en) | Have effects that the scented gel of sustained release and its preparation and the application in cigarette | |
| CN101606753A (en) | A kind of flavoring essence that is used for tobacco | |
| CN103783660B (en) | The supercritical extraction method of flavor matter and application thereof in a kind of tobacco leaf fragment | |
| CN109123775A (en) | A kind of heating of the perfume (or spice) of solid-state containing herbal odor type pearl is not burnt cigarette and preparation method thereof | |
| CN101633864A (en) | Apple-flavored essence for tobacco, preparation method and application thereof | |
| CN104489907A (en) | Sauce-fragrance E-cigarette nicotine liquid | |
| CN100593373C (en) | Bagging mouth-sucked drying tobacco products and method of preparing the same | |
| CN109730355A (en) | A kind of preparation method of the perfumed granules for cigarette filter rod | |
| CN106263025A (en) | A kind of binary filter stick of banana aldehyde plant granule and preparation method thereof | |
| CN104450192A (en) | Tobacco flavor prepared by taking fructus terminaliae immaturus, dendrobium nobile, tobacco and the like as raw materials and application thereof | |
| CN101199364A (en) | Chinese herbal medicine cigarette filter tip rod for relieving cough and reducing sputum | |
| CN103211304A (en) | Preparation method of filter stick using cigarette harm-reducing synergistic agent containing glycerol triacetate | |
| CN103451018B (en) | Special mix-fruit essence for composite chewing gum | |
| CN107815274A (en) | A kind of sweetish cork paper and preparation method | |
| CN110226774A (en) | A kind of dry pearl mouth stick of cigarette that can promote cigarette sweet moisture feeling | |
| CN106520369A (en) | Essence for cigarette lap adhesive and use method thereof | |
| CN104921292B (en) | Method for preparing spicy cigarette from cigarette beads | |
| CN105639725A (en) | Liquor aroma type spice and application thereof to cigarette | |
| CN102488330B (en) | Natural plant extract microcapsules and cigarette filter tip containing natural plant extract microcapsules | |
| CN107780302A (en) | A kind of cork paper and preparation method with sweet taste antiseep |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20180320 |