CN107811958B - Black tea fungus fermentation lubricating liquid and preparation method thereof - Google Patents
Black tea fungus fermentation lubricating liquid and preparation method thereof Download PDFInfo
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Abstract
The invention relates to a black tea fungus fermentation lubricating liquid and a preparation method thereof, wherein the black tea fungus fermentation lubricating liquid is prepared from the following raw materials in parts by weight: 15-25 parts of black tea fungus fermentation liquor, 30-40 parts of glycerol, 0.5-1.5 parts of hyaluronic acid, 1-2 parts of water-soluble camellia seed oil, 0.3-0.5 part of cananga odorata essential oil, 0.5-1 part of hydroxyethyl urea, 0.5-1 part of black tea fungus fermentation membrane modifier and 30-50 parts of deionized water. The hyaluronic acid lubricating liquid is prepared from natural plants, is convenient to carry and use, can effectively clean and improve sexual excitation effect, and is a lubricant product which can be used for a long time.
Description
Technical Field
The invention relates to a black tea fungus fermentation lubricating liquid and a preparation method thereof, belonging to the field of washing and caring products.
Background
The human body lubricant is different from a lubricant used by machinery, is especially designed for a human body, and has wide applicability and higher safety. A good lubricant for human body not only increases the lubricating effect, improves the sexual pleasure, makes the sexual life more harmonious and improves the feelings among couples; meanwhile, the skin injury is reduced, and the corrosion chance of harmful microorganisms such as bacteria, viruses and the like to the human body is reduced; effectively reduces the damage of the condom and reduces the probability of accidental pregnancy.
There have been long attempts to apply lubricants to the human body, but a wide range of applications have been after 1950. Lubricants (liquids) were first used in clinical medicine examinations of the human body: many medical devices can cause mechanical damage to various degrees when penetrating into the human body, and the lubricant can reduce the damage to body tissues and mucous membranes to the greatest extent. The use of lubricants in human sexual life has also been a long history, but in the early days vegetable oils such as olive oil have been used. But because the limited effect of the components is not ideal, the clothes are easy to be polluted and absorbed by the body; later, petroleum-based mineral oily substances such as vaseline, baby oil, bath lotion, massage oil, etc. were tried to be used as lubrication; these materials tend to be too viscous to clean easily. The condom is easy to remain after being used, even the condom can block the urethral orifices of both men and women after being used, the difficult and painful sensation of urination is generated, the stability of the condom is damaged, and the accidental pregnancy is caused, which can cause damage to the human body. Disclosure of Invention
In order to solve the problems in the prior art, the invention provides the black tea fungus fermentation lubricating liquid capable of effectively improving vaginal dryness, which is prepared by fermenting natural products, has the advantages of convenience in carrying and use, effective cleaning and sexual excitation improving effects, is a lubricating product capable of being used for a long time, and has good effects of diminishing inflammation, sterilizing and relieving itching.
The technical scheme of the invention is as follows:
a black tea fungus fermentation lubricating liquid is prepared from the following raw materials in parts by weight: 15-25 parts of black tea fungus fermentation liquor, 30-40 parts of glycerol, 0.5-1.5 parts of hyaluronic acid, 0.5-1 part of black tea fungus fermentation membrane modifier, 0.3-0.5 part of cananga odorata essential oil, 1-2 parts of water-soluble camellia seed oil, 0.5-1 part of hydroxyethyl urea and 30-50 parts of deionized water.
Further, 18-20 parts of black tea fungus fermentation liquor, 30-35 parts of glycerol, 1-1.2 parts of hyaluronic acid, 1.5-2 parts of water-soluble camellia seed oil, 0.35-0.45 part of cananga oil, 0.75-1 part of hydroxyethyl urea, 0.5-0.75 part of black tea fungus fermentation membrane modifier and 30-40 parts of deionized water.
Further, the black tea fungus fermentation liquor is prepared from the following raw materials in parts by weight: 4-9 parts of black tea, 8-12 parts of picria fel-terrae lour, 2-6 parts of wormwood, 45-55 parts of white granulated sugar, 900 parts of deionized water, 1200 parts of mangosteen fungus mother liquor and 45-60 parts of black tea fungus mother liquor.
Further, the black tea fungus fermentation membrane modifier is prepared from the following raw materials in parts by weight: 100 parts of black tea fungus fermentation membrane solution with the mass concentration of 1.5-3%, 20-35 parts of chloroethanol and 2-10 parts of acetic acid; the black tea fungus fermentation membrane solution is prepared from the following raw materials in parts by weight: 90-110 parts of mixed aqueous solution of NaOH with the mass concentration of 5% and hydroxyethyl urea with the mass concentration of 6% and 1-3 parts of black tea fungus fermentation membrane.
Further, the water-soluble camellia oleosa seed oil is prepared from the following raw materials in parts by weight: polyglycerol-10100 parts, saturated disodium hydrogen phosphate solution 1-2 parts, camellia oleosa seed oil 12-20 parts, p-toluenesulfonic acid 2 parts and saturated sodium bicarbonate solution 1-3 parts.
The invention also comprises a preparation method of the black tea fungus fermentation lubricating liquid, which comprises the following steps: (1) dissolving 0.5-1 part by weight of black tea fungus fermentation membrane modifier with 30-50 parts by weight of deionized water at normal temperature; (2) adding 0.5-1.5 parts by weight of hyaluronic acid, heating to 60 ℃, stirring to dissolve and uniformly mixing; (3) keeping the temperature at 60 ℃, adding 30-40 parts by weight of glycerol and 0.5-1 part by weight of hydroxyethyl urea, stirring to dissolve and uniformly mixing; (4) cooling to room temperature, sequentially adding 1-2 parts by weight of water-soluble camellia oleosa seed oil and 15-25 parts by weight of black tea fungus fermentation liquor, and uniformly mixing; (5) adding 0.3-0.5 weight part of cananga odorata essential oil, and mixing uniformly to obtain the lubricating liquid.
Further, the black tea fungus fermentation liquor is prepared by the following steps: mixing 4-9 parts by weight of black tea, 8-12 parts by weight of picria fel-terrae lour, 2-6 parts by weight of wormwood, 45-55 parts by weight of white granulated sugar and 1200 parts by weight of deionized water, boiling for 100-fold-cake.
Further, the black tea fungus fermentation membrane modifier is prepared by the following steps: (1) pre-cooling 90-110 parts by weight of mixed aqueous solution of 5 mass percent NaOH and 6 mass percent hydroxyethyl urea to-7 ℃; (2) rapidly adding 1-3 weight parts of black tea fungus fermentation membrane before the solution is not frozen, rapidly stirring at room temperature for 5min, and standing at-7 deg.C for 20min to obtain 1.5-3% black tea fungus fermentation membrane solution; (3) adding 20-35 parts by weight of chloroethanol into 100 parts by weight of black tea fungus fermentation membrane solution with the mass concentration of 1.5-3%, reacting for 2 hours at room temperature, heating to 50 ℃ for reaction for 2 hours, adding acetic acid for neutralization to neutrality, and stopping reaction; (4) after the solution after reaction is dialyzed, centrifuging for 10min at 400r/min for separation; (5) collecting supernatant, and vacuum drying to obtain black tea fungus fermentation membrane modified substance.
Further, the water-soluble camellia oleosa seed oil is prepared by the following steps: (1) adding 100 parts by weight of polyglycerol-10 and 1-2 parts by weight of saturated disodium hydrogen phosphate solution into a three-neck flask provided with a spherical reflux condenser pipe; (2) stirring in water bath at 60 ℃ for 1 h; (3) then, dropwise adding 12-20 parts by weight of camellia oleosa seed oil, adding 2 parts by weight of p-toluenesulfonic acid, and continuing to react for 1h at 60 ℃; (4) dropwise adding saturated sodium bicarbonate solution until the pH value of the solution is 6.5-7.5; (5) and (3) cooling the liquid, transferring the liquid into a separating funnel, and directly separating to obtain a lower-layer solution, namely the water-soluble camellia seed oil.
The invention has the following beneficial effects
The black tea fungus fermentation liquor is added into the product, the black tea fungus fermentation liquor contains rich tea polyphenol, small molecular peptide, acetic acid, heat-resistant protein, polysaccharide and other antibacterial substances, has a good inhibition effect on common pathogenic bacteria such as escherichia coli, salmonella enteritidis, shigella dysenteriae, listeria monocytogenes, pseudomonas fluorescens, staphylococcus aureus and the like, has no drug resistance on the bacteria, is not added with an artificial preservative, has a good preservative effect, has good biocompatibility of components with human skin, and has no uncomfortable effects such as allergy, stimulation and the like. The product has the effects of repairing cells and protecting mucosa.
Meanwhile, a black tea fungus fermentation membrane modifier is added into the product, and the black tea fungus fermentation membrane is natural cellulose generated by black tea fungus fermentation, has the same chemical composition as plant cellulose, belongs to typical biological nano-cellulose, and has the characteristics of high water holding capacity, high tensile strength and the like. The black tea fungus fermentation membrane modifier is modified on the basis of the black tea fungus fermentation membrane, cellulose polysaccharide and protein in the black tea fungus fermentation membrane are modified into active substances such as small molecular peptides, oligosaccharides and the like, so that the water retention property of the black tea fungus fermentation membrane modifier is maintained, and the modified small molecular bioactive substances can be well combined with the vaginal skin of a female and have the effects of beautifying, resisting relaxation and increasing elasticity.
The water-soluble oil tea seed oil is modified on the basis of the oil tea seed oil, and the water-insoluble oil tea seed oil is modified to be soluble in water, so that the oil tea seed oil can be matched with other components in the lubricating liquid, and the effects of the lubricating liquid on beautifying, resisting relaxation and increasing the vaginal elasticity of female vaginal skin are increased.
The hyaluronic acid lubricating liquid is convenient to carry and use, can effectively clean and improve sexual excitation effect, and is a lubricating product capable of being used for a long time. Can solve the problem of vaginal dryness caused by reasons such as menopause, not only can effectively lubricate, but also has the effects of relieving itching and diminishing inflammation.
In addition, the invention also has the advantages of easily obtained raw materials, easy operation, mild reaction conditions, obvious effect, low cost and the like.
Detailed Description
The present invention will be described in detail with reference to specific examples.
Example 1
A black tea fungus fermentation lubricating liquid is prepared from the following raw materials in parts by weight: 20 parts of black tea fungus fermentation liquor, 35 parts of glycerol, 1 part of hyaluronic acid, 1.5 parts of water-soluble camellia seed oil, 0.35 part of cananga odorata essential oil, 0.65 part of hydroxyethyl urea, 0.7 part of black tea fungus fermentation membrane modifier and 40.8 parts of deionized water.
A preparation method of black tea fungus fermentation lubricating liquid comprises the following steps: (1) dissolving 0.7 weight part of black tea fungus fermentation membrane modifier with 40.8 weight parts of deionized water at normal temperature; (2) adding 1 weight part of hyaluronic acid, heating to 60 ℃, stirring to dissolve and uniformly mixing; (3) keeping the temperature at 60 ℃, adding 53 parts by weight of glycerol and 0.65 part by weight of hydroxyethyl urea, stirring to dissolve and uniformly mixing; (4) cooling to room temperature, sequentially adding 1.5 parts by weight of water-soluble camellia oleosa seed oil and 20 parts by weight of black tea fungus fermentation liquor, and uniformly mixing; (5) adding 0.35 weight part of cananga odorata essential oil, and uniformly mixing to obtain the lubricating liquid.
Further, the black tea fungus fermentation liquor is prepared by the following steps: mixing 4 parts by weight of black tea, 8 parts by weight of picria felterrae lour, 2 parts by weight of wormwood, 45 parts by weight of white granulated sugar and 900 parts by weight of deionized water, boiling for 100min, standing, cooling, filtering, adding the deionized water into the filtrate to keep the filtrate at 900 parts by weight, uniformly mixing, adding the filtrate into a container, placing the container into a high-temperature sterilization and over-sterilization container for 20min, cooling to room temperature after sterilization is finished, adding 45 parts by weight of black tea fungus mother liquor, sealing the mixture with gauze, fermenting for 7 days at normal temperature and normal pressure, and filtering with a screen to obtain black tea fungus fermentation liquor.
Further, the black tea fungus fermentation membrane modifier is prepared by the following steps: (1) pre-cooling 95 parts by weight of mixed aqueous solution of 5 mass percent NaOH and 6 mass percent hydroxyethyl urea to-7 ℃; (2) rapidly adding 2 parts by weight of black tea fungus fermentation membrane before the solution is not frozen, rapidly stirring at room temperature for 5min, and standing at-7 deg.C for 20min to obtain black tea fungus fermentation membrane solution with mass concentration of 2%; (3) adding 25 parts by weight of chloroethanol into 100 parts by weight of black tea fungus fermentation membrane solution with the mass concentration of 2%, reacting for 2 hours at room temperature, heating to 50 ℃ for reaction for 2 hours, adding acetic acid for neutralization to neutrality, and stopping reaction; (4) after the solution after reaction is dialyzed, centrifuging for 10min at 400r/min for separation; (5) collecting supernatant, and vacuum drying to obtain black tea fungus fermentation membrane modified substance.
Further, the water-soluble camellia oleosa seed oil is prepared by the following steps: (1) 100 parts by weight of polyglycerol-10 and 2 parts by weight of saturated disodium hydrogen phosphate solution are added into a three-neck flask provided with a spherical reflux condenser pipe; (2) stirring in water bath at 60 ℃ for 1 h; (3) then, 14 parts by weight of camellia seed oil is firstly dripped, and then 2 parts by weight of p-toluenesulfonic acid is added to continue to react for 1 hour at 60 ℃; (4) dropwise adding saturated sodium bicarbonate solution until the pH value of the solution is 6.5-7.5; (5) and (3) cooling the liquid, transferring the liquid into a separating funnel, and directly separating to obtain a lower-layer solution, namely the water-soluble camellia seed oil.
Example 2
A black tea fungus fermentation lubricating liquid is prepared from the following raw materials in parts by weight: 22 parts of black tea fungus fermentation liquor, 38 parts of glycerol, 0.75 part of hyaluronic acid, 1.25 parts of water-soluble camellia seed oil, 0.4 part of cananga odorata essential oil, 0.65 part of hydroxyethyl urea, 0.65 part of black tea fungus fermentation membrane modifier and 36.3 parts of deionized water.
A preparation method of black tea fungus fermentation lubricating liquid comprises the following steps: (1) dissolving 0.65 weight part of black tea fungus fermentation membrane modifier with 36.3 weight parts of deionized water at normal temperature; (2) adding 0.75 weight part of hyaluronic acid, heating to 60 ℃, stirring to dissolve and uniformly mixing; (3) keeping the temperature at 60 ℃, adding 38 parts by weight of glycerol and 0.65 part by weight of hydroxyethyl urea, stirring to dissolve and uniformly mixing; (4) cooling to room temperature, sequentially adding 1.25 parts by weight of water-soluble camellia oleosa seed oil and 22 parts by weight of black tea fungus fermentation liquor, and uniformly mixing; (5) adding 0.4 weight part of cananga odorata essential oil, and uniformly mixing to obtain the lubricating liquid.
Further, the black tea fungus fermentation liquor is prepared by the following steps: mixing 5 parts by weight of black tea, 10 parts by weight of picria felterrae lour, 4 parts by weight of wormwood, 50 parts by weight of white granulated sugar and 1000 parts by weight of deionized water, boiling for 110min, standing, cooling, filtering, adding the deionized water into the filtrate to keep the filtrate at 1000 parts by weight, uniformly mixing, adding into a container, placing into a high-temperature sterilization container, carrying out re-sterilization for 20min, cooling to room temperature after sterilization is finished, adding 50 parts by weight of black tea fungus mother liquor, sealing with gauze, fermenting for 7 days at normal temperature and normal pressure, and filtering with a screen to obtain black tea fungus fermentation liquor.
Further, the black tea fungus fermentation membrane modifier is prepared by the following steps: (1) pre-cooling 95 parts by weight of mixed aqueous solution of 5 mass percent NaOH and 6 mass percent hydroxyethyl urea to-7 ℃; (2) quickly adding 1.5 weight parts of black tea fungus fermentation membrane before the solution is not frozen, quickly stirring at room temperature for 5min, and standing at-7 deg.C for 20min to obtain 1.5-3% black tea fungus fermentation membrane solution; (3) adding 20 parts by weight of chloroethanol into 100 parts by weight of black tea fungus fermentation membrane solution with the mass concentration of 1.5%, reacting for 2 hours at room temperature, heating to 50 ℃ for reaction for 2 hours, adding acetic acid for neutralization to neutrality, and stopping reaction; (4) after the solution after reaction is dialyzed, centrifuging for 10min at 400r/min for separation; (5) collecting supernatant, and vacuum drying to obtain black tea fungus fermentation membrane modified substance.
Further, the water-soluble camellia oleosa seed oil is prepared by the following steps: (1) 100 parts by weight of polyglycerol-10 and 1.5 parts by weight of saturated disodium hydrogen phosphate solution are added into a three-necked flask provided with a spherical reflux condenser pipe; (2) stirring in water bath at 60 ℃ for 1 h; (3) then, dropwise adding 15 parts by weight of camellia oleosa seed oil, adding 2 parts by weight of p-toluenesulfonic acid, and continuing to react for 1 hour at 60 ℃; (4) dropwise adding saturated sodium bicarbonate solution until the pH value of the solution is 6.5; (5) and (3) cooling the liquid, transferring the liquid into a separating funnel, and directly separating to obtain a lower-layer solution, namely the water-soluble camellia seed oil.
Example 3
A black tea fungus fermentation lubricating liquid is prepared from the following raw materials in parts by weight: 16.5 parts of black tea fungus fermentation liquor, 37.5 parts of glycerol, 1.2 parts of hyaluronic acid, 1.8 parts of water-soluble camellia seed oil, 0.35 part of cananga odorata essential oil, 0.65 part of hydroxyethyl urea, 0.75 part of black tea fungus fermentation membrane modifier and 41.25 parts of deionized water.
A preparation method of black tea fungus fermentation lubricating liquid comprises the following steps: (1) dissolving 0.75 weight part of black tea fungus fermentation membrane modifier with 41.25 weight parts of deionized water at normal temperature; (2) adding 1.2 parts by weight of hyaluronic acid, heating to 60 ℃, stirring to dissolve and uniformly mixing; (3) keeping the temperature at 60 ℃, adding 37.5 parts by weight of glycerol and 0.65 part by weight of hydroxyethyl urea, stirring to dissolve and uniformly mixing; (4) cooling to room temperature, sequentially adding 1.8 parts by weight of water-soluble camellia oleosa seed oil and 16.5 parts by weight of black tea fungus fermentation liquor, and uniformly mixing; (5) adding 0.35 weight part of cananga odorata essential oil, and uniformly mixing to obtain the lubricating liquid.
Further, the black tea fungus fermentation liquor is prepared by the following steps: mixing 5 parts by weight of black tea, 10 parts by weight of picria felterrae lour, 5 parts by weight of wormwood, 48 parts by weight of white granulated sugar and 1000 parts by weight of deionized water, boiling for 110min, standing, cooling, filtering, adding the deionized water into the filtrate to keep the filtrate at 1000 parts by weight, uniformly mixing, adding into a container, placing into a high-temperature sterilization container, carrying out re-sterilization for 20min, cooling to room temperature after sterilization is finished, adding 50 parts by weight of black tea fungus mother liquor, sealing with gauze, fermenting for 8 days at normal temperature and normal pressure, and filtering with a screen to obtain black tea fungus fermentation liquor.
Further, the black tea fungus fermentation membrane modifier is prepared by the following steps: (1) precooling 100 parts by weight of mixed aqueous solution of NaOH with the mass concentration of 5% and hydroxyethyl urea with the mass concentration of 6% to-7 ℃; (2) rapidly adding 1-3 weight parts of black tea fungus fermentation membrane before the solution is not frozen, rapidly stirring at room temperature for 5min, and standing at-7 deg.C for 20min to obtain 3% black tea fungus fermentation membrane solution; (3) adding 30 parts by weight of chloroethanol into 100 parts by weight of black tea fungus fermentation membrane solution with the mass concentration of 3%, reacting for 2 hours at room temperature, heating to 50 ℃ for reaction for 2 hours, adding acetic acid for neutralization to neutrality, and stopping reaction; (4) after the solution after reaction is dialyzed, centrifuging for 10min at 400r/min for separation; (5) collecting supernatant, and vacuum drying to obtain black tea fungus fermentation membrane modified substance.
Further, the water-soluble camellia oleosa seed oil is prepared by the following steps: (1) 100 parts by weight of polyglycerol-10 and 1.5 parts by weight of saturated disodium hydrogen phosphate solution are added into a three-necked flask provided with a spherical reflux condenser pipe; (2) stirring in water bath at 60 ℃ for 1 h; (3) then, 18 parts by weight of camellia oleosa seed oil is firstly dripped, and then 2 parts by weight of p-toluenesulfonic acid is added to continue to react for 1 hour at 60 ℃; (4) dropwise adding saturated sodium bicarbonate solution until the pH value of the solution is 6.5-7.5; (5) and (3) cooling the liquid, transferring the liquid into a separating funnel, and directly separating to obtain a lower-layer solution, namely the water-soluble camellia seed oil.
Example 4
A black tea fungus fermentation lubricating liquid is prepared from the following raw materials in parts by weight: 17.5 parts of black tea fungus fermentation liquor, 32.5 parts of glycerol, 1.2 parts of hyaluronic acid, 1.8 parts of water-soluble camellia seed oil, 0.35 part of cananga odorata essential oil, 0.65 part of hydroxyethyl urea, 0.8 part of black tea fungus fermentation membrane modifier and 45.2 parts of deionized water.
A preparation method of black tea fungus fermentation lubricating liquid comprises the following steps: (1) dissolving 0.8 weight part of black tea fungus fermentation membrane modifier with 45.2 weight parts of deionized water at normal temperature; (2) adding 1.2 parts by weight of hyaluronic acid, heating to 60 ℃, stirring to dissolve and uniformly mixing; (3) keeping the temperature at 60 ℃, adding 32.5 parts by weight of glycerol and 0.65 part by weight of hydroxyethyl urea, stirring to dissolve and uniformly mixing; (4) cooling to room temperature, sequentially adding 1.8 parts by weight of water-soluble camellia oleosa seed oil and 17.5 parts by weight of black tea fungus fermentation liquor, and uniformly mixing; (5) adding 0.35 weight part of cananga odorata essential oil, and uniformly mixing to obtain the lubricating liquid.
Further, the black tea fungus fermentation liquor is prepared by the following steps: mixing 6 parts by weight of black tea, 11 parts by weight of picria felterrae lour, 4 parts by weight of wormwood, 50 parts by weight of white granulated sugar and 1100 parts by weight of deionized water, boiling for 110min, standing, cooling, filtering, adding deionized water into the filtrate to keep the weight of the filtrate at 1100 parts, uniformly mixing, adding into a container, placing into a high-temperature sterilization container, carrying out re-sterilization for 20min, cooling to room temperature after sterilization is finished, adding 55 parts by weight of black tea fungus mother liquor, sealing with gauze, fermenting for 8 days at normal temperature and normal pressure, and filtering with a screen to obtain black tea fungus fermentation liquor.
Further, the black tea fungus fermentation membrane modifier is prepared by the following steps: (1) precooling 100 parts by weight of mixed aqueous solution of NaOH with the mass concentration of 5% and hydroxyethyl urea with the mass concentration of 6% to-7 ℃; (2) rapidly adding 2 parts by weight of black tea fungus fermentation membrane before the solution is not frozen, rapidly stirring at room temperature for 5min, and standing at-7 deg.C for 20min to obtain black tea fungus fermentation membrane solution with mass concentration of 2%; (3) adding 30 parts by weight of chloroethanol into 100 parts by weight of black tea fungus fermentation membrane solution with the mass concentration of 2%, reacting for 2 hours at room temperature, heating to 50 ℃ for reaction for 2 hours, adding acetic acid for neutralization to neutrality, and stopping reaction; (4) after the solution after reaction is dialyzed, centrifuging for 10min at 400r/min for separation; (5) collecting supernatant, and vacuum drying to obtain black tea fungus fermentation membrane modified substance.
Further, the water-soluble camellia oleosa seed oil is prepared by the following steps: (1) 100 parts by weight of polyglycerol-10 and 2 parts by weight of saturated disodium hydrogen phosphate solution are added into a three-neck flask provided with a spherical reflux condenser pipe; (2) stirring in water bath at 60 ℃ for 1 h; (3) then, 19 parts by weight of camellia oleosa seed oil is firstly dripped, and then 2 parts by weight of p-toluenesulfonic acid is added to continue to react for 1 hour at 60 ℃; (4) dropwise adding saturated sodium bicarbonate solution until the pH value of the solution is 6.5-7.5; (5) and (3) cooling the liquid, transferring the liquid into a separating funnel, and directly separating to obtain a lower-layer solution, namely the water-soluble camellia seed oil.
Example 5
A black tea fungus fermentation lubricating liquid is prepared from the following raw materials in parts by weight: 22 parts of black tea fungus fermentation liquor, 32 parts of glycerol, 1 part of hyaluronic acid, 1.75 parts of water-soluble camellia seed oil, 0.35 part of cananga odorata essential oil, 0.65 part of hydroxyethyl urea, 0.75 part of black tea fungus fermentation membrane modifier and 41.5 parts of deionized water.
A preparation method of black tea fungus fermentation lubricating liquid comprises the following steps: (1) dissolving 0.75 weight part of black tea fungus fermentation membrane modifier with 41.5 weight parts of deionized water at normal temperature; (2) adding 1 weight part of hyaluronic acid, heating to 60 ℃, stirring to dissolve and uniformly mixing; (3) keeping the temperature at 60 ℃, adding 32 parts by weight of glycerol and 0.65 part by weight of hydroxyethyl urea, stirring to dissolve and uniformly mixing; (4) cooling to room temperature, sequentially adding 1.75 parts by weight of water-soluble camellia oleosa seed oil and 22 parts by weight of black tea fungus fermentation liquor, and uniformly mixing; (5) adding 0.35 weight part of cananga odorata essential oil, and uniformly mixing to obtain the lubricating liquid.
Further, the black tea fungus fermentation liquor is prepared by the following steps: mixing 8 parts by weight of black tea, 12 parts by weight of picria felterrae lour, 6 parts by weight of wormwood, 55 parts by weight of white granulated sugar and 1200 parts by weight of deionized water, boiling for 120min, standing, cooling, filtering, adding the deionized water into the filtrate to keep the filtrate at 1200 parts by weight, uniformly mixing, adding into a container, placing into a high-temperature sterilization container, carrying out re-sterilization for 20min, cooling to room temperature after sterilization is finished, adding 60 parts by weight of black tea fungus mother liquor, sealing with gauze, fermenting for 9 days at normal temperature and normal pressure, and filtering with a screen to obtain black tea fungus fermentation liquor.
Further, the black tea fungus fermentation membrane modifier is prepared by the following steps: (1) pre-cooling 110 parts by weight of mixed aqueous solution of 5 mass percent NaOH and 6 mass percent hydroxyethyl urea to-7 ℃; (2) quickly adding 3 parts by weight of black tea fungus fermentation membrane before the solution is not frozen, quickly stirring at room temperature for 5min, and standing at-7 ℃ for 20min to obtain a black tea fungus fermentation membrane solution with the mass concentration of 3%; (3) adding 35 parts by weight of chloroethanol into 100 parts by weight of black tea fungus fermentation membrane solution with the mass concentration of 3%, reacting for 2 hours at room temperature, heating to 50 ℃ for reaction for 2 hours, adding acetic acid for neutralization to neutrality, and stopping reaction; (4) after the solution after reaction is dialyzed, centrifuging for 10min at 400r/min for separation; (5) collecting supernatant, and vacuum drying to obtain black tea fungus fermentation membrane modified substance.
Further, the water-soluble camellia oleosa seed oil is prepared by the following steps: (1) 100 parts by weight of polyglycerol-10 and 2 parts by weight of saturated disodium hydrogen phosphate solution are added into a three-neck flask provided with a spherical reflux condenser pipe; (2) stirring in water bath at 60 ℃ for 1 h; (3) then, dropwise adding 20 parts by weight of camellia oleosa seed oil, adding 2 parts by weight of p-toluenesulfonic acid, and continuing to react for 1 hour at 60 ℃; (4) dropwise adding saturated sodium bicarbonate solution until the pH value of the solution is 6.5-7.5; (5) and (3) cooling the liquid, transferring the liquid into a separating funnel, and directly separating to obtain a lower-layer solution, namely the water-soluble camellia seed oil.
Example 6
A black tea fungus fermentation lubricating liquid is prepared from the following raw materials in parts by weight: 18 parts of black tea fungus fermentation liquor, 36 parts of glycerol, 1 part of hyaluronic acid, 1.2 parts of water-soluble camellia seed oil, 0.35 part of cananga odorata essential oil, 0.65 part of hydroxyethyl urea, 0.8 part of black tea fungus fermentation membrane modifier and 42 parts of deionized water.
A preparation method of black tea fungus fermentation lubricating liquid comprises the following steps: (1) dissolving 0.8 part by weight of black tea fungus fermentation membrane modifier with 42 parts by weight of deionized water at normal temperature; (2) adding 1 weight part of hyaluronic acid, heating to 60 ℃, stirring to dissolve and uniformly mixing; (3) keeping the temperature at 60 ℃, adding 36 parts by weight of glycerol and 0.65 part by weight of hydroxyethyl urea, stirring to dissolve and uniformly mixing; (4) cooling to room temperature, sequentially adding 1.2 parts by weight of water-soluble camellia oleosa seed oil and 18 parts by weight of black tea fungus fermentation liquor, and uniformly mixing; (5) adding 0.35 weight part of cananga odorata essential oil, and uniformly mixing to obtain the lubricating liquid.
Further, the black tea fungus fermentation liquor is prepared by the following steps: mixing 8 parts by weight of black tea, 12 parts by weight of picria felterrae lour, 6 parts by weight of wormwood, 55 parts by weight of white granulated sugar and 1200 parts by weight of deionized water, boiling for 120min, standing, cooling, filtering, adding the deionized water into the filtrate to keep the filtrate at 1200 parts by weight, uniformly mixing, adding into a container, placing into a high-temperature sterilization container, carrying out re-sterilization for 20min, cooling to room temperature after sterilization is finished, adding 60 parts by weight of black tea fungus mother liquor, sealing with gauze, fermenting for 9 days at normal temperature and normal pressure, and filtering with a screen to obtain black tea fungus fermentation liquor.
Further, the black tea fungus fermentation membrane modifier is prepared by the following steps: (1) pre-cooling 110 parts by weight of mixed aqueous solution of 5 mass percent NaOH and 6 mass percent hydroxyethyl urea to-7 ℃; (2) quickly adding 3 parts by weight of black tea fungus fermentation membrane before the solution is not frozen, quickly stirring at room temperature for 5min, and standing at-7 ℃ for 20min to obtain a black tea fungus fermentation membrane solution with the mass concentration of 3%; (3) adding 35 parts by weight of chloroethanol into 100 parts by weight of black tea fungus fermentation membrane solution with the mass concentration of 3%, reacting for 2 hours at room temperature, heating to 50 ℃ for reaction for 2 hours, adding acetic acid for neutralization to neutrality, and stopping reaction; (4) after the solution after reaction is dialyzed, centrifuging for 10min at 400r/min for separation; (5) collecting supernatant, and vacuum drying to obtain black tea fungus fermentation membrane modified substance.
Further, the water-soluble camellia oleosa seed oil is prepared by the following steps: (1) 100 parts by weight of polyglycerol-10 and 2 parts by weight of saturated disodium hydrogen phosphate solution are added into a three-neck flask provided with a spherical reflux condenser pipe; (2) stirring in water bath at 60 ℃ for 1 h; (3) then, dropwise adding 20 parts by weight of camellia oleosa seed oil, adding 2 parts by weight of p-toluenesulfonic acid, and continuing to react for 1 hour at 60 ℃; (4) dropwise adding saturated sodium bicarbonate solution until the pH value of the solution is 6.5-7.5; (5) and (3) cooling the liquid, transferring the liquid into a separating funnel, and directly separating to obtain a lower-layer solution, namely the water-soluble camellia seed oil.
Example 7
A black tea fungus fermentation lubricating liquid is prepared from the following raw materials in parts by weight: 17 parts of black tea fungus fermentation liquor, 33 parts of glycerol, 1.2 parts of hyaluronic acid, 1.8 parts of water-soluble camellia seed oil, 0.35 part of cananga odorata essential oil, 0.65 part of hydroxyethyl urea, 0.7 part of black tea fungus fermentation membrane modifier and 45.3 parts of deionized water.
A preparation method of black tea fungus fermentation lubricating liquid comprises the following steps: (1) dissolving 0.7 weight part of black tea fungus fermentation membrane modifier with 45.3 weight parts of deionized water at normal temperature; (2) adding 1.2 parts by weight of hyaluronic acid, heating to 60 ℃, stirring to dissolve and uniformly mixing; (3) keeping the temperature at 60 ℃, adding 33 parts by weight of glycerol and 0.65 part by weight of hydroxyethyl urea, stirring to dissolve and uniformly mixing; (4) cooling to room temperature, sequentially adding 1.8 parts by weight of water-soluble camellia oleosa seed oil and 17 parts by weight of black tea fungus fermentation liquor, and uniformly mixing; (5) adding 0.35 weight part of cananga odorata essential oil, and uniformly mixing to obtain the lubricating liquid.
Further, the black tea fungus fermentation liquor is prepared by the following steps: mixing 6 parts by weight of black tea, 11 parts by weight of picria felterrae lour, 4 parts by weight of wormwood, 50 parts by weight of white granulated sugar and 1100 parts by weight of deionized water, boiling for 110min, standing, cooling, filtering, adding deionized water into the filtrate to keep the weight of the filtrate at 1100 parts, uniformly mixing, adding into a container, placing into a high-temperature sterilization container, carrying out re-sterilization for 20min, cooling to room temperature after sterilization is finished, adding 55 parts by weight of black tea fungus mother liquor, sealing with gauze, fermenting for 8 days at normal temperature and normal pressure, and filtering with a screen to obtain black tea fungus fermentation liquor.
Further, the black tea fungus fermentation membrane modifier is prepared by the following steps: (1) precooling 100 parts by weight of mixed aqueous solution of NaOH with the mass concentration of 5% and hydroxyethyl urea with the mass concentration of 6% to-7 ℃; (2) rapidly adding 2 parts by weight of black tea fungus fermentation membrane before the solution is not frozen, rapidly stirring at room temperature for 5min, and standing at-7 deg.C for 20min to obtain black tea fungus fermentation membrane solution with mass concentration of 2%; (3) adding 30 parts by weight of chloroethanol into 100 parts by weight of black tea fungus fermentation membrane solution with the mass concentration of 2%, reacting for 2 hours at room temperature, heating to 50 ℃ for reaction for 2 hours, adding acetic acid for neutralization to neutrality, and stopping reaction; (4) after the solution after reaction is dialyzed, centrifuging for 10min at 400r/min for separation; (5) collecting supernatant, and vacuum drying to obtain black tea fungus fermentation membrane modified substance.
Further, the water-soluble camellia oleosa seed oil is prepared by the following steps: (1) 100 parts by weight of polyglycerol-10 and 2 parts by weight of saturated disodium hydrogen phosphate solution are added into a three-neck flask provided with a spherical reflux condenser pipe; (2) stirring in water bath at 60 ℃ for 1 h; (3) then, 19 parts by weight of camellia oleosa seed oil is firstly dripped, and then 2 parts by weight of p-toluenesulfonic acid is added to continue to react for 1 hour at 60 ℃; (4) dropwise adding saturated sodium bicarbonate solution until the pH value of the solution is 6.5-7.5; (5) and (3) cooling the liquid, transferring the liquid into a separating funnel, and directly separating to obtain a lower-layer solution, namely the water-soluble camellia seed oil.
The above description is only an embodiment of the present invention, and not intended to limit the scope of the present invention, and all modifications of equivalent structures and equivalent processes, which are made by the present specification, or directly or indirectly applied to other related technical fields, are included in the scope of the present invention.
Claims (4)
1. The black tea fungus fermentation lubricating liquid is characterized by being prepared from the following raw materials in parts by weight: 15-25 parts of black tea fungus fermentation liquor, 30-40 parts of glycerol, 0.5-1.5 parts of hyaluronic acid, 0.5-1 parts of black tea fungus fermentation membrane modifier, 0.3-0.5 part of cananga odorata essential oil, 1-2 parts of water-soluble camellia seed oil, 0.5-1 part of hydroxyethyl urea and 30-50 parts of deionized water; the black tea fungus fermentation membrane modifier is prepared from the following raw materials in parts by weight: 100 parts of black tea fungus fermentation membrane solution with the mass concentration of 1.5-3%, 20-35 parts of chloroethanol and 2-10 parts of acetic acid; the black tea fungus fermentation membrane solution is prepared from the following raw materials in parts by weight: 90-110 parts of mixed aqueous solution of NaOH with the mass concentration of 5% and hydroxyethyl urea with the mass concentration of 6% and 1-3 parts of black tea fungus fermentation membrane; the water-soluble camellia seed oil is prepared from the following raw materials in parts by weight: polyglycerol-10100 parts, saturated disodium hydrogen phosphate solution 1-2 parts, camellia oleosa seed oil 12-20 parts, p-toluenesulfonic acid 2 parts and saturated sodium bicarbonate solution 1-3 parts.
2. The black tea fungus fermentation lubricating liquid as claimed in claim 1, wherein: the black tea fungus fermentation liquor is prepared from the following raw materials in parts by weight: 4-9 parts of black tea, 8-12 parts of picria fel-terrae lour, 2-6 parts of wormwood, 45-55 parts of white granulated sugar, 900 parts of deionized water, 1200 parts of mangosteen fungus mother liquor and 45-60 parts of black tea fungus mother liquor.
3. A preparation method of black tea fungus fermentation lubricating liquid is characterized by comprising the following steps: (1) dissolving 0.5-1 part by weight of black tea fungus fermentation membrane modifier with 30-50 parts by weight of deionized water at normal temperature; (2) adding 0.5-1.5 parts by weight of hyaluronic acid, heating to 60 ℃, stirring to dissolve and uniformly mixing; (3) keeping the temperature at 60 ℃, adding 30-40 parts by weight of glycerol and 0.5-1 part by weight of hydroxyethyl urea, stirring to dissolve and uniformly mixing; (4) cooling to room temperature, sequentially adding 1-2 parts by weight of water-soluble camellia oleosa seed oil and 15-25 parts by weight of black tea fungus fermentation liquor, and uniformly mixing; (5) adding 0.3-0.5 weight part of cananga odorata essential oil, and mixing uniformly to obtain a lubricating liquid; the black tea fungus fermentation membrane modifier is prepared by the following steps: (1) pre-cooling 90-110 parts by weight of mixed aqueous solution of 5 mass percent NaOH and 6 mass percent hydroxyethyl urea to-7 ℃; (2) rapidly adding 1-3 weight parts of black tea fungus fermentation membrane before the solution is not frozen, rapidly stirring at room temperature for 5min, and standing at-7 deg.C for 20min to obtain 1.5-3% black tea fungus fermentation membrane solution; (3) respectively adding 20-35 parts by weight of chloroethanol into 100 parts by weight of black tea fungus fermentation membrane solution with the mass concentration of 1.5-3%, reacting for 2 hours at room temperature, heating to 50 ℃ for reaction for 2 hours, adding acetic acid for neutralization to neutrality, and stopping reaction; (4) after the solution after reaction is dialyzed, centrifuging for 10min at 400r/min for separation; (5) collecting supernatant, and vacuum drying to obtain black tea fungus fermentation membrane modified substance; the water-soluble camellia oleosa seed oil is prepared by the following steps: (1) adding 100 parts by weight of polyglycerol-10 and 1-2 parts by weight of saturated disodium hydrogen phosphate solution into a three-neck flask provided with a spherical reflux condenser pipe; (2) stirring in water bath at 60 ℃ for 1 h; (3) then, dropwise adding 12-20 parts by weight of camellia oleosa seed oil, adding 2 parts by weight of p-toluenesulfonic acid, and continuing to react for 1h at 60 ℃; (4) dropwise adding saturated sodium bicarbonate solution until the pH value of the solution is 6.5-7.5; (5) and (3) cooling the liquid, transferring the liquid into a separating funnel, and directly separating to obtain a lower-layer solution, namely the water-soluble camellia seed oil.
4. The method of claim 3, wherein the black tea fungus fermentation broth is prepared by the steps of: mixing 4-9 parts by weight of black tea, 8-12 parts by weight of picria fel-terrae lour, 2-6 parts by weight of wormwood, 45-55 parts by weight of white granulated sugar and 1200 parts by weight of deionized water, boiling for 100-fold-cake.
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