CN107794751A - 一种抗皱免烫整理剂及其制备方法 - Google Patents

一种抗皱免烫整理剂及其制备方法 Download PDF

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CN107794751A
CN107794751A CN201710888396.1A CN201710888396A CN107794751A CN 107794751 A CN107794751 A CN 107794751A CN 201710888396 A CN201710888396 A CN 201710888396A CN 107794751 A CN107794751 A CN 107794751A
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crease
iron
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chitosan
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储平
徐有琦
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Jiangsu New Lucky Polytron Technologies Inc
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Abstract

本发明公开了一种抗皱免烫整理剂及其制备方法，所述抗皱免烫整理剂由如下重量份数的原料组成：丁烷四酸10‑20份、柠檬酸铵3‑5份、三乙醇胺3‑5份、失水山梨醇聚氧乙烯醚5‑7份、硼酸3‑5份、木质素磺酸3‑5份、聚乙烯蜡3‑5份、次磷酸钠5‑7份、有机硅树脂5‑10份、壳聚糖10‑15份、去离子水20‑30份。本发明的抗皱免烫整理剂应用织物之后，织物具有优异的防皱抗皱性能，而且耐水洗，水洗之后仍然具有良好的抗皱防皱性能。本发明的抗皱免烫整理剂制造工艺简单易操作，原料价格低廉易获得，且毒性低，对人体不刺激，挥发性低，整理后的织物其韧性、强度、手感基本不受影响。

Description

一种抗皱免烫整理剂及其制备方法
技术领域
本发明属于纺织助剂技术领域，更具体是涉及一种抗皱免烫整理剂及其制备方法。
背景技术
高新技术发展日新月异，人们生活水平不断提高，对于纺织品的需求不再局限于保暖舒适等织物固有的特性，根据不同的行业、人群、用途，人们对纺织品的要求也越来越多，对服装提出了舒适、卫生、美观、保健、防护等要求，纺织品的整理技术也不断涌现。
天然棉织物具有优良的性能，是理想的服装材料，但是棉织物经水洗之后需要熨烫，这就给服用者带来很大的麻烦。天然纤维中的毛纤维、真丝纤维等蛋白质纤维虽然比纤维素纤维好一点，但是湿弹性与防皱性都不及合成纤维。因此，这类服装水洗之后都需要熨烫。
近几年，免烫整理剂很受欢迎，但是传统的N-羟甲基酰胺类免烫抗皱整理剂，抗皱效果良好，但经它处理后的织物在加工、贮存和服用过程中会释放出对人体有害的甲醛。
发明内容
本发明的目的在于提供一种抗皱免烫整理剂及制备方法，以解决上述背景技术中提出的问题。
为实现上述目的，本发明提供如下技术方案：
一种抗皱免烫整理剂，按照重量份数，包括以下组分：丁烷四酸10-20份、柠檬酸铵3-5份、三乙醇胺3-5份、失水山梨醇聚氧乙烯醚5-7份、硼酸3-5份、木质素磺酸3-5份、聚乙烯蜡3-5份、次磷酸钠5-7份、有机硅树脂5-10份、壳聚糖10-15份、去离子水20-30份。
优选地，所述的抗皱免烫整理剂，按照重量份数，包括以下组分：丁烷四酸10份、柠檬酸铵3份、三乙醇胺3份、失水山梨醇聚氧乙烯醚5份、硼酸3份、木质素磺酸3份、聚乙烯蜡3份、次磷酸钠5份、有机硅树脂5份、壳聚糖10份、去离子水20份。
优选地，所述的抗皱免烫整理剂，按照重量份数，包括以下组分：丁烷四酸15份、柠檬酸铵4份、三乙醇胺4份、失水山梨醇聚氧乙烯醚6份、硼酸4份、木质素磺酸4份、聚乙烯蜡4份、次磷酸钠6份、有机硅树脂8份、壳聚糖13份、去离子水25份。
优选地，所述的抗皱免烫整理剂，按照重量份数，包括以下组分：丁烷四酸20份、柠檬酸铵5份、三乙醇胺5份、失水山梨醇聚氧乙烯醚7份、硼酸5份、木质素磺酸5份、聚乙烯蜡5份、次磷酸钠7份、有机硅树脂10份、壳聚糖15份、去离子水30份。
一种抗皱免烫整理剂的制备方法，具体步骤如下：
(1)在反应釜中加入聚乙烯蜡3-5份，升高温度至60-70℃，将其融化为液体；
(2)先将丁烷四酸10-20份、柠檬酸铵3-5份、壳聚糖10-15份、去离子水20-30份在另一个反应釜中搅拌均匀；
(3)步骤(1)的溶液加入步骤(2)的溶液中，500-1000转/分钟，搅拌20-30分钟；
(4)加入硼酸3-5份、木质素磺酸3-5份、次磷酸钠5-7份，500-1000转/分钟，搅拌10-20分钟；
(5)加入三乙醇胺3-5份、失水山梨醇聚氧乙烯醚5-7份、有机硅树脂5-10份，500-1000转/分钟，搅拌20-30分钟；
(6)关停搅拌，得到配制好的液体抗皱免烫整理剂；
(7)静置冷却至搅拌釜中液体抗皱免烫整理剂低于20℃，放料封装，制得成品。
与现有技术相比，本发明的有益效果是：
1、本发明的抗皱免烫整理剂应用织物之后，织物具有优异的防皱抗皱性能，而且耐水洗，水洗之后仍然具有良好的抗皱防皱性能。
2、本发明的抗皱免烫整理剂制造工艺简单易操作，原料价格低廉易获得，且毒性低，对人体不刺激，挥发性低，整理后的织物其韧性、强度、手感基本不受影响。
3、本发明的抗皱免烫整理剂所用各种原料之间相互配伍，协同作用，共同组成性能优异的产品。
4、简化工艺，操作安全简单，易于工业化生产。
5、本发明的抗皱免烫整理剂施工简单，可以通过浸渍、喷涂、辊涂等进行施加，生产效率提高。
6、本发明的使用可收到良好的经济效益。
具体实施实例
本发明公开了一种抗皱免烫整理剂，按照重量份数，包括以下组分：丁烷四酸10-20份、柠檬酸铵3-5份、三乙醇胺3-5份、失水山梨醇聚氧乙烯醚5-7份、硼酸3-5份、木质素磺酸3-5份、聚乙烯蜡3-5份、次磷酸钠5-7份、有机硅树脂5-10份、壳聚糖10-15份、去离子水20-30份。
本发明还提供了一种抗皱免烫整理剂的制备方法，具体步骤如下：
(1)在反应釜中加入聚乙烯蜡3-5份，升高温度至60-70℃，将其融化为液体；
(2)先将丁烷四酸10-20份、柠檬酸铵3-5份、壳聚糖10-15份、去离子水20-30份在另一个反应釜中搅拌均匀；
(3)步骤(1)的溶液加入步骤(2)的溶液中，500-1000转/分钟，搅拌20-30分钟；
(4)加入硼酸3-5份、木质素磺酸3-5份、次磷酸钠5-7份，500-1000转/分钟，搅拌10-20分钟；
(5)加入三乙醇胺3-5份、失水山梨醇聚氧乙烯醚5-7份、有机硅树脂5-10份，500-1000转/分钟，搅拌20-30分钟；
(6)关停搅拌，得到配制好的液体抗皱免烫整理剂；
(7)静置冷却至搅拌釜中液体抗皱免烫整理剂低于20℃，放料封装，制得成品。
实施例1
本发明公开了一种抗皱免烫整理剂，按照重量份数，包括以下组分：丁烷四酸10份、柠檬酸铵3份、三乙醇胺3份、失水山梨醇聚氧乙烯醚5份、硼酸3份、木质素磺酸3份、聚乙烯蜡3份、次磷酸钠5份、有机硅树脂5份、壳聚糖10份、去离子水20份。
本发明还提供了一种抗皱免烫整理剂的制备方法，具体步骤如下：
(1)在反应釜中加入聚乙烯蜡3份，升高温度至60℃，将其融化为液体；
(2)先将丁烷四酸10份、柠檬酸铵3份、壳聚糖10份、去离子水20份在另一个反应釜中搅拌均匀；
(3)步骤(1)的溶液加入步骤(2)的溶液中，500转/分钟，搅拌25分钟；
(4)加入硼酸3份、木质素磺酸3份、次磷酸钠5份，500转/分钟，搅拌10分钟；
(5)加入三乙醇胺3份、失水山梨醇聚氧乙烯醚5份、有机硅树脂5份，500转/分钟，搅拌25分钟；
(6)关停搅拌，得到配制好的液体抗皱免烫整理剂；
(7)静置冷却至搅拌釜中液体抗皱免烫整理剂低于20℃，放料封装，制得成品。
实施例2
本发明公开了一种抗皱免烫整理剂，按照重量份数，包括以下组分：丁烷四酸15份、柠檬酸铵4份、三乙醇胺4份、失水山梨醇聚氧乙烯醚6份、硼酸4份、木质素磺酸4份、聚乙烯蜡4份、次磷酸钠6份、有机硅树脂8份、壳聚糖13份、去离子水25份。
本发明还提供了一种抗皱免烫整理剂的制备方法，具体步骤如下：
(1)在反应釜中加入聚乙烯蜡4份，升高温度至65℃，将其融化为液体；
(2)先将丁烷四酸15份、柠檬酸铵4份、壳聚糖13份、去离子水25份在另一个反应釜中搅拌均匀；
(3)步骤(1)的溶液加入步骤(2)的溶液中，900转/分钟，搅拌25分钟；
(4)加入硼酸4份、木质素磺酸4份、次磷酸钠6份，800转/分钟，搅拌15分钟；
(5)加入三乙醇胺4份、失水山梨醇聚氧乙烯醚6份、有机硅树脂8份，800转/分钟，搅拌25分钟；
(6)关停搅拌，得到配制好的液体抗皱免烫整理剂；
(7)静置冷却至搅拌釜中液体抗皱免烫整理剂低于20℃，放料封装，制得成品。
实施例3
本发明公开了一种抗皱免烫整理剂，按照重量份数，包括以下组分：丁烷四酸20份、柠檬酸铵5份、三乙醇胺5份、失水山梨醇聚氧乙烯醚7份、硼酸5份、木质素磺酸5份、聚乙烯蜡5份、次磷酸钠7份、有机硅树脂10份、壳聚糖15份、去离子水30份。
本发明还提供了一种抗皱免烫整理剂的制备方法，具体步骤如下：
(1)在反应釜中加入聚乙烯蜡5份，升高温度至70℃，将其融化为液体；
(2)先将丁烷四酸20份、柠檬酸铵5份、壳聚糖15份、去离子水30份在另一个反应釜中搅拌均匀；
(3)步骤(1)的溶液加入步骤(2)的溶液中，1000转/分钟，搅拌30分钟；
(4)加入硼酸5份、木质素磺酸5份、次磷酸钠7份，1000转/分钟，搅拌20分钟；
(5)加入三乙醇胺5份、失水山梨醇聚氧乙烯醚7份、有机硅树脂10份，1000转/分钟，搅拌30分钟；
(6)关停搅拌，得到配制好的液体抗皱免烫整理剂；
(7)静置冷却至搅拌釜中液体抗皱免烫整理剂低于20℃，放料封装，制得成品。
实施例4
本发明公开了一种抗皱免烫整理剂，按照重量份数，包括以下组分：丁烷四酸20份、柠檬酸铵5份、三乙醇胺5份、失水山梨醇聚氧乙烯醚5份、硼酸3份、木质素磺酸5份、聚乙烯蜡5份、次磷酸钠7份、有机硅树脂5份、壳聚糖15份、去离子水20份。
本发明还提供了一种抗皱免烫整理剂的制备方法，具体步骤如下：
(1)在反应釜中加入聚乙烯蜡5份，升高温度至70℃，将其融化为液体；
(2)先将丁烷四酸20份、柠檬酸铵5份、壳聚糖15份、去离子水20份在另一个反应釜中搅拌均匀；
(3)步骤(1)的溶液加入步骤(2)的溶液中，1000转/分钟，搅拌20分钟；
(4)加入硼酸3份、木质素磺酸5份、次磷酸钠7份，900转/分钟，搅拌20分钟；
(5)加入三乙醇胺5份、失水山梨醇聚氧乙烯醚5份、有机硅树脂5份，900转/分钟，搅拌25分钟；
(6)关停搅拌，得到配制好的液体抗皱免烫整理剂；
(7)静置冷却至搅拌釜中液体抗皱免烫整理剂低于20℃，放料封装，制得成品。
测试例
将4块相同的织物放入实施例1、2、3、4的抗皱免烫整理剂溶液中浸轧，经过两浸两轧，然后升温至80-100℃预烘干，再在120-140℃烘干，然后用40-50℃热水清洗，最后用冷水冲洗，清洗后烘干，可以得到4块具有抗皱免烫性能的布。测试结果如下：
实施例 折皱回复角(°)
1 248
2 261
3 276
4 269
尽管已经示出和描述了本发明的实施例，对于本领域的普通技术人员而言，可以理解在不脱离本发明的原理和精神的情况下可以对这些实施例进行多种变化、修改、替换和变型，本发明的范围由所附权利要求及其等同物限定。

Claims (5)

1.一种抗皱免烫整理剂，其特征在于：所述抗皱免烫整理剂包括如下重量份数的原料：丁烷四酸10-20份、柠檬酸铵3-5份、三乙醇胺3-5份、失水山梨醇聚氧乙烯醚5-7份、硼酸3-5份、木质素磺酸3-5份、聚乙烯蜡3-5份、次磷酸钠5-7份、有机硅树脂5-10份、壳聚糖10-15份、去离子水20-30份。
2.根据权利要求1所述的抗皱免烫整理剂，其特征在于：按照重量份数，包括以下组分：丁烷四酸10份、柠檬酸铵3份、三乙醇胺3份、失水山梨醇聚氧乙烯醚5份、硼酸3份、木质素磺酸3份、聚乙烯蜡3份、次磷酸钠5份、有机硅树脂5份、壳聚糖10份、去离子水20份。
3.根据权利要求1所述的抗皱免烫整理剂，其特征在于：按照重量份数，包括以下组分：丁烷四酸15份、柠檬酸铵4份、三乙醇胺4份、失水山梨醇聚氧乙烯醚6份、硼酸4份、木质素磺酸4份、聚乙烯蜡4份、次磷酸钠6份、有机硅树脂8份、壳聚糖13份、去离子水25份。
4.根据权利要求1所述的抗皱免烫整理剂，其特征在于：按照重量份数，包括以下组分：丁烷四酸20份、柠檬酸铵5份、三乙醇胺5份、失水山梨醇聚氧乙烯醚7份、硼酸5份、木质素磺酸5份、聚乙烯蜡5份、次磷酸钠7份、有机硅树脂10份、壳聚糖15份、去离子水30份。
5.一种采用权利要求1-4中任一所述的抗皱免烫整理剂的制备方法，其特征在于：具体步骤如下：
步骤1，在反应釜中加入聚乙烯蜡3-5份，升高温度至60-70℃，将其融化为液体；
步骤2，先将丁烷四酸10-20份、柠檬酸铵3-5份、壳聚糖10-15份、去离子水20-30份在另一个反应釜中搅拌均匀；
步骤3，步骤1的溶液加入步骤2的溶液中，500-1000转/分钟，搅拌20-30分钟；
步骤4，加入硼酸3-5份、木质素磺酸3-5份、次磷酸钠5-7份，500-1000转/分钟，搅拌10-20分钟；
步骤5，加入三乙醇胺3-5份、失水山梨醇聚氧乙烯醚5-7份、有机硅树脂5-10份，500-1000转/分钟，搅拌20-30分钟；
步骤6，关停搅拌，得到配制好的液体抗皱免烫整理剂；
步骤7，静置冷却至搅拌釜中液体抗皱免烫整理剂低于20℃，放料封装，制得成品。
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CN110306344A (zh) * 2019-07-08 2019-10-08 东华大学 一种协同增效复配体系对棉织物抗皱整理的方法
CN115092771A (zh) * 2022-07-22 2022-09-23 杭州东南纺织有限公司 一种拉伸变形丝制备工艺及用于该工艺的设备

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CN106592223A (zh) * 2016-12-21 2017-04-26 阜阳市豹子头服饰科技有限公司 一种衬衫的防水防油防污型免烫整理液及其整理方法

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110306344A (zh) * 2019-07-08 2019-10-08 东华大学 一种协同增效复配体系对棉织物抗皱整理的方法
CN115092771A (zh) * 2022-07-22 2022-09-23 杭州东南纺织有限公司 一种拉伸变形丝制备工艺及用于该工艺的设备
CN115092771B (zh) * 2022-07-22 2023-08-11 杭州东南纺织有限公司 一种拉伸变形丝制备工艺及用于该工艺的设备

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