CN107740197A - A kind of ventilation wear-resistance and the fabric of antistatic waterproof and preparation method thereof - Google Patents
A kind of ventilation wear-resistance and the fabric of antistatic waterproof and preparation method thereof Download PDFInfo
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- CN107740197A CN107740197A CN201710843814.5A CN201710843814A CN107740197A CN 107740197 A CN107740197 A CN 107740197A CN 201710843814 A CN201710843814 A CN 201710843814A CN 107740197 A CN107740197 A CN 107740197A
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/08—Melt spinning methods
- D01D5/082—Melt spinning methods of mixed yarn
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D10/00—Physical treatment of artificial filaments or the like during manufacture, i.e. during a continuous production process before the filaments have been collected
- D01D10/02—Heat treatment
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/02—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from cellulose, cellulose derivatives, or proteins
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/14—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyester as constituent
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
- D06M13/238—Tannins, e.g. gallotannic acids
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/82—Textiles which contain different kinds of fibres
- D06P3/8204—Textiles which contain different kinds of fibres fibres of different chemical nature
- D06P3/8223—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups
- D06P3/8228—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups using one kind of dye
- D06P3/8233—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups using one kind of dye using dispersed dyes
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/32—Polyesters
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
Abstract
The present invention relates to fabric production field, more particularly to a kind of ventilation wear-resistance and the fabric of antistatic waterproof and preparation method thereof, the fabric is formed by cotton fibriia, viscose rayon and antistatic PET filament blending；The fabric is made from the following raw materials in parts by weight：30 40 parts of cotton fibriia, 35 40 parts of viscose rayon, 30 40 parts of antistatic PET filament；And 33 46 parts of PLA, 25 38 parts of metasilicic acid trimethyl, 22 28 parts of dilauryl thiodipropionate, 21 25 parts of neopelex, 13 17 parts of phosphatidyl-ethanolamine, 9 14 parts of potassium metabisulfite, 89 parts of cetyl trimethylammonium bromide, 89 parts of hydroxypropul starch, 57 parts of nano silicon, 57 parts of cetanol sulfuric ester sodium salt, 46 parts of linoleic acid, 34 parts of silane coupler, 34 parts of adhesive, 180 parts of deionized water.
Description
Technical field
The present invention relates to the fabric and its preparation of fabric production field, more particularly to a kind of ventilation wear-resistance and antistatic waterproof
Method.
Background technology
With the improvement of people's life quality, the demand in terms of clothing function is also gradually increased sharply.Especially in recent years
The influence of environmental degradation and haze so that garment material is inhaled grey degree and greatly increased.Many lives inconvenience such as face that electrostatic belt comes
Material strip electricity causes fabric corrugation, largely effects on attractive in appearance, fabric is powered so that wearer's mood is irritated, and going down for a long time, it is many to cause
Disease, fabric is powered or even can bring potential safety hazard, and such as in gas station place, build-up of static charges finally triggers the report of fire
It is not within minority.And the gas permeability and wearability of clothing are also the demand of people, the dress of ventilative clothing is more comfortable and resistance to
The clothing of mill, which can increase, wears the time.In the situation that country and society and consumer gradually improve to health and awareness of safety
Under, the rational effective fabric product new using functional raw material exploitation is the market demand.
But the functional fabric of in the market manufactures, to ventilative, wear-resisting, the fabric of antistatic and waterproof one is prepared also not
It can have both simultaneously.
The content of the invention
It is an object of the invention to provide a kind of ventilation wear-resistance and the fabric of antistatic waterproof and preparation method thereof, to realize face
Expect ventilation wear-resistance and with good antistatic and water-proof function technique effect.
In order to realize above-mentioned technical problem, the invention provides technical scheme to be：A kind of ventilation wear-resistance and antistatic waterproof
Fabric, the fabric forms by cotton fibriia, viscose rayon and antistatic PET filament blending；
The fabric is made from the following raw materials in parts by weight：Cotton fibriia 30-40 parts, viscose rayon 35-40 parts, resist quiet
Electric polyester fiber 30-40 parts；And
PLA 33-46 parts, metasilicic acid trimethyl 25-38 parts, dilauryl thiodipropionate 22-28 parts, dodecyl
Benzene sulfonic acid sodium salt 21-25 parts, phosphatidyl-ethanolamine 13-17 parts, potassium metabisulfite 9-14 parts, cetyl trimethylammonium bromide 8-
9 parts, hydroxypropul starch 8-9 parts, nano silicon 5-7 parts, cetanol sulfuric ester sodium salt 5-7 parts, linoleic acid 4-6 parts, silane
Coupling agent 3-4 parts, adhesive 3-4 parts, 180 parts of deionized water.
Further, the use of anti-static function powder is 30-150nm in the antistatic PET filament.
Further, the preparation method of described ventilation wear-resistance and the fabric of antistatic waterproof：Comprise the following steps：
Step S1：Each raw material is weighed according to parts by weight；
Step S2：By PLA, metasilicic acid trimethyl, dilauryl thiodipropionate, neopelex, phosphatide
Acyl monoethanolamine, potassium metabisulfite, cetyl trimethylammonium bromide, hydroxypropul starch and deionized water mixing, are placed in magnetic force
35-45min is stirred with rotating speed 650-750r/min on mixer, 80-90 DEG C is then raised temperature to, water-bath 15-25 minutes, obtains just
Walk mixture；、
Step S3：By cotton fibriia, viscose rayon, antistatic PET filament, nano silicon, cetanol sodium sulfovinate
Salt, which is collectively disposed in ball mill, carries out ball-milling treatment, and the rotating speed of ball mill is 220-280r/min, Ball-milling Time 1-2h, makes to mix
Each component is uniformly dispersed in compound, obtains ball-milled mixtures；
Step S4：The ball-milled mixtures that step S2 initial mixture and step S3 are obtained are added in high pressure homogenizer,
Adding linoleic acid, silane coupler, adhesive makes it well mixed, is melted at 350-360 DEG C, obtains middle production
Thing；
Step S5：The intermediate product obtained in step S4 is put into double screw extruder and carries out extrusion molding, is obtained just
Walk fabric；
Step S6：Preliminary fabric is subjected to heat treatment, treatment temperature remains 120-230 DEG C；
Step S7：Preliminary fabric is subjected to whole dye, dyed, dried and is washed respectively, wherein, the dyeing temperature is protected
Hold as 80-135 DEG C, the drying keeping temperature is 100-180 DEG C；
Step S8：Preliminary fabric is finally subjected to processing and forming, obtains final fabric.
Further, in the step S4, the pressure of the high pressure homogenizer uses 16-18Mpa.
Further, in the step S5, the screw speed of the double screw extruder is 250-280r/min；Twin-screw
Extruder is divided into four segmentations, wherein the temperature of four segmentations is respectively：One 170-190 DEG C of wise temperature, two-section temperature
200-210 DEG C, three 235-250 DEG C of wise temperatures, and 175-185 DEG C of four wise temperatures.
Further, in the step S6, water-proofing treatment is also included in heat treatment, using waterproofing agent 25-30g/L；
It is 140 DEG C of preliminary dryings that first segment oven temperature is adjusted during treatment temperature, and remaining section oven temperature is 170 bakings,
Speed is kept in 45-50r/min, the fabric goes out after baking oven through cooling down wind and cooling water temperature, after temperature is down to 30-35 DEG C
Stable fabric form.
Further, in the step S6, the sizing speed is 15-30m/min.
Further, softener washing is added in the step S7, in the washing.
Further, in the step S7, dyeing includes warming-up section, holds temperature section and temperature descending section.
Further, the warming-up section process is：Initial temperature is 25-35 DEG C, and 80-90 DEG C is warming up to 1-3 DEG C/min
And 3-8min is kept, it is being warming up to 100-120 DEG C with 2-3 DEG C/min and is being incubated 3-8min, is finally being warming up to 1-3 DEG C/min
125-135℃；
The temperature section process of holding is：Keeping temperature is 125-135 DEG C of 20-50min；
The temperature descending section process is：100-120 DEG C is cooled to 0.5-1.5 DEG C/min and keeps 3-8min, with 1-3
DEG C/min is cooled to 70-90 DEG C and is incubated 15-40min, finally it is cooled to 30-50 DEG C with 1.5-4 DEG C/min.
Face liber made of the present invention can have ventilation wear-resistance, antistatic and waterproof quadruple effect simultaneously.Antistatic side
Face, half-life period, compared with product gain 80% or so made from other method, charge density was up to 1.1uc/m up to 0.8s (A levels)2,
Product gain 75% or so is made compared with other method, product gain 80% is made compared with other method up to 80V in frictional static voltage
Left and right, at the same time, it, which can also stablize, ensures that fabric classification of waterproof is 4 grades.
Further, it is aided with magnetic agitation after the dispensing mixing that the present invention uses, heat up water-bath, abrading-ball processing, and high pressure is equal
The techniques such as matter, Screw Extrusion, the fabric good air permeability being prepared for being, anti-wear performance is strong, can meet industry requirement, and
Antistatic fibre component is not destroyed.
Embodiment
The present invention is further detailed explanation now.
Embodiment 1：
The invention provides a kind of ventilation wear-resistance and the fabric of antistatic waterproof, the fabric is fine by cotton fibriia, viscose glue
Peacekeeping antistatic PET filament blending forms；
The fabric is made from the following raw materials in parts by weight：30 parts of cotton fibriia, 40 parts of viscose rayon, anti-electrostatic polyester are fine
30 parts of dimension；And
33 parts of PLA, 25 parts of metasilicic acid trimethyl, 22 parts of dilauryl thiodipropionate, neopelex 21
Part, 13 parts of phosphatidyl-ethanolamine, 9 parts of potassium metabisulfite, 8 parts of cetyl trimethylammonium bromide, 8 parts of hydroxypropul starch, receive
5 parts of silica of rice, 5 parts of cetanol sulfuric ester sodium salt, 4 parts of linoleic acid, 3 parts of silane coupler, 3 parts of adhesive, deionized water
180 parts.
Specifically, the use of anti-static function powder is 80nm in the antistatic PET filament.
Described ventilation wear-resistance and the preparation method of the fabric of antistatic waterproof, comprise the following steps：
Step S1：Each raw material is weighed according to parts by weight；
Step S2：By PLA, metasilicic acid trimethyl, dilauryl thiodipropionate, neopelex, phosphatide
Acyl monoethanolamine, potassium metabisulfite, cetyl trimethylammonium bromide, hydroxypropul starch and deionized water mixing, are placed in magnetic force
35-45min is stirred with rotating speed 650-750r/min on mixer, 80-90 DEG C is then raised temperature to, water-bath 15-25 minutes, obtains just
Walk mixture；
Step S3：By cotton fibriia, viscose rayon, antistatic PET filament, nano silicon, cetanol sodium sulfovinate
Salt, which is collectively disposed in ball mill, carries out ball-milling treatment, and the rotating speed of ball mill is 220r/min, Ball-milling Time 1h, is made in mixture
Each component is uniformly dispersed, and obtains ball-milled mixtures；
Step S4：The ball-milled mixtures that step S2 initial mixture and step S3 are obtained are added in high pressure homogenizer,
Adding linoleic acid, silane coupler, adhesive makes it well mixed, is melted at 350 DEG C, obtains intermediate product；
Step S5：The intermediate product obtained in step S4 is put into double screw extruder and carries out extrusion molding, is obtained just
Walk fabric；
Step S6：Preliminary fabric is subjected to heat treatment, treatment temperature remains 120 DEG C；
Step S7：Preliminary fabric is subjected to whole dye, dyed, dried and is washed respectively, wherein, the dyeing temperature is protected
Hold as 80 DEG C, the drying keeping temperature is 100 DEG C；
Step S8：Preliminary fabric is finally subjected to processing and forming, obtains final fabric.
Specifically, in the step S4, the pressure of the high pressure homogenizer uses 16Mpa.
In the step S5, the screw speed of the double screw extruder is 250r/min, and double screw extruder is divided into four
Individual segmentation, wherein the temperature of four segmentations is respectively：One 170 DEG C of wise temperature, 200 DEG C of two-section temperature, three wise temperatures
235 DEG C, and 175 DEG C of four wise temperatures.
In the step S6, water-proofing treatment is also included in heat treatment, using waterproofing agent 25g/L；
It is 140 DEG C of preliminary dryings that first segment oven temperature is adjusted in treatment temperature, and remaining section oven temperature is 170 bakings, is kept
In 45r/min, the fabric goes out after baking oven through cooling down wind and cooling water temperature speed, stable fabric after temperature is down to 30 DEG C
Form.
In the step S6, the sizing speed is 15m/min.
Softener washing is added in the step S7, in the washing.Softener is handled using tannic acid.
In the step S7, dyeing includes warming-up section, holds temperature section and temperature descending section.
The warming-up section process is：Initial temperature is 25 DEG C, is warming up to 80 DEG C with 1 DEG C/min and keeps 3min, with 2
DEG C/min is warming up to 100 DEG C and is incubated 3min, finally it is warming up to 125 DEG C with 1 DEG C/min；
The temperature section process of holding is：Keeping temperature is 125 DEG C of 20min；
The temperature descending section process is：100 DEG C are cooled to 0.5 DEG C/min and keeps 3min, are cooled to 1 DEG C/min
70 DEG C and 15min is incubated, is finally cooled to 30 DEG C with 1.5 DEG C/min.
Dyestuff that the dyeing uses composition and mass parts for：The mass parts of disperse yellow 0.04, the matter of disperse red 0.0152
Part is measured, disperses 0.022 mass parts of orchid, the mass parts of 98% glacial acetic acid 0.5.
Embodiment 2：
The fabric of a kind of ventilation wear-resistance and antistatic waterproof, the fabric is by cotton fibriia, viscose rayon and Antistatic polyester
Synthetic fibre fiber blend forms；
The fabric is made from the following raw materials in parts by weight：35 parts of cotton fibriia, 35 parts of viscose rayon, anti-electrostatic polyester are fine
30 parts of dimension；And
46 parts of PLA, 38 parts of metasilicic acid trimethyl, 28 parts of dilauryl thiodipropionate, neopelex 25
Part, 17 parts of phosphatidyl-ethanolamine, 14 parts of potassium metabisulfite, 9 parts of cetyl trimethylammonium bromide, 9 parts of hydroxypropul starch, receive
7 parts of silica of rice, 7 parts of cetanol sulfuric ester sodium salt, 6 parts of linoleic acid, 4 parts of silane coupler, 4 parts of adhesive, deionized water
180 parts.
Specifically, the use of anti-static function powder is 150nm in the antistatic PET filament.
Described ventilation wear-resistance and the preparation method of the fabric of antistatic waterproof, comprise the following steps：
Step S1：Each raw material is weighed according to parts by weight；
Step S2：By PLA, metasilicic acid trimethyl, dilauryl thiodipropionate, neopelex, phosphatide
Acyl monoethanolamine, potassium metabisulfite, cetyl trimethylammonium bromide, hydroxypropul starch and deionized water mixing, are placed in magnetic force
45min is stirred with rotating speed 750r/min on mixer, 90 DEG C is then raised temperature to, water-bath 25 minutes, obtains initial mixture；
Step S3：By cotton fibriia, viscose rayon, antistatic PET filament, nano silicon, cetanol sodium sulfovinate
Salt, which is collectively disposed in ball mill, carries out ball-milling treatment, and the rotating speed of ball mill is 280r/min, Ball-milling Time 2h, is made in mixture
Each component is uniformly dispersed, and obtains ball-milled mixtures；
Step S4：The ball-milled mixtures that step S2 initial mixture and step S3 are obtained are added in high pressure homogenizer,
Adding linoleic acid, silane coupler, adhesive makes it well mixed, is melted at 360 DEG C, obtains intermediate product；
Step S5：The intermediate product obtained in step S4 is put into double screw extruder and carries out extrusion molding, is obtained just
Walk fabric；
Step S6：Preliminary fabric is subjected to heat treatment, treatment temperature remains 230 DEG C；
Step S7：Preliminary fabric is subjected to whole dye, dyed, dried and is washed respectively, wherein, the dyeing temperature is protected
Hold as 135 DEG C, the drying keeping temperature is 180 DEG C；
Step S8：Preliminary fabric is finally subjected to processing and forming, obtains final fabric.
Specifically, in the step S4, the pressure of the high pressure homogenizer uses 18Mpa.
In the step S5, the screw speed of the double screw extruder is 280r/min, and double screw extruder is divided into four
Individual segmentation, wherein the temperature of four segmentations is respectively：One 190 DEG C of wise temperature, 210 DEG C of two-section temperature, three wise temperatures
250 DEG C, and 185 DEG C of four wise temperatures.
In the step S6, water-proofing treatment is also included in heat treatment, using waterproofing agent 30g/L；
It is 140 DEG C of preliminary dryings that first segment oven temperature is adjusted in treatment temperature, and remaining section oven temperature is 170 bakings, is kept
In 50r/min, the fabric goes out after baking oven through cooling down wind and cooling water temperature speed, stable fabric after temperature is down to 35 DEG C
Form.
In the step S6, the sizing speed is 30m/min.
Softener washing is added in the step S7, in the washing.Softener is handled using tannic acid.
In the step S7, dyeing includes warming-up section, holds temperature section and temperature descending section.
The warming-up section process is：Initial temperature is 35 DEG C, is warming up to 90 DEG C with 3 DEG C/min and keeps 8min, with 3
DEG C/min is warming up to 120 DEG C and is incubated 8min, finally it is warming up to 135 DEG C with 3 DEG C/min；
The temperature section process of holding is：Keeping temperature is 135 DEG C of 50min；
The temperature descending section process is：120 DEG C are cooled to 1.5 DEG C/min and keeps 8min, are cooled to 3 DEG C/min
90 DEG C and 40min is incubated, is finally cooled to 50 DEG C with 4 DEG C/min.
Dyestuff that the dyeing uses composition and mass parts for：The mass parts of disperse yellow 0.04, the matter of disperse red 0.0152
Part is measured, disperses 0.022 mass parts of orchid, the mass parts of 98% glacial acetic acid 0.5.
Embodiment 3：
The fabric of a kind of ventilation wear-resistance and antistatic waterproof, the fabric is by cotton fibriia, viscose rayon and Antistatic polyester
Synthetic fibre fiber blend forms；
The fabric is made from the following raw materials in parts by weight：30 parts of cotton fibriia, 35 parts of viscose rayon, anti-electrostatic polyester are fine
35 parts of dimension；And
40 parts of PLA, 35 parts of metasilicic acid trimethyl, 26 parts of dilauryl thiodipropionate, neopelex 23
Part, 15 parts of phosphatidyl-ethanolamine, 10 parts of potassium metabisulfite, 8 parts of cetyl trimethylammonium bromide, 9 parts of hydroxypropul starch, receive
6 parts of silica of rice, 6 parts of cetanol sulfuric ester sodium salt, 5 parts of linoleic acid, 4 parts of silane coupler, 3 parts of adhesive, deionized water
180 parts.
Specifically, the use of anti-static function powder is 100nm in the antistatic PET filament.
Described ventilation wear-resistance and the preparation method of the fabric of antistatic waterproof, comprise the following steps：
Step S1：Each raw material is weighed according to parts by weight；
Step S2：By PLA, metasilicic acid trimethyl, dilauryl thiodipropionate, neopelex, phosphatide
Acyl monoethanolamine, potassium metabisulfite, cetyl trimethylammonium bromide, hydroxypropul starch and deionized water mixing, are placed in magnetic force
38min is stirred with rotating speed 700r/min on mixer, 75 DEG C is then raised temperature to, water-bath 20 minutes, obtains initial mixture；
Step S3：By cotton fibriia, viscose rayon, antistatic PET filament, nano silicon, cetanol sodium sulfovinate
Salt, which is collectively disposed in ball mill, carries out ball-milling treatment, and the rotating speed of ball mill is 260r/min, Ball-milling Time 1.5h, makes mixture
Middle each component is uniformly dispersed, and obtains ball-milled mixtures；
Step S4：The ball-milled mixtures that step S2 initial mixture and step S3 are obtained are added in high pressure homogenizer,
Adding linoleic acid, silane coupler, adhesive makes it well mixed, is melted at 350 DEG C, obtains intermediate product；
Step S5：The intermediate product obtained in step S4 is put into double screw extruder and carries out extrusion molding, is obtained just
Walk fabric；
Step S6：Preliminary fabric is subjected to heat treatment, treatment temperature remains 180 DEG C；
Step S7：Preliminary fabric is subjected to whole dye, dyed, dried and is washed respectively, wherein, the dyeing temperature is protected
Hold as 120 DEG C, the drying keeping temperature is 150 DEG C；
Step S8：Preliminary fabric is finally subjected to processing and forming, obtains final fabric.
Specifically, in the step S4, the pressure of the high pressure homogenizer uses 17Mpa.
In the step S5, the screw speed of the double screw extruder is 260r/min, and double screw extruder is divided into four
Individual segmentation, wherein the temperature of four segmentations is respectively：One 180 DEG C of wise temperature, 205 DEG C of two-section temperature, three wise temperatures
240 DEG C, and 180 DEG C of four wise temperatures.
In the step S6, water-proofing treatment is also included in heat treatment, using waterproofing agent 27g/L；
It is 140 DEG C of preliminary dryings that first segment oven temperature is adjusted in treatment temperature, and remaining section oven temperature is 170 bakings, is kept
In 46r/min, the fabric goes out after baking oven through cooling down wind and cooling water temperature speed, stable fabric after temperature is down to 33 DEG C
Form.
In the step S6, the sizing speed is 20m/min.
Softener washing is added in the step S7, in the washing.Softener is handled using tannic acid.
In the step S7, dyeing includes warming-up section, holds temperature section and temperature descending section.
The warming-up section process is：Initial temperature is 30 DEG C, is warming up to 85 DEG C with 2 DEG C/min and keeps 5min, with 2
DEG C/min is warming up to 110 DEG C and is incubated 5min, finally it is warming up to 130 DEG C with 2 DEG C/min；
The temperature section process of holding is：Keeping temperature is 130 DEG C of 30min；
The temperature descending section process is：110 DEG C are cooled to 1 DEG C/min and keeps 5min, and 800 are being cooled to 2 DEG C/min
DEG C and be incubated 30min, be finally cooled to 40 DEG C with 2 DEG C/min.
Dyestuff that the dyeing uses composition and mass parts for：The mass parts of disperse yellow 0.04, the matter of disperse red 0.0152
Part is measured, disperses 0.022 mass parts of orchid, the mass parts of 98% glacial acetic acid 0.5.
Embodiment 4：
The fabric of a kind of ventilation wear-resistance and antistatic waterproof, the fabric is by cotton fibriia, viscose rayon and Antistatic polyester
Synthetic fibre fiber blend forms；
The fabric is made from the following raw materials in parts by weight：33 parts of cotton fibriia, 37 parts of viscose rayon, anti-electrostatic polyester are fine
30 parts of dimension；And
44 parts of PLA, 33 parts of metasilicic acid trimethyl, 27 parts of dilauryl thiodipropionate, neopelex 23
Part, 16 parts of phosphatidyl-ethanolamine, 13 parts of potassium metabisulfite, 8 parts of cetyl trimethylammonium bromide, 8.5 parts of hydroxypropul starch,
6 parts of nano silicon, 6 parts of cetanol sulfuric ester sodium salt, 4 parts of linoleic acid, 4 parts of silane coupler, 4 parts of adhesive, deionization
180 parts of water.
Specifically, the use of anti-static function powder is 130nm in the antistatic PET filament.
Described ventilation wear-resistance and the preparation method of the fabric of antistatic waterproof, comprise the following steps：
Step S1：Each raw material is weighed according to parts by weight；
Step S2：By PLA, metasilicic acid trimethyl, dilauryl thiodipropionate, neopelex, phosphatide
Acyl monoethanolamine, potassium metabisulfite, cetyl trimethylammonium bromide, hydroxypropul starch and deionized water mixing, are placed in magnetic force
38min is stirred with rotating speed 720r/min on mixer, 88 DEG C is then raised temperature to, water-bath 20 minutes, obtains initial mixture；、
Step S3：By cotton fibriia, viscose rayon, antistatic PET filament, nano silicon, cetanol sodium sulfovinate
Salt, which is collectively disposed in ball mill, carries out ball-milling treatment, and the rotating speed of ball mill is 250r/min, Ball-milling Time 1.5h, makes mixture
Middle each component is uniformly dispersed, and obtains ball-milled mixtures；
Step S4：The ball-milled mixtures that step S2 initial mixture and step S3 are obtained are added in high pressure homogenizer,
Adding linoleic acid, silane coupler, adhesive makes it well mixed, is melted at 355 DEG C, obtains intermediate product；
Step S5：The intermediate product obtained in step S4 is put into double screw extruder and carries out extrusion molding, is obtained just
Walk fabric；
Step S6：Preliminary fabric is subjected to heat treatment, treatment temperature remains 150 DEG C；
Step S7：Preliminary fabric is subjected to whole dye, dyed, dried and is washed respectively, wherein, the dyeing temperature is protected
Hold as 110 DEG C, the drying keeping temperature is 140 DEG C；
Step S8：Preliminary fabric is finally subjected to processing and forming, obtains final fabric.
Specifically, in the step S4, the pressure of the high pressure homogenizer uses 17Mpa.
In the step S5, the screw speed of the double screw extruder is 270r/min, and double screw extruder is divided into four
Individual segmentation, wherein the temperature of four segmentations is respectively：One 180 DEG C of wise temperature, 200 DEG C of two-section temperature, three wise temperatures
240 DEG C, and 180 DEG C of four wise temperatures.
In the step S6, water-proofing treatment is also included in heat treatment, using waterproofing agent 26g/L；
It is 140 DEG C of preliminary dryings that first segment oven temperature is adjusted in treatment temperature, and remaining section oven temperature is 170 bakings, is kept
In 46r/min, the fabric goes out after baking oven through cooling down wind and cooling water temperature speed, stable fabric after temperature is down to 32 DEG C
Form.
In the step S6, the sizing speed is 28m/min.
Softener washing is added in the step S7, in the washing.Softener is handled using tannic acid.
In the step S7, dyeing includes warming-up section, holds temperature section and temperature descending section.
The warming-up section process is：Initial temperature is 32 DEG C, is warming up to 90 DEG C with 3 DEG C/min and keeps 6min, with 2
DEG C/min is warming up to 100 DEG C and is incubated 5min, finally it is warming up to 130 DEG C with 2 DEG C/min；
The temperature section process of holding is：Keeping temperature is 130 DEG C of 40min；
The temperature descending section process is：110 DEG C are cooled to 1 DEG C/min and keeps 6min, and 80 are being cooled to 2 DEG C/min
DEG C and be incubated 30min, be finally cooled to 40 DEG C with 3 DEG C/min.
Dyestuff that the dyeing uses composition and mass parts for：The mass parts of disperse yellow 0.04, the matter of disperse red 0.0152
Part is measured, disperses 0.022 mass parts of orchid, the mass parts of 98% glacial acetic acid 0.5.
It is complete by above-mentioned description, relevant staff using the above-mentioned desirable embodiment according to the present invention as enlightenment
Various changes and amendments can be carried out without departing from the scope of the technological thought of the present invention' entirely.The technology of this invention
Property scope is not limited to the content on specification, it is necessary to determines its technical scope according to right.
Claims (10)
- A kind of 1. fabric of ventilation wear-resistance and antistatic waterproof, it is characterised in that the fabric by cotton fibriia, viscose rayon and Antistatic PET filament blending forms；The fabric is made from the following raw materials in parts by weight：Cotton fibriia 30-40 parts, viscose rayon 35-40 parts, anti-electrostatic polyester Fiber 30-40 parts；AndPLA 33-46 parts, metasilicic acid trimethyl 25-38 parts, dilauryl thiodipropionate 22-28 parts, detergent alkylate sulphur Sour sodium 21-25 parts, phosphatidyl-ethanolamine 13-17 parts, potassium metabisulfite 9-14 parts, cetyl trimethylammonium bromide 8-9 parts, It is hydroxypropul starch 8-9 parts, nano silicon 5-7 parts, cetanol sulfuric ester sodium salt 5-7 parts, linoleic acid 4-6 parts, silane coupled Agent 3-4 parts, adhesive 3-4 parts, 180 parts of deionized water.
- 2. the fabric of ventilation wear-resistance according to claim 1 and antistatic waterproof, it is characterised in that the anti-electrostatic polyester The use of anti-static function powder is 30-150nm in fiber.
- 3. the preparation method of a kind of ventilation wear-resistance and the fabric of antistatic waterproof, it is characterised in that comprise the following steps：Step S1：Each raw material is weighed according to parts by weight；Step S2：By PLA, metasilicic acid trimethyl, dilauryl thiodipropionate, neopelex, phosphatidyl second Hydramine, potassium metabisulfite, cetyl trimethylammonium bromide, hydroxypropul starch and deionized water mixing, are placed in magnetic agitation 35-45min is stirred with rotating speed 650-750r/min on machine, 80-90 DEG C is then raised temperature to, water-bath 15-25 minutes, is tentatively mixed Compound；Step S3：Cotton fibriia, viscose rayon, antistatic PET filament, nano silicon, cetanol sulfuric ester sodium salt are total to Ball-milling treatment is carried out with being placed in ball mill, the rotating speed of ball mill is 220-280r/min, Ball-milling Time 1-2h, makes mixture Middle each component is uniformly dispersed, and obtains ball-milled mixtures；Step S4：The ball-milled mixtures that step S2 initial mixture and step S3 are obtained are added in high pressure homogenizer, then are added Entering linoleic acid, silane coupler, adhesive makes it well mixed, is melted at 350-360 DEG C, obtains intermediate product；Step S5：The intermediate product obtained in step S4 is put into double screw extruder and carries out extrusion molding, obtains preliminary face Material；Step S6：Preliminary fabric is subjected to heat treatment, treatment temperature remains 120-230 DEG C；Step S7：Preliminary fabric is subjected to whole dye, dyed, dried and is washed respectively, wherein, the dyeing temperature remains 80-135 DEG C, the drying keeping temperature is 100-180 DEG C；Step S8：Preliminary fabric is finally subjected to processing and forming, obtains final fabric.
- 4. the preparation method of ventilation wear-resistance according to claim 3 and the fabric of antistatic waterproof, it is characterised in that described In step S4, the pressure of the high pressure homogenizer uses 16-18Mpa.
- 5. the preparation method of ventilation wear-resistance according to claim 3 and the fabric of antistatic waterproof, it is characterised in that described In step S5, the screw speed of the double screw extruder is 250-280r/min；Double screw extruder is divided into four segmentations, wherein the temperature of four segmentations is respectively：One 170-190 DEG C of wise temperature, two 200-210 DEG C of wise temperature, three 235-250 DEG C of wise temperatures, and 175-185 DEG C of four wise temperatures.
- 6. the preparation method of ventilation wear-resistance according to claim 3 and the fabric of antistatic waterproof, it is characterised in that described In step S6, water-proofing treatment is also included in heat treatment, using waterproofing agent 25-30g/L；It is 140 DEG C of preliminary dryings that first segment oven temperature is adjusted during treatment temperature, and remaining section oven temperature is 170 bakings, and is protected Speed is held in 45-50r/min, the fabric goes out after baking oven through cooling down wind and cooling water temperature, steady after temperature is down to 30-35 DEG C Determine fabric form.
- 7. the preparation method of ventilation wear-resistance according to claim 6 and the fabric of antistatic waterproof, it is characterised in that described In step S6, the sizing speed is 15-30m/min.
- 8. the preparation method of ventilation wear-resistance according to claim 3 and the fabric of antistatic waterproof, it is characterised in that described Softener washing is added in step S7, in the washing.
- 9. the preparation method of ventilation wear-resistance according to claim 3 and the fabric of antistatic waterproof, it is characterised in that described In step S7, dyeing includes warming-up section, holds temperature section and temperature descending section.
- 10. the preparation method of ventilation wear-resistance according to claim 9 and the fabric of antistatic waterproof, it is characterised in that institute Stating warming-up section process is：Initial temperature is 25-35 DEG C, is warming up to 80-90 DEG C with 1-3 DEG C/min and keeps 3-8min, with 2-3 DEG C/min is warming up to 100-120 DEG C and is incubated 3-8min, finally it is warming up to 125-135 DEG C with 1-3 DEG C/min；The temperature section process of holding is：Keeping temperature is 125-135 DEG C of 20-50min；The temperature descending section process is：100-120 DEG C is cooled to 0.5-1.5 DEG C/min and keeps 3-8min, with 1-3 DEG C/min It is cooled to 70-90 DEG C and is incubated 15-40min, is finally cooled to 30-50 DEG C with 1.5-4 DEG C/min.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108505344A (en) * | 2018-04-04 | 2018-09-07 | 佛山市瑰栗服装材料有限公司 | A kind of waterproof and breathable composite material |
| CN108505343A (en) * | 2018-04-04 | 2018-09-07 | 佛山市瑰栗服装材料有限公司 | The preparation method of waterproof and breathable composite material |
| CN108691062A (en) * | 2018-05-29 | 2018-10-23 | 安徽英士博纺织发展有限公司 | A kind of outdoor wear production fabric |
| CN110565360A (en) * | 2019-08-30 | 2019-12-13 | 界首万昌新材料技术有限公司 | Antibacterial comfortable high-elasticity textile material |
| CN113068903A (en) * | 2021-03-26 | 2021-07-06 | 莆田市协诚鞋业有限公司 | Antifouling and antibacterial upper material and preparation method thereof |
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| CN106883459A (en) * | 2017-04-19 | 2017-06-23 | 马志明 | A kind of textile material of ventilation wear-resistance and preparation method thereof |
| CN106894187A (en) * | 2017-04-13 | 2017-06-27 | 上海中大纺织品有限公司 | A kind of preparation method of antistatic water-proof function shuttle-woven fabric and products thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106894187A (en) * | 2017-04-13 | 2017-06-27 | 上海中大纺织品有限公司 | A kind of preparation method of antistatic water-proof function shuttle-woven fabric and products thereof |
| CN106883459A (en) * | 2017-04-19 | 2017-06-23 | 马志明 | A kind of textile material of ventilation wear-resistance and preparation method thereof |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108505344A (en) * | 2018-04-04 | 2018-09-07 | 佛山市瑰栗服装材料有限公司 | A kind of waterproof and breathable composite material |
| CN108505343A (en) * | 2018-04-04 | 2018-09-07 | 佛山市瑰栗服装材料有限公司 | The preparation method of waterproof and breathable composite material |
| CN108691062A (en) * | 2018-05-29 | 2018-10-23 | 安徽英士博纺织发展有限公司 | A kind of outdoor wear production fabric |
| CN110565360A (en) * | 2019-08-30 | 2019-12-13 | 界首万昌新材料技术有限公司 | Antibacterial comfortable high-elasticity textile material |
| CN113068903A (en) * | 2021-03-26 | 2021-07-06 | 莆田市协诚鞋业有限公司 | Antifouling and antibacterial upper material and preparation method thereof |
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