CN106894187A - A kind of preparation method of antistatic water-proof function shuttle-woven fabric and products thereof - Google Patents
A kind of preparation method of antistatic water-proof function shuttle-woven fabric and products thereof Download PDFInfo
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- CN106894187A CN106894187A CN201710239890.5A CN201710239890A CN106894187A CN 106894187 A CN106894187 A CN 106894187A CN 201710239890 A CN201710239890 A CN 201710239890A CN 106894187 A CN106894187 A CN 106894187A
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- proof function
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
- D06C7/00—Heating or cooling textile fabrics
- D06C7/02—Setting
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B15/00—Removing liquids, gases or vapours from textile materials in association with treatment of the materials by liquids, gases or vapours
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B3/00—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
- D06B3/10—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fabrics
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
- D06M13/238—Tannins, e.g. gallotannic acids
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/0032—Determining dye recipes and dyeing parameters; Colour matching or monitoring
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/34—Material containing ester groups
- D06P3/52—Polyesters
- D06P3/54—Polyesters using dispersed dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/32—Polyesters
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
Abstract
The present invention provides a kind of preparation method of antistatic water-proof function shuttle-woven fabric and products thereof, including, weaving, sizing, whole dye, shaping；In fibrous raw material used, anti-electrostatic polyester or polyamide fibre weight accounting are 20~100%；Wherein, the sizing, including water-proofing treatment, its temperature is 120~230 DEG C；Wherein, the fibrous raw material, anti-static function powder is 30~150nm used in its preparation.The invention of this material is for current existing waterproof fabrics processing mode, a kind of antistatic fibre of addition of novelty, the accumulation of electrostatic charge can be efficiently reduced, frictional static voltage and electrostatic charge fade half life is reduced, so as to realize the proper, attractive in appearance of garment material, health care and security performance.
Description
Technical field
The present invention relates to field of textiles, and in particular to a kind of antistatic water-proof function shuttle-woven fabric preparation method and its product
Product.
Background technology
With the raising of people's quality of life, to clothing function in terms of demand also gradually increase sharply.Especially in recent years
The influence of environmental degradation and haze so that garment material is inhaled grey degree and greatly increased.Many lives inconvenience such as face that electrostatic belt comes
Material strip electricity causes fabric corrugation, largely effects on attractive in appearance, and fabric is powered so that wearer's mood is irritated, and going down for a long time, it is many to cause
Disease, fabric is powered or even can bring potential safety hazard, and the report of fire is such as finally triggered in gas station place build-up of static charges
Also it is not within minority.It is rational effective in the case where country and social and consumer gradually improve to health and awareness of safety
Utilization functional raw material to develop new fabric product be the market demand.
But, to the weaving of functional fabric in practice, especially antistatic, waterproof composite functional fabric preparation, not
The antistatic and aspect functional effect of waterproof two can simultaneously be taken into account excellent.The simple coating of the more use waterproofing agents of prior art, this
So that functional group is directly wrapped coating in anti-static function fiber, it is impossible to play a role.Also or by reducing coated weight,
So that microcosmic upper functional group plays its antistatic property less resistance.But, it is higher that this causes that waterproof is unable to reach again
Grade.
It would therefore be highly desirable to provide a kind of new antistatic, waterproof composite functional fabric developing thought.
The content of the invention
The purpose of this part is to summarize some aspects of embodiments of the invention and briefly introduce some preferable implementations
Example.May be done in this part and the description of the present application summary and denomination of invention a little simplified or omitted to avoid making our department
Point, the purpose of specification digest and denomination of invention obscure, and this simplification or omission cannot be used for limiting the scope of the present invention.
In view of technological gap prepared by above-mentioned and/or existing antistatic water-proof function shuttle-woven fabric, it is proposed that the present invention.
Therefore, one of purpose of the invention is to solve deficiency of the prior art, there is provided a kind of antistatic waterproof work(
The preparation method of energy shuttle-woven fabric.
In order to solve the above technical problems, the invention provides following technical scheme：Including weaving, sizing, whole dye, shaping；
In fibrous raw material used, anti-electrostatic polyester or polyamide fibre weight accounting are 20~100%；Wherein, the sizing, including at waterproof
Reason, its temperature is 120~230 DEG C；Wherein, the fibrous raw material, its preparation used in anti-static function powder be 30~
150nm。
As a kind of preferred scheme of antistatic water-proof function shuttle-woven fabric preparation method of the present invention, wherein：It is described
Water-proofing treatment, it is 25~30g/L that it uses waterproofing agent；
As a kind of preferred scheme of antistatic water-proof function shuttle-woven fabric preparation method of the present invention, wherein：It is described
Whole dye, it includes dyeing, drying, washing；Wherein, the dyeing, its temperature is 80~135 DEG C；Wherein, the drying, its temperature
Spend is 100~180 DEG C.
As a kind of preferred scheme of antistatic water-proof function shuttle-woven fabric preparation method of the present invention, wherein：It is described
Water-proofing treatment, it is that oven temperature is adjusted to 140 DEG C of preliminary dryings of first segment, and remaining is 170 DEG C and bakes, and speed is 45~50 yards,
Go out baking oven to lower the temperature through supercooling wind and cold water cylinder, temperature is down to 30~35 DEG C of stable forms.
As a kind of preferred scheme of antistatic water-proof function shuttle-woven fabric preparation method of the present invention, wherein：It is described
Dyeing, it includes the temperature rise period；Holding stage；Temperature-fall period；
Wherein, the temperature rise period, it is included from 25~35 DEG C, and 80~90 DEG C and insulation 3 are warming up to 1~3 DEG C/min
~8min, is warming up to 100~120 DEG C and is incubated 3~8min with 2~3 DEG C/min, and 125-135 DEG C is heated to 1~3 DEG C/min,
Insulation 20-50min.
As a kind of preferred scheme of antistatic water-proof function shuttle-woven fabric preparation method of the present invention, wherein：It is described
Temperature-fall period, it to be included and be cooled to 100~120 DEG C with 0.5~1.5 DEG C/min and be incubated 3~8min, lowered the temperature with 1~3 DEG C/min
To 70~90 DEG C and be incubated 15~40min, be cooled to 30~50 DEG C with 1.5~4 DEG C/min.
As a kind of preferred scheme of antistatic water-proof function shuttle-woven fabric preparation method of the present invention, wherein：It is described
Sizing, its sizing speed is 15~30m/min；The fibrous raw material, its specification is DTY and/or FDY, and its Denier number is 20
~300D, head number is 1~300F, and single fiber fiber number is 0.3~1D；The washing, it is plus softener washing.
As a kind of preferred scheme of antistatic water-proof function shuttle-woven fabric preparation method of the present invention, wherein：It is described
Anti-static function powder, it is one or more in ATO, ITO, AZO, FTO, conductive zinc oxide, conductive zinc oxide powder.
Another object of the present invention is to solve deficiency of the prior art, there is provided a kind of antistatic water-proof function tatting face
Material.
In order to solve the above technical problems, the invention provides following technical scheme：Including in fibrous raw material used, resisting quiet
Electric terylene or polyamide fibre weight accounting are 20~100%；Wherein, the fibrous raw material, anti-static function powder used in its preparation
Body is 30~150nm.
As a kind of preferred scheme of antistatic water-proof function shuttle-woven fabric of the present invention, wherein：The antistatic work(
Energy powder, it is one or more in ATO, ITO, AZO, FTO, conductive zinc oxide, conductive zinc oxide powder；The fiber is former
Material, its specification be DTY and/or FDY, its Denier number be 20~300D, head number be 1~300F, single fiber fiber number be 0.3~
1D。
Beneficial effects of the present invention：
Coordinated by the combination and weaving process adaptable therewith of plurality of raw materials, it is a kind of with function combination so as to obtain
Effect, realizes the attractive in appearance of fabric, health care and security function, is particularly suitable for the exploitation of garment material.
The inventive method is obtained product, and it can simultaneously have excellent functional effect of both antistatic and waterproof.It is anti-
Electrostatic aspect, half-life period, up to 0.8s (A grades), product gain 80% or so is obtained compared with other method, and surface density of charge is reachable
1.1uc/m2, product gain 75% or so is obtained compared with other method, frictional static voltage is obtained compared with other method and produces up to 80V
Product gain 80% or so, at the same time, it can also stablize and ensure that fabric classification of waterproof is 4 grades.
Specific embodiment
To enable the above objects, features and advantages of the present invention more obvious understandable, with reference to specific embodiment pair
Specific embodiment of the invention is described in detail.
Many details are elaborated in the following description in order to fully understand the present invention, but the present invention can be with
Other manner described here is different from using other to implement, those skilled in the art can be without prejudice to intension of the present invention
In the case of do similar popularization, therefore the present invention is not limited by following public specific embodiment.
Secondly, " one embodiment " or " embodiment " referred to herein refers to that may be included at least one realization side of the invention
Special characteristic, structure or characteristic in formula." in one embodiment " that different places occur in this manual not refers both to
Same embodiment, nor the single or selective embodiment mutually exclusive with other embodiment.
In following embodiments, unless otherwise noted, the fibrous raw material for being used, anti-static function powder used in its preparation
Body is 30~150nm.
Embodiment 1：
Be fibrous raw material with 20 weight portion polyester DTYs, 80 weight portion anti-electrostatic polyester DTY, by weaving, sizing, dyeing and finishing,
Sewing tech is made designed material.
The specification of the polyester DTY is 75D/144F, and the specification of the anti-electrostatic polyester DTY is 75D/72F.
The setting temperature of the setting process is 190 DEG C, and sizing speed is 23m/min.
The dyeing and finishing technology is comprised the technical steps that：Enter dye vat (dyeing temperature is 130 DEG C), (temperature is 150 for drying
DEG C), washing, drying (temperature is 150 DEG C), softening agent is processed using tannic acid.
The composition and mass parts of the dyestuff that the dyeing is used for：The mass parts of disperse yellow 0.04, disperse red 0.0152
Mass parts, blue 0.022 mass parts of dispersion, the mass parts of 98% glacial acetic acid 0.5.The temperature control of the dyeing is：Initial temperature
It is 30 DEG C to spend, and 85 DEG C are heated to 2 DEG C/min, is incubated 5min, then is heated to 115 DEG C with 1.5 DEG C/min, is incubated 5min, then with 2
DEG C/min is heated to 130 DEG C, is incubated 30min, then 110 DEG C are cooled to 1 DEG C/min, 5min is incubated, then lower the temperature with 1.5 DEG C/min
To 80 DEG C, 20min is incubated, is finally cooled to 33 DEG C with 2 DEG C/min.
Waterproof after finishing：As above waterproof requirement is as follows in 4 grades of techniques after dyeing drying：(this auxiliary agent is in industry to waterproofing agent
General product) to be allocated by 27g/L, oven temperature is adjusted to 140 DEG C of preliminary dryings of first segment, and remaining is 170 DEG C and bakes, and speed is
48 yards, go out baking oven and lower the temperature through supercooling wind and cold water cylinder, temperature is down to 33 DEG C of stable forms.
Specific aim performance detection is carried out to gained fabric, as a result such as table 1 below：
Table 1
Embodiment 2：
Be fibrous raw material with 50 weight portion polyester DTYs, 50 weight portion anti-electrostatic polyester DTY, by weaving, sizing, dyeing and finishing,
Sewing tech is made designed material.
The specification of the polyester DTY is 150D/288F, and the specification of the anti-electrostatic polyester DTY is 150D/96F.
The setting temperature of the setting process is 120 DEG C, and sizing speed is 23m/min.
The dyeing and finishing technology is comprised the technical steps that：Enter dye vat (dyeing temperature is 130 DEG C), (temperature is 150 for drying
DEG C), washing, drying (temperature is 150 DEG C), softening agent is processed using tannic acid.
The composition and mass parts of the dyestuff that the dyeing is used for：The mass parts of disperse yellow 0.04, disperse red 0.0152
Mass parts, blue 0.022 mass parts of dispersion, the mass parts of 98% glacial acetic acid 0.5.The temperature control of the dyeing is：Initial temperature
It is 30 DEG C to spend, and 85 DEG C are heated to 2 DEG C/min, is incubated 5min, then is heated to 115 DEG C with 1.5 DEG C/min, is incubated 5min, then with 2
DEG C/min is heated to 125 DEG C, is incubated 20min, then 100 DEG C are cooled to 1 DEG C/min, 5min is incubated, then lower the temperature with 1.5 DEG C/min
To 70 DEG C, 40min is incubated, is finally cooled to 35 DEG C with 2 DEG C/min.
Waterproof after finishing：As above waterproof requirement is as follows in 4 grades of techniques after dyeing drying：(this auxiliary agent is in industry to waterproofing agent
General product) to be allocated by 25g/L, oven temperature is adjusted to 140 DEG C of preliminary dryings of first segment, and remaining is 170 degree and bakes, and speed is
48 yards, go out baking oven and lower the temperature through supercooling wind and cold water cylinder, temperature is down to 33 DEG C of stable forms.
Specific aim performance detection is carried out to gained fabric, as a result such as table 2 below：
Table 2
Embodiment 3：
Be fibrous raw material with 80 weight portion polyester DTYs, 20 weight portion anti-electrostatic polyester DTY, by weaving, sizing, dyeing and finishing,
Sewing tech is made designed material.
The specification of the polyester DTY is 50D/96F, and the specification of the anti-electrostatic polyester DTY is 50D/36F.
The setting temperature of the setting process is 230 DEG C, and sizing speed is 23m/min.
The dyeing and finishing technology is comprised the technical steps that：Enter dye vat (dyeing temperature is 130 DEG C), (temperature is 150 for drying
DEG C), washing, drying (temperature is 150 DEG C), softening agent is processed using tannic acid.
The composition and mass parts of the dyestuff that the dyeing is used for：The mass parts of disperse yellow 0.04, disperse red 0.0152
Mass parts, blue 0.022 mass parts of dispersion, the mass parts of 98% glacial acetic acid 0.5.
The temperature control of the dyeing is：Initial temperature is 30 DEG C, and 90 DEG C are heated to 2 DEG C/min, is incubated 5min,
Be heated to 115 DEG C with 1.5 DEG C/min again, be incubated 5min, then 135 DEG C are heated to 2 DEG C/min, be incubated 50min, then with 1 DEG C/
Min is cooled to 120 DEG C, is incubated 5min, then is cooled to 90 DEG C with 1.5 DEG C/min, is incubated 30min, is finally cooled to 2 DEG C/min
35℃。
Waterproof after finishing：As above waterproof requirement is as follows in 4 grades of techniques after dyeing drying：(this auxiliary agent is in industry to waterproofing agent
General product) to be allocated by 30g/L, oven temperature is adjusted to 140 DEG C of preliminary dryings of first segment, and remaining is 170 degree and bakes, and speed is
48 yards, go out baking oven and lower the temperature through supercooling wind and cold water cylinder, temperature is down to 33 DEG C of stable forms.
Specific aim performance detection is carried out to gained fabric, as a result such as table 3 below：
Table 3
Embodiment 4：
Be fibrous raw material with 50 weight portion polyamide fibre DTY, 50 weight portion antistatic nylon DTY, by weaving, sizing, dyeing and finishing,
Sewing tech is made designed material.
The specification of the polyamide fibre DTY is 75D/72F, and the specification of the antistatic nylon DTY is 75D/72F.
The setting temperature of the setting process is 190 DEG C, and sizing speed is 20m/min.
The dyeing and finishing technology is comprised the technical steps that：Enter dye vat (dyeing temperature is 110 DEG C), (temperature is 140 for drying
DEG C), washing, drying (temperature is 140 DEG C), softening agent is processed using tannic acid.
The composition and mass parts of the dyestuff that the dyeing is used for：The mass parts of disperse yellow 0.04, disperse red 0.0152
Mass parts, blue 0.022 mass parts of dispersion, the mass parts of 98% glacial acetic acid 0.5.The temperature control of the dyeing is：Initial temperature
It is 30 DEG C to spend, and 80 DEG C are heated to 2 DEG C/min, is incubated 5min, then is heated to 105 DEG C with 1.5 DEG C/min, is incubated 5min, then with 2
DEG C/min is heated to 110 DEG C, is incubated 30min, then 100 DEG C are cooled to 1 DEG C/min, 5min is incubated, then lower the temperature with 1.5 DEG C/min
To 75 DEG C, 35min is incubated, is finally cooled to 35 DEG C with 2 DEG C/min.
Waterproof after finishing：As above waterproof requirement is as follows in 4 grades of techniques after dyeing drying：(this auxiliary agent is in industry to waterproofing agent
General product) to be allocated by 27g/L, oven temperature is adjusted to 140 DEG C of preliminary dryings of first segment, and remaining is 170 degree and bakes, and speed is
48 yards, go out baking oven and lower the temperature through supercooling wind and cold water cylinder, temperature is down to 33 DEG C of stable forms.
Specific aim performance detection is carried out to gained fabric, as a result such as table 4 below：
Table 4
Embodiment 5：
Be fibrous raw material with 50 weight portion polyamide fibre DTY, 50 weight portion antistatic nylon DTY, by weaving, sizing, dyeing and finishing,
Sewing tech is made designed material.
The specification of the polyamide fibre DTY is 75D/72F, and the specification of the antistatic nylon DTY is 75D/72F.
The setting temperature of the setting process is 250 DEG C, and sizing speed is 20m/min.
The dyeing and finishing technology is comprised the technical steps that：Enter dye vat (dyeing temperature is 130 DEG C), (temperature is 150 for drying
DEG C), washing, drying (temperature is 150 DEG C), softening agent is processed using tannic acid.
The composition and mass parts of the dyestuff that the dyeing is used for：The mass parts of disperse yellow 0.04, disperse red 0.0152
Mass parts, blue 0.022 mass parts of dispersion, the mass parts of 98% glacial acetic acid 0.5.The temperature control of the dyeing is：Initial temperature
It is 30 DEG C to spend, and 80 DEG C are heated to 2 DEG C/min, is incubated 5min, then is heated to 105 DEG C with 1.5 DEG C/min, is incubated 5min, then with 2
DEG C/min is heated to 130 DEG C, is incubated 30min, then 100 DEG C are cooled to 1 DEG C/min, 5min is incubated, then lower the temperature with 1.5 DEG C/min
To 75 DEG C, 15min is incubated, is finally cooled to 35 DEG C with 2 DEG C/min.
Waterproof after finishing：As above waterproof requirement is as follows in 4 grades of techniques after dyeing drying：(this auxiliary agent is in industry to waterproofing agent
General product) to be allocated by 40g/L, oven temperature is adjusted to 140 DEG C of preliminary dryings of first segment, and remaining is 170 degree and bakes, and speed is
48 yards, go out baking oven and lower the temperature through supercooling wind and cold water cylinder, temperature is down to 33 DEG C of stable forms.
Specific aim performance detection is carried out to gained fabric, as a result such as table 5 below：
Table 5
Embodiment 6：
Be fibrous raw material with 50 weight portion polyamide fibre DTY, 50 weight portion antistatic nylon DTY, by weaving, sizing, dyeing and finishing,
Sewing tech is made designed material.
The specification of the polyamide fibre DTY is 75D/72F, and the specification of the antistatic nylon DTY is 75D/72F.
The setting temperature of the setting process is 100 DEG C, and sizing speed is 20m/min.
The dyeing and finishing technology is comprised the technical steps that：Enter dye vat (dyeing temperature is 110 DEG C), (temperature is 140 for drying
DEG C), washing, drying (temperature is 140 DEG C), softening agent is processed using tannic acid.
The composition and mass parts of the dyestuff that the dyeing is used for：The mass parts of disperse yellow 0.04, disperse red 0.0152
Mass parts, blue 0.022 mass parts of dispersion, the mass parts of 98% glacial acetic acid 0.5.The temperature control of the dyeing is：Initial temperature
It is 30 DEG C to spend, and 80 DEG C are heated to 2 DEG C/min, is incubated 5min, then is heated to 105 DEG C with 1.5 DEG C/min, is incubated 5min, then with 2
DEG C/min is heated to 130 DEG C, is incubated 30min, then 100 DEG C are cooled to 1 DEG C/min, 5min is incubated, then lower the temperature with 1.5 DEG C/min
To 75 DEG C, 15min is incubated, is finally cooled to 35 DEG C with 2 DEG C/min.
Waterproof after finishing：As above waterproof requirement is as follows in 4 grades of techniques after dyeing drying：(this auxiliary agent is in industry to waterproofing agent
General product) to be allocated by 10g/L, oven temperature is adjusted to 140 DEG C of preliminary dryings of first segment, and remaining is 170 degree and bakes, and speed is
48 yards, go out baking oven and lower the temperature through supercooling wind and cold water cylinder, temperature is down to 33 DEG C of stable forms.
Specific aim performance detection is carried out to gained fabric, as a result such as table 6 below：
Table 6
Embodiment 7：
Be fibrous raw material with 50 weight portion polyamide fibre DTY, 50 weight portion antistatic nylon DTY, by weaving, sizing, dyeing and finishing,
Sewing tech is made designed material.
The specification of the polyamide fibre DTY is 75D/72F, and the specification of the antistatic nylon DTY is 75D/72F.
The setting temperature of the setting process is 190 DEG C, and sizing speed is 20m/min.
The dyeing and finishing technology is comprised the technical steps that：Enter dye vat (dyeing temperature is 50 DEG C), dry (temperature is 80 DEG C),
Washing, drying (temperature is 80 DEG C), softening agent is processed using tannic acid.
The composition and mass parts of the dyestuff that the dyeing is used for：The mass parts of disperse yellow 0.04, disperse red 0.0152
Mass parts, blue 0.022 mass parts of dispersion, the mass parts of 98% glacial acetic acid 0.5.The temperature control of the dyeing is：Initial temperature
It is 30 DEG C to spend, and 80 DEG C are heated to 2 DEG C/min, is incubated 5min, then is heated to 105 DEG C with 1.5 DEG C/min, is incubated 5min, then with 2
DEG C/min is heated to 180 DEG C, is incubated 30min, then 100 DEG C are cooled to 1 DEG C/min, 5min is incubated, then lower the temperature with 1.5 DEG C/min
To 75 DEG C, 15min is incubated, is finally cooled to 35 DEG C with 2 DEG C/min.
Waterproof after finishing：As above waterproof requirement is as follows in 4 grades of techniques after dyeing drying：(this auxiliary agent is in industry to waterproofing agent
General product) to be allocated by 27g/L, oven temperature is adjusted to 140 DEG C of preliminary dryings of first segment, and remaining is 170 degree and bakes, and speed is
48 yards, go out baking oven and lower the temperature through supercooling wind and cold water cylinder, temperature is down to 33 DEG C of stable forms.
Specific aim performance detection is carried out to gained fabric, as a result such as table 7 below：
Table 7
Embodiment 8：
Be fibrous raw material with 50 weight portion polyamide fibre DTY, 50 weight portion antistatic nylon DTY, by weaving, sizing, dyeing and finishing,
Sewing tech is made designed material.
The specification of the polyamide fibre DTY is 75D/72F, and the specification of the antistatic nylon DTY is 75D/72F.
The setting temperature of the setting process is 190 DEG C, and sizing speed is 20m/min.
The dyeing and finishing technology is comprised the technical steps that：Enter dye vat (dyeing temperature is 150 DEG C), (temperature is 200 for drying
DEG C), washing, drying (temperature is 140 DEG C), softening agent is processed using tannic acid.
The composition and mass parts of the dyestuff that the dyeing is used for：The mass parts of disperse yellow 0.04, disperse red 0.0152
Mass parts, blue 0.022 mass parts of dispersion, the mass parts of 98% glacial acetic acid 0.5.The temperature control of the dyeing is：Initial temperature
It is 30 DEG C to spend, and 80 DEG C are heated to 2 DEG C/min, is incubated 5min, then is heated to 105 DEG C with 1.5 DEG C/min, is incubated 5min, then with 2
DEG C/min is heated to 115 DEG C, is incubated 30min, then 100 DEG C are cooled to 1 DEG C/min, 5min is incubated, then lower the temperature with 1.5 DEG C/min
To 75 DEG C, 15min is incubated, is finally cooled to 35 DEG C with 2 DEG C/min.
Waterproof after finishing：As above waterproof requirement is as follows in 4 grades of techniques after dyeing drying：(this auxiliary agent is in industry to waterproofing agent
General product) to be allocated by 27g/L, oven temperature is adjusted to 140 DEG C of preliminary dryings of first segment, and remaining is 170 degree and bakes, and speed is
48 yards, go out baking oven and lower the temperature through supercooling wind and cold water cylinder, temperature is down to 33 DEG C of stable forms.
Specific aim performance detection is carried out to gained fabric, as a result such as table 8 below：
Table 8
Embodiment 9：
In the present embodiment, the fibrous raw material for being used, anti-static function powder is 10~20nm used in its preparation.
Be fibrous raw material with 50 weight portion polyamide fibre DTY, 50 weight portion antistatic nylon DTY, by weaving, sizing, dyeing and finishing,
Sewing tech is made designed material.
The specification of the polyamide fibre DTY is 75D/72F, and the specification of the antistatic nylon DTY is 75D/72F.
The setting temperature of the setting process is 190 DEG C, and sizing speed is 20m/min.
The dyeing and finishing technology is comprised the technical steps that：Enter dye vat (dyeing temperature is 110 DEG C), (temperature is 140 for drying
DEG C), washing, drying (temperature is 140 DEG C), softening agent is processed using tannic acid.
The composition and mass parts of the dyestuff that the dyeing is used for：The mass parts of disperse yellow 0.04, disperse red 0.0152
Mass parts, blue 0.022 mass parts of dispersion, the mass parts of 98% glacial acetic acid 0.5.The temperature control of the dyeing is：Initial temperature
It is 30 DEG C to spend, and 80 DEG C are heated to 2 DEG C/min, is incubated 5min, then is heated to 105 DEG C with 1.5 DEG C/min, is incubated 5min, then with 2
DEG C/min is heated to 110 DEG C, is incubated 30min, then 100 DEG C are cooled to 1 DEG C/min, 5min is incubated, then lower the temperature with 1.5 DEG C/min
To 75 DEG C, 35min is incubated, is finally cooled to 35 DEG C with 2 DEG C/min.
Waterproof after finishing：As above waterproof requirement is as follows in 4 grades of techniques after dyeing drying：(this auxiliary agent is in industry to waterproofing agent
General product) to be allocated by 27g/L, oven temperature is adjusted to 140 DEG C of preliminary dryings of first segment, and remaining is 170 degree and bakes, and speed is
48 yards, go out baking oven and lower the temperature through supercooling wind and cold water cylinder, temperature is down to 33 DEG C of stable forms.
Specific aim performance detection is carried out to gained fabric, as a result such as table 9 below：
Table 9
Embodiment 10：
In the present embodiment, the fibrous raw material for being used, used in its preparation anti-static function powder be 180~
200nm。
Be fibrous raw material with 50 weight portion polyamide fibre DTY, 50 weight portion antistatic nylon DTY, by weaving, sizing, dyeing and finishing,
Sewing tech is made designed material.
The specification of the polyamide fibre DTY is 75D/72F, and the specification of the antistatic nylon DTY is 75D/72F.
The setting temperature of the setting process is 190 DEG C, and sizing speed is 20m/min.
The dyeing and finishing technology is comprised the technical steps that：Enter dye vat (dyeing temperature is 110 DEG C), (temperature is 140 for drying
DEG C), washing, drying (temperature is 140 DEG C), softening agent is processed using tannic acid.
The composition and mass parts of the dyestuff that the dyeing is used for：The mass parts of disperse yellow 0.04, disperse red 0.0152
Mass parts, blue 0.022 mass parts of dispersion, the mass parts of 98% glacial acetic acid 0.5.The temperature control of the dyeing is：Initial temperature
It is 30 DEG C to spend, and 80 DEG C are heated to 2 DEG C/min, is incubated 5min, then is heated to 105 DEG C with 1.5 DEG C/min, is incubated 5min, then with 2
DEG C/min is heated to 110 DEG C, is incubated 30min, then 100 DEG C are cooled to 1 DEG C/min, 5min is incubated, then lower the temperature with 1.5 DEG C/min
To 75 DEG C, 35min is incubated, is finally cooled to 35 DEG C with 2 DEG C/min.
Waterproof after finishing：As above waterproof requirement is as follows in 4 grades of techniques after dyeing drying：(this auxiliary agent is in industry to waterproofing agent
General product) to be allocated by 27g/L, oven temperature is adjusted to 140 DEG C of preliminary dryings of first segment, and remaining is 170 degree and bakes, and speed is
48 yards, go out baking oven and lower the temperature through supercooling wind and cold water cylinder, temperature is down to 33 DEG C of stable forms.
Specific aim performance detection is carried out to gained fabric, as a result such as table 10 below：
Table 10
From above-described embodiment, product obtained in the inventive method can take into account waterproof and antistatic two kinds of functions effect
Really, and there is a preferable effect.
From embodiment 4 with embodiment 9,10 results contrasts, the present invention in fiber raw material diameter of particle it is preferred
Interior, best results, more than or less than preferred scope of the present invention, can not simultaneously take into account function effect of both antistatic and waterproof
Really.
From embodiment 4 with the results contrast of embodiment 5,6,7,8, during the present invention is to sizing, whole dyeing technique parameter, especially
It is the preferred of temperature parameter, the result for obtaining more preferably, more than or less than preferred scope of the present invention, can not simultaneously take into account antistatic
With functional effect of both waterproof.
Because, raw material, sizing, whole dyeing technique parameter preferred for this invention enable to shuttle-woven fabric microcosmic
In structure, with specific spacial framework so that hydrone cannot permeate, conductive group can island shape protrusion, possess
Required electric conductivity.
Studied through inventor and found, when powder is too small employed in raw material, surface-active is excessive so that waterproofing agent is micro-
Can be fully wrapped around to its on seeing so that completely lose anti-static function；And powder it is excessive when, because waterproofing agent cannot effectively cover
Lid so that microcosmic upper hydrone infiltration is more easy, meanwhile, excessive functional powder can influence fiber body-sensing product in itself again
Matter.
Further, from the functional powder of specified particle diameter, need also the waterproofing agent of particular flow rate do water-proofing treatment, and
In whole technical process, within the scope of narrower temperature, qualitative, whole dye processing is carried out.If flow is excessive, waterproof is easily caused
Layer is blocked up, and anti-static function group cannot protrude, and flow is too small, then cause that waterproof layer cannot be covered effectively.Temperature is too high so that
Microcosmic effective anti-static function radical oxidation inactivation, temperature is too low, for the microcosmic waterproof construction of the hot setting of waterproofing agent
Consolidation effect required for not having.
It should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted, although with reference to preferably
Embodiment has been described in detail to the present invention, it will be understood by those within the art that, can be to technology of the invention
Scheme is modified or equivalent, and without deviating from the spirit and scope of technical solution of the present invention, it all should cover in this hair
In the middle of bright right.
Claims (10)
1. a kind of preparation method of antistatic water-proof function shuttle-woven fabric, it is characterised in that：Including, weaving, sizing, whole dye, into
Type；In fibrous raw material used, anti-electrostatic polyester or polyamide fibre weight accounting are 20~100%；
Wherein, the sizing, including water-proofing treatment, its temperature is 120~230 DEG C；
Wherein, the fibrous raw material, anti-static function powder is 30~150nm used in its preparation.
2. as claimed in claim 1 antistatic water-proof function shuttle-woven fabric preparation method, it is characterised in that：At the waterproof
Reason, it is 25~30g/L that it uses waterproofing agent.
3. as claimed in claim 2 antistatic water-proof function shuttle-woven fabric preparation method, it is characterised in that：The whole dye, its
Including dyeing, drying, washing；Wherein, the dyeing, its temperature is 80~135 DEG C；Wherein, the drying, its temperature is 100
~180 DEG C.
4. as any one of claim 2~3 antistatic water-proof function shuttle-woven fabric preparation method, it is characterised in that：
The water-proofing treatment, it is that oven temperature is adjusted to 140 DEG C of preliminary dryings of first segment, and remaining is 170 DEG C and bakes, and speed is 45~50
Code, goes out baking oven and lowers the temperature through supercooling wind and cold water cylinder, temperature is down to 30~35 DEG C of stable forms.
5. as claimed in claim 4 antistatic water-proof function shuttle-woven fabric preparation method, it is characterised in that：The dyeing, its
Including the temperature rise period；Holding stage；Temperature-fall period；
Wherein, the temperature rise period, it is included from 25~35 DEG C, with 1~3 DEG C/min be warming up to 80~90 DEG C and be incubated 3~
8min, is warming up to 100~120 DEG C and is incubated 3~8min with 2~3 DEG C/min, and 125-135 DEG C is heated to 1~3 DEG C/min, protects
Warm 20-50min.
6. as claimed in claim 5 antistatic water-proof function shuttle-woven fabric preparation method, it is characterised in that：The cooling rank
Section, it includes and is cooled to 100~120 DEG C and 3~8min of insulation with 0.5~1.5 DEG C/min, 70 are cooled to 1~3 DEG C/min~
90 DEG C and 15~40min of insulation, 30~50 DEG C are cooled to 1.5~4 DEG C/min.
7. as any one of claims 1 to 3,5,6 antistatic water-proof function shuttle-woven fabric preparation method, its feature exists
In：The sizing, its sizing speed is 15~30m/min；The fibrous raw material, its specification is DTY and/or FDY, its Denier
Number is 20~300D, and head number is 1~300F, and single fiber fiber number is 0.3~1D；The washing, it is plus softener washing.
8. as any one of claims 1 to 3,5,6 antistatic water-proof function shuttle-woven fabric preparation method, its feature exists
In：The anti-static function powder, its be one kind in ATO, ITO, AZO, FTO, conductive zinc oxide, conductive zinc oxide powder or
It is various.
It is 9. a kind of to use above-mentioned any one of 1~8 obtained antistatic water-proof function shuttle-woven fabric, it is characterised in that：Bag
Include, in fibrous raw material used, anti-electrostatic polyester or polyamide fibre weight accounting are 20~100%；
Wherein, the fibrous raw material, anti-static function powder is 30~150nm used in its preparation.
10. as claimed in claim 9 antistatic water-proof function shuttle-woven fabric, it is characterised in that：The anti-static function powder, its
It is one or more in ATO, ITO, AZO, FTO, conductive zinc oxide, conductive zinc oxide powder；The fibrous raw material, its specification
It is DTY and/or FDY, its Denier number is 20~300D, head number is 1~300F, and single fiber fiber number is 0.3~1D.
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| CN107675326A (en) * | 2017-09-20 | 2018-02-09 | 苏州白云纺织科技发展有限公司 | A kind of preparation method of the ultra-thin shuttle-woven fabric of ultraviolet light catalytic antimicrobial water-proof function |
| CN107740197A (en) * | 2017-09-19 | 2018-02-27 | 江苏澳洋世家服装有限公司 | A kind of ventilation wear-resistance and the fabric of antistatic waterproof and preparation method thereof |
| CN109778417A (en) * | 2019-02-28 | 2019-05-21 | 海安启弘纺织科技有限公司 | A kind of function imitates the preparation method and products thereof of the antistatic water suction warp knitting nap class fabric of cotton |
| CN109778418A (en) * | 2019-02-28 | 2019-05-21 | 海安启弘纺织科技有限公司 | A kind of preparation method and products thereof with antistatic water-proof function warp knitting nap class fabric |
| CN111041702A (en) * | 2019-12-31 | 2020-04-21 | 海安启弘纺织科技有限公司 | Preparation method of multi-component comfortable elastic antistatic functional warp-knitted fabric |
| CN111101279A (en) * | 2019-12-31 | 2020-05-05 | 海安启弘纺织科技有限公司 | Preparation method of multi-component comfortable elastic antibacterial warp-knitted fabric and product thereof |
| CN114182412A (en) * | 2021-10-26 | 2022-03-15 | 常熟市爱尚纺织科技有限公司 | Preparation method of one-way high-shrinkage crease-like yarn style kapok velvet shuttle-woven fabric and product thereof |
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| CN107675326A (en) * | 2017-09-20 | 2018-02-09 | 苏州白云纺织科技发展有限公司 | A kind of preparation method of the ultra-thin shuttle-woven fabric of ultraviolet light catalytic antimicrobial water-proof function |
| CN107675326B (en) * | 2017-09-20 | 2020-12-15 | 苏州白云纺织科技发展有限公司 | Preparation method of ultra-thin tatted fabric with ultraviolet-resistant catalytic antibacterial waterproof function |
| CN109778417A (en) * | 2019-02-28 | 2019-05-21 | 海安启弘纺织科技有限公司 | A kind of function imitates the preparation method and products thereof of the antistatic water suction warp knitting nap class fabric of cotton |
| CN109778418A (en) * | 2019-02-28 | 2019-05-21 | 海安启弘纺织科技有限公司 | A kind of preparation method and products thereof with antistatic water-proof function warp knitting nap class fabric |
| CN109778417B (en) * | 2019-02-28 | 2021-10-26 | 海安启弘纺织科技有限公司 | Preparation method of functional cotton-like antistatic water-absorbing warp-knitted velvet fabric and product thereof |
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| CN111101279A (en) * | 2019-12-31 | 2020-05-05 | 海安启弘纺织科技有限公司 | Preparation method of multi-component comfortable elastic antibacterial warp-knitted fabric and product thereof |
| CN111041702B (en) * | 2019-12-31 | 2022-05-20 | 海安启弘纺织科技有限公司 | Preparation method of multi-component comfortable elastic antistatic functional warp-knitted fabric |
| CN114182412A (en) * | 2021-10-26 | 2022-03-15 | 常熟市爱尚纺织科技有限公司 | Preparation method of one-way high-shrinkage crease-like yarn style kapok velvet shuttle-woven fabric and product thereof |
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Effective date of registration: 20190530 Address after: 215228 No. 2687 Park Road, Shengze Town, Wujiang District, Suzhou City, Jiangsu Province Applicant after: Shanghai Zhongda Textile Co., Ltd. Applicant after: Zhejiang Semir Garment Co., Ltd Address before: 215228 No. 2687 Park Road, Shengze Town, Wujiang District, Suzhou City, Jiangsu Province Applicant before: Shanghai Zhongda Textile Co., Ltd. |
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