CN107724076A - A kind of softening agent and preparation method thereof - Google Patents
A kind of softening agent and preparation method thereof Download PDFInfo
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- CN107724076A CN107724076A CN201710825176.4A CN201710825176A CN107724076A CN 107724076 A CN107724076 A CN 107724076A CN 201710825176 A CN201710825176 A CN 201710825176A CN 107724076 A CN107724076 A CN 107724076A
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with organometallic compounds; with organic compounds containing boron, silicon, selenium or tellurium atoms
- D06M13/51—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond
- D06M13/513—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond with at least one carbon-silicon bond
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- D06M11/68—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof
- D06M11/72—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof with metaphosphoric acids or their salts; with polyphosphoric acids or their salts; with perphosphoric acids or their salts
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- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/73—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
- D06M11/76—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon oxides or carbonates
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- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
- D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/005—Compositions containing perfumes; Compositions containing deodorants
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
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- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/188—Monocarboxylic acids; Anhydrides, halides or salts thereof
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/402—Amides imides, sulfamic acids
- D06M13/41—Amides derived from unsaturated carboxylic acids, e.g. acrylamide
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- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
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- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
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Abstract
The invention discloses a kind of softening agent and preparation method thereof, the softening agent includes the raw material of following parts by weight：10 20 parts of four oxosilane of prestox ring, 57 parts of polyether-modified nanometer silane, 5 10 parts of sodium acid carbonate, 5 10 parts of plants essential oil, 10 15 parts of stearic acid sodium, 35 parts of acrylamide, 35 parts of calgon, 5 10 parts of nano silicon, 10 20 parts of ethanol, 30 50 parts of deionized water.After the softening agent application of the present invention, the stiffness of fabric declines a lot, and shearing rigidity and bending stiffness all decline a lot, and creasy recovery angle increase is a lot, and flexibility improves a lot.The softening agent manufacturing process of the present invention is simple to operation, and low in raw material price easily obtains, and nontoxic, human body is not stimulated, volatility is low.
Description
Technical field
The invention belongs to technical field of textile auxiliary agent, specifically relates to a kind of softening agent and preparation method thereof.
Background technology
Softening agent is a kind of quiet, the coefficient of kinetic friction chemical substance that can change fiber.When changing confficient of static friction, hand
Thoughts and feelings touches with smooth sense, is easy to move on fiber or fabric；It is fine between fiber and fiber when changing the coefficient of kinetic friction
Structure is easy to be mutually shifted, that is, fiber or fabric it is easily deformable.
Soft finish is the important finishing process in dyeing and printing process.Textile in process, through repeatedly processing after
Feel can become coarse, and general synthetic fabrics is worse, especially Superfine Fibre Fabric.In order that fabric has softness, slided
Refreshing, comfortable feel, it is necessary to arranged to it, widely used at present arranged with softening agent.In addition in chemistry
Softening agent largely is used during fibre spinning, the spinning of various fibers, weaving etc., because with textile processing
A large amount of uses of high speed and short liquor ratio mode, the phase mutual friction increase between fabric and equipment between fabric, be also easy to produce scratch,
Phenomena such as bar defect.It can make fiber that there is the flexible smooth being adapted with processing conditions to avoid damage in itself using softening agent.
Therefore fabric is a kind of important textile auxiliary with softening agent.
With the improvement of living standards, the enhancing of health perception, the requirement more and more higher to textile material, it is desirable to which fabric has
There is certain soft wrinkle resistance, to the quality requirements of softening agent also more and more higher, which also promotes the development of softening agent.
The content of the invention
It is an object of the invention to provide a kind of softening agent and preparation method thereof, to solve what is proposed in above-mentioned background technology
Problem.
To achieve the above object, the present invention provides following technical scheme：
A kind of softening agent, according to parts by weight, including following components：It is the oxosilane 10-20 parts of prestox ring four, polyether-modified
Nanometer silane 5-7 parts, sodium acid carbonate 5-10 parts, plants essential oil 5-10 parts, stearic acid sodium 10-15 parts, acrylamide 3-5 parts, six
Sodium metaphosphate 3-5 parts, nano silicon 5-10 parts, ethanol 10-20 parts, deionized water 30-50 parts.
Preferably, the ethanol is absolute ethyl alcohol, and purity is pure to analyze.
Preferably, the plants essential oil is Lavender, Peppermint essential oil, lemon, jasmine essential oil, rhodamine toner
It is one or more than one kinds of in oil, yulan essential oil, cape jasmine flower essential oil, narcissus flower essential oil.
Preferably, the particle diameter of the nano silicon is 50-200nm.
Preferably, described softening agent, according to parts by weight, including following components：10 parts of four oxosilane of prestox ring, gather
5 parts of ether modified Nano silane, 5 parts of sodium acid carbonate, 5 parts of plants essential oil, 10 parts of stearic acid sodium, 3 parts of acrylamide, calgon
3 parts, 5 parts of nano silicon, 10 parts of ethanol, 30 parts of deionized water.
Preferably, described softening agent, according to parts by weight, including following components：15 parts of four oxosilane of prestox ring, gather
6 parts of ether modified Nano silane, 8 parts of sodium acid carbonate, 8 parts of plants essential oil, 13 parts of stearic acid sodium, 4 parts of acrylamide, calgon
4 parts, 8 parts of nano silicon, 15 parts of ethanol, 40 parts of deionized water.
Preferably, described softening agent, according to parts by weight, including following components：20 parts of four oxosilane of prestox ring, gather
7 parts of ether modified Nano silane, 10 parts of sodium acid carbonate, 10 parts of plants essential oil, 15 parts of stearic acid sodium, 5 parts of acrylamide, hexa metaphosphoric acid
5 parts of sodium, 10 parts of nano silicon, 20 parts of ethanol, 50 parts of deionized water.
Preferably, a kind of preparation method of the softening agent, is comprised the following steps that：
(1) the oxosilane 10-20 parts of prestox ring four, deionized water 30-50 parts are added inside four-hole boiling flask, in oil bath pan
80-100 DEG C of heating, nitrogen protection, the speed for being passed through nitrogen is 1-2L/min, keeps charging flatly, and insertion flatly is equipped with 5-7 parts
The separatory funnel of polyether-modified nanometer silane, rate of addition 2-3mL/min, agitator, mixing speed 1000- is inserted flatly
2000 revs/min, reaction time 3-4h；
(2) first by calgon 3-5 parts, nano silicon 5-10 parts, ethanol 10-20 parts, with ultrasonic disperse 10-20
Minute, ultrasonic power 1000-2000W, obtain homogeneous solution；
(3) homogeneous solution of step (2) is added in the solution of step (1), 500-1000 revs/min, 20-30 points of stirring
Clock；
(4) temperature is reduced to 60-70 DEG C, addition stearic acid sodium 10-15 parts, acrylamide 3-5 parts, 500-1000 revs/min
Clock, stir 20-30 minutes；
(5) 40-50 DEG C is cooled to, sodium acid carbonate 5-10 parts, plants essential oil 5-10 parts is added, 500-1000 revs/min, stirs
Mix 1-2 hours；
(6) 20-30 DEG C is cooled to, closes down stirring, the liquid softener prepared；
(7) stand and be cooled in four-hole boiling flask liquid softener and be less than 20 DEG C, blowing encapsulation, finished product.
Compared with prior art, the beneficial effects of the invention are as follows：
1st, after softening agent of the invention application, the stiffness of fabric decline it is a lot, shearing rigidity and bending stiffness all under
Drop is a lot, and creasy recovery angle increase is a lot, and flexibility improves a lot.
2nd, after softening agent application fabric of the invention, fabric is not easy yellowing, imparting fabrics feel soft, smooth, plentiful,
And there is good drapability and bulkiness.
3rd, after softening agent application fabric of the invention, the excellent water imbibition of natural fabric and well saturating can be kept
Gas, hydrophobic fiber type is set to obtain hygroscopicity.
4th, after softening agent application fabric of the invention, fabric has good resilience, resistance to fold performance.
5th, softening agent manufacturing process of the invention is simple to operation, and low in raw material price easily obtains, and nontoxic, to people
Body does not stimulate, and volatility is low.
6th, mutual compatibility, synergy between various raw materials used in softening agent of the invention, collectively constitute excellent performance
Product.
7th, the addition of sodium acid carbonate, the softness of fabric is improved.
8th, technique is simplified, safe operation is simple, is easy to industrialized production.
9th, softening agent working solution of the invention is stable, is not demulsified, not floating oil.
10th, use of the invention can receive good economic benefit.
Example is embodied
The invention discloses a kind of softening agent, according to important number, including following components：The oxosilane 10- of prestox ring four
20 parts, polyether-modified nanometer silane 5-7 parts, sodium acid carbonate 5-10 parts, plants essential oil 5-10 parts, stearic acid sodium 10-15 parts, propylene
Acid amides 3-5 parts, calgon 3-5 parts, nano silicon 5-10 parts, ethanol 10-20 parts, deionized water 30-50 parts.
Present invention also offers a kind of preparation method of softening agent, comprise the following steps that：
(1) the oxosilane 10-20 parts of prestox ring four, deionized water 30-50 parts are added inside four-hole boiling flask, in oil bath pan
80-100 DEG C of heating, nitrogen protection, the speed for being passed through nitrogen is 1-2L/min, keeps charging flatly, and insertion flatly is equipped with 5-7 parts
The separatory funnel of polyether-modified nanometer silane, rate of addition 2-3mL/min, agitator, mixing speed 1000- is inserted flatly
2000 revs/min, reaction time 3-4h；
(2) first by calgon 3-5 parts, nano silicon 5-10 parts, ethanol 10-20 parts, with ultrasonic disperse 10-20
Minute, ultrasonic power 1000-2000W, obtain homogeneous solution；
(3) homogeneous solution of step (2) is added in the solution of step (1), 500-1000 revs/min, 20-30 points of stirring
Clock；
(4) temperature is reduced to 60-70 DEG C, addition stearic acid sodium 10-15 parts, acrylamide 3-5 parts, 500-1000 revs/min
Clock, stir 20-30 minutes；
(5) 40-50 DEG C is cooled to, sodium acid carbonate 5-10 parts, plants essential oil 5-10 parts is added, 500-1000 revs/min, stirs
Mix 1-2 hours；
(6) 20-30 DEG C is cooled to, closes down stirring, the liquid softener prepared；
(7) stand and be cooled in four-hole boiling flask liquid softener and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 1
The invention discloses a kind of softening agent, according to important number, including following components：The oxosilane 10 of prestox ring four
It is part, 5 parts of polyether-modified nanometer silane, 5 parts of sodium acid carbonate, 5 parts of plants essential oil, 10 parts of stearic acid sodium, 3 parts of acrylamide, six inclined
3 parts of sodium phosphate, 5 parts of nano silicon, 10 parts of ethanol, 30 parts of deionized water.
Present invention also offers a kind of preparation method of softening agent, comprise the following steps that：
(1) 10 parts of four oxosilane of prestox ring, 30 parts of deionized water are added inside four-hole boiling flask, 80 DEG C add in oil bath pan
Heat, nitrogen protection, the speed for being passed through nitrogen is 1L/min, keeps charging flatly, and insertion flatly is equipped with 5 parts of polyether-modified nano-silicons
The separatory funnel of alkane, rate of addition 2mL/min, agitator is inserted flatly, mixing speed is 1000 revs/min, the reaction time
For 3h；
(2) first by 3 parts of calgon, 5 parts of nano silicon, 10 parts of ethanol, with ultrasonic disperse 10 minutes, ultrasonic work(
Rate is 1000W, obtains homogeneous solution；
(3) homogeneous solution of step (2) is added in the solution of step (1), 500 revs/min, stirred 20 minutes；
(4) temperature is reduced to 60 DEG C, is added 10 parts of stearic acid sodium, 3 parts of acrylamide, 500 revs/min, is stirred 20 minutes；
(5) 40 DEG C are cooled to, 5 parts of sodium acid carbonate, 5 parts of plants essential oil is added, 500 revs/min, stirs 1 hour；
(6) 20 DEG C are cooled to, closes down stirring, the liquid softener prepared；
(7) stand and be cooled in four-hole boiling flask liquid softener and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 2
The invention discloses a kind of softening agent, according to important number, including following components：The oxosilane 15 of prestox ring four
It is part, 6 parts of polyether-modified nanometer silane, 8 parts of sodium acid carbonate, 8 parts of plants essential oil, 13 parts of stearic acid sodium, 4 parts of acrylamide, six inclined
4 parts of sodium phosphate, 8 parts of nano silicon, 15 parts of ethanol, 40 parts of deionized water.
Present invention also offers a kind of preparation method of softening agent, comprise the following steps that：
(1) 15 parts of four oxosilane of prestox ring, 40 parts of deionized water are added inside four-hole boiling flask, 90 DEG C add in oil bath pan
Heat, nitrogen protection, the speed for being passed through nitrogen is 2L/min, keeps charging flatly, and insertion flatly is equipped with 6 parts of polyether-modified nano-silicons
The separatory funnel of alkane, rate of addition 2mL/min, agitator is inserted flatly, mixing speed is 2000 revs/min, the reaction time
For 3h；
(2) first by 4 parts of calgon, 8 parts of nano silicon, 15 parts of ethanol, with ultrasonic disperse 15 minutes, ultrasonic work(
Rate is 2000W, obtains homogeneous solution；
(3) homogeneous solution of step (2) is added in the solution of step (1), 900 revs/min, stirred 30 minutes；
(4) temperature is reduced to 65 DEG C, is added 13 parts of stearic acid sodium, 4 parts of acrylamide, 800 revs/min, is stirred 25 minutes；
(5) 45 DEG C are cooled to, 8 parts of sodium acid carbonate, 8 parts of plants essential oil is added, 900 revs/min, stirs 1 hour；
(6) 25 DEG C are cooled to, closes down stirring, the liquid softener prepared；
(7) stand and be cooled in four-hole boiling flask liquid softener and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 3
The invention discloses a kind of softening agent, according to important number, including following components：The oxosilane 20 of prestox ring four
Part, 7 parts of polyether-modified nanometer silane, 10 parts of sodium acid carbonate, 10 parts of plants essential oil, 15 parts of stearic acid sodium, 5 parts of acrylamide, six
5 parts of sodium metaphosphate, 10 parts of nano silicon, 20 parts of ethanol, 50 parts of deionized water.
Present invention also offers a kind of preparation method of softening agent, comprise the following steps that：
(1) 20 parts of prestox ring four oxosilane, 50 parts of deionized water are added inside four-hole boiling flask, in 100 DEG C of oil bath pan
Heating, nitrogen protection, the speed for being passed through nitrogen is 2L/min, keeps charging flatly, and insertion flatly is equipped with 7 parts of polyether-modified nanometers
The separatory funnel of silane, rate of addition 3mL/min, agitator is inserted flatly, mixing speed is 2000 revs/min, during reaction
Between be 4h；
(2) first by 5 parts of calgon, 10 parts of nano silicon, 20 parts of ethanol, with ultrasonic disperse 20 minutes, ultrasound
Power is 2000W, obtains homogeneous solution；
(3) homogeneous solution of step (2) is added in the solution of step (1), 1000 revs/min, stirred 30 minutes；
(4) temperature is reduced to 70 DEG C, is added 15 parts of stearic acid sodium, 5 parts of acrylamide, 1000 revs/min, is stirred 30 points
Clock；
(5) 50 DEG C are cooled to, 10 parts of sodium acid carbonate, 10 parts of plants essential oil is added, 1000 revs/min, stirs 2 hours；
(6) 30 DEG C are cooled to, closes down stirring, the liquid softener prepared；
(7) stand and be cooled in four-hole boiling flask liquid softener and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 4
The invention discloses a kind of softening agent, according to important number, including following components：The oxosilane 20 of prestox ring four
It is part, 7 parts of polyether-modified nanometer silane, 10 parts of sodium acid carbonate, 5 parts of plants essential oil, 10 parts of stearic acid sodium, 3 parts of acrylamide, six inclined
5 parts of sodium phosphate, 5 parts of nano silicon, 10 parts of ethanol, 30 parts of deionized water.
Present invention also offers a kind of preparation method of softening agent, comprise the following steps that：
(1) 20 parts of prestox ring four oxosilane, 30 parts of deionized water are added inside four-hole boiling flask, in 100 DEG C of oil bath pan
Heating, nitrogen protection, the speed for being passed through nitrogen is 2L/min, keeps charging flatly, and insertion flatly is equipped with 7 parts of polyether-modified nanometers
The separatory funnel of silane, rate of addition 3mL/min, agitator is inserted flatly, mixing speed is 2000 revs/min, the reaction time
For 4h；
(2) first by 5 parts of calgon, 5 parts of nano silicon, 10 parts of ethanol, with ultrasonic disperse 10 minutes, ultrasonic work(
Rate is 2000W, obtains homogeneous solution；
(3) homogeneous solution of step (2) is added in the solution of step (1), 1000 revs/min, stirred 20 minutes；
(4) temperature is reduced to 70 DEG C, is added 10 parts of stearic acid sodium, 3 parts of acrylamide, 500 revs/min, is stirred 30 minutes；
(5) 45 DEG C are cooled to, 10 parts of sodium acid carbonate, 5 parts of plants essential oil is added, 900 revs/min, stirs 1 hour；
(6) 20 DEG C are cooled to, closes down stirring, the liquid softener prepared；
(7) stand and be cooled in four-hole boiling flask liquid softener and be less than 20 DEG C, blowing encapsulation, finished product.
Test case
The softening agent that embodiment 1,2,3,4 is respectively adopted in the fabric of four pieces of formed objects carries out soft treatment, test result
It is as follows：
| Embodiment | Stiffness | Creasy recovery angle | Shearing rigidity | Bending stiffness | Flexibility |
| Former cloth | 3.62 | 120 | 1.82 | 0.8022 | 0 |
| 1 | 1.64 | 160 | 1.38 | 0.4105 | 5 |
| 2 | 1.36 | 180 | 1.26 | 0.3724 | 5 |
| 3 | 1.02 | 196 | 1.12 | 0.3423 | 5 |
| 4 | 1.16 | 188 | 1.20 | 0.3533 | 5 |
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of changes, modification can be carried out to these embodiments, replace without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention includes appended claims and its equivalent limits.
Claims (8)
- A kind of 1. softening agent, it is characterised in that：The softening agent includes the raw material of following parts by weight：The oxosilane of prestox ring four 10-20 parts, polyether-modified nanometer silane 5-7 parts, sodium acid carbonate 5-10 parts, plants essential oil 5-10 parts, stearic acid sodium 10-15 parts, Acrylamide 3-5 parts, calgon 3-5 parts, nano silicon 5-10 parts, ethanol 10-20 parts, deionized water 30-50 parts.
- 2. softening agent according to claim 1, it is characterised in that：The ethanol is absolute ethyl alcohol, and purity is pure to analyze.
- 3. softening agent according to claim 1, it is characterised in that：The plants essential oil be Lavender, Peppermint essential oil, In lemon, jasmine essential oil, Rosa Damascana, yulan essential oil, cape jasmine flower essential oil, narcissus flower essential oil it is a kind of or a kind of with On.
- 4. softening agent according to claim 1, it is characterised in that：The particle diameter of the nano silicon is 50-200nm.
- 5. softening agent according to claim 1, it is characterised in that：According to parts by weight, including following components：Prestox ring Four 10 parts of oxosilanes, 5 parts of polyether-modified nanometer silane, 5 parts of sodium acid carbonate, 5 parts of plants essential oil, 10 parts of stearic acid sodium, acryloyl 3 parts of amine, 3 parts of calgon, 5 parts of nano silicon, 10 parts of ethanol, 30 parts of deionized water.
- 6. softening agent according to claim 1, it is characterised in that：According to parts by weight, including following components：Prestox ring Four 15 parts of oxosilanes, 6 parts of polyether-modified nanometer silane, 8 parts of sodium acid carbonate, 8 parts of plants essential oil, 13 parts of stearic acid sodium, acryloyl 4 parts of amine, 4 parts of calgon, 8 parts of nano silicon, 15 parts of ethanol, 40 parts of deionized water.
- 7. softening agent according to claim 1, it is characterised in that：According to parts by weight, including following components：Prestox ring Four 20 parts of oxosilanes, 7 parts of polyether-modified nanometer silane, 10 parts of sodium acid carbonate, 10 parts of plants essential oil, 15 parts of stearic acid sodium, propylene 5 parts of acid amides, 5 parts of calgon, 10 parts of nano silicon, 20 parts of ethanol, 50 parts of deionized water.
- A kind of 8. preparation method of any described softening agent in 1-7 using the claims, it is characterised in that：Specific steps It is as follows：Step 1, the oxosilane 10-20 parts of prestox ring four, deionized water 30-50 parts are added inside four-hole boiling flask, in oil bath pan 80-100 DEG C of heating, nitrogen protection, the speed for being passed through nitrogen is 1-2L/min, keeps charging flatly, and insertion flatly is equipped with 5-7 parts The separatory funnel of polyether-modified nanometer silane, rate of addition 2-3mL/min, agitator, mixing speed 1000- is inserted flatly 2000 revs/min, reaction time 3-4h；Step 2, first by calgon 3-5 parts, nano silicon 5-10 parts, ethanol 10-20 parts, with ultrasonic disperse 10-20 Minute, ultrasonic power 1000-2000W, obtain homogeneous solution；Step 3, the homogeneous solution of step 2 is added in the solution of step 1,500-1000 revs/min, stirs 20-30 minutes；Step 4, temperature is reduced to 60-70 DEG C, addition stearic acid sodium 10-15 parts, acrylamide 3-5 parts, 500-1000 revs/min Clock, stir 20-30 minutes；Step 5,40-50 DEG C is cooled to, sodium acid carbonate 5-10 parts, plants essential oil 5-10 parts is added, 500-1000 revs/min, stirs Mix 1-2 hours；Step 6,20-30 DEG C is cooled to, closes down stirring, the liquid softener prepared；Step 7, stand and be cooled in four-hole boiling flask liquid softener and be less than 20 DEG C, blowing encapsulation, finished product.
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| CN104762814A (en) * | 2015-03-25 | 2015-07-08 | 苏州威尔德工贸有限公司 | Linen softening agent and using method thereof |
| CN105220468A (en) * | 2015-11-13 | 2016-01-06 | 付淑珍 | A kind of novel softener for textile fabric and preparation method thereof |
| CN105603733A (en) * | 2016-02-26 | 2016-05-25 | 苏州三和开泰花线织造有限公司 | Biodegradable textile fabric softening agent and preparation method thereof |
| CN106367958A (en) * | 2016-10-13 | 2017-02-01 | 无锡市华诚印染剂厂 | Anti-fading fabric softening agent |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104762814A (en) * | 2015-03-25 | 2015-07-08 | 苏州威尔德工贸有限公司 | Linen softening agent and using method thereof |
| CN105220468A (en) * | 2015-11-13 | 2016-01-06 | 付淑珍 | A kind of novel softener for textile fabric and preparation method thereof |
| CN105603733A (en) * | 2016-02-26 | 2016-05-25 | 苏州三和开泰花线织造有限公司 | Biodegradable textile fabric softening agent and preparation method thereof |
| CN106367958A (en) * | 2016-10-13 | 2017-02-01 | 无锡市华诚印染剂厂 | Anti-fading fabric softening agent |
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Application publication date: 20180223 |