CN107740276A - A kind of radiation proof softener and preparation method thereof - Google Patents
A kind of radiation proof softener and preparation method thereof Download PDFInfo
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- CN107740276A CN107740276A CN201710897079.6A CN201710897079A CN107740276A CN 107740276 A CN107740276 A CN 107740276A CN 201710897079 A CN201710897079 A CN 201710897079A CN 107740276 A CN107740276 A CN 107740276A
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- Prior art keywords
- parts
- softener
- radiation proof
- essential oil
- nanometer
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- 230000005855 radiation Effects 0.000 title claims abstract description 59
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 70
- 239000000843 powder Substances 0.000 claims abstract description 50
- 239000000341 volatile oil Substances 0.000 claims abstract description 33
- 229920000914 Metallic fiber Polymers 0.000 claims abstract description 26
- 229910000859 α-Fe Inorganic materials 0.000 claims abstract description 23
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims abstract description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 claims abstract description 21
- 239000008367 deionised water Substances 0.000 claims abstract description 21
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 21
- 229920001661 Chitosan Polymers 0.000 claims abstract description 20
- 239000005543 nano-size silicon particle Substances 0.000 claims abstract description 20
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims abstract description 20
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims abstract description 19
- 229910000077 silane Inorganic materials 0.000 claims abstract description 19
- GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 claims abstract description 19
- HMMGMWAXVFQUOA-UHFFFAOYSA-N octamethylcyclotetrasiloxane Chemical compound C[Si]1(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O1 HMMGMWAXVFQUOA-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000002994 raw material Substances 0.000 claims abstract description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 28
- 241000196324 Embryophyta Species 0.000 claims description 22
- 235000019441 ethanol Nutrition 0.000 claims description 22
- 238000003756 stirring Methods 0.000 claims description 20
- 239000007788 liquid Substances 0.000 claims description 17
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 16
- 238000009835 boiling Methods 0.000 claims description 14
- 229910052757 nitrogen Inorganic materials 0.000 claims description 14
- 239000000835 fiber Substances 0.000 claims description 12
- 239000012456 homogeneous solution Substances 0.000 claims description 11
- 239000003921 oil Substances 0.000 claims description 9
- 239000000377 silicon dioxide Substances 0.000 claims description 8
- 238000007664 blowing Methods 0.000 claims description 7
- 238000005538 encapsulation Methods 0.000 claims description 7
- 238000003780 insertion Methods 0.000 claims description 7
- 230000037431 insertion Effects 0.000 claims description 7
- 230000035484 reaction time Effects 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 5
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 4
- 238000007747 plating Methods 0.000 claims description 3
- 235000005979 Citrus limon Nutrition 0.000 claims description 2
- 244000131522 Citrus pyriformis Species 0.000 claims description 2
- 244000111489 Gardenia augusta Species 0.000 claims description 2
- 235000018958 Gardenia augusta Nutrition 0.000 claims description 2
- 235000010254 Jasminum officinale Nutrition 0.000 claims description 2
- 240000005385 Jasminum sambac Species 0.000 claims description 2
- 244000178870 Lavandula angustifolia Species 0.000 claims description 2
- 235000010663 Lavandula angustifolia Nutrition 0.000 claims description 2
- 240000005819 Magnolia denudata Species 0.000 claims description 2
- 235000016094 Magnolia denudata Nutrition 0.000 claims description 2
- 241000234479 Narcissus Species 0.000 claims description 2
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 2
- 229910052782 aluminium Inorganic materials 0.000 claims description 2
- 239000001102 lavandula vera Substances 0.000 claims description 2
- 235000018219 lavender Nutrition 0.000 claims description 2
- DEDOPGXGGQYYMW-UHFFFAOYSA-N molinate Chemical compound CCSC(=O)N1CCCCCC1 DEDOPGXGGQYYMW-UHFFFAOYSA-N 0.000 claims description 2
- 229910052759 nickel Inorganic materials 0.000 claims description 2
- 239000002245 particle Substances 0.000 claims description 2
- 229910052709 silver Inorganic materials 0.000 claims description 2
- 239000004332 silver Substances 0.000 claims description 2
- WSPOQKCOERDWJQ-UHFFFAOYSA-N 2-methyl-1,3,5,7,2,4,6,8-tetraoxatetrasilocane Chemical compound C[SiH]1O[SiH2]O[SiH2]O[SiH2]O1 WSPOQKCOERDWJQ-UHFFFAOYSA-N 0.000 claims 3
- DCXXMTOCNZCJGO-UHFFFAOYSA-N tristearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 claims 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- 240000002853 Nelumbo nucifera Species 0.000 claims 1
- 235000006508 Nelumbo nucifera Nutrition 0.000 claims 1
- 235000006510 Nelumbo pentapetala Nutrition 0.000 claims 1
- 235000011449 Rosa Nutrition 0.000 claims 1
- 238000004458 analytical method Methods 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- 239000011734 sodium Substances 0.000 claims 1
- RSNQKPMXXVDJFG-UHFFFAOYSA-N tetrasiloxane Chemical compound [SiH3]O[SiH2]O[SiH2]O[SiH3] RSNQKPMXXVDJFG-UHFFFAOYSA-N 0.000 claims 1
- 239000004744 fabric Substances 0.000 abstract description 16
- 239000004753 textile Substances 0.000 abstract description 4
- 230000007423 decrease Effects 0.000 abstract description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 238000005452 bending Methods 0.000 abstract description 2
- 231100000252 nontoxic Toxicity 0.000 abstract description 2
- 230000003000 nontoxic effect Effects 0.000 abstract description 2
- 238000011084 recovery Methods 0.000 abstract description 2
- 238000010008 shearing Methods 0.000 abstract description 2
- 150000001335 aliphatic alkanes Chemical class 0.000 description 7
- 239000000243 solution Substances 0.000 description 6
- MOMKYJPSVWEWPM-UHFFFAOYSA-N 4-(chloromethyl)-2-(4-methylphenyl)-1,3-thiazole Chemical compound C1=CC(C)=CC=C1C1=NC(CCl)=CS1 MOMKYJPSVWEWPM-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 235000019983 sodium metaphosphate Nutrition 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 201000004384 Alopecia Diseases 0.000 description 1
- 206010021137 Hypovolaemia Diseases 0.000 description 1
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 1
- 244000246386 Mentha pulegium Species 0.000 description 1
- 235000016257 Mentha pulegium Nutrition 0.000 description 1
- 235000004357 Mentha x piperita Nutrition 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 208000013738 Sleep Initiation and Maintenance disease Diseases 0.000 description 1
- 238000003915 air pollution Methods 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 208000006218 bradycardia Diseases 0.000 description 1
- 230000036471 bradycardia Effects 0.000 description 1
- 201000011510 cancer Diseases 0.000 description 1
- 210000000748 cardiovascular system Anatomy 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 208000035475 disorder Diseases 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000005670 electromagnetic radiation Effects 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000007667 floating Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 208000024963 hair loss Diseases 0.000 description 1
- 230000003676 hair loss Effects 0.000 description 1
- 235000001050 hortel pimenta Nutrition 0.000 description 1
- 230000002209 hydrophobic effect Effects 0.000 description 1
- 238000005213 imbibition Methods 0.000 description 1
- 230000036737 immune function Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 231100000405 induce cancer Toxicity 0.000 description 1
- 206010022437 insomnia Diseases 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 208000032839 leukemia Diseases 0.000 description 1
- 201000002364 leukopenia Diseases 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000003176 neuroleptic agent Substances 0.000 description 1
- 230000000701 neuroleptic effect Effects 0.000 description 1
- 230000027758 ovulation cycle Effects 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- PYWVYCXTNDRMGF-UHFFFAOYSA-N rhodamine B Chemical compound [Cl-].C=12C=CC(=[N+](CC)CC)C=C2OC2=CC(N(CC)CC)=CC=C2C=1C1=CC=CC=C1C(O)=O PYWVYCXTNDRMGF-UHFFFAOYSA-N 0.000 description 1
- 239000012224 working solution Substances 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
- 238000004383 yellowing Methods 0.000 description 1
Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with organometallic compounds; with organic compounds containing boron, silicon, selenium or tellurium atoms
- D06M13/51—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond
- D06M13/513—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond with at least one carbon-silicon bond
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- D—TEXTILES; PAPER
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- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/49—Oxides or hydroxides of elements of Groups 8, 9,10 or 18 of the Periodic Table; Ferrates; Cobaltates; Nickelates; Ruthenates; Osmates; Rhodates; Iridates; Palladates; Platinates
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/68—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof
- D06M11/72—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof with metaphosphoric acids or their salts; with polyphosphoric acids or their salts; with perphosphoric acids or their salts
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/73—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
- D06M11/76—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon oxides or carbonates
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- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
- D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
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- D—TEXTILES; PAPER
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- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/83—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with metals; with metal-generating compounds, e.g. metal carbonyls; Reduction of metal compounds on textiles
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- D—TEXTILES; PAPER
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- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/188—Monocarboxylic acids; Anhydrides, halides or salts thereof
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
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- D—TEXTILES; PAPER
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/402—Amides imides, sulfamic acids
- D06M13/41—Amides derived from unsaturated carboxylic acids, e.g. acrylamide
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- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
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- D—TEXTILES; PAPER
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- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
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- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/25—Resistance to light or sun, i.e. protection of the textile itself as well as UV shielding materials or treatment compositions therefor; Anti-yellowing treatments
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Organic Chemistry (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a kind of preparation method of radiation proof softener, the radiation proof softener includes the raw material of following parts by weight：10 20 parts of octamethylcy-clotetrasiloxane, 57 parts of polyether-modified nanometer silane, 5 10 parts of sodium acid carbonate, 5 10 parts of plants essential oil, 10 15 parts of odium stearate, 35 parts of acrylamide, 35 parts of calgon, 5 10 parts of nano silicon, 10 20 parts of ethanol, 5 10 parts of chitosan, 5 10 parts of metallic fiber powder, 5 10 parts of nanometer ferrite powder, 30 50 parts of deionized water.After the radiation proof softener application of the present invention, the stiffness decline of fabric is a lot, and shearing rigidity and bending stiffness all decline a lot, and creasy recovery angle increase is a lot, and compliance improves a lot, and shielding property improves more than 80% than source textile.The radiation proof softener manufacturing process of the present invention is simple to operation, and low in raw material price easily obtains, and nontoxic, human body is not stimulated, volatility is low.
Description
Technical field
The invention belongs to technical field of textile auxiliary agent, specifically relates to a kind of radiation proof softener and preparation method thereof.
Background technology
It is uniformly last layer diaphragm for fabric, fiber that the effect of softener, which just looks like, fiber surface due to
Softener is adsorbed, interfibrous coefficient of friction reduces, and mobility enhances, the intrinsic smooth, extension of fiber, compressibility
Can also it be recovered, so fabric becomes more soft, fluffy, flexible.
In daily life, electromagnetic radiation turns into the third-largest " stealthy killer " after pollution of waterhead, air pollution, to me
Health have a very big impact.Such as：Radiation can cause children's intelligence incomplete, and it is most likely to cause
One of the reason for virgin cases with leukemia；Radiation can induce cancer and accelerate the cancer cell multiplication of human body；Radiation can influence people
Cardiovascular system, show as palpitaition, hair loss, insomnia, some women disorder of menstrual cycle, bradycardia, heartbeat oligemia, Dou Xingxin
Rate is uneven, Neuroleptic Leukocytopenia, and immunologic function declines etc..
With the improvement of living standards, the enhancing of the awareness of environment protection and health, the requirement more and more higher to textile material, it is desirable to
Fabric has certain submissive wrinkle resistance, radiation resistance, and to the quality requirements of feature softener also more and more higher, this also promotees
The development of multi-functional softener is entered.
The content of the invention
It is an object of the invention to provide a kind of radiation proof softener and preparation method, to solve to carry in above-mentioned background technology
The problem of going out.
To achieve the above object, the present invention provides following technical scheme：
A kind of radiation proof softener, according to parts by weight, including following components：Octamethylcy-clotetrasiloxane 10-20 parts, gather
Ether modified Nano silane 5-7 parts, sodium acid carbonate 5-10 parts, plants essential oil 5-10 parts, odium stearate 10-15 parts, acrylamide 3-5
Part, calgon 3-5 parts, nano silicon 5-10 parts, ethanol 10-20 parts, chitosan 5-10 parts, metallic fiber powder 5-
10 parts, nanometer ferrite powder 5-10 parts, deionized water 30-50 parts.
Preferably, the ethanol is absolute ethyl alcohol, and purity is pure to analyze.
Preferably, the plants essential oil is Lavender, Peppermint essential oil, lemon, jasmine essential oil, rhodamine toner
It is one or more than one kinds of in oil, yulan essential oil, cape jasmine flower essential oil, narcissus flower essential oil.
Preferably, the nanometer ferrite powder, metallic fiber powder, the particle diameter of nano silicon are 50-200nm.
Preferably, the metallic fiber powder is one kind in silver plated fiber, plating aluminum fiber, Cu coated fibre, nickel plating fiber
Or more than one.
Preferably, described radiation proof softener, according to parts by weight, including following components：Octamethylcy-clotetrasiloxane
10 parts, 5 parts of polyether-modified nanometer silane, 5 parts of sodium acid carbonate, 5 parts of plants essential oil, 10 parts of odium stearate, 3 parts of acrylamide, six
3 parts of sodium metaphosphate, 5 parts of nano silicon, 10 parts of ethanol, 5 parts of chitosan, 5 parts of metallic fiber powder, nanometer ferrite powder
5 parts, 30 parts of deionized water.
Preferably, described radiation proof softener, according to parts by weight, including following components：Octamethylcy-clotetrasiloxane
15 parts, 6 parts of polyether-modified nanometer silane, 8 parts of sodium acid carbonate, 8 parts of plants essential oil, 13 parts of odium stearate, 4 parts of acrylamide, six
4 parts of sodium metaphosphate, 8 parts of nano silicon, 15 parts of ethanol, 8 parts of chitosan, 8 parts of metallic fiber powder, nanometer ferrite powder
8 parts, 40 parts of deionized water.
Preferably, described radiation proof softener, according to parts by weight, including following components：Octamethylcy-clotetrasiloxane
20 parts, 7 parts of polyether-modified nanometer silane, 10 parts of sodium acid carbonate, 10 parts of plants essential oil, 15 parts of odium stearate, 5 parts of acrylamide,
5 parts of calgon, 10 parts of nano silicon, 20 parts of ethanol, 10 parts of chitosan, 10 parts of metallic fiber powder, Nanoscale Iron oxygen
10 parts of body powder, 50 parts of deionized water.
A kind of preparation method of radiation proof softener, is comprised the following steps that：
(1) octamethylcy-clotetrasiloxane 10-20 parts, deionized water 30-50 parts are added inside four-hole boiling flask, in oil bath pan
80-100 DEG C of heating, nitrogen protection, the speed for being passed through nitrogen is 1-2L/min, keeps charging flatly, and insertion flatly is equipped with 5-7 parts
The separatory funnel of polyether-modified nanometer silane, rate of addition 2-3mL/min, agitator, mixing speed 1000- is inserted flatly
2000 revs/min, reaction time 3-4h；
(2) first by calgon 3-5 parts, metallic fiber powder 5-10 parts, nanometer ferrite powder 5-10 parts, nanometer two
Silica 5-10 parts, ethanol 10-20 parts, with ultrasonic disperse 10-20 minutes, ultrasonic power 1000-2000W, obtain uniformly molten
Liquid；
(3) homogeneous solution of step (2) is added in the solution of step (1), 500-1000 revs/min, 20-30 points of stirring
Clock；
(4) temperature is reduced to 60-70 DEG C, addition odium stearate 10-15 parts, acrylamide 3-5 parts, 500-1000 revs/min
Clock, stir 20-30 minutes；
(5) 40-50 DEG C is cooled to, adds chitosan 5-10 parts, sodium acid carbonate 5-10 parts, plants essential oil 5-10 parts, 500-
1000 revs/min, stir 1-2 hours；
(6) 20-30 DEG C is cooled to, closes down stirring, the liquid radiation proof softener prepared；
(7) stand and be cooled in four-hole boiling flask liquid radiation proof softener and be less than 20 DEG C, blowing encapsulation, finished product.
Compared with prior art, the beneficial effects of the invention are as follows：
1st, after radiation proof softener of the invention application, the stiffness of fabric declines a lot, and shearing rigidity is firm with bending
Degree all decline is a lot, and creasy recovery angle increase is a lot, and compliance improves a lot, and the shielding property of fabric improves than source textile
More than 80%.
2nd, after radiation proof softener application fabric of the invention, fabric is not easy yellowing, and it is soft to assign fabric feeling radiation proof
It is suitable, smooth, plentiful, and there is good drapability and bulkiness.
3rd, after radiation proof softener application fabric of the invention, the excellent water imbibition of natural fabric and good can be kept
Good gas permeability, hydrophobic fiber type is set to obtain hygroscopicity.
4th, after radiation proof softener application fabric of the invention, fabric has good resilience, resistance to fold performance.
5th, radiation proof softener manufacturing process of the invention is simple to operation, and low in raw material price easily obtains, and nontoxic nothing
Evil, is not stimulated human body, volatility is low.
6th, mutual compatibility between various raw materials used in radiation proof softener of the invention, synergy, collectively constitutes performance
Excellent product.
7th, the addition of sodium acid carbonate improves the submissive performance of fabric, metallic fiber powder, nanometer ferrite powder plus
Enter to improve the shielding property of fabric.
8th, technique is simplified, safe operation is simple, is easy to industrialized production.
9th, radiation proof softener working solution of the invention is stable, is not demulsified, not floating oil
10th, use of the invention can receive good economic benefit.
Example is embodied
The invention discloses a kind of radiation proof softener, according to parts by weight, including following components：The silica of prestox ring four
Alkane 10-20 parts, polyether-modified nanometer silane 5-7 parts, sodium acid carbonate 5-10 parts, plants essential oil 5-10 parts, odium stearate 10-15
Part, acrylamide 3-5 parts, calgon 3-5 parts, nano silicon 5-10 parts, ethanol 10-20 parts, chitosan 5-10 parts,
Metallic fiber powder 5-10 parts, nanometer ferrite powder 5-10 parts, deionized water 30-50 parts.
Present invention also offers a kind of preparation method of radiation proof softener, comprise the following steps that：
(1) octamethylcy-clotetrasiloxane 10-20 parts, deionized water 30-50 parts are added inside four-hole boiling flask, in oil bath pan
80-100 DEG C of heating, nitrogen protection, the speed for being passed through nitrogen is 1-2L/min, keeps charging flatly, and insertion flatly is equipped with 5-7 parts
The separatory funnel of polyether-modified nanometer silane, rate of addition 2-3mL/min, agitator, mixing speed 1000- is inserted flatly
2000 revs/min, reaction time 3-4h；
(2) first by calgon 3-5 parts, metallic fiber powder 5-10 parts, nanometer ferrite powder 5-10 parts, nanometer two
Silica 5-10 parts, ethanol 10-20 parts, with ultrasonic disperse 10-20 minutes, ultrasonic power 1000-2000W, obtain uniformly molten
Liquid；
(3) homogeneous solution of step (2) is added in the solution of step (1), 500-1000 revs/min, 20-30 points of stirring
Clock；
(4) temperature is reduced to 60-70 DEG C, addition odium stearate 10-15 parts, acrylamide 3-5 parts, 500-1000 revs/min
Clock, stir 20-30 minutes；
(5) 40-50 DEG C is cooled to, adds chitosan 5-10 parts, sodium acid carbonate 5-10 parts, plants essential oil 5-10 parts, 500-
1000 revs/min, stir 1-2 hours；
(6) 20-30 DEG C is cooled to, closes down stirring, the liquid radiation proof softener prepared；
(7) stand and be cooled in four-hole boiling flask liquid radiation proof softener and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 1
The invention discloses a kind of radiation proof softener, according to parts by weight, including following components：The silica of prestox ring four
10 parts of alkane, 5 parts of polyether-modified nanometer silane, 5 parts of sodium acid carbonate, 5 parts of plants essential oil, 10 parts of odium stearate, 3 parts of acrylamide,
3 parts of calgon, 5 parts of nano silicon, 10 parts of ethanol, 5 parts of chitosan, 5 parts of metallic fiber powder, nanometer ferrite powder
Last 5 parts, 30 parts of deionized water.
Present invention also offers a kind of preparation method of radiation proof softener, comprise the following steps that：
(1) 10 parts of octamethylcy-clotetrasiloxane, 30 parts of deionized water are added inside four-hole boiling flask, 80 DEG C add in oil bath pan
Heat, nitrogen protection, the speed for being passed through nitrogen is 1L/min, keeps charging flatly, and insertion flatly is equipped with 5 parts of polyether-modified nano-silicons
The separatory funnel of alkane, rate of addition 2mL/min, agitator is inserted flatly, mixing speed is 1000 revs/min, the reaction time
For 3h；
(2) first by 3 parts of calgon, 5 parts of metallic fiber powder, 5 parts of nanometer ferrite powder, nano silicon 5
Part, 10 parts of ethanol, with ultrasonic disperse 10 minutes, ultrasonic power 1000W, obtain homogeneous solution；
(3) homogeneous solution of step (2) is added in the solution of step (1), 500 revs/min, stirred 20 minutes；
(4) temperature is reduced to 60 DEG C, is added 10 parts of odium stearate, 3 parts of acrylamide, 500 revs/min, is stirred 20 minutes；
(5) 40 DEG C are cooled to, 5 parts of chitosan, 5 parts of sodium acid carbonate, 5 parts of plants essential oil is added, 500 revs/min, stirs 1
Hour；
(6) 20 DEG C are cooled to, closes down stirring, the liquid radiation proof softener prepared；
(7) stand and be cooled in four-hole boiling flask liquid radiation proof softener and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 2
The invention discloses a kind of radiation proof softener, according to parts by weight, including following components：The silica of prestox ring four
15 parts of alkane, 6 parts of polyether-modified nanometer silane, 8 parts of sodium acid carbonate, 8 parts of plants essential oil, 13 parts of odium stearate, 4 parts of acrylamide,
4 parts of calgon, 8 parts of nano silicon, 15 parts of ethanol, 8 parts of chitosan, 8 parts of metallic fiber powder, nanometer ferrite powder
Last 8 parts, 40 parts of deionized water.
Present invention also offers a kind of preparation method of radiation proof softener, comprise the following steps that：
(1) 15 parts of octamethylcy-clotetrasiloxane, 40 parts of deionized water are added inside four-hole boiling flask, 90 DEG C add in oil bath pan
Heat, nitrogen protection, the speed for being passed through nitrogen is 2L/min, keeps charging flatly, and insertion flatly is equipped with 6 parts of polyether-modified nano-silicons
The separatory funnel of alkane, rate of addition 2mL/min, agitator is inserted flatly, mixing speed is 2000 revs/min, the reaction time
For 3h；
(2) first by 4 parts of calgon, 8 parts of metallic fiber powder, 8 parts of nanometer ferrite powder, nano silicon 8
Part, 15 parts of ethanol, with ultrasonic disperse 15 minutes, ultrasonic power 2000W, obtain homogeneous solution；
(3) homogeneous solution of step (2) is added in the solution of step (1), 900 revs/min, stirred 30 minutes；
(4) temperature is reduced to 65 DEG C, is added 13 parts of odium stearate, 4 parts of acrylamide, 800 revs/min, is stirred 25 minutes；
(5) 45 DEG C are cooled to, 8 parts of chitosan, 8 parts of sodium acid carbonate, 8 parts of plants essential oil is added, 900 revs/min, stirs 1
Hour；
(6) 25 DEG C are cooled to, closes down stirring, the liquid radiation proof softener prepared；
(7) stand and be cooled in four-hole boiling flask liquid radiation proof softener and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 3
The invention discloses a kind of radiation proof softener, according to parts by weight, including following components：The silica of prestox ring four
20 parts of alkane, 7 parts of polyether-modified nanometer silane, 10 parts of sodium acid carbonate, 10 parts of plants essential oil, 15 parts of odium stearate, acrylamide 5
Part, 5 parts of calgon, 10 parts of nano silicon, 20 parts of ethanol, 10 parts of chitosan, 10 parts of metallic fiber powder, Nanoscale Iron
10 parts of ferrite powder, 50 parts of deionized water.
Present invention also offers a kind of preparation method of radiation proof softener, comprise the following steps that：
(1) 20 parts of octamethylcy-clotetrasiloxane, 50 parts of deionized water are added inside four-hole boiling flask, in 100 DEG C of oil bath pan
Heating, nitrogen protection, the speed for being passed through nitrogen is 2L/min, keeps charging flatly, and insertion flatly is equipped with 7 parts of polyether-modified nanometers
The separatory funnel of silane, rate of addition 3mL/min, agitator is inserted flatly, mixing speed is 2000 revs/min, during reaction
Between be 4h；
(2) first by 5 parts of calgon, 10 parts of metallic fiber powder, 10 parts of nanometer ferrite powder, nano silicon
10 parts, 20 parts of ethanol, with ultrasonic disperse 20 minutes, ultrasonic power 2000W, obtain homogeneous solution；
(3) homogeneous solution of step (2) is added in the solution of step (1), 1000 revs/min, stirred 30 minutes；
(4) temperature is reduced to 70 DEG C, is added 15 parts of odium stearate, 5 parts of acrylamide, 1000 revs/min, is stirred 30 points
Clock；
(5) 50 DEG C are cooled to, 10 parts of chitosan, 10 parts of sodium acid carbonate, 10 parts of plants essential oil is added, 1000 revs/min, stirs
Mix 2 hours；
(6) 30 DEG C are cooled to, closes down stirring, the liquid radiation proof softener prepared；
(7) stand and be cooled in four-hole boiling flask liquid radiation proof softener and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 4
The invention discloses a kind of radiation proof softener, according to parts by weight, including following components：The silica of prestox ring four
20 parts of alkane, 7 parts of polyether-modified nanometer silane, 10 parts of sodium acid carbonate, 5 parts of plants essential oil, 10 parts of odium stearate, 3 parts of acrylamide,
5 parts of calgon, 5 parts of nano silicon, 10 parts of ethanol, 5 parts of chitosan, 5 parts of metallic fiber powder, nanometer ferrite powder
Last 10 parts, 30 parts of deionized water.
Present invention also offers a kind of preparation method of radiation proof softener, comprise the following steps that：
(1) 20 parts of octamethylcy-clotetrasiloxane, 30 parts of deionized water are added inside four-hole boiling flask, in 100 DEG C of oil bath pan
Heating, nitrogen protection, the speed for being passed through nitrogen is 2L/min, keeps charging flatly, and insertion flatly is equipped with 7 parts of polyether-modified nanometers
The separatory funnel of silane, rate of addition 3mL/min, agitator is inserted flatly, mixing speed is 2000 revs/min, the reaction time
For 4h；
(2) first by 5 parts of calgon, 5 parts of metallic fiber powder, 10 parts of nanometer ferrite powder, nano silicon 5
Part, 10 parts of ethanol, with ultrasonic disperse 10 minutes, ultrasonic power 2000W, obtain homogeneous solution；
(3) homogeneous solution of step (2) is added in the solution of step (1), 1000 revs/min, stirred 20 minutes；
(4) temperature is reduced to 70 DEG C, is added 10 parts of odium stearate, 3 parts of acrylamide, 500 revs/min, is stirred 30 minutes；
(5) 45 DEG C are cooled to, 5 parts of chitosan, 10 parts of sodium acid carbonate, 5 parts of plants essential oil is added, 900 revs/min, stirs 1
Hour；
(6) 20 DEG C are cooled to, closes down stirring, the liquid radiation proof softener prepared；
(7) stand and be cooled in four-hole boiling flask liquid radiation proof softener and be less than 20 DEG C, blowing encapsulation, finished product.
Test case
The softener that embodiment 1,2,3,4 is respectively adopted in the fabric of four pieces of formed objects carries out submissive processing, test result
It is as follows：
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of changes, modification can be carried out to these embodiments, replace without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention includes appended claims and its equivalent limits.
Claims (9)
- A kind of 1. radiation proof softener, it is characterised in that：The radiation proof softener includes the raw material of following parts by weight：Eight first Basic ring tetrasiloxane 10-20 parts, polyether-modified nanometer silane 5-7 parts, sodium acid carbonate 5-10 parts, plants essential oil 5-10 parts, tristearin Sour sodium 10-15 parts, acrylamide 3-5 parts, calgon 3-5 parts, nano silicon 5-10 parts, ethanol 10-20 parts, shell gather Sugared 5-10 parts, metallic fiber powder 5-10 parts, nanometer ferrite powder 5-10 parts, deionized water 30-50 parts.
- 2. radiation proof softener according to claim 1, it is characterised in that：The ethanol is absolute ethyl alcohol, and purity is point Analyse pure.
- 3. radiation proof softener according to claim 1, it is characterised in that：The plants essential oil is Lavender, thin Lotus essential oil, lemon, jasmine essential oil, Rosa Damascana, yulan essential oil, cape jasmine flower essential oil, one kind in narcissus flower essential oil or Person more than one.
- 4. radiation proof softener according to claim 1, it is characterised in that：The metallic fiber powder, nanometer ferrite Powder, the particle diameter of nano silicon are 50-200nm.
- 5. radiation proof softener according to claim 1, it is characterised in that：The metallic fiber powder be silver plated fiber, Plate the one or more in aluminum fiber, Cu coated fibre, nickel plating fiber.
- 6. radiation proof softener according to claim 1, it is characterised in that：According to parts by weight, including following components：Eight 10 parts of methyl cyclotetrasiloxane, 5 parts of polyether-modified nanometer silane, 5 parts of sodium acid carbonate, 5 parts of plants essential oil, 10 parts of odium stearate, 3 parts of acrylamide, 3 parts of calgon, 5 parts of nano silicon, 10 parts of ethanol, 5 parts of chitosan, 5 parts of metallic fiber powder, 5 parts of nanometer ferrite powder, 30 parts of deionized water.
- 7. radiation proof softener according to claim 1, it is characterised in that：According to parts by weight, including following components：Eight 15 parts of methyl cyclotetrasiloxane, 6 parts of polyether-modified nanometer silane, 8 parts of sodium acid carbonate, 8 parts of plants essential oil, 13 parts of odium stearate, 4 parts of acrylamide, 4 parts of calgon, 8 parts of nano silicon, 15 parts of ethanol, 8 parts of chitosan, 8 parts of metallic fiber powder, 8 parts of nanometer ferrite powder, 40 parts of deionized water.
- 8. radiation proof softener according to claim 1, it is characterised in that：According to parts by weight, including following components：Eight 20 parts of methyl cyclotetrasiloxane, 7 parts of polyether-modified nanometer silane, 10 parts of sodium acid carbonate, 10 parts of plants essential oil, odium stearate 15 Part, 5 parts of acrylamide, 5 parts of calgon, 10 parts of nano silicon, 20 parts of ethanol, 10 parts of chitosan, metallic fiber powder 10 parts of end, 10 parts of nanometer ferrite powder, 50 parts of deionized water.
- A kind of 9. preparation method of any described radiation proof softener in 1-8 using the claims, it is characterised in that：Tool Body step is as follows：Step 1, octamethylcy-clotetrasiloxane 10-20 parts, deionized water 30-50 parts are added inside four-hole boiling flask, in oil bath pan 80-100 DEG C of heating, nitrogen protection, the speed for being passed through nitrogen is 1-2L/min, keeps charging flatly, and insertion flatly is equipped with 5-7 parts The separatory funnel of polyether-modified nanometer silane, rate of addition 2-3mL/min, agitator, mixing speed 1000- is inserted flatly 2000 revs/min, reaction time 3-4h；Step 2, first by calgon 3-5 parts, metallic fiber powder 5-10 parts, nanometer ferrite powder 5-10 parts, nanometer two Silica 5-10 parts, ethanol 10-20 parts, with ultrasonic disperse 10-20 minutes, ultrasonic power 1000-2000W, obtain uniformly molten Liquid；Step 3, the homogeneous solution of step 2 is added in the solution of step 1,500-1000 revs/min, stirs 20-30 minutes；Step 4, temperature is reduced to 60-70 DEG C, addition odium stearate 10-15 parts, acrylamide 3-5 parts, 500-1000 revs/min Clock, stir 20-30 minutes；Step 5,40-50 DEG C is cooled to, adds chitosan 5-10 parts, sodium acid carbonate 5-10 parts, plants essential oil 5-10 parts, 500- 1000 revs/min, stir 1-2 hours；Step 6,20-30 DEG C is cooled to, closes down stirring, the liquid radiation proof softener prepared；Step 7, stand and be cooled in four-hole boiling flask liquid radiation proof softener and be less than 20 DEG C, blowing encapsulation, finished product.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112663334A (en) * | 2020-12-23 | 2021-04-16 | 杭州宏达装饰布织造有限公司 | Mosquito-repelling sleep-aiding fabric and processing method thereof |
| CN113832739A (en) * | 2021-10-26 | 2021-12-24 | 高梵(浙江)信息技术有限公司 | Radiation-proof metal fiber fabric and preparation method thereof |
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| CN103266484A (en) * | 2013-05-16 | 2013-08-28 | 湖州厉华妤婕联合纺织有限公司 | Fabric softening agent |
| CN105568671A (en) * | 2016-02-16 | 2016-05-11 | 渤扬复合面料科技(昆山)有限公司 | Processing method for quick-dried antibacterial dacron textile |
| CN106367958A (en) * | 2016-10-13 | 2017-02-01 | 无锡市华诚印染剂厂 | Anti-fading fabric softening agent |
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| CN103266484A (en) * | 2013-05-16 | 2013-08-28 | 湖州厉华妤婕联合纺织有限公司 | Fabric softening agent |
| CN105568671A (en) * | 2016-02-16 | 2016-05-11 | 渤扬复合面料科技(昆山)有限公司 | Processing method for quick-dried antibacterial dacron textile |
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| CN112663334A (en) * | 2020-12-23 | 2021-04-16 | 杭州宏达装饰布织造有限公司 | Mosquito-repelling sleep-aiding fabric and processing method thereof |
| CN113832739A (en) * | 2021-10-26 | 2021-12-24 | 高梵(浙江)信息技术有限公司 | Radiation-proof metal fiber fabric and preparation method thereof |
| CN113832739B (en) * | 2021-10-26 | 2024-04-30 | 高梵(浙江)信息技术有限公司 | Radiation-proof metal fiber fabric and preparation method thereof |
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