CN104631112A - Multifunctional modified moisturizing finishing agent for wig - Google Patents
Multifunctional modified moisturizing finishing agent for wig Download PDFInfo
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- CN104631112A CN104631112A CN201310543717.6A CN201310543717A CN104631112A CN 104631112 A CN104631112 A CN 104631112A CN 201310543717 A CN201310543717 A CN 201310543717A CN 104631112 A CN104631112 A CN 104631112A
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Abstract
The invention discloses a multifunctional modified moisturizing finishing agent for wigs. The finishing agent is characterized by comprising the following components by weight: 15-25 parts of alkyl quaternary ammonium salt cationic surfactant, 5-10 parts of fatty alcohol polyoxyethylene ether, 5-10 parts of polyether modified polysiloxane containing epoxypropane and oxirane block, 5-10 parts of an efficient penetrant, 5-8 parts of trimethylsiloxysilicate, 5-8 parts of trimethyl alkyl polydimethylsiloxane amine, 3-5 parts of polyvinylpyrrolidone, 15-20 parts of glycerol, 10-15 parts of aliphatic alcohol amide, 5-8 parts of amino silicone oil, 3-5 parts of sorbitol and150 parts of deionized water with hardness less than or equal to 0.03 mmol / L. The product obtained by the invention can dilute with water by any proportion, has strong immersion permeability, good adsorption film-forming and moisturizing function, can endow the curved hair fiber with excellent sensory characteristics such as softness, smoothness, brightness, high elasticity, fouling resistance and electrostatic resistance, and has the advantages of good feel, lasting shaping curvature effect, good elasticity and no toxicity or stimulation.
Description
Technical field
The invention belongs to hair products finishing agent manufacture technology field, be specifically related to a kind of multifunctional modification wig wet keeping finishing agent.
Background technology
Hair product industry, before fibre completes, mostly will carry out impregnation process through various auxiliary agent.Through the fiber of auxiliary agent impregnation process, one deck auxiliary agent film can be formed to give product multiple excellent performance at fiber surface, thus improve quality scale and the added value of product.Middle nineteen nineties has grown up the organic silicone finishing agent taking aminoethyl and aminopropyl silicone oil as key component, but the shortcoming such as the fibre after arranging has static electrification, inhales dust, hand feel performance is single.
In hair products production process before extracorporeal hair goods complete, mostly to carry out impregnation process through various auxiliary agent.Carry out the fiber of impregnation process through auxiliary agent, one deck auxiliary agent film can be formed to give product various excellent performance at fiber surface, thus improve quality scale and the added value of product.In recent years, along with socioeconomic development, people are day by day strong to the personalization of artificial hair product, requirement that is superior, various shapes, and high organoleptic wig fibre is gained great popularity.Common organic silicone finishing agent can not meet this demand, and the hair fiber after arrangement exists poor flexibility, easily hair and falls apart, shapes lastingly, the shortcomings such as hand feel performance is single.
Summary of the invention
Object of the present invention will provide a kind of multifunctional modification wig wet keeping finishing agent exactly, have after making straight fiber impregnation process that antistatic behaviour is strong, bright soft, smooth, high-elastic and nontoxic, non-stimulated, manufacture craft simple, cost is low.
The invention provides a kind of multifunctional modification wig wet keeping finishing agent, it is characterized in that, feed components is composed as follows according to weight portion: quaternary ammonium alkyl cationic surfactants 15-25 part, fatty alcohol-polyoxyethylene ether 5-10 part, containing Siloxane-Oxyalkylene Copolymers 5-10 part of expoxy propane ethylene oxide block, high-efficient penetrant 5-10 part, trimethylsiloxysilicates 5-8 part, trimethyl alkyl dimethicone amine 5-8 part, polyvinylpyrrolidone 3-5 part, glycerol 15-20 part, fatty alkanol amide 10-15 part, amido silicon oil 5-8 part, sorbierite 3-5 part, hardness≤0.03 milli rub/liter deionized water 150 parts.
A preparation method for multifunctional modification wig wet keeping finishing agent, is characterized in that, comprise the following steps:
(1) solution A processed: at 80-90 DEG C of temperature, the deionized water of quaternary ammonium alkyl cationic surfactants, fatty alcohol-polyoxyethylene ether, Siloxane-Oxyalkylene Copolymers containing expoxy propane ethylene oxide block, high-efficient penetrant and 80 parts is stirred and evenly mixed in mulser, obtains the liquid of clear homogeneous;
(2) solution B processed: control temperature is 55-60 DEG C, in 30 parts of deionized waters, with salt acid for adjusting pH=4-5, add trimethylsiloxysilicates, trimethyl alkyl dimethicone amine, polyvinylpyrrolidone and, constant temperature stirs 1-1.5 h to mixing, be cooled to room temperature, leave standstill 20-30min;
(3) solution C processed: slowly add glycerol in 40 parts of deionized waters, stirs 15-20 min, after leaving standstill 20 min, adds fatty alkanol amide, amido silicon oil, stir 30-40 min, after leaving standstill 25 min, add sorbierite, when being warming up to 50 DEG C, constant temperature stirs 30-35 min, is cooled to room temperature;
(4) wet keeping finishing agent processed: with the pH=4-5 of hydrochloric acid conditioning solution C, add solution A, solution B successively while stirring, stir, raised temperature 50 DEG C, isothermal reaction 40-50min makes it mix completely, can obtain product after cooling.
The mixture that above-mentioned quaternary ammonium alkyl cationic surfactants is made up of according to weight ratio 2:1 octadecyldimethyl ammonium chloride and hexadecyltrimethylammonium chloride.
Above-mentioned high-efficient penetrant be Octylphenol polyoxyethylene ether, sodium alkyl benzene sulfonate one or more.
The beneficial effect of the invention:
Multifunctional modification wig wet keeping finishing agent provided by the invention, constant temperature is utilized to stir, raw material components more easily reacts completely, and product is more stable, emulsifying makes the particle diameter of emulsion less, whole emulsion is evenly not stratified, whole synthesis technique is fairly simple, can with water arbitrarily than dilution, flood easy to use, and natural hair and artificial fiber are sent out all have good treatment effect, immersion permeability is strong, there is good absorption film-forming moisture-keeping functions, curly hair fiber softening can be given smooth, light is high-elastic, the excellent organoleptic feature such as antifouling and antistatic, there is good hand touch, sizing curvature persistent, good springiness and nontoxic, non-stimulated advantage, production equipment is simple, cost is low.
Detailed description of the invention
Embodiment 1
A kind of multifunctional modification wig wet keeping finishing agent, it is characterized in that, feed components is composed as follows according to weight portion: the quaternary ammonium alkyl cationic surfactants 25 parts be made up of according to weight ratio 2:1 octadecyldimethyl ammonium chloride and hexadecyltrimethylammonium chloride, fatty alcohol-polyoxyethylene ether 10 parts, containing the Siloxane-Oxyalkylene Copolymers 5 parts of expoxy propane ethylene oxide block, high-efficient penetrant 5 parts, trimethylsiloxysilicates 8 parts, trimethyl alkyl dimethicone amine 5 parts, polyvinylpyrrolidone 5 parts, glycerol 15 parts, fatty alkanol amide 10 parts, amido silicon oil 8 parts, sorbierite 5 parts, hardness≤0.03 milli rub/liter deionized water 150 parts.
A preparation method for multifunctional modification wig wet keeping finishing agent, is characterized in that, comprise the following steps:
(1) solution A processed: at 90 DEG C of temperature, the deionized water of quaternary ammonium alkyl cationic surfactants, fatty alcohol-polyoxyethylene ether, Siloxane-Oxyalkylene Copolymers containing expoxy propane ethylene oxide block, Octylphenol polyoxyethylene ether, sodium alkyl benzene sulfonate high-efficient penetrant and 80 parts is stirred and evenly mixed in mulser, obtains the liquid of clear homogeneous;
(2) solution B processed: control temperature is 60 DEG C, in 30 parts of deionized waters, with salt acid for adjusting pH=5, add trimethylsiloxysilicates, trimethyl alkyl dimethicone amine, polyvinylpyrrolidone and, constant temperature stirs 1.5 h to mixing, and is cooled to room temperature, leaves standstill 30min;
(3) solution C processed: slowly add glycerol in 40 parts of deionized waters, stirs 20 min, after leaving standstill 20 min, adds fatty alkanol amide, amido silicon oil, stir 40 min, after leaving standstill 25 min, add sorbierite, when being warming up to 50 DEG C, constant temperature stirs 35 min, is cooled to room temperature;
(4) wet keeping finishing agent processed: with the pH=5 of hydrochloric acid conditioning solution C, add solution A, solution B successively while stirring, stir, raised temperature 50 DEG C, isothermal reaction 50min makes it mix completely, can obtain product after cooling.
The maceration extract that above-mentioned obtained multifunctional modification wig wet keeping finishing agent is formed according to consumption 10%, bath raio 1: 10, temperature 28 DEG C, fully immerses pending fiber in maceration extract and floods 15 min, then take out fiber, centrifugal dehydration post-drying.
Embodiment 2
A kind of multifunctional modification wig wet keeping finishing agent, it is characterized in that, feed components is composed as follows according to weight portion: the quaternary ammonium alkyl cationic surfactants 15 parts be made up of according to weight ratio 2:1 octadecyldimethyl ammonium chloride and hexadecyltrimethylammonium chloride, fatty alcohol-polyoxyethylene ether 5 parts, containing the Siloxane-Oxyalkylene Copolymers 10 parts of expoxy propane ethylene oxide block, high-efficient penetrant 5 parts, trimethylsiloxysilicates 5 parts, trimethyl alkyl dimethicone amine 5 parts, polyvinylpyrrolidone 3 parts, glycerol 15 parts, fatty alkanol amide 10 parts, amido silicon oil 5 parts, sorbierite 3 parts, hardness≤0.03 milli rub/liter deionized water 150 parts.
A preparation method for multifunctional modification wig wet keeping finishing agent, is characterized in that, comprise the following steps:
(1) solution A processed: at 80 DEG C of temperature, the deionized water of quaternary ammonium alkyl cationic surfactants, fatty alcohol-polyoxyethylene ether, Siloxane-Oxyalkylene Copolymers containing expoxy propane ethylene oxide block, Octylphenol polyoxyethylene ether and 80 parts is stirred and evenly mixed in mulser, obtains the liquid of clear homogeneous;
(2) solution B processed: control temperature is 55 DEG C, in 30 parts of deionized waters, with salt acid for adjusting pH=4, add trimethylsiloxysilicates, trimethyl alkyl dimethicone amine, polyvinylpyrrolidone and, constant temperature stirs 1 h to mixing, and is cooled to room temperature, leaves standstill 20 min;
(3) solution C processed: slowly add glycerol in 40 parts of deionized waters, stirs 15 min, after leaving standstill 20 min, adds fatty alkanol amide, amido silicon oil, stir 30 min, after leaving standstill 25 min, add sorbierite, when being warming up to 50 DEG C, constant temperature stirs 30 min, is cooled to room temperature;
(4) wet keeping finishing agent processed: with the pH=4 of hydrochloric acid conditioning solution C, add solution A, solution B successively while stirring, stir, raised temperature 50 DEG C, isothermal reaction 40min makes it mix completely, can obtain product after cooling.
The maceration extract that above-mentioned obtained multifunctional modification wig wet keeping finishing agent is formed according to consumption 10%, bath raio 1: 10, temperature 28 DEG C, fully immerses pending fiber in maceration extract and floods 15 min, then take out fiber, centrifugal dehydration post-drying.
Claims (4)
1. a multifunctional modification wig wet keeping finishing agent, it is characterized in that, feed components is composed as follows according to weight portion: quaternary ammonium alkyl cationic surfactants 15-25 part, fatty alcohol-polyoxyethylene ether 5-10 part, containing Siloxane-Oxyalkylene Copolymers 5-10 part of expoxy propane ethylene oxide block, high-efficient penetrant 5-10 part, trimethylsiloxysilicates 5-8 part, trimethyl alkyl dimethicone amine 5-8 part, polyvinylpyrrolidone 3-5 part, glycerol 15-20 part, fatty alkanol amide 10-15 part, amido silicon oil 5-8 part, sorbierite 3-5 part, hardness≤0.03 milli rub/liter deionized water 150 parts.
2. a preparation method for multifunctional modification wig wet keeping finishing agent, is characterized in that, comprises the following steps:
(1) solution A processed: at 80-90 DEG C of temperature, the deionized water of quaternary ammonium alkyl cationic surfactants, fatty alcohol-polyoxyethylene ether, Siloxane-Oxyalkylene Copolymers containing expoxy propane ethylene oxide block, high-efficient penetrant and 80 parts is stirred and evenly mixed in mulser, obtains the liquid of clear homogeneous;
(2) solution B processed: control temperature is 55-60 DEG C, in 30 parts of deionized waters, with salt acid for adjusting pH=4-5, add trimethylsiloxysilicates, trimethyl alkyl dimethicone amine, polyvinylpyrrolidone and, constant temperature stirs 1-1.5 h to mixing, be cooled to room temperature, leave standstill 20-30min;
(3) solution C processed: slowly add glycerol in 40 parts of deionized waters, stirs 15-20 min, after leaving standstill 20 min, adds fatty alkanol amide, amido silicon oil, stir 30-40 min, after leaving standstill 25 min, add sorbierite, when being warming up to 50 DEG C, constant temperature stirs 30-35 min, is cooled to room temperature;
(4) wet keeping finishing agent processed: with the pH=4-5 of hydrochloric acid conditioning solution C, add solution A, solution B successively while stirring, stir, raised temperature 50 DEG C, isothermal reaction 40-50min makes it mix completely, can obtain product after cooling.
3. according to a kind of multifunctional modification wig wet keeping finishing agent described in claim 1, it is characterized in that, the mixture that described quaternary ammonium alkyl cationic surfactants is made up of according to weight ratio 2:1 octadecyldimethyl ammonium chloride and hexadecyltrimethylammonium chloride.
4., according to a kind of multifunctional modification wig wet keeping finishing agent described in claim 1, it is characterized in that, described high-efficient penetrant be Octylphenol polyoxyethylene ether, sodium alkyl benzene sulfonate one or more.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310543717.6A CN104631112A (en) | 2013-11-06 | 2013-11-06 | Multifunctional modified moisturizing finishing agent for wig |
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| CN201310543717.6A CN104631112A (en) | 2013-11-06 | 2013-11-06 | Multifunctional modified moisturizing finishing agent for wig |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105177998A (en) * | 2015-09-15 | 2015-12-23 | 苏州顺唐化纤有限公司 | Softener for green chemical fiber fabric and preparation method of softener |
| CN108677541A (en) * | 2018-05-31 | 2018-10-19 | 江苏尼美达科技有限公司 | The agent of wool fabric soft and bright and preparation method |
| CN109098018A (en) * | 2018-06-08 | 2018-12-28 | 姜永达 | A kind of dyeing used additives and preparation method thereof |
| CN109393613A (en) * | 2018-10-22 | 2019-03-01 | 安徽罗曼丝发制品有限公司 | A kind of means of defence extending wig service life |
| CN111394527A (en) * | 2020-05-09 | 2020-07-10 | 金湖金凌新材料科技有限公司 | Novel leather assistant and preparation method thereof |
| CN111423848A (en) * | 2020-03-29 | 2020-07-17 | 连云港中意航空材料有限公司 | Novel antistatic liquid compatibility method |
| CN112127164A (en) * | 2020-09-17 | 2020-12-25 | 河南瑞贝卡发制品股份有限公司 | Preparation and impregnation method of post-finishing soft-keeping agent for synthetic fibers |
| CN112210997A (en) * | 2020-09-17 | 2021-01-12 | 河南瑞贝卡发制品股份有限公司 | Preparation and impregnation method of hair fiber pretreatment auxiliary agent |
-
2013
- 2013-11-06 CN CN201310543717.6A patent/CN104631112A/en active Pending
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105177998A (en) * | 2015-09-15 | 2015-12-23 | 苏州顺唐化纤有限公司 | Softener for green chemical fiber fabric and preparation method of softener |
| CN108677541A (en) * | 2018-05-31 | 2018-10-19 | 江苏尼美达科技有限公司 | The agent of wool fabric soft and bright and preparation method |
| CN109098018A (en) * | 2018-06-08 | 2018-12-28 | 姜永达 | A kind of dyeing used additives and preparation method thereof |
| CN109393613A (en) * | 2018-10-22 | 2019-03-01 | 安徽罗曼丝发制品有限公司 | A kind of means of defence extending wig service life |
| CN111423848A (en) * | 2020-03-29 | 2020-07-17 | 连云港中意航空材料有限公司 | Novel antistatic liquid compatibility method |
| CN111394527A (en) * | 2020-05-09 | 2020-07-10 | 金湖金凌新材料科技有限公司 | Novel leather assistant and preparation method thereof |
| CN112127164A (en) * | 2020-09-17 | 2020-12-25 | 河南瑞贝卡发制品股份有限公司 | Preparation and impregnation method of post-finishing soft-keeping agent for synthetic fibers |
| CN112210997A (en) * | 2020-09-17 | 2021-01-12 | 河南瑞贝卡发制品股份有限公司 | Preparation and impregnation method of hair fiber pretreatment auxiliary agent |
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