CN107663771A - A kind of fabric radiation agent and preparation method thereof - Google Patents
A kind of fabric radiation agent and preparation method thereof Download PDFInfo
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- CN107663771A CN107663771A CN201710680174.0A CN201710680174A CN107663771A CN 107663771 A CN107663771 A CN 107663771A CN 201710680174 A CN201710680174 A CN 201710680174A CN 107663771 A CN107663771 A CN 107663771A
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- parts
- fabric
- radiation agent
- metallic fiber
- resin
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- 239000004744 fabric Substances 0.000 title claims abstract description 66
- 230000005855 radiation Effects 0.000 title claims abstract description 51
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 41
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 41
- 229920000914 Metallic fiber Polymers 0.000 claims abstract description 38
- 239000000843 powder Substances 0.000 claims abstract description 28
- 239000006185 dispersion Substances 0.000 claims abstract description 25
- 229920005989 resin Polymers 0.000 claims abstract description 24
- 239000011347 resin Substances 0.000 claims abstract description 24
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims abstract description 23
- 239000002105 nanoparticle Substances 0.000 claims abstract description 23
- 229910000077 silane Inorganic materials 0.000 claims abstract description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 23
- 229920000058 polyacrylate Polymers 0.000 claims abstract description 21
- 239000002202 Polyethylene glycol Substances 0.000 claims abstract description 20
- 229920001223 polyethylene glycol Polymers 0.000 claims abstract description 20
- 239000002994 raw material Substances 0.000 claims abstract description 12
- 238000003756 stirring Methods 0.000 claims description 21
- 239000007788 liquid Substances 0.000 claims description 18
- 239000000718 radiation-protective agent Substances 0.000 claims description 15
- 239000000203 mixture Substances 0.000 claims description 13
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 11
- 239000000835 fiber Substances 0.000 claims description 9
- 238000007664 blowing Methods 0.000 claims description 7
- 238000005538 encapsulation Methods 0.000 claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 7
- 239000012456 homogeneous solution Substances 0.000 claims description 7
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 4
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 4
- 238000007747 plating Methods 0.000 claims description 4
- 239000004593 Epoxy Substances 0.000 claims description 3
- 239000002245 particle Substances 0.000 claims description 3
- 241000219357 Cactaceae Species 0.000 claims description 2
- 235000011305 Capsella bursa pastoris Nutrition 0.000 claims description 2
- 240000008867 Capsella bursa-pastoris Species 0.000 claims description 2
- 239000004952 Polyamide Substances 0.000 claims description 2
- 240000005319 Sedum acre Species 0.000 claims description 2
- 235000014327 Sedum acre Nutrition 0.000 claims description 2
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical group [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims description 2
- 150000001335 aliphatic alkanes Chemical class 0.000 claims description 2
- 229910052782 aluminium Inorganic materials 0.000 claims description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 2
- YYAQTLYICNKRPF-UHFFFAOYSA-N aniline 3,5,5-trimethylcyclohex-2-en-1-one Chemical compound NC1=CC=CC=C1.CC1=CC(=O)CC(C)(C)C1 YYAQTLYICNKRPF-UHFFFAOYSA-N 0.000 claims description 2
- INJVFBCDVXYHGQ-UHFFFAOYSA-N n'-(3-triethoxysilylpropyl)ethane-1,2-diamine Chemical compound CCO[Si](OCC)(OCC)CCCNCCN INJVFBCDVXYHGQ-UHFFFAOYSA-N 0.000 claims description 2
- 229910052759 nickel Inorganic materials 0.000 claims description 2
- 229910052760 oxygen Inorganic materials 0.000 claims description 2
- 239000001301 oxygen Substances 0.000 claims description 2
- 229920002647 polyamide Polymers 0.000 claims description 2
- 229920000647 polyepoxide Polymers 0.000 claims description 2
- 239000004332 silver Substances 0.000 claims description 2
- 229910052709 silver Inorganic materials 0.000 claims description 2
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims 3
- 210000000481 breast Anatomy 0.000 claims 2
- YYNZKBLHWUQRKB-UHFFFAOYSA-N NCCC[Si](OCC(OCC)(OCC)OCC)OCC Chemical compound NCCC[Si](OCC(OCC)(OCC)OCC)OCC YYNZKBLHWUQRKB-UHFFFAOYSA-N 0.000 claims 1
- 239000000839 emulsion Substances 0.000 claims 1
- ARYZCSRUUPFYMY-UHFFFAOYSA-N methoxysilane Chemical compound CO[SiH3] ARYZCSRUUPFYMY-UHFFFAOYSA-N 0.000 claims 1
- 229910052710 silicon Inorganic materials 0.000 claims 1
- 239000010703 silicon Substances 0.000 claims 1
- 239000004408 titanium dioxide Substances 0.000 claims 1
- -1 γ-methacryloxypropyl trimethoxy silicon Alkane Chemical class 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 231100000252 nontoxic Toxicity 0.000 abstract description 2
- 230000003000 nontoxic effect Effects 0.000 abstract description 2
- 238000005516 engineering process Methods 0.000 description 3
- 206010028980 Neoplasm Diseases 0.000 description 2
- 201000011510 cancer Diseases 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- ZHUWIYQJHBMTCY-UHFFFAOYSA-N 3-[ethoxy(2,2,2-triethoxyethoxy)silyl]propan-1-amine Chemical compound NCCC[SiH](OCC(OCC)(OCC)OCC)OCC ZHUWIYQJHBMTCY-UHFFFAOYSA-N 0.000 description 1
- SJECZPVISLOESU-UHFFFAOYSA-N 3-trimethoxysilylpropan-1-amine Chemical group CO[Si](OC)(OC)CCCN SJECZPVISLOESU-UHFFFAOYSA-N 0.000 description 1
- XDLMVUHYZWKMMD-UHFFFAOYSA-N 3-trimethoxysilylpropyl 2-methylprop-2-enoate Chemical compound CO[Si](OC)(OC)CCCOC(=O)C(C)=C XDLMVUHYZWKMMD-UHFFFAOYSA-N 0.000 description 1
- 206010000234 Abortion spontaneous Diseases 0.000 description 1
- 201000004384 Alopecia Diseases 0.000 description 1
- 208000032170 Congenital Abnormalities Diseases 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 206010020751 Hypersensitivity Diseases 0.000 description 1
- 206010021137 Hypovolaemia Diseases 0.000 description 1
- 208000030961 allergic reaction Diseases 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000036471 bradycardia Effects 0.000 description 1
- 208000006218 bradycardia Diseases 0.000 description 1
- 210000004556 brain Anatomy 0.000 description 1
- 210000000748 cardiovascular system Anatomy 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000001186 cumulative effect Effects 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000003822 epoxy resin Substances 0.000 description 1
- CWAFVXWRGIEBPL-UHFFFAOYSA-N ethoxysilane Chemical compound CCO[SiH3] CWAFVXWRGIEBPL-UHFFFAOYSA-N 0.000 description 1
- 208000024963 hair loss Diseases 0.000 description 1
- 230000003676 hair loss Effects 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000036737 immune function Effects 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 208000032839 leukemia Diseases 0.000 description 1
- 201000002364 leukopenia Diseases 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000005543 nano-size silicon particle Substances 0.000 description 1
- 239000003176 neuroleptic agent Substances 0.000 description 1
- 230000000701 neuroleptic effect Effects 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 210000004994 reproductive system Anatomy 0.000 description 1
- 208000000995 spontaneous abortion Diseases 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/45—Oxides or hydroxides of elements of Groups 3 or 13 of the Periodic Table; Aluminates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/46—Oxides or hydroxides of elements of Groups 4 or 14 of the Periodic Table; Titanates; Zirconates; Stannates; Plumbates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/49—Oxides or hydroxides of elements of Groups 8, 9,10 or 18 of the Periodic Table; Ferrates; Cobaltates; Nickelates; Ruthenates; Osmates; Rhodates; Iridates; Palladates; Platinates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
- D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/83—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with metals; with metal-generating compounds, e.g. metal carbonyls; Reduction of metal compounds on textiles
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/55—Epoxy resins
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/59—Polyamides; Polyimides
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/25—Resistance to light or sun, i.e. protection of the textile itself as well as UV shielding materials or treatment compositions therefor; Anti-yellowing treatments
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a kind of preparation method of fabric radiation agent, the fabric radiation agent is made up of the raw material of following parts by weight:25 30 parts of resin, 5 10 parts of nano particle, 35 parts of silane coupler, 10 20 parts of metallic fiber powder, 35 parts of polyacrylate dispersion, 10 20 parts of water, 35 parts of polyethylene glycol, 50 100 parts of ethanol.After the fabric radiation agent application fabric of the present invention, the radiation proof efficiency of fabric reaches more than 90%.The fabric radiation agent manufacturing process of the present invention is simple to operation, and low in raw material price is easily obtained, and nontoxic, and human body is not stimulated, and volatility is low, and the fabric after arrangement its toughness, intensity, feel are substantially unaffected.
Description
Technical field
The invention belongs to technical field of textile auxiliary agent, specifically relates to a kind of fabric radiation agent.
Background technology
With the further development of electrical technology, radiate and be seen everywhere around us.The hand being either seen everywhere
Mechanical, electrical brain, printer, or household electrical appliance micro-wave oven, electric blanket, hair-dryer, can all there is certain radiation.Although household electrical appliance
Harm of the radiation for people without very big, but when the electric radiation of human body local environment exceedes certain intensity or produces certain
Cumulative effect when, can have the weaker old man of certain infringement, especially resistance, child, pregnant woman etc. to health.
The harm of radiation is a lot, such as:Children's intelligence can be caused incomplete;It is most likely the reason for causing children's cases with leukemia
One of;Cancer can be induced and accelerate the cancer cell multiplication of human body;The reproductive system of people is influenceed, is mainly shown as man's sperm matter
Amount reduces, and spontaneous abortion and fetal anomaly etc. occur for pregnant woman;The cardiovascular system of people is influenceed, palpitaition is shown as, hair loss, loses
Sleep, bradycardia, heartbeat oligemia, Neuroleptic Leukocytopenia, immunologic function decline etc..
Radiation-proof fabric in the market, usually with blending metallic fiber, conductive fiber, cost is high, not water-fastness,
Some people has allergic reaction, therefore, finds a kind of durable, comfortable fabric radiation agent and is very important.
The content of the invention
It is an object of the invention to provide a kind of fabric radiation agent and preparation method, to solve to carry in above-mentioned background technology
The problem of going out.
To achieve the above object, the present invention provides following technical scheme:
A kind of fabric radiation agent, the fabric radiation agent include the raw material of following parts by weight:Resin 25-30 parts,
Nano particle 5-10 parts, silane coupler 3-5 parts, metallic fiber powder 10-20 parts, polyacrylate dispersion 3-5 parts, plant juice
Liquid 10-20 parts, polyethylene glycol 3-5 parts, ethanol 50-100 parts.
Preferably, described resin is in organic siliconresin, epoxy resin, polyamide, polyacrylics
One or more than one kinds of mixtures.
Preferably, described nano particle is nano silicon, nano titanium oxide, nano ferriferrous oxide, nanometer
One or more than one kinds of mixtures in aluminum oxide.
Preferably, described silane coupler is 3- aminopropyl trimethoxysilanes, γ-(2,3- the third oxygen of epoxy) propyl group three
Ethoxysilane, γ-methacryloxypropyl trimethoxy silane, N- (β-aminoethyl)-gamma-aminopropyl-triethoxy silicon
Any one in alkane, aniline isophorone and γ-aminopropyltriethoxy diethoxy silane or more than one mixture.
Preferably, described metallic fiber be silver plated fiber, plating aluminum fiber, Cu coated fibre, one kind in nickel plating fiber or
More than one mixture of person.
Preferably, described water is Gem flower-shaped three-dimensional jig-saw puzzle juice, red-spotted stonecrop juice, cactus juice, rape juice, shepherd's purse juice
One or more than one kinds of mixtures in liquid.
Preferably, the fabric radiation agent is made up of the raw material of following parts by weight:25 parts of resin, 5 parts of nano particle,
3 parts of silane coupler, 10 parts of metallic fiber powder, 3 parts of polyacrylate dispersion, 10 parts of water, 3 parts of polyethylene glycol, second
50 parts of alcohol.
Preferably, the fabric radiation agent is made up of the raw material of following parts by weight:28 parts of resin, 8 parts of nano particle,
4 parts of silane coupler, 15 parts of metallic fiber powder, 4 parts of polyacrylate dispersion, 15 parts of water, 4 parts of polyethylene glycol, second
75 parts of alcohol.
Preferably, the fabric radiation agent is made up of the raw material of following parts by weight:30 parts of resin, nano particle 10
Part, 5 parts of silane coupler, 20 parts of metallic fiber powder, 5 parts of polyacrylate dispersion, 20 parts of water, 5 parts of polyethylene glycol,
100 parts of ethanol.
Preferably, a kind of preparation method of fabric radiation agent, it is characterised in that:Comprise the following steps that:
Step 1, resin 25-30 parts, silane coupler 3-5 parts, nano particle 5-10 parts, 1000- are added in a kettle
3000 revs/min, stir 30-40 minutes;
Step 2, first the metallic fiber of 10-20 parts is crushed with pulverizer, then ground with grinder so that metallic fiber powder
The particle diameter at end is in 1-100nm;
Step 3, the metallic fiber powder of step 2 is added in ethanol 50-100 parts, ultrasonic disperse, rate of dispersion 2000-
3000 revs/min, jitter time 20-30 minutes;
Step 4, the homogeneous solution of step 3 is poured into the solution of step 1,1000-3000 revs/min, 20-30 points of stirring
Clock;
Step 5, heating temperature adds polyacrylate dispersion 3-5 parts, water 10-20 parts, poly- second two to 70-80 DEG C
Alcohol 3-5 parts, 500-1000 revs/min, stir 20-30 minutes;
Step 6, room temperature is cooled to, closes down stirring, the liquid fabric antiradiation agent prepared;
Step 7, stand and be cooled in stirred tank liquid fabric antiradiation agent and be less than 20 DEG C, blowing encapsulation, finished product.
Compared with prior art, the beneficial effects of the invention are as follows:
1st, after fabric radiation agent application fabric of the invention, the radiation proof efficiency of fabric reaches more than 90%.
2nd, fabric radiation agent manufacturing process of the invention is simple to operation, and low in raw material price easily obtains, and nontoxic nothing
Evil, is not stimulated human body, and volatility is low, and the fabric after arrangement its toughness, intensity, feel are substantially unaffected.
3rd, mutual compatibility, synergy between various raw materials used in fabric radiation agent of the invention, collectively constitute performance
Excellent product.
4th, the addition of water, the shielding property of fabric is improved.
5th, technique is simplified, safe operation is simple, is easy to industrialized production.
6th, fabric radiation coating construction is simple of the invention, can by impregnating, spraying, roller coat etc. applied, it is raw
Efficiency is produced to improve.
7th, use of the invention can receive good economic benefit.
Example is embodied
The invention discloses a kind of fabric radiation agent, according to important number, it is prepared from the following components:Resin 25-
30 parts, nano particle 5-10 parts, silane coupler 3-5 parts, metallic fiber powder 10-20 parts, polyacrylate dispersion 3-5 parts,
Water 10-20 parts, polyethylene glycol 3-5 parts, ethanol 50-100 parts.
Present invention also offers a kind of preparation method of fabric radiation agent, comprise the following steps that:
(1) resin 25-30 parts, silane coupler 3-5 parts, nano particle 5-10 parts, 1000-3000 are added in a kettle
Rev/min, stir 30-40 minutes;
(2) first the metallic fiber of 10-20 parts is crushed with pulverizer, then ground with grinder so that metallic fiber powder
Particle diameter in 1-100nm;
(3) the metallic fiber powder of step (2) is added in ethanol 50-100 parts, ultrasonic disperse, rate of dispersion 2000-
3000 revs/min, jitter time 20-30 minutes;
(4) homogeneous solution of step (3) is poured into the solution of step (1), 1000-3000 revs/min, stirs 20-30
Minute;
(5) heating temperature adds polyacrylate dispersion 3-5 parts, water 10-20 parts, polyethylene glycol 3- to 70-80 DEG C
5 parts, 500-1000 revs/min, stir 20-30 minutes;
(6) room temperature is cooled to, closes down stirring, the liquid fabric antiradiation agent prepared;
(7) stand and be cooled in stirred tank liquid fabric antiradiation agent and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 1
The invention discloses a kind of fabric radiation agent, according to important number, it is prepared from the following components:Resin 25
Part, 5 parts of nano particle, 3 parts of silane coupler, 10 parts of metallic fiber powder, 3 parts of polyacrylate dispersion, 10 parts of water,
3 parts of polyethylene glycol, 50 parts of ethanol.
Present invention also offers a kind of preparation method of fabric radiation agent, comprise the following steps that:
(1) 25 parts of resin, 3 parts of silane coupler, 5 parts of nano particle are added in a kettle, 1000 revs/min, are stirred
30 minutes;
(2) first 10 parts of metallic fiber is crushed with pulverizer, then ground with grinder so that the grain of metallic fiber powder
Footpath is in 1-100nm;
(3) the metallic fiber powder of step (2) is added in 50 parts of ethanol, ultrasonic disperse, 2000 revs/min of rate of dispersion
Clock, jitter time 20 minutes;
(4) homogeneous solution of step (3) is poured into the solution of step (1), 1000 revs/min, stirred 20 minutes;
(5) heating temperature is to 70 DEG C, 3 parts of polyacrylate dispersion of addition, 10 parts of water, 3 parts of polyethylene glycol, 500 turns/
Minute, stir 20 minutes;
(6) room temperature is cooled to, closes down stirring, the liquid fabric antiradiation agent prepared;
(7) stand and be cooled in stirred tank liquid fabric antiradiation agent and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 2
The invention discloses a kind of fabric radiation agent, according to important number, it is prepared from the following components:Resin 28
Part, 8 parts of nano particle, 4 parts of silane coupler, 15 parts of metallic fiber powder, 4 parts of polyacrylate dispersion, 15 parts of water,
4 parts of polyethylene glycol, 75 parts of ethanol.
Present invention also offers a kind of preparation method of fabric radiation agent, comprise the following steps that:
(1) 28 parts of resin, 4 parts of silane coupler, 8 parts of nano particle are added in a kettle, 2000 revs/min, are stirred
35 minutes;
(2) first 15 parts of metallic fiber is crushed with pulverizer, then ground with grinder so that the grain of metallic fiber powder
Footpath is in 1-100nm;
(3) the metallic fiber powder of step (2) is added in 75 parts of ethanol, ultrasonic disperse, 2500 revs/min of rate of dispersion
Clock, jitter time 25 minutes;
(4) homogeneous solution of step (3) is poured into the solution of step (1), 2000 revs/min, stirred 25 minutes;
(5) heating temperature is to 75 DEG C, 4 parts of polyacrylate dispersion of addition, 15 parts of water, 4 parts of polyethylene glycol, 750 turns/
Minute, stir 25 minutes;
(6) room temperature is cooled to, closes down stirring, the liquid fabric antiradiation agent prepared;
(7) stand and be cooled in stirred tank liquid fabric antiradiation agent and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 3
The invention discloses a kind of fabric radiation agent, according to important number, it is prepared from the following components:Resin 30
Part, 10 parts of nano particle, 5 parts of silane coupler, 20 parts of metallic fiber powder, 5 parts of polyacrylate dispersion, water 20
Part, 5 parts of polyethylene glycol, 100 parts of ethanol.
Present invention also offers a kind of preparation method of fabric radiation agent, comprise the following steps that:
(1) 30 parts of resin, 5 parts of silane coupler, 10 parts of nano particle are added in a kettle, 3000 revs/min, are stirred
40 minutes;
(2) first 20 parts of metallic fiber is crushed with pulverizer, then ground with grinder so that the grain of metallic fiber powder
Footpath is in 1-100nm;
(3) the metallic fiber powder of step (2) is added in 100 parts of ethanol, ultrasonic disperse, 3000 revs/min of rate of dispersion
Clock, jitter time 30 minutes;
(4) homogeneous solution of step (3) is poured into the solution of step (1), 3000 revs/min, stirred 30 minutes;
(5) heating temperature is to 80 DEG C, 5 parts of polyacrylate dispersion of addition, 20 parts of water, 5 parts of polyethylene glycol, and 1000
Rev/min, stir 30 minutes;
(6) room temperature is cooled to, closes down stirring, the liquid fabric antiradiation agent prepared;
(7) stand and be cooled in stirred tank liquid fabric antiradiation agent and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 4
The invention discloses a kind of fabric radiation agent, according to important number, it is prepared from the following components:Resin 25
Part, 10 parts of nano particle, 4 parts of silane coupler, 15 parts of metallic fiber powder, 3 parts of polyacrylate dispersion, water 20
Part, 3 parts of polyethylene glycol, 80 parts of ethanol.
Present invention also offers a kind of preparation method of fabric radiation agent, comprise the following steps that:
(1) 25 parts of resin, 4 parts of silane coupler, 10 parts of nano particle are added in a kettle, 3000 revs/min, are stirred
40 minutes;
(2) first 15 parts of metallic fiber is crushed with pulverizer, then ground with grinder so that the grain of metallic fiber powder
Footpath is in 1-100nm;
(3) the metallic fiber powder of step (2) is added in 80 parts of ethanol, ultrasonic disperse, 2000 revs/min of rate of dispersion
Clock, jitter time 30 minutes;
(4) homogeneous solution of step (3) is poured into the solution of step (1), 3000 revs/min, stirs 20-30 minutes;
(5) heating temperature is to 80 DEG C, 3 parts of polyacrylate dispersion of addition, 20 parts of water, 3 parts of polyethylene glycol, and 1000
Rev/min, stir 30 minutes;
(6) room temperature is cooled to, closes down stirring, the liquid fabric antiradiation agent prepared;
(7) stand and be cooled in stirred tank liquid fabric antiradiation agent and be less than 20 DEG C, blowing encapsulation, finished product.
Test case
4 pieces of identical pure cotton cloths are put into the antiradiation agent solution of embodiment 1,2,3,4, roll, dry by two leachings two,
Bake, wash, drying, 4 pieces of cloth with shielding property can be obtained.The result for testing radiation proof efficiency is as follows:
Embodiment | Radiation proof efficiency (%) |
1 | 90 |
2 | 95 |
3 | 99 |
4 | 98 |
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of changes, modification can be carried out to these embodiments, replace without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (10)
- A kind of 1. fabric radiation agent, it is characterised in that:The fabric radiation agent includes the raw material of following parts by weight:Resin 25-30 parts, nano particle 5-10 parts, silane coupler 3-5 parts, metallic fiber powder 10-20 parts, polyacrylate dispersion 3-5 Part, water 10-20 parts, polyethylene glycol 3-5 parts, ethanol 50-100 parts.
- 2. fabric radiation agent according to claim 1, it is characterised in that:Described resin is organic siliconresin, epoxy One or more than one kinds of mixtures in resin, polyamide, polyacrylics.
- 3. fabric radiation agent according to claim 1, it is characterised in that:Described nano particle is nanometer titanium dioxide One or more than one kinds of mixtures in silicon, nano titanium oxide, nano ferriferrous oxide, nano aluminium oxide.
- 4. fabric radiation agent according to claim 1, it is characterised in that:Described silane coupler is 3- aminopropyls three Methoxy silane, γ-(oxygen of 2,3- epoxies third) propyl-triethoxysilicane, γ-methacryloxypropyl trimethoxy silicon Alkane, N- (β-aminoethyl)-gamma-aminopropyl-triethoxy-silane, aniline isophorone and γ-aminopropyltriethoxy diethoxy silicon Any one in alkane or more than one mixture.
- 5. fabric radiation agent according to claim 1, it is characterised in that:Described metallic fiber is silver plated fiber, plating One or more than one kinds of mixtures in aluminum fiber, Cu coated fibre, nickel plating fiber.
- 6. fabric radiation agent according to claim 1, it is characterised in that:Described water be Gem flower-shaped three-dimensional jig-saw puzzle juice, One or more than one kinds of mixtures in red-spotted stonecrop juice, cactus juice, rape juice, shepherd's purse juice.
- 7. fabric radiation agent according to claim 1, it is characterised in that:The fabric radiation agent is by following parts by weight Several raw material compositions:25 parts of resin, 5 parts of nano particle, 3 parts of silane coupler, 10 parts of metallic fiber powder, polyacrylate breast 3 parts of liquid, 10 parts of water, 3 parts of polyethylene glycol, 50 parts of ethanol.
- 8. fabric radiation agent according to claim 1, it is characterised in that:The fabric radiation agent is by following parts by weight Several raw material compositions:28 parts of resin, 8 parts of nano particle, 4 parts of silane coupler, 15 parts of metallic fiber powder, polyacrylate breast 4 parts of liquid, 15 parts of water, 4 parts of polyethylene glycol, 75 parts of ethanol.
- 9. fabric radiation agent according to claim 1, it is characterised in that:The fabric radiation agent is by following parts by weight Several raw material compositions:30 parts of resin, 10 parts of nano particle, 5 parts of silane coupler, 20 parts of metallic fiber powder, polyacrylate 5 parts of emulsion, 20 parts of water, 5 parts of polyethylene glycol, 100 parts of ethanol.
- 10. a kind of preparation method of any described fabric radiation agent, its feature exist in a kind of 1-9 using the claims In:Comprise the following steps that:Step 1, resin 25-30 parts, silane coupler 3-5 parts, nano particle 5-10 parts, 1000-3000 are added in a kettle Rev/min, stir 30-40 minutes;Step 2, first the metallic fiber of 10-20 parts is crushed with pulverizer, then ground with grinder so that metallic fiber powder Particle diameter is in 1-100nm;Step 3, the metallic fiber powder of step 2 is added in ethanol 50-100 parts, ultrasonic disperse, rate of dispersion 2000-3000 Rev/min, jitter time 20-30 minutes;Step 4, the homogeneous solution of step 3 is poured into the solution of step 1,1000-3000 revs/min, stirs 20-30 minutes;Step 5, heating temperature adds polyacrylate dispersion 3-5 parts, water 10-20 parts, polyethylene glycol 3-5 to 70-80 DEG C Part, 500-1000 revs/min, stir 20-30 minutes;Step 6, room temperature is cooled to, closes down stirring, the liquid fabric antiradiation agent prepared;Step 7, stand and be cooled in stirred tank liquid fabric antiradiation agent and be less than 20 DEG C, blowing encapsulation, finished product.
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