CN108285658A - A kind of preparation method of antiradiation coating - Google Patents
A kind of preparation method of antiradiation coating Download PDFInfo
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- CN108285658A CN108285658A CN201710680175.5A CN201710680175A CN108285658A CN 108285658 A CN108285658 A CN 108285658A CN 201710680175 A CN201710680175 A CN 201710680175A CN 108285658 A CN108285658 A CN 108285658A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D1/00—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
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- General Preparation And Processing Of Foods (AREA)
Abstract
The invention discloses a kind of preparation method of antiradiation coating, the antiradiation coating is made of the raw material of following parts by weight：15 25 parts of calcium carbonate, 24 parts of soybean lecithin, 4 10 parts of diatomite, 10 15 parts of nano particle, 10 20 parts of water, 20 30 parts of barium sulfate, 28 parts of silica flour, 37 parts of polyethylene glycol, 50 100 parts of deionized water.The antiradiation coating radiation protection efficiency of the present invention reaches 99% or more.The antiradiation coating manufacturing process of the present invention is simple to operation, and low in raw material price easily obtains, and nontoxic, does not stimulate human body, and volatility is low, and the various performances of the matrix after arrangement are substantially unaffected.
Description
Technical field
The invention belongs to auxiliary agent technical fields, specifically relate to a kind of antiradiation coating.
Background technology
In the age that this science and technology is with rapid changepl. never-ending changes and improvements, just around us, we are inevasible to be affected radiation source.Spoke
There are many harm penetrated, such as：Children's intelligence can be caused incomplete；It is most likely one of the reason of causing children's cases with leukemia；It can
It induces cancer and accelerates the cancer cell multiplication of human body；The reproductive system for influencing people is mainly shown as the reduction of man's sperm quality, pregnant
Spontaneous abortion and fetal anomaly etc. occur for woman；The cardiovascular system for influencing people shows as palpitaition, hair loss, insomnia, mistake aroused in interest
It is slow, heartbeat oligemia, Neuroleptic Leukocytopenia, immune function decline etc..
Radiation-proof fabric currently on the market, it is of high cost usually with blended metallic fiber, conductive fiber, it is not water-fastness,
Some people has allergic reaction, and therefore, a kind of blanket antiradiation coating of searching is very important.
Invention content
The purpose of the present invention is to provide a kind of antiradiation coating and preparation methods, to solve to propose in above-mentioned background technology
The problem of.
To achieve the above object, the present invention provides the following technical solutions：
A kind of antiradiation coating, the antiradiation coating include the raw material of following parts by weight：It is 15-25 parts of calcium carbonate, big
2-4 parts of Fabaceous Lecithin, 4-10 parts of diatomite, 10-15 parts of nano particle, 10-20 parts of water, 20-30 parts of barium sulfate, silica flour
2-8 parts, 3-7 parts of polyethylene glycol, 50-100 parts of deionized water.
Preferably, the water is Gem flower-shaped three-dimensional jig-saw puzzle juice, red-spotted stonecrop juice, cactus juice, rape juice, shepherd's purse juice
One or more than one kinds of mixtures in liquid.
Preferably, the nano particle is nano silicon dioxide, nano-titanium dioxide, ferroso-ferric oxide, neodymium boron, barium
One or more than one kinds of mixtures in ferrite.
Preferably, it according to parts by weight, is at least prepared from the following components：15 parts of calcium carbonate, 2 parts of soybean lecithin, silicon
4 parts of diatomaceous earth, 10 parts of nano particle, 10 parts of water, 20 parts of barium sulfate, 2 parts of silica flour, 3 parts of polyethylene glycol, deionized water 50
Part.
Preferably, it according to parts by weight, is at least prepared from the following components：20 parts of calcium carbonate, 3 parts of soybean lecithin, silicon
7 parts of diatomaceous earth, 13 parts of nano particle, 15 parts of water, 25 parts of barium sulfate, 5 parts of silica flour, 5 parts of polyethylene glycol, deionized water 75
Part.
Preferably, it according to parts by weight, is at least prepared from the following components：25 parts of calcium carbonate, 4 parts of soybean lecithin, silicon
10 parts of diatomaceous earth, 15 parts of nano particle, 20 parts of water, 30 parts of barium sulfate, 8 parts of silica flour, 7 parts of polyethylene glycol, deionized water
50-100 parts.
Preferably, a kind of preparation method of antiradiation coating, it is characterised in that：It is as follows：
Step 1,50-100 parts of deionized water, 4-10 parts of diatomite are added in a kettle, 500-1000 revs/min, stirs
It mixes 5-10 minutes；
Step 2, first by 10-20 parts of water, 3-7 parts of polyethylene glycol, 10-15 parts of nano particle, with sonic oscillation 10-
20 minutes, obtain homogeneous solution；
Step 3, the homogeneous solution of step 2 is added in the solution of step 1,1000-3000 revs/min, 20-30 points of stirring
Clock；
Step 4, raising temperature is to 60-80 DEG C, 2-4 parts of soybean lecithin of addition, 2-8 parts of silica flour, 500-1000 revs/min
Clock stirs 20-30 minutes；
Step 5, it is cooled to 20-30 DEG C, is added 15-25 parts of calcium carbonate, 20-30 parts of barium sulfate, 1000-3000 revs/min,
Stirring 20-30 minutes；
Step 6, stirring is shut down, prepared liquid antiradiation coating is obtained；
Step 7, it stands and is cooled in stirred tank liquid antiradiation coating and is less than 20 DEG C, blowing encapsulation, finished product.
Compared with prior art, the beneficial effects of the invention are as follows：
1, antiradiation coating of the invention is of wide application, and can be used for fabric, wall etc..Using later, matrix
Radiation protection efficiency can reach 99% or more.
2, antiradiation coating manufacturing process of the invention is simple to operation, and low in raw material price easily obtains, and nontoxic,
Human body is not stimulated, volatility is low, and the matrix basic performance after arrangement is unaffected.
3, mutual compatibility, synergistic effect between various raw materials used in antiradiation coating of the invention, it is excellent to collectively constitute performance
Different product.
4, the addition of water improves the shielding property of matrix.
5, simplify technique, safe operation is simple, is easy to industrialized production.
6, fabric radiation coating construction is simple of the invention, can be applied by dipping, spraying, roller coating etc., raw
Efficiency is produced to improve.
7, antiradiation coating of the invention can make motley appearance by the pigment of addition 2-5%.
8, antiradiation coating of the invention is very thin, probably in 0.03-0.05mm.
9, use of the invention can receive good economic benefit.
Example is embodied
The invention discloses a kind of antiradiation coatings to be prepared from the following components according to important number：Calcium carbonate 15-
25 parts, 2-4 parts of soybean lecithin, 4-10 parts of diatomite, 10-15 parts of nano particle, 10-20 parts of water, barium sulfate 20-30
Part, 2-8 parts of silica flour, 3-7 parts of polyethylene glycol, 50-100 parts of deionized water.
The present invention also provides a kind of preparation methods of antiradiation coating, are as follows：
(1) 50-100 parts of deionized water, 4-10 parts of diatomite are added in a kettle, 500-1000 revs/min, stirs 5-
10 minutes；
(2) first by 10-20 parts of water, 3-7 parts of polyethylene glycol, 10-15 parts of nano particle, with sonic oscillation 10-20
Minute, obtain homogeneous solution；
(3) homogeneous solution of step (2) is added in the solution of step (1), 1000-3000 revs/min, stirs 20-30
Minute；
(4) temperature is increased to 60-80 DEG C, and 2-4 parts of soybean lecithin, 2-8 parts of silica flour is added, 500-1000 revs/min, stirs
It mixes 20-30 minutes；
(5) it is cooled to 20-30 DEG C, 15-25 parts of calcium carbonate, 20-30 parts of barium sulfate is added, 1000-3000 revs/min, stirs
It mixes 20-30 minutes；
(6) stirring is shut down, prepared liquid antiradiation coating is obtained；
(7) it stands and is cooled in stirred tank liquid antiradiation coating and is less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 1
The invention discloses a kind of antiradiation coatings to be prepared from the following components according to important number：Calcium carbonate 15
Part, 2 parts of soybean lecithin, 4 parts of diatomite, 10 parts of nano particle, 10 parts of water, 20 parts of barium sulfate, 2 parts of silica flour, poly- second
3 parts of glycol, 50 parts of deionized water.
The present invention also provides a kind of preparation methods of antiradiation coating, are as follows：
(1) 50 parts of deionized water, 4 parts of diatomite are added in a kettle, 500 revs/min, stirs 5 minutes；
(2) it first by 10 parts of water, 3 parts of polyethylene glycol, 10 parts of nano particle, with sonic oscillation 10 minutes, obtains
Even solution；
(3) homogeneous solution of step (2) is added in the solution of step (1), 1000 revs/min, is stirred 20 minutes；
(4) temperature is increased to 60 DEG C, and 2 parts of soybean lecithin, 2 parts of silica flour is added, 500 revs/min, stirs 20 minutes；
(5) 20 DEG C are cooled to, 15 parts of calcium carbonate, 20 parts of barium sulfate is added, 1000 revs/min, stirs 20 minutes；
(6) stirring is shut down, prepared liquid antiradiation coating is obtained；
(7) it stands and is cooled in stirred tank liquid antiradiation coating and is less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 2
The invention discloses a kind of antiradiation coatings to be prepared from the following components according to important number：Calcium carbonate 20
Part, 3 parts of soybean lecithin, 7 parts of diatomite, 13 parts of nano particle, 15 parts of water, 25 parts of barium sulfate, 5 parts of silica flour, poly- second
5 parts of glycol, 75 parts of deionized water.
The present invention also provides a kind of preparation methods of antiradiation coating, are as follows：
(1) 75 parts of deionized water, 7 parts of diatomite are added in a kettle, 750 revs/min, stirs 8 minutes；
(2) it first by 15 parts of water, 5 parts of polyethylene glycol, 13 parts of nano particle, with sonic oscillation 15 minutes, obtains
Even solution；
(3) homogeneous solution of step (2) is added in the solution of step (1), 2000 revs/min, is stirred 20-30 minutes；
(4) temperature is increased to 70 DEG C, and 3 parts of soybean lecithin, 5 parts of silica flour is added, 750 revs/min, stirs 25 minutes；
(5) 25 DEG C are cooled to, 20 parts of calcium carbonate, 25 parts of barium sulfate is added, 2000 revs/min, stirs 25 minutes；
(6) stirring is shut down, prepared liquid antiradiation coating is obtained；
(7) it stands and is cooled in stirred tank liquid antiradiation coating and is less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 3
The invention discloses a kind of antiradiation coatings to be prepared from the following components according to important number：Calcium carbonate 25
Part, 4 parts of soybean lecithin, 10 parts of diatomite, 15 parts of nano particle, 20 parts of water, 30 parts of barium sulfate, 8 parts of silica flour, poly- second
7 parts of glycol, 100 parts of deionized water.
The present invention also provides a kind of preparation methods of antiradiation coating, are as follows：
(1) 100 parts of deionized water, 10 parts of diatomite are added in a kettle, 1000 revs/min, stirs 10 minutes；
(2) it first by 20 parts of water, 7 parts of polyethylene glycol, 15 parts of nano particle, with sonic oscillation 20 minutes, obtains
Even solution；
(3) homogeneous solution of step (2) is added in the solution of step (1), 3000 revs/min, is stirred 20-30 minutes；
(4) temperature is increased to 80 DEG C, and 4 parts of soybean lecithin, 8 parts of silica flour is added, 1000 revs/min, stirs 30 minutes；
(5) 30 DEG C are cooled to, 25 parts of calcium carbonate, 30 parts of barium sulfate is added, 3000 revs/min, stirs 30 minutes；
(6) stirring is shut down, prepared liquid antiradiation coating is obtained；
(7) it stands and is cooled in stirred tank liquid antiradiation coating and is less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 4
The invention discloses a kind of antiradiation coatings to be prepared from the following components according to important number：Calcium carbonate 25
Part, 2 parts of soybean lecithin, 8 parts of diatomite, 15 parts of nano particle, 20 parts of water, 20 parts of barium sulfate, 2 parts of silica flour, poly- second
5 parts of glycol, 80 parts of deionized water.
The present invention also provides a kind of preparation methods of antiradiation coating, are as follows：
(1) 80 parts of deionized water, 8 parts of diatomite are added in a kettle, 1000 revs/min, stirs 10 minutes；
(2) it first by 20 parts of water, 5 parts of polyethylene glycol, 15 parts of nano particle, with sonic oscillation 20 minutes, obtains
Even solution；
(3) homogeneous solution of step (2) is added in the solution of step (1), 3000 revs/min, is stirred 25 minutes；
(4) temperature is increased to 65 DEG C, and 2 parts of soybean lecithin, 2 parts of silica flour is added, 800 revs/min, stirs 20-30 minutes；
(5) it is cooled to 20-30 DEG C, 25 parts of calcium carbonate, 20 parts of barium sulfate is added, 3000 revs/min, stirs 20 minutes；
(6) stirring is shut down, prepared liquid antiradiation coating is obtained；
(7) it stands and is cooled in stirred tank liquid antiradiation coating and is less than 20 DEG C, blowing encapsulation, finished product.
Test case
4 pieces of identical pure cotton cloths are put into the radiation protection solution of embodiment 1,2,3,4, roll, dry by two leachings two, roasting
It dries, washes, drying can obtain 4 pieces of cloth with shielding property.Test result is as follows：
| Embodiment | Radiation protection efficiency (%) |
| 1 | 99.0 |
| 2 | 99.5 |
| 3 | 99.9 |
| 4 | 99.7 |
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace
And modification, the scope of the present invention is defined by the appended.
Claims (7)
1. a kind of antiradiation coating, it is characterised in that：The antiradiation coating includes the raw material of following parts by weight：Calcium carbonate
15-25 parts, 2-4 parts of soybean lecithin, 4-10 parts of diatomite, 10-15 parts of nano particle, 10-20 parts of water, barium sulfate 20-
30 parts, 2-8 parts of silica flour, 3-7 parts of polyethylene glycol, 50-100 parts of deionized water.
2. antiradiation coating according to claim 1, it is characterised in that：The water is Gem flower-shaped three-dimensional jig-saw puzzle juice, scape
One or more than one kinds of mixtures in its juice, cactus juice, rape juice, shepherd's purse juice.
3. antiradiation coating according to claim 1, it is characterised in that：The nano particle be nano silicon dioxide,
One or more than one kinds of mixtures in nano-titanium dioxide, ferroso-ferric oxide, neodymium boron, barium ferrite.
4. a kind of antiradiation coating according to claim 1, it is characterised in that：According to parts by weight, at least by with the following group
Divide and is prepared：15 parts of calcium carbonate, 2 parts of soybean lecithin, 4 parts of diatomite, 10 parts of nano particle, 10 parts of water, barium sulfate
20 parts, 2 parts of silica flour, 3 parts of polyethylene glycol, 50 parts of deionized water.
5. a kind of antiradiation coating according to claim 1, it is characterised in that：According to parts by weight, at least by with the following group
Divide and is prepared：20 parts of calcium carbonate, 3 parts of soybean lecithin, 7 parts of diatomite, 13 parts of nano particle, 15 parts of water, barium sulfate
25 parts, 5 parts of silica flour, 5 parts of polyethylene glycol, 75 parts of deionized water.
6. a kind of antiradiation coating according to claim 1, it is characterised in that：According to parts by weight, at least by with the following group
Divide and is prepared：25 parts of calcium carbonate, 4 parts of soybean lecithin, 10 parts of diatomite, 15 parts of nano particle, 20 parts of water, barium sulfate
30 parts, 8 parts of silica flour, 7 parts of polyethylene glycol, 50-100 parts of deionized water.
7. the preparation method of any a kind of antiradiation coating in a kind of 1-6 using the claims, it is characterised in that：
It is as follows：
Step 1,50-100 parts of deionized water, 4-10 parts of diatomite are added in a kettle, 500-1000 revs/min, stirs 5-
10 minutes；
Step 2, first by 10-20 parts of water, 3-7 parts of polyethylene glycol, 10-15 parts of nano particle, with sonic oscillation 10-20 points
Clock obtains homogeneous solution；
Step 3, the homogeneous solution of step 2 is added in the solution of step 1,1000-3000 revs/min, is stirred 20-30 minutes；
Step 4, temperature is increased to 60-80 DEG C, and 2-4 parts of soybean lecithin, 2-8 parts of silica flour is added, 500-1000 revs/min, stirs
It mixes 20-30 minutes；
Step 5, it is cooled to 20-30 DEG C, 15-25 parts of calcium carbonate, 20-30 parts of barium sulfate is added, 1000-3000 revs/min, stirs
20-30 minutes；
Step 6, stirring is shut down, prepared liquid antiradiation coating is obtained；
Step 7, it stands and is cooled in stirred tank liquid antiradiation coating and is less than 20 DEG C, blowing encapsulation, finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201710680175.5A CN108285658A (en) | 2017-08-10 | 2017-08-10 | A kind of preparation method of antiradiation coating |
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| CN201710680175.5A CN108285658A (en) | 2017-08-10 | 2017-08-10 | A kind of preparation method of antiradiation coating |
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| CN108285658A true CN108285658A (en) | 2018-07-17 |
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| CN201710680175.5A Pending CN108285658A (en) | 2017-08-10 | 2017-08-10 | A kind of preparation method of antiradiation coating |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111321500A (en) * | 2020-03-31 | 2020-06-23 | 江西服装学院 | Anti-radiation fabric and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102146593A (en) * | 2011-04-21 | 2011-08-10 | 扬州大学 | Production method of radiation-proof fabric |
-
2017
- 2017-08-10 CN CN201710680175.5A patent/CN108285658A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102146593A (en) * | 2011-04-21 | 2011-08-10 | 扬州大学 | Production method of radiation-proof fabric |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111321500A (en) * | 2020-03-31 | 2020-06-23 | 江西服装学院 | Anti-radiation fabric and preparation method thereof |
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Application publication date: 20180717 |
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