CN107684555A - The composition of raw materials and preparation method of a kind of B B-complex for animals, oligosaccharide nanoemulsion - Google Patents
The composition of raw materials and preparation method of a kind of B B-complex for animals, oligosaccharide nanoemulsion Download PDFInfo
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- CN107684555A CN107684555A CN201711089682.8A CN201711089682A CN107684555A CN 107684555 A CN107684555 A CN 107684555A CN 201711089682 A CN201711089682 A CN 201711089682A CN 107684555 A CN107684555 A CN 107684555A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/045—Hydroxy compounds, e.g. alcohols; Salts thereof, e.g. alcoholates
- A61K31/07—Retinol compounds, e.g. vitamin A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/105—Aliphatic or alicyclic compounds
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/111—Aromatic compounds
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/163—Sugars; Polysaccharides
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/174—Vitamins
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K50/00—Feeding-stuffs specially adapted for particular animals
- A23K50/70—Feeding-stuffs specially adapted for particular animals for birds
- A23K50/75—Feeding-stuffs specially adapted for particular animals for birds for poultry
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/33—Heterocyclic compounds
- A61K31/335—Heterocyclic compounds having oxygen as the only ring hetero atom, e.g. fungichromin
- A61K31/365—Lactones
- A61K31/375—Ascorbic acid, i.e. vitamin C; Salts thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/33—Heterocyclic compounds
- A61K31/395—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins
- A61K31/435—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins having six-membered rings with one nitrogen as the only ring hetero atom
- A61K31/44—Non condensed pyridines; Hydrogenated derivatives thereof
- A61K31/4415—Pyridoxine, i.e. Vitamin B6
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/33—Heterocyclic compounds
- A61K31/395—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins
- A61K31/495—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins having six-membered rings with two or more nitrogen atoms as the only ring heteroatoms, e.g. piperazine or tetrazines
- A61K31/505—Pyrimidines; Hydrogenated pyrimidines, e.g. trimethoprim
- A61K31/506—Pyrimidines; Hydrogenated pyrimidines, e.g. trimethoprim not condensed and containing further heterocyclic rings
- A61K31/51—Thiamines, e.g. vitamin B1
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/33—Heterocyclic compounds
- A61K31/395—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins
- A61K31/495—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins having six-membered rings with two or more nitrogen atoms as the only ring heteroatoms, e.g. piperazine or tetrazines
- A61K31/505—Pyrimidines; Hydrogenated pyrimidines, e.g. trimethoprim
- A61K31/519—Pyrimidines; Hydrogenated pyrimidines, e.g. trimethoprim ortho- or peri-condensed with heterocyclic rings
- A61K31/525—Isoalloxazines, e.g. riboflavins, vitamin B2
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/59—Compounds containing 9, 10- seco- cyclopenta[a]hydrophenanthrene ring systems
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/70—Carbohydrates; Sugars; Derivatives thereof
- A61K31/702—Oligosaccharides, i.e. having three to five saccharide radicals attached to each other by glycosidic linkages
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- Coloring Foods And Improving Nutritive Qualities (AREA)
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Abstract
The present invention discloses the composition of raw materials and preparation method of a kind of B B-complex for animals, oligosaccharide nanoemulsion, including 0.1%~1% vitamin A, 0.01%~0.1% vitamin D, 0.1%~1% vitamin E, 1%~5% vitamin C, 0.1%~1% vitamin B1, 0.01%~0.1% vitamin B2, 0.1%~1% vitamin B6, 1%~20% emulsifying agent, 0.1%~1% PH conditioning agents, 0.075%~0.75% antioxidant, 0.0008~0.0075% chelating agent, 5%~20% oligosaccharide, surplus is purified water, they and purified water is mixed to form into emulsifying agent, finished product stability is high, it is easy to use, it can infinitely expand in drinking-water molten, be uniformly dispersed, efficient absorption, efficiently utilize, and eliminate the difference that individual absorbs.
Description
Technical field
It is particularly a kind of B B-complex for animals, oligomeric the present invention relates to one kind cultivation B B-complex, oligosaccharide preparation
The composition of raw materials and preparation method of sugared nanoemulsion.
Background technology
Vitamin is that animal maintains organic substance necessary to normal activities.The effect of its principal biological is to participate in body
The coenzyme of interior enzyme or the composition of prothetic group, the metabolic process of indirect Auto-regulator in vivo.Although animal body is to the need of vitamin
Very little is measured, but its effect is particularly significant.Each vitamin has special function to animal body.Animal lacks any
A kind of vitamin can all cause specific Nutrition and Metabolism obstacle, i.e. vitamin-deficiency.The lighter causes animal growth and development to be obstructed,
Production capacity declines, and large quantities of animal deads can be caused when serious.
Oligosaccharide is a kind of new type functional sugar source, is widely used in food, health products, beverage, medicine, feed addictive
Deng field.Oligosaccharide integrates nutrition, health care, dietotherapy, is widely used in food, health products, beverage, medicine, feed addition
The fields such as agent.Oligosaccharide can improve micro-ecological environment in animal body, be advantageous to the propagation of Bifidobacterium and other beneficial bacteriums, through generation
Thanking to generation organic acid reduces intestinal pH, suppresses the growth of enteral salmonella and spoilage organisms, adjusts gastrointestinal function, suppresses intestines
Interior corrupt substance, change stool, it is anti-to treat constipation, and increase vitamin synthesis, improve animal body immunologic function.
Nanoemulsion (nanoemulsion) is also known as micro emulsion (microemulsion), be by water, oil, surfactant and
Cosurfactant etc. spontaneously forms, and particle diameter is 1~100nm Thermodynamically stable, isotropism, and transparent or semitransparent is homogeneous
Dispersion.
The content of the invention
The present invention provides a kind of B B-complex for animals, the composition of raw materials and preparation method of oligosaccharide nanoemulsion, purpose
It is to improve B B-complex, the stability of oligosaccharide nano-emulsion agent, improves the assimilation effect of vitamin.
The present invention adopts the following technical scheme that：
A kind of B B-complex for animals, the composition of raw materials of oligosaccharide nanoemulsion, it is characterised in that including following quality point
Several components：
The vitamin A is one kind in retinol, vitamine A acetate, Retinol Palmitate.
The vitamin D is one kind in calciferol, vitamine D3.
The vitamin E is at least one of Vitwas E, VE-succinate, vitamine E nicotinate
The vitamin B1It is thiamine mononitrate element, one kind of thiamine hydrochloride
The emulsifying agent include be lauryl sodium sulfate, poloxamer 108, PLURONICS F87, polysorbas20, polysorbate40,
Polysorbate60, polysorbate65, Tween 80, polysorbate85, Emulsifier EL-60 EL20, Emulsifier EL-60 EL40 and polyethylene glycol
At least two in 400 monostearates.
The PH conditioning agents include be citric acid, butanedioic acid, malic acid, fumaric acid etc. at least one.
It is antioxidant (EMQ), butylated hydroxyarisol (BHA) that the antioxidant, which includes, 2,6- di-t-butyl -4-
Methylphenol (BHT) and TBHQ (TBHQ), at least one of sodium pyrosulfite.
The chelating agent is disodium ethylene diamine tetraacetate (EDTA-2Na).
The oligosaccharide is oligoisomaltose, FOS, galactooligosaccharide, one kind of soyabean oligosaccharides.
A kind of B B-complex for animals as described in, the preparation method of oligosaccharide nanoemulsion, it is characterised in that including as follows
Step：
1. by PH conditioning agents, chelating agent, vitamin C, vitamin B1, vitamin B2, vitamin B6, it is prebiotic
Member is added in appropriate purified water, and stirring and dissolving obtains A liquid；
2. B liquid is mixed evenly to obtain in vitamin A, vitamin D, vitamin E, antioxidant, emulsifying agent；
3. B liquid is added in A liquid and stirs to obtain C liquid；
4.C liquid adds purified water to filter to obtain slightly yellow clarification emulsion to full dose.
5. the inspection of semifinished product, embedding (full dress), labeling, vanning, product inspection, storage.
Compared to the prior art, present invention B B-complex for animals, oligosaccharide nanoemulsion formula are reasonable, preparation method letter
Single, process for preparation is low without complex device, energy consumption without heating；Finished product stability is high, easy to use, can be unlimited in drinking-water
Expand molten, be uniformly dispersed, efficient absorption, efficiently utilize, and eliminate the difference that individual absorbs, ensure breeding scale collection group motion
Thing nutrition and health have a very important role.Both it can for a long time add when nourishing additive agent, can be added again in disease duration
To the effect for treating and shortening the course of disease, it is especially suitable for scale livestock farming and uses.
Embodiment
The present invention is elaborated with reference to embodiment.
Embodiment 1
Implementation steps：
1. citric acid, disodium ethylene diamine tetraacetate (EDTA-2Na) are added in 500kg purified waters, stirring and dissolving, then add
Enter vitamin C, vitamin B1, vitamin B2, vitamin B6Stirring and dissolving, add oligoisomaltose and stir to obtain A liquid；
2. by Retinol Palmitate, vitamine D3, Vitwas E, BHT, TBHQ, Tween 80, polyoxyethylene castor
B liquid is mixed evenly to obtain in sesame oil EL20；
3. B liquid is added in A liquid and stirs to obtain C liquid；
It is 1000kg that 4.C liquid, which adds purified water to add to the gross mass of emulsion, filters to obtain slightly yellow clarification emulsion.
5. the inspection of semifinished product, embedding (full dress), labeling, vanning, product inspection, storage.
Embodiment 2
Implementation steps：
1. butanedioic acid, disodium ethylene diamine tetraacetate (EDTA-2Na) are added in 500kg purified waters, stirring and dissolving, then add
Enter vitamin C, vitamin B1, vitamin B2, vitamin B6Stirring and dissolving, add FOS and stir to obtain A liquid；
2. by vitamine A acetate, calciferol, Vitwas E, BHT, TBHQ, Tween 80, polyethylene glycol 400
B liquid is mixed evenly to obtain in monostearate；
3. B liquid is added in A liquid and stirs to obtain C liquid；
It is 1000kg that 4.C liquid, which adds purified water to add to the gross mass of emulsion, filters to obtain slightly yellow clarification emulsion.
5. the inspection of semifinished product, embedding (full dress), labeling, vanning, product inspection, storage.
Embodiment 3
Implementation steps：
1. malic acid, disodium ethylene diamine tetraacetate (EDTA-2Na) are added in 500kg purified waters, stirring and dissolving, then add
Enter vitamin C, vitamin B1, vitamin B2, vitamin B6Stirring and dissolving, add oligomeric lactose and stir to obtain A liquid；
2. by Retinol Palmitate, vitamine D3, vitamine E nicotinate, BHT, polysorbate85, Emulsifier EL-60
B liquid is mixed evenly to obtain in EL40；
3. B liquid is added in A liquid and stirs to obtain C liquid；
It is 1000kg that 4.C liquid, which adds purified water to add to the gross mass of emulsion, filters to obtain slightly yellow clarification emulsion.
5. the inspection of semifinished product, embedding (full dress), labeling, vanning, product inspection, storage.
Embodiment 4
Implementation steps：
1. citric acid, disodium ethylene diamine tetraacetate (EDTA-2Na) are added in 500kg purified waters, stirring and dissolving, then add
Enter vitamin C, vitamin B1, vitamin B2, vitamin B6Stirring and dissolving, add soyabean oligosaccharides and stir to obtain A liquid；
2. by vitamine A acetate, vitamine D3, Vitwas E, TBHQ, Emulsifier EL-60 EL40, poly- second
B liquid is mixed evenly to obtain in the monostearate of glycol 400；
3. B liquid is added in A liquid and stirs to obtain C liquid；
It is 1000kg that 4.C liquid, which adds purified water to add to the gross mass of emulsion, filters to obtain slightly yellow clarification emulsion.
5. the inspection of semifinished product, embedding (full dress), labeling, vanning, product inspection, storage.
One group of experimental data is provided below, is compared to illustrate that the present invention meets vitamin with routine, there is good feeding
Support effect.
In experiment, chick is divided into 7,12000 every.
Wherein, the chick of 1-4 is raised with the emulsion that in the present invention prepared by embodiment 1-4 respectively, water addition 1Kg breasts per ton
Agent, it is used in conjunction 20 days.
Remaining 3 chick is raised with the conventional powders shape vitamin purchased on the market.
It was found from upper table statistics, the indices of chick raised with the present invention, hence it is evident that better than with ordinary powder shape
The chick of vitamin raising.
Claims (10)
1. a kind of B B-complex for animals, the composition of raw materials of oligosaccharide nanoemulsion, it is characterised in that including following parts by weight
Component：
2. B B-complex for animals, the composition of raw materials of oligosaccharide nanoemulsion according to claim 1, it is characterised in that institute
It is one kind in retinol, vitamine A acetate, Retinol Palmitate to state vitamin A.
3. the composition of raw materials of oral B B-complex oil-in-water type nano-emulsion agent for animals, its feature exist according to claim 1
In the vitamin D is one kind in calciferol, vitamine D3.
4. B B-complex for animals, the composition of raw materials of oligosaccharide nanoemulsion according to claim 1, it is characterised in that institute
It is one kind in Vitwas E, VE-succinate, vitamine E nicotinate to state vitamin E.
5. B B-complex for animals, the composition of raw materials of oligosaccharide nanoemulsion according to claim 1, it is characterised in that institute
To state emulsifying agent and include be lauryl sodium sulfate, poloxamer 108, PLURONICS F87, polysorbas20, polysorbate40, polysorbate60, is told
Temperature 65, Tween 80, polysorbate85, Emulsifier EL-60 EL20, Emulsifier EL-60 EL40 and polyethylene glycol 400 monostearate
At least two in ester.
6. B B-complex for animals, the composition of raw materials of oligosaccharide nanoemulsion according to claim 1, it is characterised in that institute
State PH conditioning agents include be citric acid, butanedioic acid, malic acid, fumaric acid etc. at least one.
7. B B-complex for animals, the composition of raw materials of oligosaccharide nanoemulsion according to claim 1, it is characterised in that institute
Stating antioxidant includes being antioxidant (EMQ), butylated hydroxyarisol (BHA), 2,6- di-tert-butyl-4-methy phenols
And at least one of TBHQ (TBHQ), sodium pyrosulfite (BHT).
8. B B-complex for animals, the composition of raw materials of oligosaccharide nanoemulsion according to claim 1, it is characterised in that institute
It is disodium ethylene diamine tetraacetate to state chelating agent.
9. B B-complex for animals, the composition of raw materials of oligosaccharide nanoemulsion according to claim 1, it is characterised in that institute
It is oligoisomaltose to state oligosaccharide, FOS, galactooligosaccharide, one kind of soyabean oligosaccharides.
10. a kind of B B-complex for animals as claimed in claim 1, the preparation method of oligosaccharide nanoemulsion, it is characterised in that
Comprise the following steps：
By PH conditioning agents, chelating agent, vitamin C, vitamin B1, vitamin B2, vitamin B6, prebiotics add appropriate purified water
In, stirring and dissolving obtains A liquid；
B liquid is mixed evenly to obtain in vitamin A, vitamin D, vitamin E, antioxidant, emulsifying agent；
B liquid is added in A liquid and stirs to obtain C liquid；
C liquid adds purified water to filter to obtain slightly yellow clarification emulsion to full dose；
The inspection of semifinished product, embedding (full dress), labeling, vanning, product inspection, storage.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711089682.8A CN107684555A (en) | 2017-10-27 | 2017-10-27 | The composition of raw materials and preparation method of a kind of B B-complex for animals, oligosaccharide nanoemulsion |
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| CN201711089682.8A CN107684555A (en) | 2017-10-27 | 2017-10-27 | The composition of raw materials and preparation method of a kind of B B-complex for animals, oligosaccharide nanoemulsion |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108576781A (en) * | 2018-05-11 | 2018-09-28 | 山东信得科技股份有限公司 | A kind of multi-vitamins and preparation method thereof |
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| CN102326676A (en) * | 2011-09-30 | 2012-01-25 | 佛山市正典生物技术有限公司 | Complex vitamin molecule microemulsion and preparation method thereof |
| CN104068219A (en) * | 2014-06-18 | 2014-10-01 | 广东金品动物营养有限公司 | Composite vitamin immunopolysaccharide nano micro-emulsion for livestock and poultry as well as preparation method and application of micro-emulsion |
| CN104997794A (en) * | 2015-07-31 | 2015-10-28 | 郑州赛科药业科技有限公司 | Long-acting composite vitamin oral emulsion for livestock and preparation method thereof |
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2017
- 2017-10-27 CN CN201711089682.8A patent/CN107684555A/en active Pending
Patent Citations (3)
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| CN102326676A (en) * | 2011-09-30 | 2012-01-25 | 佛山市正典生物技术有限公司 | Complex vitamin molecule microemulsion and preparation method thereof |
| CN104068219A (en) * | 2014-06-18 | 2014-10-01 | 广东金品动物营养有限公司 | Composite vitamin immunopolysaccharide nano micro-emulsion for livestock and poultry as well as preparation method and application of micro-emulsion |
| CN104997794A (en) * | 2015-07-31 | 2015-10-28 | 郑州赛科药业科技有限公司 | Long-acting composite vitamin oral emulsion for livestock and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108576781A (en) * | 2018-05-11 | 2018-09-28 | 山东信得科技股份有限公司 | A kind of multi-vitamins and preparation method thereof |
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