CN107684001A - A kind of Honegsukle flower P.E concentrate removes the production method of bitter taste - Google Patents
A kind of Honegsukle flower P.E concentrate removes the production method of bitter taste Download PDFInfo
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- CN107684001A CN107684001A CN201710752235.XA CN201710752235A CN107684001A CN 107684001 A CN107684001 A CN 107684001A CN 201710752235 A CN201710752235 A CN 201710752235A CN 107684001 A CN107684001 A CN 107684001A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/70—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/35—Caprifoliaceae (Honeysuckle family)
- A61K36/355—Lonicera (honeysuckle)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/333—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using mixed solvents, e.g. 70% EtOH
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/53—Liquid-solid separation, e.g. centrifugation, sedimentation or crystallization
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Abstract
The production method that Honegsukle flower P.E concentrate of the present invention removes bitter taste is to use acid-hydrolysis method, hydrolyzes the bitter substance in Honegsukle flower P.E concentrate.Specifically include following steps:1. add food-grade acid in Honegsukle flower P.E concentrate；2. constant temperature stands certain time at a certain temperature；3. stand at low temperature certain time again, filtering precipitation, obtain bitter taste Honegsukle flower P.E concentrate.This method can remove most of bitter substance in Honegsukle flower P.E concentrate, make the product using the allotment of Honegsukle flower P.E concentrate（Such as beverage, oral-cavity article or Chinese patent drug）The addition of sweetener can be reduced, and the original characteristic flavor of honeysuckle can be retained, product is more healthy, more conducively promotes.
Description
Technical field
The present invention relates to honeysuckle manufacture field, and in particular to the side of bitter taste is removed to a kind of Honegsukle flower P.E concentrate
Method.
Background technology
Honeysuckle is honeysuckle category caprifoliaceae plant, takes in integration of drinking and medicinal herbs list by country.The sweet cold air of honeysuckle property
Taste fragrance, clear heat with drugs of sweet flavour and cold nature does not injure one's stomach, and is good medicine clearing heat and detoxicating in ancient prescription.Honeysuckle be good at it is clearing heat and detoxicating, to various febrile diseases,
Such as dermexanthesis, heat toxin sore carbuncle, hair spot, body heat, abscess of throat, Yao fruit are notable.In recent years, many clinical research confirmations honeysuckle
With a variety of pharmacological effects such as broad-spectrum antiviral, antitumor, antibacterial, hepatic cholagogic, antipyretic and anti-inflammatory.Honeysuckle is often directly brewed
As tea-drinking, quench one's thirst relieving summer-heat.
Honeysuckle nutritive value enriches, but after brew, tea has a bitter taste, strong influence honeysuckle tea-drinking
Flavor.At present, beverage " honeysuckle tea " on the market, this bitter taste is covered by adding essence mostly.It is consequently, it is possible to bitter
Astringent taste is no doubt blanked, and the distinctive flowers and plants delicate fragrance of honeysuckle itself and sweet fragrance are also blanked, and tastes flavor and gold
Honeysuckle flower flavor difference is extremely remote, have impact on the popularization of product.
The content of the invention
It is an object of the invention to problem and shortage be present for above-mentioned, there is provided one kind can cut Honegsukle flower P.E bitter taste
It is weak, make when Honegsukle flower P.E is deployed into drink that taste is better, more conducively promote, and process easy Honegsukle flower P.E concentration
Liquid removes the production method of bitter taste.
The technical proposal of the invention is realized in this way：
Inventor assert that the bitter principle in Honegsukle flower P.E is mainly in caprifoliaceae plant growth course by studying repeatedly
Spontaneous iridoid glycosides, saponins material or chemical constitution are similar to caused by the material of bitters.Therefore, remove
These bitter substances will substantially improve the product taste of the concentrate containing Honegsukle flower P.E.
Solution provided by the invention is to decompose iridoid glycoside and saponins material using acid-hydrolyzed method, is reached
Remove the purpose of bitter taste.Specific production method comprises the following steps：1., add food-grade in Honegsukle flower P.E concentrate
Acid；2., stand 2-5h at 50-65 DEG C；3., stand at low temperature again, filtering precipitation, obtain the concentration of bitter taste Honegsukle flower P.E
Liquid.
1. food-grade acid that above-mentioned steps are added can be the various acid available for acid-catalyzed hydrolysis, including organic acid and nothing
Machine acid.Preferably acetic acid, citric acid or concentration are 31% food grade hydrochloric acid, low-concentration sulfuric acid, nitric acid etc..Above-mentioned food-grade acid
Addition be Honegsukle flower P.E concentrate weight 1%-3%（The addition of instant grade acid is per the extraction of 100g honeysuckles
Thing concentrate adds 1-3g acid, and after sour addition is more than 3g, tart flavour is may feel that in the beverage of allotment.Preferable amount is every
100g Honegsukle flower P.Es concentrate adds 1.5g acid.If certain client wishes that product has certain tart flavour, can also add some points more
Acid.）
Above-mentioned steps 2. in acidolysis dwell temperature be 50-65 DEG C, temperature is too high to be charred the carbohydrate in concentrate, make product
With caramel, mouthfeel is influenceed.Preferable temperature is 55 DEG C, and the preferably time is 3h.
Above-mentioned steps 3. in, stand at low temperature is after concentrate drops to room temperature, then is placed in 5 DEG C of refrigerators and stands 8-12h.It is preferred that
Time is 10h.
The present invention can remove due to hydrolyzing the bitter substance in Honegsukle flower P.E concentrate using acid-hydrolysis method
Most of bitter substance in concentrate, its mouthfeel bitter taste is reduced by more than 50, improves the mouth of Honegsukle flower P.E concentrate
Sense, the sweetener for covering bitter taste of required addition when reducing Honegsukle flower P.E concentrate allotment concerned drink or Chinese patent drug etc.
（Sweetener used in current most of beverage is mostly sucrose）Addition, also cause the more healthy containing honeysuckle flower product of production,
So as to save cost, application is expanded, is also more conducive to promote.And the distinctive flowers and plants delicate fragrance of honeysuckle in product itself
It also can preferably be showed with sweet fragrance, the original characteristic flavor of honeysuckle can be effectively maintained, product special flavour is more preferably.This
Invention can be widely used in the various products containing honeysuckle concentrate（Such as beverage, oral-cavity article）Or in Chinese patent drug, especially
It is to be applied in beverage.
Embodiment
Honegsukle flower P.E concentrate of the present invention removes the production method of bitter taste, is to use acid-hydrolysis method, hydrolysis gold
Bitter substance in honeysuckle flower extract concentrated solution.Specifically include following steps：1., in Honegsukle flower P.E concentrate add tool
There is the food-grade acid of acid-catalyzed hydrolysis function；2., stand 2-5h at 50-65 DEG C；3., stand at low temperature again, filtering precipitation, obtain
Remove bitter taste Honegsukle flower P.E concentrate.Because the present invention can remove most of bitter substance in concentrate, therefore effectively improve
The mouthfeel of Honegsukle flower P.E concentrate, reduce Honegsukle flower P.E concentrate allotment concerned drink or Chinese patent drug etc. when institute
What need to be added covers the sweetener addition of bitter taste, also causes the more healthy containing honeysuckle flower product of production, is also more conducive to promote.
And the distinctive flowers and plants delicate fragrance of honeysuckle itself and sweet fragrance also can be showed preferably in product, processing is simple again.
The food-grade acid that wherein 1. above-mentioned steps are added can be the various acid available for acid-catalyzed hydrolysis, including organic acid
And inorganic acid.The food grade hydrochloric acid, low-concentration sulfuric acid, nitric acid that preferably acetic acid, citric acid or concentration are 31%.Above-mentioned food-grade
The addition of acid is the 1%-3% of Honegsukle flower P.E concentrate weight.It is preferred that addition is Honegsukle flower P.E concentrate weight
1.5%.2. middle dwell temperature is 50-65 DEG C to above-mentioned steps.It can be charred the carbohydrate in concentrate because temperature is too high, make product
With caramel, mouthfeel is influenceed.Preferably 55 DEG C, the method that constant temperature water bath can be used.It is preferred that the time is 3h.Above-mentioned steps 3. in
Stand at low temperature is：After concentrate drops to room temperature, then it is placed in 5 DEG C of refrigerators and stands 8-12h.It is preferred that the time is 10h.
Below in conjunction with specific embodiment, the present invention is described in further detail：
The first step of embodiment one, 100g Honegsukle flower P.E concentrates are taken, the food-grade acetic acid 1g of 99% concentration is added dropwise；Second
Step, the water-bath 5h under the conditions of 50 DEG C；3rd step, after concentrate drops to room temperature, it is placed in 5 DEG C of refrigerators and stands 12h；There is precipitation after static
Produce, bitter taste Honegsukle flower P.E concentrate 95.1g, yield 95.1% are obtained after filtering.
Contrast experiment：The aqueous sucrose solution 100g of allotment 8%, is divided into two parts, every part of 50g, adds 1g respectively and goes bitter taste golden
Honeysuckle flower extract concentrated solution and 1g Honegsukle flower P.E concentrate stostes, are tasted after mixing, go bitter taste Honegsukle flower P.E to concentrate
The beverage of liquid allotment does not feel bitter taste, and the beverage for adding the allotment of Honegsukle flower P.E concentrate stoste has obvious bitterness
Sense.
The first step of embodiment two, 100g Honegsukle flower P.E concentrates are taken, the food-grade acetic acid 1.5g of 99% concentration is added dropwise；
Second step, the water-bath 3h under the conditions of 55 DEG C；3rd step, after concentrate drops to room temperature, it is placed in 5 DEG C of refrigerators and stands 10h；Have after static
Precipitation is produced, and bitter taste Honegsukle flower P.E concentrate 93.5g, yield 93.5% are obtained after filtering.Acidolysis is thorough, has precipitated
Entirely.
Contrast experiment：The aqueous sucrose solution 100g of allotment 8%, is divided into two parts, every part of 50g, adds 1g respectively and goes bitter taste golden
Honeysuckle flower extract concentrated solution and 1g Honegsukle flower P.E concentrate stostes, are tasted after mixing, go bitter taste Honegsukle flower P.E to concentrate
The beverage of liquid allotment does not feel bitter taste, and the beverage for adding the allotment of Honegsukle flower P.E concentrate stoste has obvious bitterness
Sense.
The first step of embodiment three, 100g Honegsukle flower P.E concentrates are taken, the food-grade acetic acid 3g of 99% concentration is added dropwise；The
Two steps, the water-bath 2h under the conditions of 65 DEG C；3rd step, after concentrate drops to room temperature, it is placed in 5 DEG C of refrigerators and stands 8h；There have after static to be heavy
Form sediment and produce, bitter taste Honegsukle flower P.E concentrate 94.7g, yield 94.7% are obtained after filtering.
Contrast experiment：The aqueous sucrose solution 100g of allotment 8%, is divided into two parts, every part of 50g, adds 1g respectively and goes bitter taste golden
Honeysuckle flower extract concentrated solution and 1g Honegsukle flower P.E concentrate stostes, are tasted after mixing, go bitter taste Honegsukle flower P.E to concentrate
The beverage of liquid allotment does not feel bitter taste, and the beverage for adding the allotment of Honegsukle flower P.E concentrate stoste has obvious bitterness
Sense.
The example IV first step, 100g Honegsukle flower P.E concentrates are taken, the food-grade citric acid of 99.5% content is added dropwise
3g, the water-bath 5h under the conditions of 65 DEG C；Second step, after concentrate drops to room temperature, it is placed in 5 DEG C of refrigerators and stands 12h；3rd step, it is static
After have precipitation produce, bitter taste Honegsukle flower P.E concentrate 94.1g, yield 94.1% are obtained after filtering.
Contrast experiment：The aqueous sucrose solution 100g of allotment 8%, is divided into two parts, every part of 50g, adds 1g respectively and goes bitter taste golden
Honeysuckle flower extract concentrated solution and 1g Honegsukle flower P.E concentrate stostes, are tasted after mixing, go bitter taste Honegsukle flower P.E to concentrate
The beverage of liquid allotment does not feel bitter taste, and the beverage for adding the allotment of Honegsukle flower P.E concentrate stoste has obvious bitterness
Sense.
The first step of embodiment five, 100g Honegsukle flower P.E concentrates are taken, the food-grade citric acid of 99.5% content is added dropwise
1.5g；Second step, the water-bath 3h under the conditions of 55 DEG C；3rd step, after concentrate drops to room temperature, it is placed in 5 DEG C of refrigerators and stands 10h；It is quiet
There is precipitation to produce after only, bitter taste Honegsukle flower P.E concentrate 93.6g is obtained after filtering, yield 93.6%, acidolysis is thorough,
Precipitation is complete.
Contrast experiment：The aqueous sucrose solution 100g of allotment 8%, is divided into two parts, every part of 50g, adds 1g respectively and goes bitter taste golden
Honeysuckle flower extract concentrated solution and 1g Honegsukle flower P.E concentrate stostes, are tasted after mixing, go bitter taste Honegsukle flower P.E to concentrate
The beverage of liquid allotment does not feel bitter taste, and the beverage for adding the allotment of Honegsukle flower P.E concentrate stoste has obvious bitterness
Sense.
The first step of embodiment six, 100g Honegsukle flower P.E concentrates are taken, the food-grade citric acid of 99.5% content is added dropwise
1g；Second step, the water-bath 2h under the conditions of 50 DEG C；3rd step, after concentrate drops to room temperature, it is placed in 5 DEG C of refrigerators and stands 8h；After static
There is precipitation to produce, bitter taste Honegsukle flower P.E concentrate 95.6g, yield 95.6% are obtained after filtering.
Contrast experiment：The aqueous sucrose solution 100g of allotment 8%, is divided into two parts, every part of 50g, adds 1g respectively and goes bitter taste golden
Honeysuckle flower extract concentrated solution and 1g Honegsukle flower P.E concentrate stostes, are tasted after mixing, go bitter taste Honegsukle flower P.E to concentrate
The beverage of liquid allotment does not feel bitter taste, and the beverage for adding the allotment of Honegsukle flower P.E concentrate stoste has obvious bitterness
Sense.
The first step of embodiment seven, 100g Honegsukle flower P.E concentrates are taken, the food grade hydrochloric acid 1g of 31% concentration is added dropwise；The
Two steps, the water-bath 5h under the conditions of 50 DEG C；3rd step, after concentrate drops to room temperature, it is placed in 5 DEG C of refrigerators and stands 8h；There have after static to be heavy
Form sediment and produce, bitter taste Honegsukle flower P.E concentrate 95.3g, yield 95.3% are obtained after filtering.
Contrast experiment：The aqueous sucrose solution 100g of allotment 8%, is divided into two parts, every part of 50g, adds 1g respectively and goes bitter taste golden
Honeysuckle flower extract concentrated solution and 1g Honegsukle flower P.E concentrate stostes, are tasted after mixing, go bitter taste Honegsukle flower P.E to concentrate
The beverage of liquid allotment does not feel bitter taste, and the beverage for adding the allotment of Honegsukle flower P.E concentrate stoste has obvious bitterness
Sense.
The first step of embodiment eight, 100g Honegsukle flower P.E concentrates are taken, the food grade hydrochloric acid 1.5g of 31% concentration is added dropwise；
Second step, the water-bath 3h under the conditions of 55 DEG C；3rd step, after concentrate drops to room temperature, it is placed in 5 DEG C of refrigerators and stands 10h；Have after static
Precipitation produces, and bitter taste Honegsukle flower P.E concentrate 93.5g is obtained after filtering, yield 93.5%, acidolysis is thorough, has precipitated
Entirely.
Contrast experiment：The aqueous sucrose solution 100g of allotment 8%, is divided into two parts, every part of 50g, adds 1g respectively and goes bitter taste golden
Honeysuckle flower extract concentrated solution and 1g Honegsukle flower P.E concentrate stostes, are tasted after mixing, go bitter taste Honegsukle flower P.E to concentrate
The beverage of liquid allotment does not feel bitter taste, and the beverage for adding the allotment of Honegsukle flower P.E concentrate stoste has obvious bitterness
Sense.
The first step of embodiment nine, 100g Honegsukle flower P.E concentrates are taken, the food grade hydrochloric acid 3g of 31% concentration is added dropwise；The
Two steps, the water-bath 2h under the conditions of 65 DEG C；3rd step, after concentrate drops to room temperature, it is placed in 5 DEG C of refrigerators and stands 12h；There have after static to be heavy
Form sediment and produce, bitter taste Honegsukle flower P.E concentrate 94.4g, yield 94.4% are obtained after filtering.
Contrast experiment：The aqueous sucrose solution 100g of allotment 8%, is divided into two parts, every part of 50g, adds 1g respectively and goes bitter taste golden
Honeysuckle flower extract concentrated solution and 1g Honegsukle flower P.E concentrate stostes, are tasted after mixing, go bitter taste Honegsukle flower P.E to concentrate
The beverage of liquid allotment does not feel bitter taste, and the beverage for adding the allotment of Honegsukle flower P.E concentrate stoste has obvious bitterness
Sense.
Although the present invention is to be described with reference to specific embodiments, this description is not meant to form limit to the present invention
System.Other changes of the disclosed embodiments, all it is to be anticipated that for those skilled in the art with reference to description of the invention
, this change should belong in appended claims limited range.
Claims (7)
1. a kind of Honegsukle flower P.E concentrate removes the production method of bitter taste, it is characterised in that：Using acid-hydrolysis method, hydrolysis gold
Bitter substance in honeysuckle flower extract concentrated solution.
2. the production method of bitter taste is removed according to Honegsukle flower P.E concentrate described in claim 1, it is characterised in that：Including with
Lower step：1., in Honegsukle flower P.E concentrate add with acid-catalyzed hydrolysis function food-grade acid；2., at 50-65 DEG C
Lower standing 2-5h；3., stand at low temperature again, filtering precipitation, obtain bitter taste Honegsukle flower P.E concentrate.
3. the production method of bitter taste is removed according to Honegsukle flower P.E concentrate described in claim 2, it is characterised in that：The food
Grade acid includes the food grade hydrochloric acid, low-concentration sulfuric acid, nitric acid that acetic acid, citric acid or concentration are 31%.
4. the production method of bitter taste is removed according to Honegsukle flower P.E concentrate described in Claims 2 or 3, it is characterised in that：On
In stating step 1., the addition of above-mentioned food-grade acid is the 1%-3% of Honegsukle flower P.E concentrate weight.
5. the production method of bitter taste is removed according to Honegsukle flower P.E concentrate described in claim 4, it is characterised in that：Above-mentioned food
The addition of grade acid is the 1.5% of Honegsukle flower P.E concentrate weight.
6. the production method of bitter taste is removed according to Honegsukle flower P.E concentrate described in claim 2, it is characterised in that：Above-mentioned step
Rapid 2. middle dwell temperature is 55 DEG C, and the time is 3h.
7. the production method of bitter taste is removed according to Honegsukle flower P.E concentrate described in claim 2, it is characterised in that：Above-mentioned step
Suddenly 3. middle stand at low temperature is：After concentrate drops to room temperature, then it is placed in 5 DEG C of refrigerators and stands 8-12h.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201710752235.XA CN107684001B (en) | 2017-08-28 | 2017-08-28 | Production method for removing bitter taste of honeysuckle extract concentrated solution |
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| CN201710752235.XA CN107684001B (en) | 2017-08-28 | 2017-08-28 | Production method for removing bitter taste of honeysuckle extract concentrated solution |
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| CN107684001B CN107684001B (en) | 2021-06-15 |
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| CN107684001B (en) | 2021-06-15 |
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