CN107668688A - A kind of preparation method of high grade of transparency donkey-hide gelatin - Google Patents
A kind of preparation method of high grade of transparency donkey-hide gelatin Download PDFInfo
- Publication number
- CN107668688A CN107668688A CN201710772478.XA CN201710772478A CN107668688A CN 107668688 A CN107668688 A CN 107668688A CN 201710772478 A CN201710772478 A CN 201710772478A CN 107668688 A CN107668688 A CN 107668688A
- Authority
- CN
- China
- Prior art keywords
- donkey
- glue
- water
- transparency
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Mycology (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Cereal-Derived Products (AREA)
Abstract
The present invention relates to a kind of high grade of transparency, the easy preparation method for absorbing donkey-hide gelatin, belongs to health products exploitation preparing technical field.Its preparation method is：After donkey hide is chosen into impurity elimination, soaked 5 10 days in 20 35 DEG C under water sealing condition, change water in time；After shaving, cutting, washing；In mass ratio, water：Donkey hide=4 6:1；Toward equipped with drinking water is added in load weighted donkey hide extractor, in confined conditions, 100 120 DEG C are heated to；Extraction about 12 hours or so by several times；Glue is released, glue is concentrated in vacuo through coarse filtration, essence filtering and centrifugal filtration；Then the concentration and removal in the concentrator of open type, after removal of impurities, the soya-bean oil, yellow rice wine and the rock sugar that add after filtering；Continue agitating and heating concentration, fill basin, gel through receiving glue successively after the completion of concentration, cut glue, the glue that dries in the air processing；After the glue that dries in the air processing, through drying, watt glue shaping, re-dry, rubber, lettering, packaging, finished product is obtained.
Description
Technical field
The present invention relates to a kind of high grade of transparency, the easy preparation method for absorbing donkey-hide gelatin, belongs to health products exploitation technology of preparing neck
Domain.
Background technology
Donkey-hide gelatin starts from Qin Han, so far the existing history of more than 2000 years, is traditional nourishing, top grade of enriching blood.Donkey-hide gelatin product
Quality, typically determined by its extraction process.In existing disclosed extraction process, generally there are low output capacity, impurity content,
The nutriment rate of recovery has much room for improvement or taken the problems such as rear absorptivity is not high.
The content of the invention
The present invention in the prior art, raw material availability is low, product impurity content height, absorption of human body DeGrain,
The deficiencies such as transparency is low；A kind of preparation method of high grade of transparency donkey-hide gelatin is provided.
A kind of preparation method of high grade of transparency donkey-hide gelatin of the present invention；Comprise the steps：
Step 1
After donkey hide impurity elimination, soaked 3-5 days in 30-60 DEG C under water sealing condition；After shaving, broken, washing in mass ratio,
Water：Donkey hide=4-6:1st, it is preferably 5：1；Water is added into the donkey hide taken, after adding water, under air-proof condition, will warm up
100-120 DEG C, preferably 105-120 DEG C；Stirring extraction 15-20 hours；Liquid is released, obtains the first liquid, it is remaining in container
Residue；Water is added in toward residual residue, under air-proof condition, will warm up 105-120 DEG C；Stirring extraction 15-20 hours, release
Liquid, obtain second liquid；After adding water, the filling rate of container is 40-50%；
Step 2
Coarse filtration is first carried out to the first liquid and second liquid and then carries out smart filtering, after essence filtering, it is dense to carry out vacuum
Contracting；The weight/mass percentage composition for obtaining water is 48-52% thick glue liquid；
Step 3
It is placed in after carrying out filtration treatment to colloid obtained by step 2 in the concentrator of open type, is heated to seething with excitement, is stirred,
Remove surface offscum, impurity；When the water content in colloid is 33-36%, the soya-bean oil, yellow rice wine and the rock sugar that add after filtering
Water；Continue agitating and heating, when the water content in colloid is 24-26wt%, stop heating；Continue after stirring 0.5-1.5 hours,
Glue, which are received, at 23-26 DEG C, preferably 25 DEG C fills basins；After receiving glue filling basin, in 2-5 DEG C, preferably 4 DEG C or so gels；Designed after gel
Size carries out cutting glue, obtains blob of viscose；
Step 4
Blob of viscose obtained by step 3 is placed in 4 DEG C of refrigerating chamber after refrigerating 8 hours, carries out glue processing of drying in the air；The glue that dries in the air processing
Afterwards, it is dried in D level clean areas, watt glue shaping, re-dry, rubber, lettering, packaging, obtains finished product；In the refrigerating chamber
Air humidity is 50-70%；To control temperature is 16-25 DEG C for the glue that dries in the air processing, humidity 50-65%, time are 7-15 days；It is described dry
Dry temperature is 25-30 DEG C, the time is 7-15 days；Described watt of glue is shaped as film being neatly stacked in case, and closed 20-28 is small
When, be preferably 24 hours, then show the glue that dries in the air；The temperature of re-dry is 25-35 DEG C, the time is 5-10 days.
A kind of preparation method of high grade of transparency donkey-hide gelatin of the present invention；Heating-up temperature in step 1 is preferably 105-110 DEG C.
A kind of preparation method of high grade of transparency donkey-hide gelatin of the present invention；The place of production of the donkey hide is preferably northeast, Xinjiang or Gansu
At least one of.
A kind of preparation method of high grade of transparency donkey-hide gelatin of the present invention；In step 2, the hole of filter screen is used in the coarse filtration
100 mesh.
A kind of preparation method of high grade of transparency donkey-hide gelatin of the present invention；In step 2, the hole of filter screen is used in the essence filtering
260 mesh.
A kind of preparation method of high grade of transparency donkey-hide gelatin of the present invention；In step 2, when being concentrated in vacuo, vacuum is controlled
For -0.02~-0.06Pa；It is 80-90 DEG C to control temperature.
A kind of preparation method of high grade of transparency donkey-hide gelatin of the present invention；In step 3, the concentrator of the open type is that band presss from both sides
The concentration pan of layer；The interlayer is used to be passed through superheated water.
A kind of preparation method of high grade of transparency donkey-hide gelatin of the present invention；In step 3, colloid obtained by step 2 is carried out at filtering
It is placed in after reason in the concentrator of open type, before heating, colloid, the area with air contact surfaces obtained by step 2 after filtering per ton
Control as 3.14-7.065m2。
A kind of preparation method of high grade of transparency donkey-hide gelatin of the present invention；In step 3, by colloid gross mass obtained by step 2
1.8-2.2%, it is preferably 2% addition soya-bean oil；Add by the 0.08-0.12% of step 2 gained colloid gross mass, preferably 0.1%
Enter yellow rice wine；Rock sugar is added by the 8-12% of step 2 gained colloid gross mass, preferably 10%.
A kind of preparation method of high grade of transparency donkey-hide gelatin of the present invention；It is a length of 97mm of gained blob of viscose, a width of in step 3
42mm, thickness 6mm.
A kind of preparation method of high grade of transparency donkey-hide gelatin of the present invention；In step 3, before soya-bean oil, yellow rice wine, rock sugar is added, institute is used
Obtain dry weight=25-40% of donkey hide before being extracted in quality * (weight/mass percentage composition of 1- colloid reclaimed waters)/step 1 of colloid.(i.e.
Rate of gum output is 25-40%)
A kind of preparation method of high grade of transparency donkey-hide gelatin of the present invention；In step 3, before adding soya-bean oil, yellow rice wine, rock sugar, with gained
In colloid, the quality of organic matter of the molecular weight less than or equal to 3000 accounts for the 97-98.5% of organic matter quality in a word.
A kind of preparation method of high grade of transparency donkey-hide gelatin of the present invention；In step 4, after drying process, the OD values of blob of viscose are
2.0-3.0。
A kind of preparation method of high grade of transparency donkey-hide gelatin of the present invention；In step 4, gained finished product, match somebody with somebody by 1g finished products and take 10g temperature
The ratio of water, finished product is added in warm water, stirring, after 30-50 seconds, is completely dissolved；The temperature of the warm water is 38-40
℃。
Principle and advantage
The present invention has attempted under confined conditions, first carries out appropriate water seal fermentation；Then in sealing and appropriate container
Filling rate under conditions of, in appropriate high temperature, high pressure donkey-hide gelatin is extracted；Promote donkey hide using appropriate HTHP
In, the extraction and decomposition of macro-nutrients；The nutriment decomposited easily facilitates absorption of human body；Appropriate containers simultaneously
Filling rate when can also control extraction well, the content of oxygen；Appropriate oxygen content will not only cause the small molecule decomposited
Active material fast decoupled；Be advantageous to its surface oxygen uptake on the contrary, and then stablize the purpose of its structure.
Coarse filtration and essence filtering are selected afterwards, and most of impurity in slurry is removed；Then using felicity condition
It is concentrated in vacuo and (concentrates for the first time), appropriate vacuum concentration not only contributes to water, and also helps macromolecular nutrients
Matter enters a decomposition and keeps activity；It is concentrated in vacuo to the thick glue liquid that water content is 48-52%；Using appropriate water, it is realized
The holding of suitable active；Then it is concentrated again under the system of opening wide, when concentrating again, realized using the oxygen in the external world
Further removal of impurities；But time of removing impurities by oxidation is unsuitable long, at the same the area contacted with oxygen be not easy to it is excessive, once it is long
It is and/or excessive, it will the content of nutriment in finished product is influenceed, can not be too small/or too short, so not only bad for removal of impurities
And it can also influence the later stage and take assimilation effect.When opening wide concentration, control when water content is 33-36wt%, add appropriate filtering
Soya-bean oil, yellow rice wine and rock sugar water afterwards, using the synergy of soya-bean oil, yellow rice wine and rock sugar, realize it to small molecule nutrients
The holding of matter.While in appropriate soya-bean oil, yellow rice wine, rock sugar, blob of viscose water content and refrigerate technique, the synergy for the adhesive process that dries in the air
Under；Realize the further lifting to product transparency.
In a word, the present invention is by the synergy of each conditional parameter, obtained impurity content is low, absorption of human body effect is high,
The high product of transparency.
Brief description of the drawings
Accompanying drawing 1 is the photo figure obtained by the products obtained therefrom of embodiment 1 and market.
First piece of the left side is sample block for what is bought on the market for the products obtained therefrom of embodiment 1, first piece of the right；Can from figure
To find out the translucency of the products obtained therefrom of the embodiment of the present invention 1 much due to the donkey-hide gelatin product of in the market.Middle point from left to right
Not Wei our company production colla carapacis et plastri testudinis and deer horn glue.
Embodiment
Embodiment 1
Step 1
After donkey hide impurity elimination, soaked 3 days in 30 DEG C under water sealing condition；After unhairing, broken, washing in mass ratio, water：Donkey
Skin=5：1；Water is added into the donkey hide taken, after adding water, under air-proof condition, will warm up 105 DEG C；Stirring extraction 18 is small
When；Liquid is released, obtains the first liquid, residual residue in container；Water is added in toward residual residue, under air-proof condition, will be added
Heat is to 120 DEG C；Stirring extraction 15 hours, releases liquid, obtains second liquid；After adding water, the filling rate of container is 45%；
The content of organic matter in residual substance is detected, testing result is：The content of organic matter is less than 2.5%.
Step 2
By volume, the first liquid：Second liquid=1:1 mixing, then first carry out coarse filtration, carry out smart filtering again, essence
After filtering, it is concentrated in vacuo；The weight/mass percentage composition for obtaining water is 60% colloid；, the hole of filter screen used in the coarse filtration
Gap is 100 mesh, and the hole of filter screen is 260 mesh used in the essence filtering., when being concentrated in vacuo, it is -0.04Pa to control vacuum
(reading on table)；It is 90 DEG C to control temperature.
Step 3
It is placed in after carrying out filtration treatment to colloid obtained by step 2 in the concentration pan of sandwich, hot water heating is led into interlayer
To boiling, (before heating, colloid obtained by step 2 after filtering per ton, the area control with air contact surfaces is 7.065m2) stirring,
Remove surface offscum, impurity；When the water content in colloid is 30-35wt%, the soya-bean oil, yellow rice wine and the rock sugar that add after filtering
Water；Continue to heat, when the water content in colloid is 23-25wt%, stop heating；After continuing stirring 1 hour, glue is received at 60 DEG C
Fill basin；After receiving glue filling basin, in 4 DEG C of gels；Design size carries out cutting glue after gel, obtains blob of viscose；It is total by colloid obtained by step 2
The 2% of quality adds soya-bean oil；Yellow rice wine is added by 0.1% of colloid gross mass obtained by step 2；By the total matter of colloid obtained by step 2
The 10% of amount adds rock sugar；
Step 4
By blob of viscose obtained by step 3, a length of 97mm, a width of 42mm, the thickness 6mm of gained blob of viscose., it is placed in 4 DEG C of refrigerating chamber
After interior refrigeration 8 hours (air humidity of refrigerating chamber be 70%), glue processing of drying in the air is carried out；After the glue that dries in the air processing, carried out in D levels clean area
Dry, packaging, obtain finished product；Air humidity in the refrigerating chamber is 70%；It is 18 DEG C that the glue that dries in the air processing, which controls temperature, humidity is
60%th, the time is 12 days；The temperature of the drying is 30 DEG C, the time is 10 days.
In step 4, after drying process, the OD values of blob of viscose are 2.85.
In step 4, gained finished product, the ratio for taking 10g warm water is matched somebody with somebody in 1g finished products, finished product is added in warm water, stirred,
After 48 seconds, it is completely dissolved；The temperature of the warm water is 38-40 DEG C.
The present embodiment, in step 3, before soya-bean oil, yellow rice wine, rock sugar is added, with quality * (the 1- colloid reclaimed waters of gained colloid
Weight/mass percentage composition) extract in/step 1 before donkey hide dry weight=30%.(i.e. rate of gum output is 30%)
This present embodiment, in step 3.Before adding soya-bean oil, yellow rice wine, rock sugar, with gained colloid, molecular weight is less than or equal to
The quality of 3000 organic matter account for organic matter in a word quality 97%.
A kind of preparation method of high grade of transparency donkey-hide gelatin of the present invention；In step 4, after drying process, the OD values of blob of viscose are
2.85。
The nitrogen content of finished product is detected, is 14.95%.
Embodiment 2
Step 1
After donkey hide impurity elimination, fermented 5 days in 30 DEG C under water sealing condition；After unhairing, broken, washing in mass ratio, water：Donkey
Skin=5：1；Water is added into the donkey hide taken, after adding water, under air-proof condition, will warm up 118 DEG C；Stirring extraction 15 is small
When；Liquid is released, obtains the first liquid, residual residue in container；Water is added in toward residual residue, under air-proof condition, will be added
Heat is to 120 DEG C；Stirring extraction 15 hours, releases liquid, obtains second liquid；After adding water, the filling rate of container is 48%；
The content of organic matter in residual substance is detected, testing result is：The content of organic matter is less than 2%.
Step 2
By volume, the first liquid：Second liquid=2:1 mixing, then first carry out coarse filtration, carry out smart filtering again, essence
After filtering, it is concentrated in vacuo；The weight/mass percentage composition for obtaining water is 65% colloid；, the hole of filter screen used in the coarse filtration
Gap is 100 mesh, and the hole of filter screen is 260 mesh used in the essence filtering., when being concentrated in vacuo, it is -0.04Pa to control vacuum
(meter reading is -0.04Pa)；It is 90 DEG C to control temperature.
Step 3
It is placed in after carrying out filtration treatment to colloid obtained by step 2 in the concentration pan of sandwich, hot water heating is led into interlayer
To boiling, (before heating, colloid obtained by step 2 after filtering per ton, the area control with air contact surfaces is 6.28m2) stirring,
Remove surface offscum, impurity；When the water content in colloid is 30-35wt%, the soya-bean oil, yellow rice wine and the rock sugar that add after filtering
Water；Continue to heat, when the water content in colloid is 23-25wt%, stop heating；After continuing stirring 1 hour, glue is received at 60 DEG C
Fill basin；After receiving glue filling basin, in 4 DEG C of gels；Design size carries out cutting glue after gel, obtains blob of viscose；It is total by colloid obtained by step 2
The 2% of quality adds soya-bean oil；Yellow rice wine is added by 0.1% of colloid gross mass obtained by step 2；By the total matter of colloid obtained by step 2
The 10% of amount adds rock sugar；
Step 4
By blob of viscose obtained by step 3, a length of 97mm, a width of 42mm, the thickness 6mm of gained blob of viscose., it is placed in 4 DEG C of refrigerating chamber
After interior refrigeration 8 hours (air humidity of refrigerating chamber be 70%), glue processing of drying in the air is carried out；After the glue that dries in the air processing, carried out in D levels clean area
Dry, packaging, obtain finished product；Air humidity in the refrigerating chamber is 65%；It is 18 DEG C that the glue that dries in the air processing, which controls temperature, humidity is
60%th, the time is 15 days；The temperature of the drying is 30 DEG C, the time is 12 days.
In step 4, after drying process, the light transmittance of blob of viscose is OD3.75.
In step 4, gained finished product, the ratio for taking 10g warm water is matched somebody with somebody in 1g finished products, finished product is added in warm water, stirred,
After 45 seconds, it is completely dissolved；The temperature of the warm water is 38-40 DEG C.
The present embodiment, in step 3, before soya-bean oil, yellow rice wine, rock sugar is added, with quality * (the 1- colloid reclaimed waters of gained colloid
Weight/mass percentage composition) extract in/step 1 before donkey hide dry weight=20.85%.(i.e. rate of gum output is 20.85%)
This present embodiment, in step 3.Before adding soya-bean oil, yellow rice wine, rock sugar, with gained colloid, molecular weight is less than or equal to
The quality of 3000 organic matter account for organic matter in a word quality 97.3%.
A kind of preparation method of high grade of transparency donkey-hide gelatin of the present invention；In step 4, after drying process, the OD of blob of viscose is most
2.88。
The nitrogen content of finished product is detected, is 14.93%
Comparative example 1
Fresh donkey hide is taken, after removing flesh and blood, is crushed, under the system of opening wide, 2 ultrasonic extractions is carried out in 60 DEG C, carries every time
The time is taken (to detect the content of organic matter in residual substance, testing result is for 2 hours：The content of organic matter is 5.5%.)；So
Operated afterwards according to the step 2 of embodiment 1,3,4；Difference is：In step 3, glue obtained by step 2 after filtering per ton
Body, the area control with air contact surfaces are 15m2, and soya-bean oil is not added with, the temperature refrigerated in step 4 is 4 DEG C, the sky of refrigerating chamber
Air humidity degree is 65%；
After drying process, the OD values of blob of viscose are 4.75.
Gained finished product, the ratio for taking 10g warm water is matched somebody with somebody in 1g finished products, finished product is added in warm water, stirred, after 300 seconds,
It is completely dissolved；The temperature of the warm water is 38-40 DEG C.
The nitrogen content of finished product is detected, is 14.19%；Well below the content of N in embodiment 1.
Comparative example 2
The uniform embodiment 1 of other steps it is completely the same, difference is：
In step 1, heating-up temperature is 130 DEG C；In step 3, colloid obtained by step 2 after filtering per ton, with air contact
The area control in face is 1m2), and soya-bean oil is not added with, the temperature refrigerated in step 4 is 4 DEG C, the air humidity of refrigerating chamber is 65%；
The formed product is more difficult.
The nitrogen content of finished product is detected, is 13.95%；Well below the content of N in embodiment 1.This says to a certain extent
Bright nutriment has begun to be lost in.
Effect example
Using the products obtained therefrom of embodiment 1 as research object：Match somebody with somebody the ratio for taking 10g warm water in 1g finished products, finished product is added to temperature
In water.
Take 45 days by the dosage of each 10g sooner or later, mainly using the readme of Hengdong area crowd (crowd of 45-60 year) as
Standard, question and answer think there is improvement to insomnia and dreamful sleep disease, that is, thought to be effective, invalid without being improved as；With the further consultation result after 90 days
It is defined.Using 80 people as one group (each 40 people of men and women)；5 groups of investigations are carried out, it the results are shown in Table 1；
Table 1
From table 1, average effectiveness level is calculated as 63%.
Using the products obtained therefrom of comparative example 1 as research object：Match somebody with somebody the ratio for taking 10g warm water in 1g finished products, finished product is added to temperature
In water.
Take 45 days by the dosage of each 10g sooner or later, mainly using the readme of Hengdong area crowd (crowd of 45-60 year) as
Standard, question and answer think there is improvement to insomnia and dreamful sleep disease, that is, thought to be effective, invalid without being improved as；With the further consultation result after 90 days
It is defined.Using 80 people as one group (each 40 people of men and women)；5 groups of investigations are carried out, it the results are shown in Table 2；
Table 2
From table 1, average effectiveness level is calculated as 56.25%.
From table 1,2 as can be seen that in 45 days, take the donkey-hide gelatin of Isodose, but still have gap in effect, then from
For side illustration products obtained therefrom of the present invention for comparative example 1, its assimilation effect is more superior.
Claims (10)
- A kind of 1. preparation method of high grade of transparency donkey-hide gelatin；It is characterized in that；Comprise the steps：Step 1After donkey hide impurity elimination, soaked 5-10 days in 20-35 DEG C under water sealing condition；After shaving, broken, washing in mass ratio, water： Donkey hide=4-6:1；Water is added into the donkey hide taken, after adding water, under air-proof condition, will warm up 105-120 DEG C；Stirring carries Take 15-20 hours；Liquid is released, obtains the first liquid, residual residue in container；Water is added in toward residual residue, in sealing strip Under part, 105-120 DEG C will warm up；Stirring extraction 15-20 hours, liquid is released, obtains second liquid；After adding water, container Filling rate is 40-50%；Step 2Coarse filtration is first carried out to the first liquid and second liquid and then carries out smart filtering, after essence filtering, is concentrated in vacuo； The thick glue liquid that weight/mass percentage composition to water is 48-52%；Step 3It is placed in the concentrator of open type after colloid obtained by step 2 is carried out into filtration treatment, before heating, is walked after filtering per ton Rapid two gained colloid, the area control with air contact surfaces are 3.14-7.065m2；It is heated to seething with excitement, stirs, removes surface and float Foam, impurity；When the water content in colloid is 33-36%, the soya-bean oil, yellow rice wine and the rock sugar water that add after filtering；Continue to stir Heating, when the water content in colloid is 24-26wt%, stop heating；Continue after stirring 0.5-1.5 hours, in 23-26 DEG C of receipts Glue fills basin；After receiving glue filling basin, in 2-5 DEG C of gel；Design size carries out cutting glue after gel, obtains blob of viscose；Step 4Blob of viscose obtained by step 3 is placed in 1-5 DEG C of refrigerating chamber after refrigeration 6-10 hours, carries out glue processing of drying in the air；The glue that dries in the air processing Afterwards, it is dried in D level clean areas, watt glue shaping, re-dry, rubber, lettering, packaging, obtains finished product；In the refrigerating chamber Air humidity is 50-70%；To control temperature is 16-25 DEG C for the glue that dries in the air processing, humidity 50-65%, time are 7-15 days；It is described dry Dry temperature is 25-30 DEG C, the time is 7-15 days；Described watt of glue is shaped as film being neatly stacked in case, and closed 20-28 is small When, then show the glue that dries in the air；The temperature of re-dry is 25-35 DEG C, the time is 5-10 days.
- A kind of 2. preparation method of high grade of transparency donkey-hide gelatin according to claim 1；It is characterized in that：Heating in step 1 Temperature is 105-110 DEG C.
- A kind of 3. preparation method of high grade of transparency donkey-hide gelatin according to claim 1；It is characterized in that：The place of production of the donkey hide It is at least one in northeast, Xinjiang or Gansu；In step 2, the hole of filter screen used in the coarse filtration is 100 mesh；In step 2, the hole of filter screen is 260 mesh used in the essence filtering.
- A kind of 4. preparation method of high grade of transparency donkey-hide gelatin according to claim 1；It is characterized in that：In step 2, carry out During vacuum concentration, it is -0.02~-0.06Pa to control vacuum；It is 80-90 DEG C to control temperature.
- A kind of 5. preparation method of high grade of transparency donkey-hide gelatin according to claim 1；It is characterized in that in step 3, by step The 1.8-2.2% of two gained colloid gross masses, it is preferably 2% addition soya-bean oil；By the 0.08- of colloid gross mass obtained by step 2 0.12%th, it is preferably 0.1% addition yellow rice wine；Rock sugar is added by the 8-12% of step 2 gained colloid gross mass, preferably 10%.
- A kind of 6. preparation method of high grade of transparency donkey-hide gelatin according to claim 5；It is characterized in that in step 3, by step The 2% of two gained colloid gross masses adds soya-bean oil；Yellow rice wine is added by 0 0.1% of colloid gross mass obtained by step 2；By step The 10% of two gained colloid gross masses adds rock sugar.
- A kind of 7. preparation method of high grade of transparency donkey-hide gelatin according to claim 1；It is characterized in that：In step 3, adding Before entering soya-bean oil, yellow rice wine, rock sugar, before being extracted in quality * (weight/mass percentage composition of 1- colloid reclaimed waters)/step 1 of gained colloid Dry weight=25-40% of donkey hide.
- A kind of 8. preparation method of high grade of transparency donkey-hide gelatin according to claim 1；It is characterized in that：In step 3, add Before soya-bean oil, yellow rice wine, rock sugar, with gained colloid, the quality of organic matter of the molecular weight less than or equal to 3000 accounts for organic matter matter in a word The 97-98.5% of amount.
- A kind of 9. preparation method of high grade of transparency donkey-hide gelatin according to claim 1；It is characterized in that：In step 4, through dry After dry processing, the OD values of blob of viscose are 2.0-3.0.
- A kind of 10. preparation method of high grade of transparency donkey-hide gelatin according to claim 1；It is characterized in that：In step 4, gained finished product, the ratio for taking 10g warm water is matched somebody with somebody in 1g finished products, finished product is added in warm water, stirred, 30-50 After second, it is completely dissolved；The temperature of the warm water is 38-40 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710772478.XA CN107668688A (en) | 2017-08-31 | 2017-08-31 | A kind of preparation method of high grade of transparency donkey-hide gelatin |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710772478.XA CN107668688A (en) | 2017-08-31 | 2017-08-31 | A kind of preparation method of high grade of transparency donkey-hide gelatin |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107668688A true CN107668688A (en) | 2018-02-09 |
Family
ID=61135380
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710772478.XA Pending CN107668688A (en) | 2017-08-31 | 2017-08-31 | A kind of preparation method of high grade of transparency donkey-hide gelatin |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107668688A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113679037A (en) * | 2021-08-25 | 2021-11-23 | 陈梅 | Method for purifying crude gelatin in donkey-hide gelatin preparation |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1840000A (en) * | 2006-01-20 | 2006-10-04 | 哈尔滨绿色春天食品有限公司 | Nutrition oral liquor |
| CN101559078A (en) * | 2009-05-25 | 2009-10-21 | 山东华信制药集团股份有限公司 | Glue series medicine |
| CN104351793A (en) * | 2014-11-27 | 2015-02-18 | 赵向阳 | Preparation process of transparent high-purity donkey-hide gelatin |
| CN105901535A (en) * | 2016-04-14 | 2016-08-31 | 旌德县马家溪生态农业开发有限公司 | Health-preserving donkey-hide gelatin and processing method thereof |
-
2017
- 2017-08-31 CN CN201710772478.XA patent/CN107668688A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1840000A (en) * | 2006-01-20 | 2006-10-04 | 哈尔滨绿色春天食品有限公司 | Nutrition oral liquor |
| CN101559078A (en) * | 2009-05-25 | 2009-10-21 | 山东华信制药集团股份有限公司 | Glue series medicine |
| CN104351793A (en) * | 2014-11-27 | 2015-02-18 | 赵向阳 | Preparation process of transparent high-purity donkey-hide gelatin |
| CN105901535A (en) * | 2016-04-14 | 2016-08-31 | 旌德县马家溪生态农业开发有限公司 | Health-preserving donkey-hide gelatin and processing method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113679037A (en) * | 2021-08-25 | 2021-11-23 | 陈梅 | Method for purifying crude gelatin in donkey-hide gelatin preparation |
| CN113679037B (en) * | 2021-08-25 | 2024-08-20 | 陈梅 | Crude gelatin purification method in donkey-hide gelatin preparation |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103756844B (en) | Functional compound berry wine and production method thereof | |
| CN102860550A (en) | Functional beverage having functions of tonifying kidney, boosting virility and raising immunity and preparation method thereof | |
| CN102676341A (en) | Method for producing flavone-rich hawthorn wine | |
| CN103931839A (en) | Clear sugar-free tartary buckwheat tea and production method thereof | |
| CN103146536B (en) | Method for brewing bamboo health-care wine by high concentration bamboo juice | |
| CN102273625B (en) | Sugar-free American ginseng donkey-hide gelatin sheet and production technology thereof | |
| CN106721699A (en) | A kind of sobering-up beverage and preparation method thereof | |
| CN107373652A (en) | A kind of preparation method of the high deer horn glue of transparency | |
| CN107668688A (en) | A kind of preparation method of high grade of transparency donkey-hide gelatin | |
| CN107440053A (en) | A kind of donkey-hide gelatin colla carapacis et plastri testudinis deer horn glue walnut cake and preparation method thereof | |
| RU2316582C2 (en) | Method for producing strong drinks | |
| CN104920927B (en) | A kind of preparation method of lemon jam | |
| CN101884426B (en) | Method and device for removing red jujube peel | |
| CN109078024B (en) | Preparation method of deer glue as traditional Chinese medicine decoction pieces | |
| CN110037215A (en) | A kind of preparation method of highland barley bran beverage | |
| CN106135984B (en) | Thickened red jujube pulp and production process thereof | |
| CN104489803A (en) | Making method of health beverage containing red dates and ginger juice | |
| CN107440105A (en) | A kind of preparation method of high grade of transparency colla carapacis et plastri testudinis | |
| CN107397214A (en) | A kind of high grade of transparency donkey-hide gelatin prepares production line | |
| CN106539075A (en) | A kind of preparation method of efficient absorption sea cucumber nutrient buccal tablet | |
| CN107536040A (en) | A kind of high grade of transparency colla carapacis et plastri testudinis prepares production line | |
| CN107397184A (en) | A kind of donkey-hide gelatin walnut cake and preparation method thereof | |
| CN107412427A (en) | A kind of Control for Ejiao Buxue particle and preparation method thereof | |
| TW200810704A (en) | Fermentation, extraction and concentration method for nutrients of green plum flesh | |
| CN107279822A (en) | A kind of preparation method of multicomponent sea cucumber nutrient powder |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180209 |
|
| RJ01 | Rejection of invention patent application after publication |