CN101559078A - Glue series medicine - Google Patents
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- CN101559078A CN101559078A CNA2009100154460A CN200910015446A CN101559078A CN 101559078 A CN101559078 A CN 101559078A CN A2009100154460 A CNA2009100154460 A CN A2009100154460A CN 200910015446 A CN200910015446 A CN 200910015446A CN 101559078 A CN101559078 A CN 101559078A
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Abstract
The invention discloses a nutritious glue series medicine for enriching blood, nourishing blood and stop bleeding, which is characterized by mainly comprising the following raw materials based on part by weight: 100 parts of initial rubbers, 3-5 parts of sugar candies, 1-3 parts of soybean oil and 0.5-3 parts of yellow wine; the initial rubber is donkey skin, buckhorn or tortoise shell. The glue series medicine is prepared by the following processes: raw material soaking, washing, extracting, glue extract precipitating, gelatinating, glue cutting, glue drying and frictionating. The glue series medicine has the advantages of good healing effect, simple administration, low price and the like, meanwhile, the glue series medicine has little side effect, has the functions of nourishing blood and enriching blood and is worthy of clinical spread.
Description
(1) technical field
The present invention relates to a kind of Chinese medicine, particularly a kind of glue series class nourishing glue series medicine of enriching blood, nourish blood, stop blooding belongs to the medicine preparation field.
(2) background technology
Along with the quickening of people's rhythm of life and the enhancing of operating pressure, the sub-health state crowd is more and more.Modern Chinese medicine think disease generation, develop and lapse to the growth and decline of depending on good and evil, closely related with body's immunological function, thus the principle of mainly curing the disease of " strengthening vital QI to eliminate pathogenic factors " has been proposed.Chinese medicine mostly is natural drug, property of medicine gentleness, and untoward reaction is few, much the Chinese medicine of " strengthening the body resistance " is by conditioning viscera, benefiting vital QI and blood, supporing yang YIN nourishing, they are had an effect to the different links of immunologic process, are coordinating the body whole machine balancing, and enhancing body resistance against diseases aspect has unique curative effect.
(3) summary of the invention
The present invention provides a kind of steady quality, safety, effective, few side effects in order to remedy the deficiencies in the prior art, has and nourishes blood, the glue series medicine of blood tonification effect.
The present invention is achieved through the following technical solutions:
A kind of glue series medicine is characterized in that: mainly be to be made by the raw material of following parts by weight: 100 parts of raw material glue, 3～5 parts in crystal sugar, 1～3 part in Oleum Glycines, 0.5～3 part of yellow wine; Described raw material glue is donkey skin, Cornu Cervi or Carapax Et Plastrum Testudinis.
Glue series medicine of the present invention, this medicine series are to be made by following preparation technology: raw material soaking, cleaning, extraction, glue juice precipitation, concentrate, gel, cut glue, the glue that dries in the air, rubber.
Glue series clinical drug observation of curative effect of the present invention:
(1) physical data:
The observation case is the outpatient who seeks medical advice to the Heze City hospital of traditional Chinese hospital over 2008 in 2005, and totally 83 examples are divided into two groups at random, and 48 examples are organized in treatment, matched group 35 examples.Minimum 26 years old of age, maximum 47 years old, average 37 years old.83 routine patient's diseases are all seen the vaginal hemorrhage of non-menstruation, and are not to the utmost dripping, and firmly the bowel movement bleeding from anus is more than cruelly down, and the pale complexion of holding concurrently is moving then breathe hard, vexed hectic fever, and constipation with dry stool, tongue fur is light red, thready pulse.The metrorrhagia that 83 routine patients all cause with modern medicine method eliminating makings disease or systemic disease, tcm diagnosis is the metrorrhagia of type of deficiency of both QI and YIN.Differences such as two groups of patient ages, the course of disease, disease there are no significant meaning.Has comparability.
(2), Therapeutic Method: get Colla Corii Asini 15 grams that Shandong Huaxin Pharmaceutical Group Corporation adopts embodiment 4 methods to produce, boiled water molten or add boiled water with 10 milliliters of yellow wine and steam to stew molten is taken the pungent pyretic toxicity diet of period in a medicine fasting before sleeping every night, menstrual phase needn't drug withdrawal, and 15 days is a course of treatment.
(3), the course of treatment evaluation criteria: according to " Gynecology of Chinese Medicine " diagnostic criteria with " omni-doctor's application manual " relevant metrorrhagia.Determine its criterion of therapeutical effect: cure: menstrual cycle 26--28 days, menstrual phase 3-4 days, amount of bleeding 30-40 milliliter, no hemorrhage and oozing of blood between the menstrual cycle, firmly bowel movement does not have hemorrhage; Effectively: menstrual cycle, menstrual phase, normal through measuring; Invalid: non-menstrual period are more than or not to the utmost dripping cruelly down.
(4), therapeutic outcome: two groups of clinical efficacies relatively see the following form.48 examples are organized in treatment, cure 41 examples, effective 4 examples, invalid 3 examples, total effective rate 93.75%; Matched group 35 examples are cured 22 examples, effective 4 examples, invalid 9 examples, total effective rate 74.28%.Two groups relatively, and the total effective rate difference has statistical significance.
Show-two groups of clinical efficacies relatively (example, %)
| Group | Cure | Effectively | Invalid | Total effective rate |
| The treatment group | 41 | 4 | 3 | 93.75 |
| Matched group | 22 | 4 | 9 | 74.28 |
Annotate: P＜0.05 is compared with matched group in the treatment back
(5), sum up: metrorrhagia is a deficiency of both QI and YIN, dashes to appoint and loses admittedly, causes and the capable arteries and veins of blood is outer.And the organic disease of eliminating modern medical diagnosis or the metrorrhagia that systemic disease causes.Colla Corii Asini has hemostasis, enriches blood, and the effect of nourishing YIN and moistening the lung is assumed overall responsibility for and controlled the metrorrhagia plug flow, and the restoration of old ways three therapeutic methods of traditional Chinese medicine so single have good effect, take advantages such as simple, inexpensive with promptly having good effect, is worth clinical expansion.Inflammation, the metrorrhagia that organic disease such as tumor or systemic disease cause is then at etiological treatment.Colla Corii Asini character is sticky, hinders digestion, weakness of the spleen and stomach, and the vomiting person of having loose bowels all suspends and takes.
The present invention has good effect, takes advantages such as simple, inexpensive, simultaneously few side effects, have and nourish blood, blood tonification effect is worth clinical expansion.
(4) description of drawings
The present invention is further illustrated below in conjunction with accompanying drawing.
Accompanying drawing is a process flow diagram of the present invention.
(5) specific embodiment
Embodiment 1, accompanying drawing are a kind of specific embodiment of the present invention.1., remove impurity and dis-medicinal part in the Cornu Cervi this embodiment adopts following steps:, take by weighing the Cornu Cervi 100kg fermentation vat of packing into, soaked 7 days, change water every day once, go out the pond, cleaned 3 hours.2., extract: extract the water that adds 0.8 times of amount for the first time, extract pressure and remain on 0.16mpa, extract temperature at 100 ℃, extracted 95 minutes, and extracted the water that adds 0.8 times of amount of skin amount for the second time, extract pressure at 0.12mpa, extract temperature at 100 ℃, extracted the glue juice filtered while hot of extraction, merging filtrate 70 minutes.3., glue juice precipitation, concentrated: glue juice precipitates 2.0 hours in settling tank, supernatant concentrates.Thickening temperature should remain on 65 ℃, steam pressure remains on 0.06Mpa, the relative density that is concentrated into glue juice is 1.05 (70 ℃), the filtration of glue juice is transferred in the steam-jacked kettle, continuing hydrolysis concentrates, and when hydrolysis concentrates, constantly carry assortedly, and remove floating foam in upper strata and impurity at any time, end when to send out clear shinny to glue juice.Be filtered to the homogenizing jar, continue to concentrate,, stir with crystal sugar 5kg, Oleum Glycines 1.5kg and yellow wine 2kg.Plastic emitting when continuing to be concentrated into water content 25.5%.4., gel, cut glue: when gel begins temperature with 13 ℃, refrigerated temperature with 1 ℃, freezing 4.0 hours.Jiao Tuo after solidifying should not feel like jelly, and presses no significant depressions phenomenon with hands.To solidify the stick together bulk of cutting growth 3.6cm, wide 2.5cm, thick about 0.6cm of good glue.5., the glue that dries in the air: glue dries in the air for the first time: turn over glue after 1～2 day; Vexed glue after 1～3 day; Vexed glue is upright case after 1～3 day; Plastic emitting after 1～2 day; Glue dries in the air for the second time: turn over glue after 3～6 days; Carried out vexed glue in 3～6 days; Upright case after 2～3 days; Fall case after 2 days; Plastic emitting after 2～3 days; Glue for the third time dries in the air: turn over glue after 3～6 days; Carried out vexed glue in 3～6 days; Upright case after 2～3 days; Fall case after 2 days; Plastic emitting after 2～3 days.Dry in the air and received glue to the water content of blob of viscose at 11.5% o'clock, blob of viscose should reach surfacing, phenomenons such as no arrisdefect, scarce limit.6., rubber: rubber is polished the blob of viscose surface with 78 ℃ purified water, dries, and the blob of viscose after the wiping should reach surface-brightening, and silking is straight and obvious, oil stains-less, fingerprint, water wave, blister.7., pack, put in storage after the assay was approved.
Usage and dosage: molten is converted clothes, 3～9g.
Embodiment 2,1., remove impurity and dis-medicinal part in the Cornu Cervi, take by weighing the Cornu Cervi 100kg fermentation vat of packing into, soaked 5 days, change water every day once, go out the pond, cleaned 2.5 hours.2., extract: extract the water that adds 1.0 times of amounts for the first time, extract pressure and remain on 0.18mpa, extract temperature at 105 ℃, extracted 105 minutes, and extracted the water that adds 0.9 times of amount of skin amount for the second time, extract pressure at 0.16mpa, extract temperature at 90 ℃, extracted the glue juice filtered while hot of extraction, merging filtrate 60 minutes.3., glue juice precipitation, concentrated: glue juice precipitates 2.5 hours in settling tank, supernatant concentrates.Thickening temperature should remain on 75 ℃, steam pressure remains on 0.08Mpa, the relative density that is concentrated into glue juice is 1.10 (70 ℃), the filtration of glue juice is transferred in the steam-jacked kettle, continuing hydrolysis concentrates, and when hydrolysis concentrates, constantly carry assortedly, and remove floating foam in upper strata and impurity at any time, end when to send out clear shinny to glue juice.Be filtered to the homogenizing jar, continue to concentrate,, stir with crystal sugar 5kg, Oleum Glycines 1.5kg and yellow wine 2kg.Plastic emitting when continuing to be concentrated into water content 26.5%.4., gel, cut glue: when gel begins temperature with 16 ℃, refrigerated temperature with 2 ℃, freezing 5.0 hours.Jiao Tuo after solidifying should not feel like jelly, and presses no significant depressions phenomenon with hands.To solidify the stick together bulk of cutting growth 3.6cm, wide 2.5cm, thick about 0.6cm of good glue.5., the glue that dries in the air: glue dries in the air for the first time: turn over glue after 1～2 day; Vexed glue after 1～3 day; Vexed glue is upright case after 1～3 day; Plastic emitting after 1～2 day; Glue dries in the air for the second time: turn over glue after 3～6 days; Carried out vexed glue in 3～6 days; Upright case after 2～3 days; Fall case after 2 days; Plastic emitting after 2～3 days; Glue for the third time dries in the air: turn over glue after 3～6 days; Carried out vexed glue in 3～6 days; Upright case after 2～3 days; Fall case after 2 days; Plastic emitting after 2～3 days.Dry in the air and received glue to the water content of blob of viscose at 11.5% o'clock, blob of viscose should reach surfacing, phenomenons such as no arrisdefect, scarce limit.6., rubber: rubber is polished the blob of viscose surface with 80 ℃ purified water, dries, and the blob of viscose after the wiping should reach surface-brightening, and silking is straight and obvious, oil stains-less, fingerprint, water wave, blister.7., pack, put in storage after the assay was approved.
Usage and dosage: molten is converted clothes, 3～9g.
Embodiment 3,1., remove impurity and dis-medicinal part in the Cornu Cervi, take by weighing the Cornu Cervi 100kg fermentation vat of packing into, soaked 6 days, change water every day once, go out the pond, cleaned 2.0 hours.2., extract: extract the water that adds 0.9 times of amount for the first time, extract pressure and remain on 0.17mpa, extract temperature at 95 ℃, extracted 100 minutes, and extracted the water that adds 0.85 times of amount of skin amount for the second time, extract pressure at 0.14mpa, extract temperature at 95 ℃, extracted the glue juice filtered while hot of extraction, merging filtrate 80 minutes.3., glue juice precipitation, concentrated: glue juice precipitates 3.0 hours in settling tank, supernatant concentrates.Thickening temperature should remain on 85 ℃, steam pressure remains on 0.09Mpa, the relative density that is concentrated into glue juice is 1.15 (70 ℃), the filtration of glue juice is transferred in the steam-jacked kettle, continuing hydrolysis concentrates, and when hydrolysis concentrates, constantly carry assortedly, and remove floating foam in upper strata and impurity at any time, end when to send out clear shinny to glue juice.Be filtered to the homogenizing jar, continue to concentrate,, stir with crystal sugar 5kg, Oleum Glycines 1.5kg and yellow wine 2kg.Plastic emitting when continuing to be concentrated into water content 27.5%.4., gel, cut glue: when gel begins temperature with 17 ℃, refrigerated temperature with 3 ℃, freezing 3.0 hours.Jiao Tuo after solidifying should not feel like jelly, and presses no significant depressions phenomenon with hands.To solidify the stick together bulk of cutting growth 3.6cm, wide 2.5cm, thick about 0.6cm of good glue.5., the glue that dries in the air: glue dries in the air for the first time: turn over glue after 1～2 day; Vexed glue after 1～3 day; Vexed glue is upright case after 1～3 day; Plastic emitting after 1～2 day; Glue dries in the air for the second time: turn over glue after 3～6 days; Carried out vexed glue in 3～6 days; Upright case after 2～3 days; Fall case after 2 days; Plastic emitting after 2～3 days; Glue for the third time dries in the air: turn over glue after 3～6 days; Carried out vexed glue in 3～6 days; Upright case after 2～3 days; Fall case after 2 days; Plastic emitting after 2～3 days.Dry in the air and received glue to the water content of blob of viscose at 12.5% o'clock, blob of viscose should reach surfacing, phenomenons such as no arrisdefect, scarce limit.6., rubber: rubber is polished the blob of viscose surface with 82 ℃ purified water, dries, and the blob of viscose after the wiping should reach surface-brightening, and silking is straight and obvious, oil stains-less, fingerprint, water wave, blister.7., pack, put in storage after the assay was approved.
Embodiment 4: the raw material by following parts by weight is made Colla Corii Asini: 100 parts of donkey skin, 3 parts in crystal sugar, 2.4 parts in Oleum Glycines, 0.5 part of yellow wine;
1., remove impurity and dis-medicinal part in the raw material donkey skin preparation method of this Colla Corii Asini adopts following steps:, the donkey skin that the takes by weighing recipe quantity fermentation vat of packing into, soak 4～5 days, every day change water once, stir, go out the pond, the unhairing rate reaches more than 70%, cleans 4～5 hours.2., the skin of scalding: will soak, cleaned donkey skin is packed in the rotary spherical digester, adds alkali and water, feeds steam, 60 ℃ of insulations, the skin twice of scalding, each 3～6 minutes.3., extract: extract the water that adds 0.8～1.0 times of amount for the first time, extract pressure and remain on 0.08mpa～0.09mpa, extract temperature at 90～105 ℃, extracted 90～110 minutes, extract the water that adds 0.8～0.9 times of amount of skin amount for the second time, extract pressure below 0.10mpa, extract temperature at 90～100 ℃, extracted 60～90 minutes, and extracted the water that adds 0.5～0.8 times of amount of skin amount for the third time, extract pressure below 0.10mpa, extract temperature at 90～100 ℃, extracted the glue juice filtered while hot of extraction, merging filtrate 15～45 minutes.4., glue juice precipitation, concentrated: glue juice precipitates 1.5～3.0 hours in settling tank, supernatant concentrates.Thickening temperature should remain on 60～85 ℃, steam pressure remains on 0.05～0.1Mpa, the relative density that is concentrated into glue juice is about about 1.10 (70 ℃), the filtration of glue juice is transferred in the steam-jacked kettle, continuing hydrolysis concentrates, and when hydrolysis concentrates, constantly carry assortedly, and remove floating foam in upper strata and impurity at any time, end when to send out clear shinny to glue juice.Be filtered to the homogenizing jar, continue to concentrate, add crystal sugar, Oleum Glycines and the yellow wine of recipe quantity, stir.Continue to be concentrated into water content and be not higher than plastic emitting in 28.0% o'clock.5., gel, cut glue: when gel begins temperature with 12 ℃～18 ℃, refrigerated temperature with-2 ℃～3 ℃, freezing 2～6 hours.Jiao Tuo after solidifying should not feel like jelly, and presses no significant depressions phenomenon with hands.To solidify the stick together bulk of cutting growth 3.6cm, wide 2.5cm, thick about 0.6cm of good glue.6., the glue that dries in the air: glue dries in the air for the first time: turn over glue after 1～2 day; Vexed glue after 1～3 day; Vexed glue is upright case after 1～3 day; Plastic emitting after 1～2 day; Glue dries in the air for the second time: turn over glue after 3～6 days; Carried out vexed glue in 3～6 days; Upright case after 2～3 days; Fall case after 2 days; Plastic emitting after 2～3 days; Glue for the third time dries in the air: turn over glue after 3～6 days; Carried out vexed glue in 3～6 days; Upright case after 2～3 days; Fall case after 2 days; Plastic emitting after 2～3 days.Dry in the air and receive glue 13.5% when following to the water content of blob of viscose, blob of viscose should reach surfacing, no arrisdefect, lacks phenomenon such as limit.7., rubber: rubber is polished the blob of viscose surface greater than 75 ℃ purified water with temperature, dries, and the blob of viscose after the wiping should reach surface-brightening, and silking is straight and obvious, oil stains-less, fingerprint, water wave, blister.8., pack, put in storage after the assay was approved.
Embodiment 5: the raw material by following parts by weight is made Colla Plastri Testudinis: 100 parts of Carapax Et Plastrum Testudiniss, 3 parts in crystal sugar, 1 part in Oleum Glycines, 0.5 part of yellow wine;
1., remove impurity and dis-medicinal part in the raw material Carapax Et Plastrum Testudinis preparation method of this Colla Plastri Testudinis adopts following method:, the Carapax Et Plastrum Testudinis that the takes by weighing recipe quantity fermentation vat of packing into soaked 5～7 days, changed water every day once, went out the pond, cleaned 2～3 hours.2., extract: extract: extract the water that adds 0.8～1.0 times of amount for the first time, extract pressure and remain on 0.16mpa～0.18mpa, extract temperature at 90～105 ℃, extracted 90～110 minutes, and extracted the water that adds 0.8～0.9 times of amount of skin amount for the second time, extract pressure at 0.12mpa～0.16mpa, extract temperature at 90～100 ℃, extracted the glue juice filtered while hot of extraction, merging filtrate 60～90 minutes.3., glue juice precipitation, concentrated: glue juice precipitates 1.5～3.0 hours in settling tank, supernatant concentrates.Thickening temperature should remain on 60～85 ℃, steam pressure remains on 0.05～0.1Mpa, the relative density that is concentrated into glue juice is about about 1.10 (70 ℃), the filtration of glue juice is transferred in the steam-jacked kettle, continuing hydrolysis concentrates, and when hydrolysis concentrates, constantly carry assortedly, and remove floating foam in upper strata and impurity at any time, end when to send out clear shinny to glue juice.Be filtered to the homogenizing jar, continue to concentrate, add crystal sugar, Oleum Glycines and the yellow wine of recipe quantity, stir.Continue to be concentrated into water content and be not higher than plastic emitting in 28.0% o'clock.4., gel, cut glue: when gel begins temperature with 12 ℃～18 ℃, refrigerated temperature with-2 ℃～3 ℃, freezing 2～6 hours.Jiao Tuo after solidifying should not feel like jelly, and presses no significant depressions phenomenon with hands.To solidify the stick together bulk of cutting growth 3.6cm, wide 2.5cm, thick about 0.6cm of good glue.5., the glue that dries in the air: glue dries in the air for the first time: turn over glue after 1～2 day; Vexed glue after 1～3 day; Vexed glue is upright case after 1～3 day; Plastic emitting after 1～2 day; Glue dries in the air for the second time: turn over glue after 3～6 days; Carried out vexed glue in 3～6 days; Upright case after 2～3 days; Fall case after 2 days; Plastic emitting after 2～3 days; Glue for the third time dries in the air: turn over glue after 3～6 days; Carried out vexed glue in 3～6 days; Upright case after 2～3 days; Fall case after 2 days; Plastic emitting after 2～3 days.Dry in the air and receive glue 13.5% when following to the water content of blob of viscose, blob of viscose should reach surfacing, no arrisdefect, lacks phenomenon such as limit.6., rubber: rubber is polished the blob of viscose surface greater than 75 ℃ purified water with temperature, dries, and the blob of viscose after the wiping should reach surface-brightening, and silking is straight and obvious, oil stains-less, fingerprint, water wave, blister.7., pack, put in storage after the assay was approved.
Claims (5)
1. a glue series medicine is characterized in that: mainly be to be made by the raw material of following parts by weight: 100 parts of raw material glue, 3～5 parts in crystal sugar, 1～3 part in Oleum Glycines, 0.5～3 part of yellow wine; Described raw material glue is donkey skin, Cornu Cervi or Carapax Et Plastrum Testudinis.
2, glue series medicine according to claim 1 is characterized in that: this medicine series is to be made by following preparation technology: raw material soaking, cleaning, extraction, glue juice precipitation, concentrate, gel, cut glue, the glue that dries in the air, rubber.
3, glue series medicine according to claim 1, it is characterized in that: the raw material by following parts by weight is made Colla Corii Asini: 100 parts of donkey skin, 3 parts in crystal sugar, 2.4 parts in Oleum Glycines, 0.5 part of yellow wine; 1., remove impurity and dis-medicinal part in the raw material donkey skin this Colla Corii Asini is made by being prepared as follows method:, the donkey skin that the takes by weighing recipe quantity fermentation vat of packing into, soak 4～5 days, every day change water once, stir, go out the pond, the unhairing rate reaches more than 70%, cleans 4～5 hours; 2., the skin of scalding: will soak, cleaned donkey skin is packed in the rotary spherical digester, adds alkali and water, feeds steam, 60 ℃ of insulations, the skin twice of scalding, each 3～6 minutes; 3., extract: extract the water that adds 0.8～1.0 times of amount for the first time, extract pressure and remain on 0.08～0.09mpa, extract temperature at 90～105 ℃, extracted 90～110 minutes, extract the water that adds 0.8～0.9 times of amount of skin amount for the second time, extract pressure below 0.10mpa, extract temperature at 90～100 ℃, extracted 60～90 minutes, and extracted the water that adds 0.5～0.8 times of amount of skin amount for the third time, extract pressure below 0.10mpa, extract temperature at 90～100 ℃, extracted the glue juice filtered while hot of extraction, merging filtrate 15～45 minutes; 4., glue juice precipitation, concentrated: glue juice precipitates 1.5～3.0 hours in settling tank, supernatant concentrates; Thickening temperature remains on 60～85 ℃, and steam pressure remains on 0.05～0.1Mpa, and the relative density that is concentrated into 70 ℃ in glue juice is 1.10 ± 0.10, glue juice is filtered be transferred in the steam-jacked kettle, continues hydrolysis and concentrates, and constantly carry assorted when hydrolysis concentrates; Be filtered to the homogenizing jar, continue to concentrate, add crystal sugar, Oleum Glycines and the yellow wine of recipe quantity, stir; Continue to be concentrated into water content and be not higher than plastic emitting in 28.0% o'clock; 5., gel, cut glue: when gel begins temperature with 12 ℃～18 ℃, refrigerated temperature with-2 ℃～3 ℃, freezing 2～6 hours; To solidify good Jiao Tuo and cut into bulk; 6., the glue that dries in the air: glue dries in the air for the first time: turn over glue after 1～2 day; Vexed glue after 1～3 day; Vexed glue is upright case after 1～3 day; Plastic emitting after 1～2 day; Glue dries in the air for the second time: turn over glue after 3～6 days; Carried out vexed glue in 3～6 days; Upright case after 2～3 days; Fall case after 2 days; Plastic emitting after 2～3 days; Glue for the third time dries in the air: turn over glue after 3～6 days; Carried out vexed glue in 3～6 days; Upright case after 2～3 days; Fall case after 2 days; Plastic emitting after 2～3 days; Dry in the air to the water content of blob of viscose and receive glue when following 13.5%; 7., rubber: rubber is polished the blob of viscose surface greater than 75 ℃ purified water with temperature, dries; 8., pack, put in storage after the assay was approved.
4, glue series medicine according to claim 1, it is characterized in that: the raw material by following parts by weight is made Colla Plastri Testudinis: 100 parts of Carapax Et Plastrum Testudiniss, 3 parts in crystal sugar, 1 part in Oleum Glycines, 0.5 part of yellow wine; 1., remove impurity and dis-medicinal part in the raw material Carapax Et Plastrum Testudinis this Colla Plastri Testudinis is made by being prepared as follows method:, the Carapax Et Plastrum Testudinis that the takes by weighing recipe quantity fermentation vat of packing into soaked 5～7 days, changed water every day once, went out the pond, cleaned 2～3 hours; 2., extract: extract the water that adds 0.8～1.0 times of amount for the first time, extract pressure and remain on 0.16mpa～0.18mpa, extract temperature at 90～105 ℃, extracted 90～110 minutes, and extracted the water that adds 0.8～0.9 times of amount of skin amount for the second time, extract pressure at 0.12mpa～0.16mpa, extract temperature at 90～100 ℃, extracted the glue juice filtered while hot of extraction, merging filtrate 60～90 minutes; 3., glue juice precipitation, concentrated: glue juice precipitates 1.5～3.0 hours in settling tank, supernatant concentrates; Thickening temperature remains on 60～85 ℃, and steam pressure remains on 0.05～0.1Mpa, and the relative density that is concentrated into 70 ℃ in glue juice is 1.10 ± 0.10, glue juice is filtered be transferred in the steam-jacked kettle, continues hydrolysis and concentrates, and constantly carry assorted when hydrolysis concentrates; Be filtered to the homogenizing jar, continue to concentrate, add crystal sugar, Oleum Glycines and the yellow wine of recipe quantity, stir; Continue to be concentrated into water content and be not higher than plastic emitting in 28.0% o'clock; 4., gel, cut glue: when gel begins temperature with 12 ℃～18 ℃, refrigerated temperature with-2 ℃～3 ℃, freezing 2～6 hours; To solidify good Jiao Tuo and cut into bulk; 5., the glue that dries in the air: glue dries in the air for the first time: turn over glue after 1～2 day; Vexed glue after 1～3 day; Vexed glue is upright case after 1～3 day; Plastic emitting after 1～2 day; Glue dries in the air for the second time: turn over glue after 3～6 days; Carried out vexed glue in 3～6 days; Upright case after 2～3 days; Fall case after 2 days; Plastic emitting after 2～3 days; Glue for the third time dries in the air: turn over glue after 3～6 days; Carried out vexed glue in 3～6 days; Upright case after 2～3 days; Fall case after 2 days; Plastic emitting after 2～3 days; Dry in the air to the water content of blob of viscose and receive glue when following 13.5%; 6., rubber: rubber is polished the blob of viscose surface greater than 75 ℃ purified water with temperature, dries; 7., pack, put in storage after the assay was approved.
5, glue series medicine according to claim 1, it is characterized in that: the raw material by following parts by weight is made Colla cornus cervi: 100 parts on Cornu Cervi, 5 parts in crystal sugar, 1.5 parts in Oleum Glycines, 2 parts of yellow wine; 1., remove impurity and dis-medicinal part in the raw material Cornu Cervi this Colla cornus cervi is made by being prepared as follows method:, the Cornu Cervi that the takes by weighing recipe quantity fermentation vat of packing into soaked 5～7 days, changed water every day once, went out the pond, cleaned 2～3 hours; 2., extract: extract the water that adds 0.8～1.0 times of amount for the first time, extract pressure and remain on 0.16mpa～0.18mpa, extract temperature 90～105, extracted 90～110 minutes, and extracted the water that adds 0.8～0.9 times of amount of skin amount for the second time, extract pressure at 0.12mpa～0.16mpa, extract temperature at 90～100 ℃, extracted 60～90 minutes, the glue juice of extraction filters, merging filtrate; 3., glue juice precipitation, concentrated: glue juice precipitates 1.5～3.0 hours in settling tank, supernatant concentrates, thickening temperature remains on 60～85 ℃, steam pressure remains on 0.05～0.1Mpa, the relative density that is concentrated into 70 ℃ in glue juice is 1.10 ± 0.10, the filtration of glue juice is transferred in the steam-jacked kettle, continues hydrolysis and concentrate; Be filtered to the homogenizing jar, continue to concentrate, add crystal sugar, Oleum Glycines and the yellow wine of recipe quantity, stir; Continue to be concentrated into water content and be not higher than plastic emitting in 28.0% o'clock; 4., gel, cut glue: when gel begins temperature with 12 ℃～18 ℃, refrigerated temperature with-2 ℃～3 ℃, freezing 2～6 hours; To solidify good Jiao Tuo and cut into bulk; 5., the glue that dries in the air: glue dries in the air for the first time: turn over glue after 1～2 day; Vexed glue after 1～3 day; Vexed glue is upright case after 1～3 day; Plastic emitting after 1～2 day; Glue dries in the air for the second time: turn over glue after 3～6 days; Carried out vexed glue in 3～6 days; Upright case after 2～3 days; Fall case after 2 days; Plastic emitting after 2～3 days; Glue for the third time dries in the air: turn over glue after 3～6 days; Carried out vexed glue in 3～6 days; Upright case after 2～3 days; Fall case after 2 days; Plastic emitting after 2～3 days; Dry in the air to the water content of blob of viscose and receive glue when following 13.5%; 6., rubber: rubber is polished the blob of viscose surface greater than 75 ℃ purified water with temperature, dries; 7., pack, put in storage after the assay was approved.
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| CNA2009100154460A CN101559078A (en) | 2009-05-25 | 2009-05-25 | Glue series medicine |
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| CNA2009100154460A CN101559078A (en) | 2009-05-25 | 2009-05-25 | Glue series medicine |
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| CN101869308A (en) * | 2010-06-11 | 2010-10-27 | 山东省农业科学院农产品研究所 | Ass bone gel |
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| CN103623000A (en) * | 2013-10-31 | 2014-03-12 | 山东东阿阿胶股份有限公司 | Instant fresh donkey-hide gelatin and preparation method thereof |
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| CN107551058A (en) * | 2017-08-31 | 2018-01-09 | 湖南东健药业有限公司 | A kind of donkey-hide gelatin colla carapacis et plastri testudinis hematinic ointment and preparation method thereof |
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| CN107981349A (en) * | 2017-12-12 | 2018-05-04 | 黎泽高 | A kind of preparation method of geoclemys reevesii |
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| CN108685949B (en) * | 2018-08-07 | 2020-05-12 | 河北君临药业有限公司 | Preparation process of tortoise-shell glue |
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| CN108635374A (en) * | 2018-08-08 | 2018-10-12 | 河北君临药业有限公司 | A kind of oxhide gelatin preparation process |
| CN109010370A (en) * | 2018-08-08 | 2018-12-18 | 河北君临药业有限公司 | A kind of extraction process of donkey-hide gelatin |
| CN109010370B (en) * | 2018-08-08 | 2022-01-25 | 河北君临药业有限公司 | Extraction process of donkey-hide gelatin |
| CN108904535A (en) * | 2018-08-09 | 2018-11-30 | 河北君临药业有限公司 | A kind of deer horn glue preparation method |
| CN108904535B (en) * | 2018-08-09 | 2022-01-25 | 河北君临药业有限公司 | Preparation method of antler glue |
| CN109078024B (en) * | 2018-10-25 | 2020-09-29 | 贵州广济堂药业有限公司 | Preparation method of deer glue as traditional Chinese medicine decoction pieces |
| CN109078024A (en) * | 2018-10-25 | 2018-12-25 | 贵州广济堂药业有限公司 | The preparation method of deer horn glue as the prepared slices of Chinese crude drugs |
| CN110353181A (en) * | 2019-05-07 | 2019-10-22 | 金晟中科(吉林)生物科技有限公司 | A kind of preparation process of pure deer horn glue |
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