CN107625651A - A kind of sanding sponge and preparation method thereof - Google Patents

A kind of sanding sponge and preparation method thereof Download PDF

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Publication number
CN107625651A
CN107625651A CN201710821298.6A CN201710821298A CN107625651A CN 107625651 A CN107625651 A CN 107625651A CN 201710821298 A CN201710821298 A CN 201710821298A CN 107625651 A CN107625651 A CN 107625651A
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China
Prior art keywords
sponge
particle
sanding sponge
preparation
konjaku powder
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Granted
Application number
CN201710821298.6A
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Chinese (zh)
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CN107625651B (en
Inventor
王晓军
陈怀新
潘启胜
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Wuhan Bibiweisha Biological Technology Co Ltd
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Wuhan Bibiweisha Biological Technology Co Ltd
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Priority to CN201710821298.6A priority Critical patent/CN107625651B/en
Publication of CN107625651A publication Critical patent/CN107625651A/en
Priority to PCT/CN2018/082707 priority patent/WO2019047525A1/en
Priority to EP18853388.9A priority patent/EP3679916B1/en
Application granted granted Critical
Publication of CN107625651B publication Critical patent/CN107625651B/en
Priority to US16/720,616 priority patent/US11529305B2/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0208Tissues; Wipes; Patches
    • AHUMAN NECESSITIES
    • A47FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
    • A47KSANITARY EQUIPMENT NOT OTHERWISE PROVIDED FOR; TOILET ACCESSORIES
    • A47K7/00Body washing or cleaning implements
    • A47K7/02Bathing sponges, brushes, gloves, or similar cleaning or rubbing implements
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0241Containing particulates characterized by their shape and/or structure
    • A61K8/0245Specific shapes or structures not provided for by any of the groups of A61K8/0241
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0241Containing particulates characterized by their shape and/or structure
    • A61K8/0279Porous; Hollow
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29BPREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B11/00Making preforms
    • B29B11/14Making preforms characterised by structure or composition
    • B29B11/16Making preforms characterised by structure or composition comprising fillers or reinforcement
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29BPREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00Mixing; Kneading
    • B29B7/80Component parts, details or accessories; Auxiliary operations
    • B29B7/88Adding charges, i.e. additives
    • B29B7/90Fillers or reinforcements, e.g. fibres
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C35/00Heating, cooling or curing, e.g. crosslinking or vulcanising; Apparatus therefor
    • B29C35/16Cooling
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C08J9/28Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof by elimination of a liquid phase from a macromolecular composition or article, e.g. drying of coagulum
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/20Chemical, physico-chemical or functional or structural properties of the composition as a whole
    • A61K2800/28Rubbing or scrubbing compositions; Peeling or abrasive compositions; Containing exfoliants
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/84Products or compounds obtained by lyophilisation, freeze-drying
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29KINDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
    • B29K2001/00Use of cellulose, modified cellulose or cellulose derivatives, e.g. viscose, as moulding material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29KINDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
    • B29K2105/00Condition, form or state of moulded material or of the material to be shaped
    • B29K2105/06Condition, form or state of moulded material or of the material to be shaped containing reinforcements, fillers or inserts
    • B29K2105/16Fillers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29LINDEXING SCHEME ASSOCIATED WITH SUBCLASS B29C, RELATING TO PARTICULAR ARTICLES
    • B29L2031/00Other particular articles
    • B29L2031/74Domestic articles
    • B29L2031/7406Sponges; Cleaning equipment
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2201/00Foams characterised by the foaming process
    • C08J2201/04Foams characterised by the foaming process characterised by the elimination of a liquid or solid component, e.g. precipitation, leaching out, evaporation
    • C08J2201/048Elimination of a frozen liquid phase
    • C08J2201/0484Elimination of a frozen liquid phase the liquid phase being aqueous
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2201/00Foams characterised by the foaming process
    • C08J2201/04Foams characterised by the foaming process characterised by the elimination of a liquid or solid component, e.g. precipitation, leaching out, evaporation
    • C08J2201/05Elimination by evaporation or heat degradation of a liquid phase
    • C08J2201/0504Elimination by evaporation or heat degradation of a liquid phase the liquid phase being aqueous
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2305/00Characterised by the use of polysaccharides or of their derivatives not provided for in groups C08J2301/00 or C08J2303/00
    • C08J2305/14Hemicellulose; Derivatives thereof

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Public Health (AREA)
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  • Dermatology (AREA)
  • Chemical & Material Sciences (AREA)
  • Mechanical Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Oral & Maxillofacial Surgery (AREA)
  • Chemical Kinetics & Catalysis (AREA)
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  • Medicinal Chemistry (AREA)
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Abstract

The present invention discloses a kind of sanding sponge and preparation method thereof, and the preparation method of the sanding sponge comprises the following steps:After basifier, pore-foaming agent, konjaku powder, frosted particle and water are stirred, inject in mould, form just base;Carry out boiling and freezing processing successively to first base, form parison;Parison is dehydrated and drying process successively after defrosting.The present invention combines the exfoliating effect of the effect of antibacterial cleaning for Rhizoma amorphophalli fiber product, replenishing water and preserving moisture and frosted particle, make sanding sponge while there is the effect of exfoliating, massaging skin and cleaning skin, replenishing water and preserving moisture, and its raw material is natural plant composition, without any pungent, it is adapted to the user of different skin quality to use.

Description

A kind of sanding sponge and preparation method thereof
Technical field
The present invention relates to sponge preparing technical field, more particularly to a kind of sanding sponge and preparation method thereof.
Background technology
As a rule, existing exfoliating product is the addition frosted particle in cream, frost or emulsion, is using such beveling When matter product cleans to skin, the effect of exfoliating is reached by the friction between frosted particle and skin, is using it After also need to wipe moisture retention water, the product such as breast carries out replenishing water and preserving moisture, process is relatively complicated, inconvenient for use.And existing beveling Typically all contain substantial amounts of chemical composition in matter product, although the cleaning effect of exfoliating is good, being irritating to the skin property is long Phase damages skin or formation sensitive skin using easily causing cuticula excessively thin.
The content of the invention
The main object of the present invention is to propose a kind of sanding sponge and preparation method thereof, it is intended to makes sponge while has beveling Two kinds of effects of matter and replenishing water and preserving moisture.
To achieve the above object, a kind of sanding sponge proposed by the present invention, including konjac sponge and frosted particle, the mill Sand particle is uniformly embedded at the konjac sponge, wherein, the frosted particle is natural plants particle.
Preferably, the konjac sponge includes the first spongy layer and the second spongy layer, and the frosted particle, which is divided equally, to be embedded at First spongy layer.
Preferably, the natural plants particle includes at least one of almond particle, grape pip particle and walnut seed;
The size of the natural plants particle is 80~200 mesh.
The present invention also proposes a kind of preparation method of sanding sponge, comprises the following steps:
Step S10, after stirring basifier, pore-foaming agent, konjaku powder, frosted particle and water, inject in mould, formed just Base;
Step S20, boiling and freezing processing are carried out successively to first base, forms parison;
Step S30, parison is after defrosting, is dehydrated successively and drying process.
Preferably, the step S10 includes:
After basifier, pore-foaming agent, konjaku powder, frosted particle and water are stirred, inject in mould, stand and form the first sea Continuous layer;
Injected after basifier, pore-foaming agent, konjaku powder and water are stirred in mould, form the second spongy layer;
First spongy layer bonds to form the just base with second spongy layer.
Preferably, the content of glucomannans is not less than 80% in the konjaku powder.
Preferably, the mass fraction of konjaku powder and water is respectively 3~15% and 85~97%;
The addition of the basifier is the 0.3~3% of the konjaku powder quality, and the addition of the pore-foaming agent is institute The 0.5~4% of konjaku powder quality is stated, the addition of the frosted particle is the 20~45% of the konjaku powder quality.
Preferably, the basifier is included in calcium hydroxide, calcium oxide, sodium hydroxide, sodium carbonate and sodium acid carbonate It is at least one;
The pore-foaming agent includes at least one of polysorbas20, polysorbate60 and Tween 80.
Preferably, in the step S20:Boiling temperature is 100~105 DEG C, and digestion time be 2~3h, cryogenic temperature is- 20~-30 DEG C, a length of 3~5 days during freezing.
Preferably, in the step S30:The drying process is vacuum freeze drying, wherein, vacuum freeze drying it is true Reciprocal of duty cycle is 1.3~10Pa, and the cryogenic temperature of vacuum freeze drying is -30~-50 DEG C, a length of 16 during the drying of vacuum freeze drying ~20h.
In technical solution of the present invention, it is added in Rhizoma amorphophalli fiber sponge, realizes using natural plants particle as frosted particle Merging between solid frosted particle and solid-state sponge, with reference to Rhizoma amorphophalli fiber product the effect of cleaning is antibacterial, replenishing water and preserving moisture and mill The exfoliating effect of sand particle, makes sanding sponge while has the effect of exfoliating, massaging skin and cleaning skin, replenishing water and preserving moisture Effect, and its raw material is natural plant composition, without any pungent, is adapted to the user of different skin quality to make With.
Brief description of the drawings
In order to illustrate more clearly about the embodiment of the present invention or technical scheme of the prior art, below will be to embodiment or existing There is the required accompanying drawing used in technology description to be briefly described, it should be apparent that, drawings in the following description are only this Some embodiments of invention, for those of ordinary skill in the art, on the premise of not paying creative work, can be with Structure according to these accompanying drawings obtains other accompanying drawings.
Fig. 1 is the structural representation of an embodiment of sanding sponge provided by the invention;
Fig. 2 is the structural representation of another embodiment of sanding sponge provided by the invention;
Fig. 3 is the schematic flow sheet of an embodiment of the preparation method of sanding sponge provided by the invention;
Fig. 4 is the schematic flow sheet of another embodiment of the preparation method of sanding sponge provided by the invention.
The realization, functional characteristics and advantage of the object of the invention will be described further referring to the drawings in conjunction with the embodiments.
Embodiment
It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not intended to limit the present invention.
A kind of sanding sponge proposed by the present invention, Fig. 1 are an embodiment of sanding sponge provided by the invention.Refer to figure 1, the sanding sponge 100 includes konjaku sponge 10 and frosted particle 20, and the frosted particle 20 is uniformly embedded at the konjaku Sponge 10, wherein, the frosted particle 20 is natural plants particle.
Due to containing abundant glucomannans in konjaku, and glucomannans has excellent cleaning bacteria resistance function and strong Water imbibition, therefore, the product prepared by Rhizoma amorphophalli fiber has cleaning antibacterial simultaneously and the double effects of replenishing water and preserving moisture.By frosted Particle is added in konjaku powder and prepares sanding sponge, and the exfoliating effect of frosted particle and the cleaning of Rhizoma amorphophalli fiber product are pressed down Bacterium, replenishing water and preserving moisture effect combine, and make sanding sponge while have the function of exfoliating, cleaning skin care and replenishing water and preserving moisture, In use, exclusive use can synchronously complete exfoliating and replenishing water and preserving moisture, it is not necessary to use the products such as moisture retention water, breast Carry out secondary nursing.
In another embodiment of sanding sponge provided by the invention, referring to Fig. 2, the konjac sponge 100 includes the One spongy layer 11 and the second spongy layer 12, the frosted particle 20 are uniformly embedded at first spongy layer 11.
, can be by the frosted even particulate dispersion in whole konjaku sea for the sanding sponge containing frosted particle , can also be by controlling moulding process to obtain the sponge with double-decker, wherein one layer is to be embedded with frosted particle in silk floss First spongy layer, another layer are the second spongy layer for not containing frosted particle.The sanding sponge of the double-decker was using Cheng Zhong, the first spongy layer can be first passed through exfoliating and massage treatment are carried out to skin, then skin is entered by the second spongy layer Row replenishing water and preserving moisture is nursed.
Alternatively, the natural plants particle includes at least one of almond particle, grape pip particle and walnut seed. Reach exfoliating by chemical composition to act on, easily cause in use the problems such as allergic, the mill that the present invention selects Sand particle is natural plants particle, is avoided using caused by chemical composition exfoliating product the problems such as skin sensitivity.
It is preferred that the size of the natural plants particle is 80~200 mesh.The oversized of frosted particle can cause frosted Sponge is excessively coarse, easily skin is caused to damage in use, therefore frosted particle carried out into sieving processing, sieve aperture it is big Small is 80~200 mesh, and the frosted particle after sieving is used to prepare sanding sponge, sanding sponge is unlikely to excess abrasive and is damaged Hinder skin.
The present invention also proposes a kind of preparation method of sanding sponge, and Fig. 3 is the preparation side of sanding sponge provided by the invention One embodiment of method, referring to Fig. 1, the preparation method of the sanding sponge comprises the following steps:
Step S10, after stirring basifier, pore-foaming agent, konjaku powder, frosted particle and water, inject in mould, formed just Base;
The basifier, pore-foaming agent, konjaku powder and frosted particle are weighed respectively, and the basifier and pore-foaming agent is complete Then fully dissolved adds the konjaku powder and frosted particle is stirred in water, stir 6~15min, to mixture in half After gel state in injection moulding mould, just base is formed.
Alternatively, the mass fraction of the konjaku powder and water is respectively 3~15% and 85~97%;The basifier Addition is the 0.3~3% of the konjaku powder quality, and the addition of the pore-foaming agent is the 0.5 of the konjaku powder quality ~4%, the addition of the frosted particle is the 20~45% of the konjaku powder quality.
Step S20, boiling and freezing processing are carried out successively to first base, forms parison;
Feed liquid in semigel shape is filled into mould after forming just base, thermophilic digestion directly is carried out to first base, with shape Into fibre structure, freezing processing then being carried out again, makes fibre structure shrink to form reticulated porous structures, there is exquisiteness so as to obtain The sanding sponge parison of dense porous structure.
Alternatively, in step S20:Boiling temperature is 100~105 DEG C, and digestion time is 2~3h, and cryogenic temperature is -20 ~-30 DEG C, a length of 3~5 days during freezing.
Step S30, parison is after defrosting, is dehydrated successively and drying process.
After the parison thaws, dewater treatment is carried out by supercentrifuge, moisture therein is removed, then by drying Processing further removes moisture therein, you can obtains sanding sponge.The sanding sponge when in use, is first soaked in water, When sanding sponge water swelling to when recovering elastic, you can skin is cleaned, after use, hung at aeration-drying Dry.
Alternatively, in step S30:The drying process is vacuum freeze drying, wherein, the vacuum of vacuum freeze drying For 1.3~10Pa, the cryogenic temperature of vacuum freeze drying is -30~-50 DEG C, a length of 16 during the drying of vacuum freeze drying~ 20h。
In another embodiment of the preparation method of sanding sponge provided by the invention, referring to Fig. 4, step S10 includes:
Step S11, after stirring basifier, pore-foaming agent, konjaku powder, frosted particle and water, inject in mould, stand shape Into the first spongy layer;
, can be by controlling moulding process to prepare for the sanding sponge of double-decker.First by basifier, pore-foaming agent, konjaku Fine powder, frosted particle and water the first mixture to be formed that stirs are filled into mould, stand 20~40min, are formed First spongy layer, wherein, the filling amount of first mixture is the 45~55% of the mold volumes.Certainly, described first The filling amount of mixture can be depending on the specific thickness requirement of the first spongy layer in the sanding sponge.
Step S12, injected after stirring basifier, pore-foaming agent, konjaku powder and water in mould, form the second spongy layer;
The second mixture to be formed that basifier, pore-foaming agent, konjaku powder and water are stirred is filled into formed with described In the mould of first spongy layer, by post forming, the second spongy layer is formed.Certainly, in technical solution of the present invention, step S11 and step S12 sequencing are not especially limited herein, can be first molded first spongy layer, can also be first molded Second spongy layer.In other embodiments of the present invention, first spongy layer and second spongy layer can also be distinguished Pass through two mould moldings.
Step S13, described first spongy layer bonds to form the just base with second spongy layer.
Because first spongy layer after shaping and second spongy layer are spawn, one is easily bonded in Rise and form the first base with double-decker.
Alternatively, the content of glucomannans is not less than 80% in the konjaku powder.Glucomannans is as konjaku essence Main component in powder, there is the effect of cleaning antibacterial and replenishing water and preserving moisture, if its content is too low, Rhizoma amorphophalli fiber product can be caused Insufficient strength, the sponge of preparation is easily deformed damage.Made from konjaku powder of the content of glucomannans not less than 80% Sanding sponge is prepared for primary raw material, the intensity of its Rhizoma amorphophalli fiber is guaranteed, and then improves netted more in the sanding sponge The intensity of hollow structure, the sanding sponge is set to be unlikely to deform damage with Reusability.
Alternatively, the basifier is included in calcium hydroxide, calcium oxide, sodium hydroxide, sodium carbonate and sodium acid carbonate It is at least one;The pore-foaming agent includes at least one of polysorbas20, polysorbate60 and Tween 80.The basifier main function It is to provide weakly alkaline environment, neutralizes after the konjaku powder mixes with water, form caused a small amount of acidic materials in gel process. The addition of the pore-foaming agent contributes to the just base to form stable, fine and close poroid fibre structure in digestion process, and tween is made For a kind of generally acknowledged nontoxic, nonirritant material, using tween as the pore-foaming agent for preparing sanding sponge, the mill can be avoided Sand sponge produces stimulation to skin in use.
In order that the preparation technology of sanding sponge provided by the invention is more directly perceived, with reference to Application Example and contrast Example illustrates:
Specific embodiment 1
(1) first sponge formable layer:It is pure that 3g sodium hydroxides, 5g polysorbas20s, 1000g konjaku powders and 15000g are weighed respectively Change water, after sodium hydroxide and tween are dissolved in the water, add konjaku powder and stir 10min, obtain the first mixture, take The mixtures of 30g first, 20min is stood after being injected by bottle placer in mould, forms the first spongy layer;
(2) second sponge formable layers:3g sodium hydroxides, 5g polysorbas20s, 1000g konjaku powders, 250g almonds are weighed respectively (80 mesh) and 15000g purified waters, after sodium hydroxide and tween are dissolved in the water, add konjaku powder and stir 10min, so Almond is added afterwards to continue to stir 5min, the second mixture is obtained, takes the mixtures of 30g second, by bottle placer injection formed with the In the mould of one spongy layer, just base is formed;
(3) boiling and freezing:Gradient type boiling is carried out to the first base of acquisition, boiling temperature is controlled at 100~105 DEG C, is steamed Radiating is then placed in freezer to normal temperature and carries out freezing processing, freezed 3 days in -20 DEG C, obtain parison after boiling 2h;
(4) dehydration is with drying:By parison successively after thawing, rinse, trim, first pass through supercentrifuge and be dehydrated Processing, be subsequently placed in vacuum be 1.3Pa, temperature carry out vacuum freeze drying in the environment of being -30 DEG C, sealed after drying 20h Packaging, that is, obtain sanding sponge product.
Specific embodiment 2
(1) first sponge formable layer:20g ammonium hydrogen carbonate, 10g polysorbate60s, 1000g konjaku powders and 15000g are weighed respectively Purified water, after sodium hydroxide and tween are dissolved in the water, add konjaku powder and stir 10min, obtain the first mixture, take The mixtures of 30g first, 30min is stood after being injected by bottle placer in mould, forms the first spongy layer;
(2) second sponge formable layers:20g ammonium hydrogen carbonate, 10g polysorbate60s, 1000g konjaku powders, 250g apricots are weighed respectively Core (120 mesh) and 15000g purified waters, after sodium hydroxide and tween are dissolved in the water, add konjaku powder and stir 10min, Then add almond continue stir 5min, obtain the second mixture, take the mixtures of 30g second, by bottle placer injection formed with In the mould of first spongy layer, just base is formed;
(3) boiling and freezing:Gradient type boiling is carried out to the first base of acquisition, boiling temperature is controlled at 100~105 DEG C, is steamed Radiating is then placed in freezer to normal temperature and carries out freezing processing, freezed 4 days in -25 DEG C, obtain parison after boiling 2h;
(4) dehydration is with drying:By parison successively after thawing, rinse, trim, first pass through supercentrifuge and be dehydrated Processing, be subsequently placed in vacuum be 4Pa, temperature carry out vacuum freeze drying in the environment of being -40 DEG C, dry sealed bundle after 18h Dress, that is, obtain sanding sponge product.
Specific embodiment 3
(1) first sponge formable layer:30g calcium hydroxides, 25g polysorbate60s, 10g Tween 80s, 1000g konjaku essences are weighed respectively Powder and 15000g purified waters, after sodium hydroxide and tween are dissolved in the water, add konjaku powder and simultaneously stir 10min, obtain the One mixture, the mixtures of 30g first are taken, stand 20min after being injected by bottle placer in mould, form the first spongy layer;
(2) second sponge formable layers:30g calcium hydroxides, 25g polysorbate60s, 10g Tween 80s, 1000g konjaku essences are weighed respectively Powder, 250g almonds (200 mesh) and 15000g purified waters, after sodium hydroxide and tween are dissolved in the water, add konjaku powder simultaneously 10min is stirred, almond is then added and continues to stir 5min, obtain the second mixture, take the mixtures of 30g second, pass through bottle placer Inject in the mould formed with the first spongy layer, form just base;
(3) boiling and freezing:Gradient type boiling is carried out to the first base of acquisition, boiling temperature is controlled at 100~105 DEG C, is steamed Radiating is then placed in freezer to normal temperature and carries out freezing processing, freezed 5 days in -20 DEG C, obtain parison after boiling 2h;
(4) dehydration is with drying:By parison successively after thawing, rinse, trim, first pass through supercentrifuge and be dehydrated Processing, be subsequently placed in vacuum be 8Pa, temperature carry out vacuum freeze drying in the environment of being -50 DEG C, dry sealed bundle after 16h Dress, that is, obtain sanding sponge product.
Specific embodiment 4
(1) first sponge formable layer:It is pure that 20g sodium carbonate, 40g polysorbate60s, 1000g konjaku powders and 15000g are weighed respectively Change water, after sodium hydroxide and tween are dissolved in the water, add konjaku powder and stir 10min, obtain the first mixture, take The mixtures of 30g first, 20min is stood after being injected by bottle placer in mould, forms the first spongy layer;
(2) second sponge formable layers:20g sodium carbonate, 40g polysorbate60s, 1000g konjaku powders, 300g grapes are weighed respectively Seed (120 mesh) and 15000g purified waters, after sodium hydroxide and tween are dissolved in the water, add konjaku powder and stir 10min, Then add almond continue stir 5min, obtain the second mixture, take the mixtures of 30g second, by bottle placer injection formed with In the mould of first spongy layer, just base is formed;
(3) boiling and freezing:Gradient type boiling is carried out to the first base of acquisition, boiling temperature is controlled at 100~105 DEG C, is steamed Radiating is then placed in freezer to normal temperature and carries out freezing processing, freezed 4 days in -30 DEG C, obtain parison after boiling 2h;
(4) dehydration is with drying:By parison successively after thawing, rinse, trim, first pass through supercentrifuge and be dehydrated Processing, be subsequently placed in vacuum be 10Pa, temperature carry out vacuum freeze drying in the environment of being -40 DEG C, dry sealed bundle after 16h Dress, that is, obtain sanding sponge product.
The sanding sponge prepared by the various embodiments described above, by the exfoliating effect of frosted particle and Rhizoma amorphophalli fiber product Antibacterial, replenishing water and preserving moisture effect is cleaned to combine, wherein, the first spongy layer (containing frosted particle) of sanding sponge has beveling Matter, the effect for cleaning skin care, the second spongy layer (not containing frosted particle) of sanding sponge have the function of replenishing water and preserving moisture, made During, exclusive use can synchronously complete exfoliating and replenishing water and preserving moisture, it is not necessary to be carried out using products such as moisture retention water, breasts Secondary nursing, and its raw material is natural plant composition, without any pungent, is adapted to the user of different skin quality to make With.
The preferred embodiments of the present invention are these are only, are not intended to limit the scope of the invention, it is every to utilize this hair The equivalent structure or equivalent flow conversion that bright specification and accompanying drawing content are made, or directly or indirectly it is used in other related skills Art field, is included within the scope of the present invention.

Claims (10)

1. a kind of sanding sponge, it is characterised in that including konjac sponge and frosted particle, the frosted particle is uniformly embedded at institute Konjac sponge is stated, wherein, the frosted particle is natural plants particle.
2. sanding sponge as claimed in claim 1, it is characterised in that the konjac sponge includes the first spongy layer and the second sea Continuous layer, the frosted particle, which is divided equally, is embedded at first spongy layer.
3. sanding sponge as claimed in claim 1, it is characterised in that the natural plants particle includes almond particle, grape At least one of seed particle and walnut seed;
The size of the natural plants particle is 80~200 mesh.
4. a kind of preparation method of sanding sponge, it is characterised in that comprise the following steps:
Step S10, after stirring basifier, pore-foaming agent, konjaku powder, frosted particle and water, inject in mould, form just base;
Step S20, boiling and freezing processing are carried out successively to first base, forms parison;
Step S30, parison is after defrosting, is dehydrated successively and drying process.
5. the preparation method of sanding sponge as claimed in claim 4, it is characterised in that the step S10 includes:
After basifier, pore-foaming agent, konjaku powder, frosted particle and water are stirred, inject in mould, stand and form the first sponge Layer;
Injected after basifier, pore-foaming agent, konjaku powder and water are stirred in mould, form the second spongy layer;
First spongy layer bonds to form the just base with second spongy layer.
6. the preparation method of sanding sponge as claimed in claim 4, it is characterised in that glucomannans in the konjaku powder Content be not less than 80%.
7. the preparation method of sanding sponge as claimed in claim 4, it is characterised in that the mass fraction of konjaku powder and water point Wei 3~15% and 85~97%;
The addition of the basifier is the 0.3~3% of the konjaku powder quality, and the addition of the pore-foaming agent is the evil spirit The 0.5~4% of taro fine powder quality, the addition of the frosted particle are the 20~45% of the konjaku powder quality.
8. the preparation method of sanding sponge as claimed in claim 4, it is characterised in that the basifier include calcium hydroxide, At least one of calcium oxide, sodium hydroxide, sodium carbonate and sodium acid carbonate;
The pore-foaming agent includes at least one of polysorbas20, polysorbate60 and Tween 80.
9. the preparation method of sanding sponge as claimed in claim 4, it is characterised in that in the step S20:Boiling temperature is 100~105 DEG C, digestion time is 2~3h, and cryogenic temperature is -20~-30 DEG C, a length of 3~5 days during freezing.
10. the preparation method of sanding sponge as claimed in claim 4, it is characterised in that in the step S30:The drying Handle as vacuum freeze drying, wherein, the vacuum of vacuum freeze drying is 1.3~10Pa, the freezing temperature of vacuum freeze drying Spend for -30~-50 DEG C, a length of 16~20h during the drying of vacuum freeze drying.
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EP18853388.9A EP3679916B1 (en) 2017-09-08 2018-04-11 Scrub sponge and preparation method therefor
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CN115025006A (en) * 2022-07-29 2022-09-09 广东博然堂生物科技有限公司 Mud-rubbing exfoliating shower gel and preparation method thereof

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CN107625651B (en) 2019-03-19
WO2019047525A1 (en) 2019-03-14
EP3679916B1 (en) 2023-06-07
EP3679916A4 (en) 2021-06-02

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