CN108451776A - A kind of natto gel membrane material material and preparation method thereof - Google Patents
A kind of natto gel membrane material material and preparation method thereof Download PDFInfo
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- CN108451776A CN108451776A CN201810348825.0A CN201810348825A CN108451776A CN 108451776 A CN108451776 A CN 108451776A CN 201810348825 A CN201810348825 A CN 201810348825A CN 108451776 A CN108451776 A CN 108451776A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/88—Polyamides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/54—Polymers characterized by specific structures/properties
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
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- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The invention belongs to cosmetic technical fields, and in particular to a kind of natto gel membrane material material and preparation method thereof.The present invention is provided, a kind of natto gel membrane material material is provided, including a natto gel membrane material body, natto gel membrane material body surface face is molded tiny concave-convex hole by equipment, these concave-convex holes can store Essence in the immersion of membrane material Essence, release again in use.The membrane material structure of more bumps holes makes natto gel membrane material of the present invention have good absorption and release function, and more full of elasticity and toughness, withstanding compression and folding；The natto gel membrane material is not only hydrophilic, but also obtains the function of water storage and oily solution by blister cavities and communicating passage structure.
Description
Technical field
The invention belongs to cosmetic technical fields, and in particular to a kind of natto gel membrane material material and preparation method thereof.
Background technology
In general, cosmetic facial mask has work(by being added known to Essence or toner or addition to non-woven fabrics
Can extract etc. of property manufacture.However, the facial mask of nonwoven type is manufactured by synthesizing macromolecule, if addition toner
Or functional Essence, then use feeling can be caused bad because it is hardened.In addition, for by non-woven fabrics in additives such as toners
Middle infiltration and the case where promote the mode of beautifying liquid constant absorption, have the disadvantage that：It is low to the adhesion of skin, it is difficult to avoid
The denaturation of Cosmetic Ingredient caused by beautifying liquid is exposed to air, because Cosmetic Ingredient and the skin contact of initial stage excessive concentrations are led
The possibility of the generation skin irritatin of cause is high.
The shortcomings that in order to overcome such non-woven fabrics facial mask, in recent years, for the research of hydrogel (hydrogel) facial mask
It develops more.However, when previous hydrogel is manufactured into lamellar form, due to only cannot keep shape with hydrogel, because
This is used after being usually additional to synthetic resin, non-woven fabrics, reticulated (mesh), net.But what hydrogel fell off from non-woven fabrics
The case where situation is more, hydrogel for using synthetic resin etc., from the aspect of organism well-formedness and safety, need into
The a large amount of evaluations of row and research.
Based on problem as described above, the cosmetic facial mask of the collagen used as native protein had been used in the past, but
Collagen is derived from the material of animal, and it is weak without easy-operating disadvantage that there are intensity.As a result, in order to overcome above-mentioned organism to close
The problems such as adaptive and weak intensity, to having used the hydrogel facial mask for deriving from natural materials to carry out numerous studies.For natural
The case where hydrogel facial mask, does not use non-woven fabrics etc. or synthetic resin etc., but the substance itself obtained from the Nature is direct
Film Morphology is manufactured, therefore there are following advantages：The sensibility skin caused by non-woven fabrics or synthetic resin etc. can not only be eliminated
The side effects such as the itch of skin, and can directly nutrition be provided to skin.
Natto gum is called polyglutamic acid sodium, is extracted by natto fermentation, is pure natural plant moisturizing agent.It has deep
It spends water lock, superpower moisturizing, repair the effect of skin, natural containment can be formed in skin surface, reduce trans epidermal water loss；
Go deep into skin bottom to keep the skin wet, there is perfect performance of keeping humidity.
Currently, natto gel membrane material body be base material make beauty mask, because its with carrier-free, it is all natural, without barrier,
The advantages that water lock efficiency is powerful, skin sense is good and environmentally friendly, more and more favored by consumers, the market share climbs up and up.Cause
This, real need develops natto gel membrane material body, is improved further design to natto gel membrane material body and design is a set of
Good production method, with to the just right adhesiveness of skin while making it have excellent strength, cosmetic result is excellent,
And cosmetic result to skin and the excellent gel component of safety.To make natto gel membrane material body have more liquid
Good absorption and release function, and have suitable toughness and crush resistance, so that it is easier and is economized on resources in packaging.
Invention content
The invention aims to overcome the deficiencies of the prior art and provide a kind of natto gel membrane material material, for liquid
Body has good absorption and release function；When applied to beauty mask, it can absorb a large amount of effect object and Essence and releases
It puts and works well.
Another object of the present invention is to provide a kind of production method of natto gel membrane material material.
In order to achieve the above object, present invention employs following technical schemes：
On the one hand, the present invention provides a kind of natto gel membrane material material, including a natto gel membrane material body, and the natto is solidifying
Glued membrane material body surface face is molded tiny concave-convex hole by equipment, these concave-convex holes can store in the immersion of membrane material Essence
Essence releases again in use, and more traditional non-woven fabrics facial mask carries more Essences, and continues to convey
It is longer to the time of the beauty functions Essence of skin.
Specifically, a kind of natto gel membrane material, raw material includes the component of following mass percentage,
Glycerine 0.1-1%；
Butanediol 0-0.5%；
Propylene glycol 0.2-2%；
Natto gum 0.1-5%；
Gel accelerating agent 0.1-5%；
Surfactant 0.1-3%；
Dissolve out agent 0.1-2%；
Preservative 0.01-0.5%；
Solid content 0.01~10%；
Surplus is deionized water.
Further, being enclosed with several can be sustained out inside the natto gel mould body in above-mentioned natto membrane material is beneficial to human body
The effect of skin ingredient solid content；The solid content is the mineral rich in various trace elements, processed cloth fabric, for warp
The leaves of plants of processing, petal, seed enhance the cloth fabric of membrane material toughness.Further, it is described through handle leaves of plants, petal,
Seed is lavender petal, pot marigold petal, leaf, lily petal, seaweed particle, coreopsis tinctoria petal etc..
Further, in the group that the gel accelerating agent is magnesium chloride, potassium chloride, calcium chloride and sodium chloride form extremely
Few one kind.
Further, the surfactant is Natrulon H-10.
Further, the preservative is methyl hydroxybenzoate.
Further, the natto gel membrane material is the membrane material structure of more concave-convex holes.
Further, the raw material of the natto gel membrane material is following component：
Glycerine 0.1-1%；
Butanediol 0-0.5%；
Propylene glycol 0.2-2%；
Natto gum 0.1-5%；
Alginic acid and/or sodium alginate：1.0%-2.0%；
Xanthans：0.3%-2.0%；
Guar gum：0.5%-2.0%；
Sodium chloride 0.1-5%；
Surfactant 0.1-3%；
Dissolve out agent 0.1-2%；
Preservative 0.01-0.5%；
Carboxymethyl cellulose 0.1-5%；
Chamomile 2%；
Dandelion 1%
Surplus is deionized water.
On the other hand, the present invention discloses a kind of preparation method of natto gel membrane material, natto gel membrane material body surface face
Tiny bumps cavity is molded by equipment, these concave-convex holes can store Essence in the immersion of membrane material Essence, including
Following steps：
A, prepared by natto gel membrane body feed liquid：Deionized water is added in ingredients pot, ingredients pot switch is started, ingredients pot is opened
Beginning agitating deionized water simultaneously heats up；Potassium chloride, butanediol, propylene glycol are added into ingredients pot, controls the acid-base value of liquid in pot；
Natto gel is added into ingredients pot, and liquid agitation in pot is uniformly dispersed, fluid temperature is at 80-90 DEG C in control pot；Extremely
After the raw material of addition is completely dissolved, solid content is added, being added to when special installation prepares natto gel membrane material for cloth fabric carries out
When；Liquid in ingredients pot is cooled to 50-80 DEG C, and preservative and surfactant is added, agitated liquid is made to uniform
Feed liquid, it is spare；
B, solid content processing step；
C, mixing step：Processed solid content is added in natto gel membrane material base-material and is uniformly dispersed or by special
Equipment solid content is placed among natto gel membrane material；
D, it forms a film：By special filling formation equipment, it is shaped to through mold natural cooling and external physics mode of implementing
Semi-finished product membrane material is spare, and semi-finished product film is the membrane material structure of more concave-convex holes；
E, drying：By in the special drying equipment of semi-finished product membrane material, 50-60 DEG C of drying temperature saves backup after dry；
F, it cuts：Membrane body is determined to required shape.
Wherein, the sodium carboxymethylcellulose in the present invention has thickening and peptizaiton, can improve the stickiness of gel
Dispersion effect is played with to other components in gel.
Natto gum is called polyglutamic acid sodium, is extracted by natto fermentation, is pure natural plant moisturizing agent.It has deep
It spends water lock, superpower moisturizing, repair the effect of skin, natural containment can be formed in skin surface, reduce trans epidermal water loss；
Go deep into skin bottom to keep the skin wet, there is perfect performance of keeping humidity.
Advantageous effects：
The membrane material structure of more bumps holes makes natto gel membrane material of the present invention have good absorption and release work(
Can, and more full of elasticity and toughness, withstanding compression and folding；The natto gel membrane material is not only hydrophilic, but also passes through blister cavities
And communicating passage structure obtains the function of water storage and oily solution.When applied to beauty mask, can absorb a large amount of effect object and
Essence, effect object and the releasing effect of essence are also good when use, the effect of improving beauty mask.The structure of multilayer also makes
Membrane body is full of elasticity and toughness, withstanding compression and folding.Above structure saves material about 20-40%, the membrane body of same area, this hair
Bright membrane body material cost substantially reduces.The material is widely used, and other than being used for beauty and skin care industry, applies also for curing
The industries such as treatment, health care and bioengineering.
Production method of the present invention can produce absorption and the good membrane body of release function, and membrane body is full of elasticity
And toughness, withstanding compression and folding.In addition, preparing natto gel membrane material using the above method, make natto gel in preparation process
Membrane material generates more concave-convex pore space structures, and the mode cut after dry to cut more convenient and quicker, also, in dry conditions
It is not easy cooperating microorganisms and mould, whole preparation process efficiency and reliability higher.
Specific implementation mode
With reference to specific embodiment, the present invention is described further, but following embodiments absolutely not to the present invention have appoint
What is limited.
Embodiment 1：
(1), prepared by natto gel membrane body feed liquid：Deionized water is added in ingredients pot, ingredients pot switch, ingredients pot are started
Start agitating deionized water and heats up；Potassium chloride, butanediol, propylene glycol are added into ingredients pot, controls the soda acid of liquid in pot
Degree adjusts PH to 5.0；Natto gel is added into ingredients pot, and liquid agitation in pot is uniformly dispersed, controls liquid temperature in pot
Degree is at 80-90 DEG C；To addition raw material be completely dissolved after, solid content is added, the special installation that is added to of cloth fabric prepares natto
When being carried out when gel membrane material；Liquid in ingredients pot is cooled to 50-80 DEG C, and preservative and surfactant is added, is stirred
Feed liquid is made to uniform in liquid, spare；
(2), solid content processing step；By chamomile 2%；Dandelion 1% is cleaned, smashes, is dried for standby.
(3), mixing step：Chamomile petal 2% that preservative, essence, step 2 are handled well, dandelion 1% are added and are received
In beans gel membrane material base-material and it is uniformly dispersed or by special equipment, makes chamomile；It is solidifying that dandelion is uniformly dispersed in natto
Among glued membrane material；
(4), it forms a film：By special filling formation equipment, through mold natural cooling and external implementation physics mode molding
Spare for semi-finished product membrane material, semi-finished product film is the membrane material structure of more concave-convex holes；
(5), dry：By in the special drying equipment of semi-finished product membrane material, saved backup after dry；
(6), it cuts：Membrane body is determined to required shape.
Embodiment 2：
(1) sodium carboxymethylcellulose, alginic acid and/or sodium alginate, xanthans, guar gum and mixed with propylene glycol is equal
It is even, dispersion liquid is made；Wherein, each group distribution ratio is：Sodium carboxymethylcellulose：0.1%；Alginic acid and/or sodium alginate：
1.0%；Xanthans：0.1%；Guar gum：0.1%；Propylene glycol：0.1%
(2) dispersion liquid made of step (1) is added in pure water, is heated to 80-90 DEG C, stirs evenly, is then added
Sodium chloride obtains crosslinked fluid；
(3) natto extracting solution 5% is added to 60-70 DEG C in cooling crosslinked fluid；Camomile extract 2%；Dandelion extract
1%；Obtain solution A；
(4) lactic acid or the pH to 5.5-6.0 of citric acid regulating solution A are used, hydrogel is made；
(5) hydrogel is put into hydrogel facial mask machine, hydrogel is made to penetrate into the screen cloth of hydrogel facial mask machine, dropped
Temperature, it is film adhered with silk, form gel slice；
(6) gel slice is cut and formed with cutting die.
Example is used for 60 users, and after each thorough cleaning skin of user, the facial mask paster for preparing gained is pasted
On skin, is torn off after waiting for 30min, warm water is used in combination to wash away face's residue.By above-mentioned 50 users 6-12 months
Use identical facial mask paster the case where analyze, wherein 20 people are to use daily, 20 people are interval 1-2 days using once, 20
Artificial interval 3 days or more unstable use.Wherein, being used continuously and stablizing the face that user shows improves feature the most
Obviously, there is good gloss, pore contractive effect, skin-tightening and moistening effect stabilization in skin.In unstable user, there is one
It is 13 to determine improver, and it is 7 to improve unobvious.After deactivating 7 days, obviously changing does not occur above-mentioned 60 users in face skin
Kind feature does not occur the situations such as apparent melanin pigmentation and skin quality deterioration, shows that the facial mask paster of the present invention nourishes effect
Fruit is preferable, can improve skin quality, and skin dependence is relatively low.After deactivating 14 days, there are 26 the slight change of skin quality occur, but
The skin quality being still better than before being not used can be improved rapidly using common moisturizing and nourishing class skin care item at this time.By above-mentioned
Experiment, it was demonstrated that facial mask paster of the invention plays expected effect to skin quality improvement, and tolerance and dependence are relatively low.
Claims (9)
1. a kind of natto gel membrane material, which is characterized in that its raw material includes the component of following mass percentage,
Glycerine 0.1-1%；
Butanediol 0-0.5%；
Propylene glycol 0.2-2%；
Natto gel 0.1-5%；
Gel accelerating agent 0.1-5%；
Surfactant 0.1-3%；
Dissolve out agent 0.1-2%；
Preservative 0.01-0.5%；
Solid content 0.01~10%；
Surplus is deionized water.
2. natto gel membrane material according to claim 1, which is characterized in that if being enclosed with inside the natto gel mould body
The dry solid content that can be sustained out ingredient the effect of being beneficial to human skin；The solid content is the mine rich in various trace elements
Object, processed cloth fabric are processed leaves of plants, petal, seed, enhance the cloth fabric of membrane material toughness.
3. natto gel membrane material according to claim 2, which is characterized in that described through handling leaves of plants, petal, seed
For lavender petal, pot marigold petal, leaf, lily petal, seaweed particle, coreopsis tinctoria petal.
4. natto gel membrane material according to claim 1, which is characterized in that the gel accelerating agent is magnesium chloride, chlorine
Change at least one of the group of potassium, calcium chloride and sodium chloride composition.
5. natto gel membrane material according to claim 1, which is characterized in that the surfactant is Natrulon H-10.
6. natto gel membrane material according to claim 1, which is characterized in that the preservative is methyl hydroxybenzoate.
7. natto gel membrane material according to claim 1, which is characterized in that the natto gel membrane material is more concave-convex holes
The membrane material structure in hole.
8. natto gel membrane material according to claim 1, which is characterized in that the raw material of the natto gel membrane material is such as
Lower component：
Glycerine 0.1-1%；
Butanediol 0-0.5%；
Propylene glycol 0.2-2%；
Natto gum 0.1-5%；
Alginic acid and/or sodium alginate：1.0%-2.0%；
Xanthans：0.3%-2.0%；
Guar gum：0.5%-2.0%；
Sodium chloride 0.1-5%；
Surfactant 0.1-3%；
Dissolve out agent 0.1-2%；
Preservative 0.01-0.5%；
Carboxymethyl cellulose 0.1-5%；
Chamomile 2%；
Dandelion 1%
Surplus is deionized water.
9. a kind of preparation method of natto gel membrane material as described in claim 1, which is characterized in that the natto gel membrane material
Body surface face is molded tiny concave-convex hole by equipment, these concave-convex holes can store essence in the immersion of membrane material Essence
Liquid, described method includes following steps：
A, prepared by natto gel membrane body feed liquid：Deionized water is added in ingredients pot, ingredients pot switch is started, ingredients pot starts to stir
It mixes deionized water and heats up；Potassium chloride, butanediol, propylene glycol are added into ingredients pot, controls the acid-base value of liquid in pot, adjusts
PH is 5.0~6.0；Natto gum is added into ingredients pot, and liquid agitation in pot is uniformly dispersed, controls fluid temperature in pot and exists
80-90℃；To addition raw material be completely dissolved after, solid content is added, the special installation that is added to of cloth fabric prepares natto gel
When being carried out when membrane material；Liquid in ingredients pot is cooled to 50-80 DEG C, and preservative and surfactant is added, agitated liquid
To uniform, feed liquid is made, it is spare；
B, solid content processing step；
C, mixing step：Processed solid content is added in natto gel membrane material base-material and is uniformly dispersed or is set by special
It is standby that solid content is placed among natto gel membrane material；
D, it forms a film：By special filling formation equipment, through mold natural cooling and it is external implement physics mode be shaped to half at
Product membrane material is spare；
E, drying：By in the special drying equipment of semi-finished product membrane material, saved backup after dry；
F, it cuts：Membrane body is determined to required shape.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810348825.0A CN108451776A (en) | 2018-04-18 | 2018-04-18 | A kind of natto gel membrane material material and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201810348825.0A CN108451776A (en) | 2018-04-18 | 2018-04-18 | A kind of natto gel membrane material material and preparation method thereof |
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| CN108451776A true CN108451776A (en) | 2018-08-28 |
Family
ID=63235819
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| CN201810348825.0A Pending CN108451776A (en) | 2018-04-18 | 2018-04-18 | A kind of natto gel membrane material material and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110393692A (en) * | 2019-09-04 | 2019-11-01 | 广东丸美生物技术股份有限公司 | Wire drawing plant thickener and its preparation method and application |
| CN114438775A (en) * | 2021-12-21 | 2022-05-06 | 广东美凡芮科技有限公司 | Functional mask matrix preparation method and mask |
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| CN110393692A (en) * | 2019-09-04 | 2019-11-01 | 广东丸美生物技术股份有限公司 | Wire drawing plant thickener and its preparation method and application |
| CN114438775A (en) * | 2021-12-21 | 2022-05-06 | 广东美凡芮科技有限公司 | Functional mask matrix preparation method and mask |
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Application publication date: 20180828 |