CN107595725A - One kind smears tea flavour mouthwash and preparation method thereof - Google Patents
One kind smears tea flavour mouthwash and preparation method thereof Download PDFInfo
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- CN107595725A CN107595725A CN201711111334.6A CN201711111334A CN107595725A CN 107595725 A CN107595725 A CN 107595725A CN 201711111334 A CN201711111334 A CN 201711111334A CN 107595725 A CN107595725 A CN 107595725A
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- chitosan
- mouthwash
- tea flavour
- sweetener
- smear
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Abstract
The invention discloses one kind to smear tea flavour mouthwash and preparation method thereof, consists of the following composition：Water soluble chitosan, glycerine, propane diols, sorbierite, preservative, solubilizer, menthol, naturally smear tea perfume essence, sweetener, laruyl alcohol sodium sulfovinate, citric acid, purified water.The water security of gargling of the present invention has no side effect, and mouthfeel is soft, has the taste that delicate fragrance smears tea, and pH value is between 6.6 7.1, close to human saliva pH value, therefore long-term use can well maintain, adjust intraoral microecological balance, can prevent and treat mouth disease.
Description
Technical field
The invention belongs to oral cleaning nursing article technical field, and in particular to one kind smears tea flavour mouthwash and its preparation side
Method.
Background technology
It is the easy method of oral health most convenient to gargle, and it can remove the soft dirt of intraoral swill and part, also
The quantity of oral cavity bacterium can temporarily be reduced.In recent years, being capable of fresh breath protection with the enhancing that people's oral health is realized
The mouthwash of tooth is favored by more and more people.
Prepare chitosan mouthwash and need to use water-soluble chitosan, but water soluble chitosan mouthfeel is bitter, it is simple to adjust
Section pol is difficult to cover.Therefore as a big difficult point of chitosan mouthwash commercialization.
Existing mouthwash on the market in order to ensure stability often in acid or alkalescence, therefore have ignored mouthwash pH value with
The difference of human oral cavity pH value, long-term use of acid mouthwash can cause tooth moth to damage, and the mouthwash of long-term use of alkalescence,
Oral cavity flora can be made to lack of proper care, so as to cause the symptoms such as ozostomia and canker sore, therefore can not only played a role in health care, on the contrary
Oral health can be influenceed.
The content of the invention
It is an object of the invention to provide one kind to smear tea flavour mouthwash, can well maintain, adjust intraoral Tiny ecosystem
Balance, can prevent mouth disease.
Another object of the present invention is to provide a kind of preparation method for smearing tea flavour mouthwash.
The present invention realizes that the scheme of purpose is as follows：One kind smears tea flavour mouthwash, consists of the following components in percentage by weight：
Water soluble chitosan 0.05% ~ 1%
Glycerine 0.5% ~ 10%
Propane diols 0.5% ~ 10%
Sorbierite 0.01% ~ 2%
Preservative 0.001% ~ 0.2%
Solubilizer 0.01% ~ 5%
Menthol 0.001% ~ 0.2%
Naturally smear tea perfume essence 0.001% ~ 0.2%
Sweetener 0.001% ~ 0.2%
Laruyl alcohol sodium sulfovinate 0.01% ~ 2%
Appropriate citric acid
Purify water surplus.
Preferably；The water soluble chitosan is sulfonated chitosan, sulfonated chitin, succinyl-chitosan, shell gather
Sugared quaternary ammonium salt, Glucosamine, 2-Acetamido-2-deoxy-D-glucose, chitosan oligosaccharide, chitin oligo saccharide, carboxymethyl chitin, carboxymethyl chitosan
One kind in sugar, hydroxypropyl chitosan, Hydroxypropyl chitosan, hydroxyethyl chitosan, ethoxyl chitin and chitosan oligomer or
It is several.
Preferably；The sweetener is Sucralose or saccharin sodium.
Preferably；The solubilizer is poloxamer188.
Preferably；The preservative is potassium sorbate.
The preparation method for smearing tea flavour mouthwash, comprises the following steps：
(1) menthol is dissolved in propane diols, then adds glycerine and stir, obtain A group mixed solutions；
(2) water soluble chitosan is dissolved in purified water under agitation and obtains chitosan aqueous solution；
(3) by sorbierite, preservative, solubilizer, natural smear tea perfume essence, sweetener, laruyl alcohol sodium sulfovinate and be dissolved in step
（2）In chitosan aqueous solution in, obtain B group mixed solutions；
(4) above-mentioned B groups mixed solution is added gradually in A group mixed solutions under agitation, is well mixed, then adds lemon
Lemon acid for adjusting pH value is 6.6-7.1, produces and smears tea flavour mouthwash.
Beneficial effects of the present invention：
(1) water security of gargling of the invention has no side effect, and scientific formulation is reasonable, after each composition combination and compatibility, what is mutually cooperateed with
Effect is lower can to make pH value keep higher stability between 6.6-7.1, because the pH value of the present invention is close to human saliva pH value,
In addition water soluble chitosan, which has, suppresses harmful bacteria breeding effect, therefore long-term use can maintain, adjust Tiny ecosystem in oral cavity
Balance, promote beneficial bacteria growth, suppress harmful bacteria breeding, improve oral environment, the acid-base value in oral cavity is maintained normally
Level, so as to reach the effect of preventing and treating mouth disease.
(2) sweetener in mouthwash formula of the present invention and natural smear can be with water soluble chitosans after tea perfume essence is applied in combination
Bitter taste be perfectly combined, coordinate the regulation of menthol, the mouthwash mouthfeel of the present invention can be made soft and smear tea with delicate fragrance
Taste, consumer demand is more suitable for, there is higher economic benefit.
Embodiment
The present invention is raw materials used to be commercially available or the industry is conventional.
Table 1 is that following examples smear the component of tea flavour mouthwash and the percentage by weight of each component
Embodiment 1：
One kind smears tea flavour mouthwash, and each component and its percentage by weight are shown in Table 1, and wherein water soluble chitosan is that sulfonated shell gathers
Sugar, sweetener are Sucraloses, and lemon acid for adjusting pH value is 6.6-7.1.
The preparation method for smearing tea flavour mouthwash, comprises the following steps：
(1) menthol is dissolved in propane diols, then adds glycerine and stir, obtain A group mixed solutions；
(2) water soluble chitosan is dissolved in purified water under agitation and obtains chitosan aqueous solution；
(3) sorbierite, potassium sorbate, poloxamer188, natural tea perfume essence, sweetener, the laruyl alcohol sodium sulfovinate of smearing are dissolved
In step（2）In chitosan aqueous solution in, obtain B group mixed solutions；
(4) above-mentioned B groups mixed solution is added gradually in A group mixed solutions under agitation, is well mixed, then adds lemon
Lemon acid for adjusting pH value is 6.6-7.1, produces and smears tea flavour mouthwash.
Embodiment 2：
One kind smears tea flavour mouthwash, and each component and its percentage by weight are shown in Table 1, and wherein water soluble chitosan is N- acetylaminos Portugal
Grape sugar, sweetener is Sucralose, and lemon acid for adjusting pH value is 6.6-7.1.
The preparation method for smearing tea flavour mouthwash is the same as embodiment 1.
Embodiment 3：
One kind smears tea flavour mouthwash, and each component and its percentage by weight are shown in Table 1, and wherein water soluble chitosan is carboxymethyl crusta
Element, sweetener are Sucraloses, and lemon acid for adjusting pH value is 6.6-7.1.
The preparation method for smearing tea flavour mouthwash is the same as embodiment 1.
Embodiment 4：
One kind smears tea flavour mouthwash, and each component and its percentage by weight are shown in Table 1, and wherein water soluble chitosan is hydroxypropyl
Sugar, sweetener are saccharin sodiums, and lemon acid for adjusting pH value is 6.6-7.1.
The preparation method for smearing tea flavour mouthwash is the same as embodiment 1.
Embodiment 5：
One kind smears tea flavour mouthwash, and each component and its percentage by weight are shown in Table 1, and wherein water soluble chitosan is that succinyl shell gathers
Sugar, sweetener are saccharin sodiums, and lemon acid for adjusting pH value is 6.6-7.1.
The preparation method for smearing tea flavour mouthwash is the same as embodiment 1.
Embodiment 6：Stable type is tested
Example 1 smears tea flavour mouthwash, is divided into 3 experimental groups, respectively experimental group 1, experimental group 2, experimental group 3, is placed in and examines
Examine after being deposited in case, respectively the stability of the character of inspection mouthwash, pH value and mouthfeel.
The storage temperature of experimental group 1 is 4 DEG C ± 2, and the storage temperature of experimental group 2 is 40 DEG C ± 2；The storage temperature of experimental group 3 is 60
℃±2。
Experimental group 1 was deposited in 10 days, and character is unchanged：Solution is clarified, no muddy and precipitation；PH value, which becomes, turns to ± 0.01,
Mouthfeel is unchanged：It is sweet, there is the salubrious sense of peppermint, smear tea smell.
Experimental group 2 was deposited in 6 months, and character is unchanged：Solution is clarified, no muddy and precipitation；PH value, which becomes, turns to ± 0.01,
Mouthfeel is unchanged：It is sweet, there is the salubrious sense of peppermint, smear tea smell.
Experimental group 3 was deposited in 10 days, and character is unchanged：Solution is clarified, no muddy and precipitation；PH value, which becomes, turns to ± 0.01,
Mouthfeel is unchanged：It is sweet, there is the salubrious sense of peppermint, smear tea smell.
Test result indicates that：Character, mouthfeel are stable in 6 months under the conditions of 40 DEG C for the mouthwash of the present invention, pH value change
In normal range (NR), and under extreme temperature environment 60 DEG C and 4 DEG C deposit 10 days, can also keep stable.
Embodiment described above is the preferable scheme of the present invention, not makees any formal limitation to the present invention,
There are other variants and remodeling on the premise of without departing from the technical scheme described in claim.
Claims (6)
1. one kind smears tea flavour mouthwash, it is characterised in that consists of the following components in percentage by weight：
Water soluble chitosan 0.05% ~ 1%
Glycerine 0.5% ~ 10%
Propane diols 0.5% ~ 10%
Sorbierite 0.01% ~ 2%
Preservative 0.001% ~ 0.2%
Solubilizer 0.01% ~ 5%
Menthol 0.001% ~ 0.2%
Naturally smear tea perfume essence 0.001% ~ 0.2%
Sweetener 0.001% ~ 0.2%
Laruyl alcohol sodium sulfovinate 0.01% ~ 2%
Appropriate citric acid
Purify water surplus.
2. according to claim 1 smear tea flavour mouthwash, it is characterised in that：The water soluble chitosan is that sulfonated shell gathers
Sugared, sulfonated chitin, succinyl-chitosan, chitosan quaternary ammonium salt, Glucosamine, 2-Acetamido-2-deoxy-D-glucose, chitosan oligosaccharide,
Chitin oligo saccharide, carboxymethyl chitin, carboxymethyl chitosan, hydroxypropyl chitosan, Hydroxypropyl chitosan, hydroxyethyl chitosan, hydroxyl
One or more in ethyl chitin and chitosan oligomer.
3. according to claim 1 smear tea flavour mouthwash, it is characterised in that：The sweetener is Sucralose or saccharin
Sodium.
4. according to claim 1 smear tea flavour mouthwash, it is characterised in that：The solubilizer is poloxamer188.
5. according to claim 1 smear tea flavour mouthwash, it is characterised in that：The preservative is potassium sorbate.
6. the preparation method for smearing tea flavour mouthwash described in a kind of any one of claim 1-5, it is characterised in that including following step
Suddenly：
(1) menthol is dissolved in propane diols, then adds glycerine and stir, obtain A group mixed solutions；
(2) water soluble chitosan is dissolved in purified water under agitation and obtains chitosan aqueous solution；
(3) by sorbierite, preservative, solubilizer, natural smear tea perfume essence, sweetener, laruyl alcohol sodium sulfovinate and be dissolved in step
（2）In chitosan aqueous solution in, obtain B group mixed solutions；
(4) above-mentioned B groups mixed solution is added gradually in A group mixed solutions under agitation, is well mixed, then adds lemon
Lemon acid for adjusting pH value is 6.6-7.1, produces and smears tea flavour mouthwash.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711111334.6A CN107595725A (en) | 2017-11-13 | 2017-11-13 | One kind smears tea flavour mouthwash and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711111334.6A CN107595725A (en) | 2017-11-13 | 2017-11-13 | One kind smears tea flavour mouthwash and preparation method thereof |
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| CN107595725A true CN107595725A (en) | 2018-01-19 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110897929A (en) * | 2019-12-27 | 2020-03-24 | 河北考力森生物科技有限公司 | Chitosan mouthwash |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105796379A (en) * | 2016-05-06 | 2016-07-27 | 青岛蓝百合生物科技有限公司 | Water soluble chitosan oral care solution and preparation method thereof |
-
2017
- 2017-11-13 CN CN201711111334.6A patent/CN107595725A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105796379A (en) * | 2016-05-06 | 2016-07-27 | 青岛蓝百合生物科技有限公司 | Water soluble chitosan oral care solution and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 裘炳毅等: "《现代化妆品科学与技术 下册》", 31 March 2016, 中国轻工业出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110897929A (en) * | 2019-12-27 | 2020-03-24 | 河北考力森生物科技有限公司 | Chitosan mouthwash |
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Application publication date: 20180119 |