CN107595026A - A kind of antibacterial anti-mite mulberry silk quilt - Google Patents

A kind of antibacterial anti-mite mulberry silk quilt Download PDF

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Publication number
CN107595026A
CN107595026A CN201710776404.3A CN201710776404A CN107595026A CN 107595026 A CN107595026 A CN 107595026A CN 201710776404 A CN201710776404 A CN 201710776404A CN 107595026 A CN107595026 A CN 107595026A
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China
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hybrid particles
tire
continuous piece
bag
silk
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CN201710776404.3A
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Chinese (zh)
Inventor
卢受坤
张同洪
胡勇
黄农审
梁就荣
黄娇连
梁晓玲
杨兴
黄小龙
宋志谊
黄杰容
梁有
甘少秋
辛德强
麦巧燕
苏小林
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Guangxi Guihua Silk Co Ltd
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Guangxi Guihua Silk Co Ltd
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Priority to CN201710776404.3A priority Critical patent/CN107595026A/en
Publication of CN107595026A publication Critical patent/CN107595026A/en
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Abstract

A kind of antibacterial anti-mite mulberry silk quilt, making step are:(1)It is online that matured silkworm is put into spinning;(2)Strip hair silk floss piece;(3)The continuous piece degumming process of hair;(4)Cleaning and dewatering;(5)Continuous piece drying;(6)Continuous piece is weighed;(7)Cut continuous piece;(8)Continuous piece is pulled open one by one and is divided into two parts, respectively by two parts of continuous piece layings;(9)Put anti-race gauze cloth in continuous piece top and bottom;(10)Two parts of continuous one layer of tire sets of piece overcoat, three sides are got ready suture respectively, while staying mouth to turn into tire core bag;(11)Harvesting, drying honeysuckle, sweet wormwood and pyrrosia lingua;(12)Prepare hybrid particles;(13)Hybrid particles coating, drying;(14)Prepare non-woven bag;(15)Prepare hybrid particles tire;(16)Finally hybrid particles tire is fixed in fetal rhythm bag, then fetal rhythm bag is placed in quilt cover.This mulberry silk quilt good product quality, play antibacterial anti-mite effect.

Description

A kind of antibacterial anti-mite mulberry silk quilt
Technical field
The present invention relates to the processing technique field of mulberry silk quilt, is specifically a kind of antibacterial anti-mite mulberry silk quilt and its preparation Method.
Background technology
Silk quilt is a kind of quilt using silk fiber as filler, and its silk fiber is to use silk cocoon or filature byproduct It is process, silk floss manufacturing process is that matured silkworm spinning is cocoond → silk floss → arrangement → baking is washed in cocoon drying → system continuous → practicing continuous → continuous, tradition Processing method can pollute cocoon layer by pupal fat caused by cocoon drying, and obtained silk floss sheet oil-containing is higher;Needed in the process such as system is continuous, white silk silk floss Chemical assistant is added, has a small amount of chemical residual, and causes a certain degree of environmental pollution.In order to obtain more natural environmental-protective Silk silk floss raw material, the present invention research it is a kind of from matured silkworm spinning starts from silk floss, artificially break the normal habit that silkworms spin silk, Change traditional cluster tool condition that silkworm cocooning needs, instead of with plane spinning net, making matured silkworm be formed in online directly spinning flat The silkworm silk floss sheet of planar, instead of matured silkworm spinning and cocoons → continuous traditional silk floss the process of cocoon drying → system, and processing is easier;Pass Processing method of uniting can pollute cocoon layer by pupal fat caused by cocoon drying, and obtained silk floss sheet oil-containing is higher, and directly spins into silk floss by matured silkworm Without rib, it is more excellent without pupal fat, quality.Need to add chemical assistant in the process such as traditional system is continuous, white silk silk floss, have few The chemical residual of amount, and a certain degree of environmental pollution is caused, the preparation method of pure mulberry silk quilt provided by the invention is with matured silkworm The plane silk floss of discharge is as raw material, and employ uniqueness boils continuous method, and the scouring processes of continuous piece need not add chemical assistant, more Natural environmental-protective, while reduce processing cost.
As the improvement of people's living standards, existing silk quilt can not meet the needs of people, therefore, develop A kind of more natural environmental-protective, antibacterial anti-mite silk quilt are desirabilities.
The content of the invention
It is an object of the invention to provide a kind of antibacterial anti-mite mulberry silk quilt, the mulberry silk quilt good product quality, mulberry silk quilt In be placed with honeysuckle, sweet wormwood and pyrrosia lingua, the fragrance of light Chinese medicine can be distributed, play antibacterial anti-mite effect, and fragrance discharges Slowly, fragrance can be kept for a long time.
To achieve these goals, the present invention adopts the technical scheme that:
A kind of antibacterial anti-mite mulberry silk quilt, is made of following processing step:
(1)The matured silkworm for emptying fecaluria is put into spinning on the net, the density of matured silkworm is 800-900 Tiao/㎡.Described spinning net is flat Plate spinning net, its mesh width is 2-5 millimeters, and the thickness for the net that spins is 1-2 millimeters.
(2)After matured silkworm spinning terminates, silk is peeled off from spinning is online, obtains smooth hair silk floss piece.
(3)Practiced with 98-100 DEG C of temperature, the hydrogen peroxide solution that mass percentage concentration is 4% and boil 30-40 minutes, to hair silk floss piece Degumming process is carried out, until content of silk gum is 2.5-3.5%.
(4)The continuous piece after degumming is cleaned up with clear water, then is placed into dewaterer and carries out dewater treatment.
(5)Continuous piece after dehydration is dried after the Shape correction that cleans, and obtains doing continuous piece, standby;Drying temperature is 65-85 degree, regain are controlled below 12%.
(6)Dry continuous piece weight as needed is weighed, pullled after weighing, makes continuous piece fluffy.
(7)Cut according to cotton-wadded quilt size to doing continuous piece.
(8)Dry continuous piece is divided into two parts, does the continuous crisscross laying of piece on platform by two parts respectively, after the completion of laying, Inspection arrangement is carried out to upper and lower surface, goes the removal of impurity and stiff bar.
(9)It will check that two parts put in order dry continuous piece top and bottom respectively place one layer of anti-gauze cloth that runs and get ready and fix respectively It is good, avoid running silk, obtain two silk floss batting cores.
(10)Two silk floss batting cores are overlapped, put cotton tire set, suture is got on three sides ready, makes silk floss batting core and two gauzes Tire core fixes, wherein while staying mouth to turn into tire core bag;Bar tied rope is respectively left in corner in tire core bag.Described tire set is using high branch Highly dense pure cotton cloth is made.Described tire set is made of high-count and high-density pure cotton cloth.
(11)Clean honeysuckle, sweet wormwood and pyrrosia lingua are plucked, 2~5min is dried with microwave vacuum low-temperature drying machine, makes to contain Water is less than 10%, is saved backup with plastic bag sealing.Microwave vacuum low-temperature drying machine is in the limited public affairs of Guangzhou Yong Ze microwave energy equipment Department's purchase, network address:http://www.gz-yongze.com/, address:Guangzhou, Guangdong Baiyun District good farmland town Jin Pan industrial areas No. 8.
(12)It is 2 by weight after honeysuckle, sweet wormwood and pyrrosia lingua are broken into powder respectively:3:1 is well mixed;Sprinkling is suitable Amount carboxymethyl cellulose gum sticks agent and is pressed into grain shape, and the hybrid particles of even particle size are obtained through screening.Spray carboxymethyl The amount of cellulose adhesive enables honeysuckle, sweet wormwood and pyrrosia lingua powder to be pressed into particle.Particle is unsuitable excessive, like cassia seed size It is advisable.
(13)Mixing is coated using coating agent made of Potato Porous Starch slurries and water soluble chitosan, will Hybrid particles and coating agent are with 6-8:1 weight makes hybrid particles surface be wrapped in one layer of coating agent, after coating than mixing Hybrid particles dry 3~5min in microwave vacuum low-temperature drying machine, water content is less than 10%.
(14)Non-woven fabrics is selected according to tire core bag inside dimension, doubling sewing margin to seam, while stay mouth, turned welt is into non-woven bag.
(15)Hybrid particles after coating are put into non-woven bag, then non-woven bag is shakeout on work top, nothing The hybrid particles spun in cloth bag shakeout, it is impossible to and allow hybrid particles to stack, then open-wire line sealing, non-woven bag is finally subjected to netted sew with long stitches Seam, avoids hybrid particles from walking, corner is sewed with tied rope, turns into hybrid particles tire.
(16)Finally hybrid particles tire corner is fixed in tire core bag by tied rope, then fetal rhythm bag is placed in quilt cover .After hybrid particles tire does not have fragrance, change hybrid particles tire or can obtain new silk after removing hybrid particles tire Cotton quilt.
The hydrogen peroxide solution that described mass percentage concentration is 4% is by hydrogen peroxide, sodium metasilicate, sodium EDTA salt It is formulated with clear water, the weight ratio of hydrogen peroxide, sodium metasilicate and sodium EDTA salt is(2-3):(0.5-0.8):(0.2- 0.3).
Described coating agent is that suitable quantity of water slurrying is added after peeling potatoes are cooked and is digested, and enzymatic hydrolysis condition is:Saccharification Enzyme:α~amylase=2:1, farinaceous size concentration 30%, enzyme concentration 1.2%, 55 DEG C, reaction time 12h of reaction temperature, reaction system PH is 5~6, prepares Potato Porous Starch;Then it is 5000~10000 that molecular weight is added into Potato Porous Starch slurries Water soluble chitosan stir, Potato Porous Starch and water soluble chitosan weight content are 2:1, obtain moisture content 40 ~60% coating agent solutions;5% carbon dioxide is filled with by coating agent weight so that coating agent solutions carry more gas Bubble.
Described carboxymethyl cellulose gum sticks what agent was formed by carboxymethyl cellulose with appropriate water modulation, wherein carboxymethyl Cellulose is prepared by being acted in the basic conditions by monochloroacetic acid and cellulose, and quaternization occurs for cellulose and alkali effect Alkali cellulose is generated, alkali cellulose occurs etherification reaction with monochloroacetic acid again, obtains carboxymethyl cellulose.
In order that silk floss has more preferable intensity and pliability, 5 minutes before end is refiningly cooked to hair silk floss piece, hydrogen peroxide is added Solution weight 1.5-2% ethylene glycol diglycidylether;Ethylene glycol diglycidylether, English name:Glycol Diglycidyl ether, alias:Tetramethyl ammonium chloride tetramethyl ammonium chloride tetramethyl ammonium chloride, No. CAS:2224-15-9, point Minor:C8H14O3
Honeysuckle, also known as:Honeysuckle, Caulis Lonicerae, silvernine, two dyeing defect rattans, two precious rattans, right-hand rotation rattan, sub- wind rattan, mandarin duck rattan, (scientific name:Lonicera japonica)." honeysuckle " one is come from《Compendium of Materia Medica》, it is rear to turn because honeysuckle flowers are just opened as white For yellow, hence obtain one's name honeysuckle.Medicinal material honeysuckle is Caprifoliaceae woodbine honeysuckle and congener dry flower or band The flower just opened.Honeysuckle, March bloom, and five go out, micro-perfume, and base of a fruit band is red, and then color is white by Hua Chukai, through one, two day then color it is yellow, it is therefore named Honeysuckle.Again because a base of a fruit two is spent, two pistils are visited outside, in pairs, are never left each other, and shape is such as male female associated, and like mandarin duck To dance, therefore there is the title of mandarin duck rattan.Honeysuckle is described as clearing heat and detoxicating good medicine from ancient times.Its property sweet cold air fragrance, clear heat with drugs of sweet flavour and cold nature and Do not injure one's stomach, fragrance reaches thoroughly again can eliminating evil.Honeysuckle can dispelling wind-heat, also kind removing summer-heat blood poison, for various febrile diseases, such as body The diseases such as heat, dermexanthesis, hair spot, heat toxin sore carbuncle, abscess of throat, equal significant effect.《Sheng Nong's herbal classic》Carry:" honeysuckle is cold in nature sweet, The effect of being become silted up with clearing heat and detoxicating, cool bloodization, cure mainly affection of exogenous wind-heat, seasonal febrile diseases from the beginning of, sore serious case of furuncle, red and swollen heat pain, passing stool with pus and blood " Deng.《Compendium of Materia Medica》In honeysuckle has been discussed in detail there is the effect of " long term usage is made light of one's life by commiting suicide, promoted longevity ".Twentieth century 80 years Generation, health ministry have successively carried out chemical analysis to honeysuckle, the results showed that:It is necessary micro that honeysuckle contains a variety of human bodies Element and chemical composition, simultaneously containing a variety of active enzyme materials favourable to human body, there is anti-aging, anti-canceration, make light of one's life by commiting suicide and be healthy and strong Good effects.Honeysuckle cultivates record and sees the Song Dynasty earliest《Writing brush good recipe in Soviet Union Shen》, wherein claiming:" between the column of removable front yard, in case It is anxious." many local county annals are also on the books, such as letter out thread 22 years《Fei County will》Claim:" flower has yellowish-white therefore named honeysuckle, in the past Between have it, but adopt with for tea, at the beginning of Jiaqing, travelling merchants are bought to resell toward elsewhere, and several years mountain angle water river bank is not transplanted several times." it follows that gold Honeysuckle flower has long cultivation history.State Administration of Traditional Chinese Medicine in 1984 is defined as one of 35 kinds of rare traditional Chinese medicines, after To be confirmed as dietotherapeutic kind again.Honeysuckle medicinal history is long, and before 3000, our ancestors begin to anti-with it Disease is controlled,《Mingyi Bielu》In be listed in top grade.
Sweet wormwood (Artemisia carvifolia) annual herb.Stem is upright, top multi-branched, has vertical rib line.Leaf Alternate, the leaf two in the middle part of stem return pinnation, linear lobelet.Summer-flowering, capitulum hemispherical is most, into circular cone Shape, floral tube shape, outside are female flower, and internal layer is hermaphrodite flower.The certified products of Chinese medicine " sweet wormwood ", Chinese medicine sweet wormwood, it is feverfew sweet wormwoodArtemisia annua L.Dry aerial parts.Bud stage harvests, and extracts aerial part, shreds, dries.Ancient name " Qin " (q ìn).Clearing away summerheat, except steaming, preventing malaria.Generated heat for summer-heat evil, fever due to yin deficiency, night fever abating at dawn, hectic fever due to yin labor is hot, and malaria fever and chills are damp and hot Jaundice.It is a kind of cheap Anti-Malarial.Sweet wormwood stem cylinder, top branch is long 30 to 80 centimetres, 0.2 to 0.6 li of diameter Rice;Surface yellow green or brown color, has vertical rib line;Matter is slightly hard, frangibility, has marrow in the middle part of section.Leaf alternate, dirty-green or brown green Color, crispatura frangible, complete person is in three times pinniform drastic cracks, lobelet square circle or oblong, and two sides is by undercoat.Gas is fragrant special, Mildly bitter flavor, there is refrigerant sense.Green with color, Ye Duo, the dense person of fragrance is preferred.Function is with curing mainly:Clear abnormal heat, cool blood, except steaming, are cut except steaming Malaria.Generated heat for summer-heat evil, fever due to yin deficiency, night fever abating at dawn, hectic fever due to yin labor heat, malaria fever and chills, jaundice with damp-heat pathogen.The product bitter-cold herbs expelling heat, it is pungent It is fragrant to dissipate thoroughly, it is kind to make the moon divide latent heat to be dissipated thoroughly up to outer, it is fever due to yin deficiency key medicine, has relieving summer-heat concurrently in addition, cuts cruel work(.
Pyrrosia lingua (Latin literary fame:Pyrrosia lingua (Thunb.) Farwell) Polypodiaceaes, Genus Pyrrosia be medium-sized attached Raw pteridophyte, plant is up to 30 centimetres.It is horizontal walk root-like stock, scale lanceolar, Ye Yuansheng, do after keratin, above celadon, spore Telium is closely oval, is at the beginning starlike light brown, and maturation is in brick-red.Grow nonparasitically upon another plant on low altitude area sylvan life trunk, or it is slightly dry On rock, height above sea level 100-1800 rice.It is distributed in China, India, Vietnam, Korea and Japan.Pyrrosia lingua alias:Stone Zhe (《This warp》), Stone skin (《Do not record》), stone reed (《The southern regions of the Yunnan Province book on Chinese herbal medicine》), bigfruit phymatopsis herb, Shi Lan (《Detailed outline》), it is raw pull (《Classify herbal》), rainbow sword Grass, Shi Jian, pool sword (《Fujian traditional herbal medicine》), golden soupspoon, stone the back of the body willow (《Chinese medicine handbook》), pyrrosia lingua, its nature and flavor is sweet, bitter, micro- It is cold.Enter lung, bladder warp.There is the effect of expelling the heat-evil etc. of promoting diuresis for stranguria, clearing lung-heat.Energy clearing away damp-heat, diuresis lead to beautiful jade, control knife wound, scald, de- power void Damage.
Beneficial effects of the present invention are:
The antibacterial anti-mite adopted silk work flow of mulberry silk of the present invention is short, starts from from matured silkworm spinning, artificially breaks The normal habit that silkworms spin silk, change traditional cluster tool condition that silkworm cocooning needs, instead of with plane spinning net, making matured silkworm in net Upper directly spinning forms plane silkworm silk floss sheet, instead of matured silkworm spinning cocoon → the continuous traditional silk floss of cocoon drying → system is processed Journey, processing are easier;Traditional diamond-making technique can pollute cocoon layer by pupal fat caused by cocoon drying, and obtained silk floss sheet oil-containing is higher, and by Matured silkworm directly spins more excellent without rib, without pupal fat, quality into silk floss.Need to add in the process such as traditional system is continuous, white silk silk floss Chemical assistant, a small amount of chemical residual is had, and cause a certain degree of environmental pollution, pure mulberry silk quilt provided by the invention Preparation method employs the continuous method of boiling of uniqueness, the scouring processes of continuous piece need not using the plane silk floss that matured silkworm spues as raw material Chemical assistant, more natural environmental-protective are added, while reduces processing cost.Honeysuckle, sweet wormwood and pyrrosia lingua are placed with mulberry silk quilt, is had There is light fragrance, play antibacterial anti-mite effect;Farina is prepared into Potato Porous Starch by enzymatic treatment, used Potato Porous Starch and water soluble chitosan prepare coating agent, and then hybrid particles are coated with processing;Farina Cost is low, and preparation method is simple;And coating agent can delay the fragrance release of mixing, fragrance release is slow, and fragrance can be protected for a long time Hold;If finding humidity using a period of time, dried as long as being put into time below sunlight, it is impossible to be exposed to the sun, fragrance can keep one More than year.
Embodiment
With reference to embodiment, the technical scheme in invention is clearly and completely described, described embodiment is only Only it is the part of the present invention, rather than whole embodiments.
Embodiment 1
Complete that antibacterial anti-mite mulberry silk quilt can be made using following steps:
(1)The matured silkworm for emptying fecaluria is put into spinning on the net, the density of matured silkworm is 800-900 Tiao/㎡.Described spinning net is flat Plate spinning net, its mesh width is 2-5 millimeters, and the thickness for the net that spins is 1-2 millimeters.
(2)After matured silkworm spinning terminates, silk is peeled off from spinning is online, obtains smooth hair silk floss piece.
(3)Practiced with 98-100 DEG C of temperature, the hydrogen peroxide solution that mass percentage concentration is 4% and boil 30-40 minutes, to hair silk floss piece Degumming process is carried out, until content of silk gum is 2.5-3.5%.
(4)The continuous piece after degumming is cleaned up with clear water, then is placed into dewaterer and carries out dewater treatment.
(5)Continuous piece after dehydration is dried after the Shape correction that cleans, and obtains doing continuous piece, standby;Drying temperature is 65-85 degree, regain are controlled below 12%.
(6)Dry continuous piece weight as needed is weighed, pullled after weighing, makes continuous piece fluffy.
(7)Cut according to cotton-wadded quilt size to doing continuous piece.
(8)Dry continuous piece is divided into two parts, does the continuous crisscross laying of piece on platform by two parts respectively, after the completion of laying, Inspection arrangement is carried out to upper and lower surface, goes the removal of impurity and stiff bar.
(9)It will check that two parts put in order dry continuous piece top and bottom respectively place one layer of anti-gauze cloth that runs and get ready and fix respectively It is good, avoid running silk, obtain two silk floss batting cores.
(10)Two silk floss batting cores are overlapped, put cotton tire set, suture is got on three sides ready, makes silk floss batting core and two gauzes Tire core fixes, wherein while staying mouth to turn into tire core bag;Bar tied rope is respectively left in corner in tire core bag.Described tire set is using high branch Highly dense pure cotton cloth is made.Described tire set is made of high-count and high-density pure cotton cloth.
(11)Clean honeysuckle, sweet wormwood and pyrrosia lingua are plucked, 2~5min is dried with microwave vacuum low-temperature drying machine, makes to contain Water is less than 10%, is saved backup with plastic bag sealing.Microwave vacuum low-temperature drying machine is in the limited public affairs of Guangzhou Yong Ze microwave energy equipment Department's purchase, network address:http://www.gz-yongze.com/, address:Guangzhou, Guangdong Baiyun District good farmland town Jin Pan industrial areas No. 8.
(12)It is 2 by weight after honeysuckle, sweet wormwood and pyrrosia lingua are broken into powder respectively:3:1 is well mixed;Sprinkling is suitable Amount carboxymethyl cellulose gum sticks agent and is pressed into grain shape, and the hybrid particles of even particle size are obtained through screening.Spray carboxymethyl The amount of cellulose adhesive enables honeysuckle, sweet wormwood and pyrrosia lingua powder to be pressed into particle.Particle is unsuitable excessive, like cassia seed size It is advisable.
(13)Mixing is coated using coating agent made of Potato Porous Starch slurries and water soluble chitosan, will Hybrid particles and coating agent are with 6-8:1 weight makes hybrid particles surface be wrapped in one layer of coating agent, after coating than mixing Hybrid particles dry 3~5min in microwave vacuum low-temperature drying machine, water content is less than 10%.
(14)Non-woven fabrics is selected according to tire core bag inside dimension, doubling sewing margin to seam, while stay mouth, turned welt is into non-woven bag.
(15)Hybrid particles after coating are put into non-woven bag, then non-woven bag is shakeout on work top, nothing The hybrid particles spun in cloth bag shakeout, it is impossible to and allow hybrid particles to stack, then open-wire line sealing, non-woven bag is finally subjected to netted sew with long stitches Seam, avoids hybrid particles from walking, corner is sewed with tied rope, turns into hybrid particles tire.
(16)Finally hybrid particles tire corner is fixed in tire core bag by tied rope, then fetal rhythm bag is placed in quilt cover .After hybrid particles tire does not have fragrance, change hybrid particles tire or can obtain new silk after removing hybrid particles tire Cotton quilt.
The hydrogen peroxide solution that described mass percentage concentration is 4% is by hydrogen peroxide, sodium metasilicate, sodium EDTA salt It is formulated with clear water, the weight ratio of hydrogen peroxide, sodium metasilicate and sodium EDTA salt is(2-3):(0.5-0.8):(0.2- 0.3).
Described coating agent is that suitable quantity of water slurrying is added after peeling potatoes are cooked and is digested, and enzymatic hydrolysis condition is:Saccharification Enzyme:α~amylase=2:1, farinaceous size concentration 30%, enzyme concentration 1.2%, 55 DEG C, reaction time 12h of reaction temperature, reaction system PH is 5~6, prepares Potato Porous Starch;Then it is 5000~10000 that molecular weight is added into Potato Porous Starch slurries Water soluble chitosan stir, Potato Porous Starch and water soluble chitosan weight content are 2:1, obtain moisture content 40 ~60% coating agent solutions;5% carbon dioxide is filled with by coating agent weight so that coating agent solutions carry more gas Bubble.
Described carboxymethyl cellulose gum sticks what agent was formed by carboxymethyl cellulose with appropriate water modulation, wherein carboxymethyl Cellulose is prepared by being acted in the basic conditions by monochloroacetic acid and cellulose, and quaternization occurs for cellulose and alkali effect Alkali cellulose is generated, alkali cellulose occurs etherification reaction with monochloroacetic acid again, obtains carboxymethyl cellulose.
Embodiment 2
Complete that antibacterial anti-mite mulberry silk quilt can be made using following steps:
(1)The matured silkworm for emptying fecaluria is put into spinning on the net, the density of matured silkworm is 800-900 Tiao/㎡.Described spinning net is flat Plate spinning net, its mesh width is 2-5 millimeters, and the thickness for the net that spins is 1-2 millimeters.
(2)After matured silkworm spinning terminates, silk is peeled off from spinning is online, obtains smooth hair silk floss piece.
(3)Practiced with 98-100 DEG C of temperature, the hydrogen peroxide solution that mass percentage concentration is 4% and boil 30-40 minutes, to hair silk floss piece Degumming process is carried out, until content of silk gum is 2.5-3.5%;Refiningly cook before terminating 5 minutes, add hydrogen peroxide solution weight 1.5-2% Ethylene glycol diglycidylether.
(4)The continuous piece after degumming is cleaned up with clear water, then is placed into dewaterer and carries out dewater treatment.
(5)Continuous piece after dehydration is dried after the Shape correction that cleans, and obtains doing continuous piece, standby;Drying temperature is 65-85 degree, regain are controlled below 12%.
(6)Dry continuous piece weight as needed is weighed, pullled after weighing, makes continuous piece fluffy.
(7)Cut according to cotton-wadded quilt size to doing continuous piece.
(8)Dry continuous piece is divided into two parts, does the continuous crisscross laying of piece on platform by two parts respectively, after the completion of laying, Inspection arrangement is carried out to upper and lower surface, goes the removal of impurity and stiff bar.
(9)It will check that two parts put in order dry continuous piece top and bottom respectively place one layer of anti-gauze cloth that runs and get ready and fix respectively It is good, avoid running silk, obtain two silk floss batting cores.
(10)Two silk floss batting cores are overlapped, put cotton tire set, suture is got on three sides ready, makes silk floss batting core and two gauzes Tire core fixes, wherein while staying mouth to turn into tire core bag;Bar tied rope is respectively left in corner in tire core bag.Described tire set is using high branch Highly dense pure cotton cloth is made.Described tire set is made of high-count and high-density pure cotton cloth.
(11)Clean honeysuckle, sweet wormwood and pyrrosia lingua are plucked, 2~5min is dried with microwave vacuum low-temperature drying machine, makes to contain Water is less than 10%, is saved backup with plastic bag sealing.Microwave vacuum low-temperature drying machine is in the limited public affairs of Guangzhou Yong Ze microwave energy equipment Department's purchase, network address:http://www.gz-yongze.com/, address:Guangzhou, Guangdong Baiyun District good farmland town Jin Pan industrial areas No. 8.
(12)It is 2 by weight after honeysuckle, sweet wormwood and pyrrosia lingua are broken into powder respectively:3:1 is well mixed;Sprinkling is suitable Amount carboxymethyl cellulose gum sticks agent and is pressed into grain shape, and the hybrid particles of even particle size are obtained through screening.Spray carboxymethyl The amount of cellulose adhesive enables honeysuckle, sweet wormwood and pyrrosia lingua powder to be pressed into particle.Particle is unsuitable excessive, like cassia seed size It is advisable.
(13)Mixing is coated using coating agent made of Potato Porous Starch slurries and water soluble chitosan, will Hybrid particles and coating agent are with 6-8:1 weight makes hybrid particles surface be wrapped in one layer of coating agent, after coating than mixing Hybrid particles dry 3~5min in microwave vacuum low-temperature drying machine, water content is less than 10%.
(14)Non-woven fabrics is selected according to tire core bag inside dimension, doubling sewing margin to seam, while stay mouth, turned welt is into non-woven bag.
(15)Hybrid particles after coating are put into non-woven bag, then non-woven bag is shakeout on work top, nothing The hybrid particles spun in cloth bag shakeout, it is impossible to and allow hybrid particles to stack, then open-wire line sealing, non-woven bag is finally subjected to netted sew with long stitches Seam, avoids hybrid particles from walking, corner is sewed with tied rope, turns into hybrid particles tire.
(16)Finally hybrid particles tire corner is fixed in tire core bag by tied rope, then fetal rhythm bag is placed in quilt cover .After hybrid particles tire does not have fragrance, change hybrid particles tire or can obtain new silk after removing hybrid particles tire Cotton quilt.
The hydrogen peroxide solution that described mass percentage concentration is 4% is by hydrogen peroxide, sodium metasilicate, sodium EDTA salt It is formulated with clear water, the weight ratio of hydrogen peroxide, sodium metasilicate and sodium EDTA salt is(2-3):(0.5-0.8):(0.2- 0.3).
Described coating agent is that suitable quantity of water slurrying is added after peeling potatoes are cooked and is digested, and enzymatic hydrolysis condition is:Saccharification Enzyme:α~amylase=2:1, farinaceous size concentration 30%, enzyme concentration 1.2%, 55 DEG C, reaction time 12h of reaction temperature, reaction system PH is 5~6, prepares Potato Porous Starch;Then it is 5000~10000 that molecular weight is added into Potato Porous Starch slurries Water soluble chitosan stir, Potato Porous Starch and water soluble chitosan weight content are 2:1, obtain moisture content 40 ~60% coating agent solutions;5% carbon dioxide is filled with by coating agent weight so that coating agent solutions carry more gas Bubble.
Described carboxymethyl cellulose gum sticks what agent was formed by carboxymethyl cellulose with appropriate water modulation, wherein carboxymethyl Cellulose is prepared by being acted in the basic conditions by monochloroacetic acid and cellulose, and quaternization occurs for cellulose and alkali effect Alkali cellulose is generated, alkali cellulose occurs etherification reaction with monochloroacetic acid again, obtains carboxymethyl cellulose.
Application Example
1st, Hengxian County's silk company, the said firm use the antibacterial anti-mite mulberry silk quilt of the present invention to 10 volunteers, should Quilt has light fragrance, after 10 volunteers use three months, detect sheet and silk quilt find no it is common on sheet Bacterium and acarid.
Described above is not limitation of the present invention, and the present invention is also not limited to examples detailed above, the art it is general Logical technical staff, in the essential scope of the present invention, the variations, modifications, additions or substitutions made, it should all belong to the guarantor of the present invention Protect scope.

Claims (7)

  1. A kind of 1. antibacterial anti-mite mulberry silk quilt, it is characterised in that:It is made of following processing step:
    (1)The matured silkworm for emptying fecaluria is put into spinning on the net, the density of matured silkworm is 800-900 Tiao/㎡;
    (2)After matured silkworm spinning terminates, silk is peeled off from spinning is online, obtains smooth hair silk floss piece;
    (3)Practiced with 98-100 DEG C of temperature, the hydrogen peroxide solution that mass percentage concentration is 4% and boil 30-40 minutes, hair silk floss piece is carried out Degumming process, until content of silk gum is 2.5-3.5%;
    (4)The continuous piece after degumming is cleaned up with clear water, then is placed into dewaterer and carries out dewater treatment;
    (5)Continuous piece after dehydration is dried after the Shape correction that cleans, and obtains doing continuous piece, standby;Drying temperature is 65-85 Degree, regain are controlled below 12%;
    (6)Dry continuous piece weight as needed is weighed, pullled after weighing, makes continuous piece fluffy;
    (7)Cut according to cotton-wadded quilt size to doing continuous piece;
    (8)Dry continuous piece is divided into two parts, the continuous crisscross laying of piece is done on platform by two parts respectively, after the completion of laying, to upper Lower two sides carries out inspection arrangement, goes the removal of impurity and stiff bar;
    (9)It will check that two parts put in order dry continuous piece top and bottom respectively place one layer of anti-gauze cloth that runs and get ready and fix respectively, keep away Exempt to run silk, obtain two silk floss batting cores;
    (10)Two silk floss batting cores are overlapped, put cotton tire set, suture is got on three sides ready, makes silk floss batting core and two gauze tire cores Fix, wherein while staying mouth to turn into tire core bag;Bar tied rope is respectively left in corner in tire core bag;
    (11)Clean honeysuckle, sweet wormwood and pyrrosia lingua are plucked, 2~5min is dried with microwave vacuum low-temperature drying machine, makes water content Less than 10%, saved backup with plastic bag sealing;
    (12)It is 2 by weight after honeysuckle, sweet wormwood and pyrrosia lingua are broken into powder respectively:3:1 is well mixed;Spray appropriate carboxylic Methylcellulose adhesive is pressed into grain shape, and the hybrid particles of even particle size are obtained through screening;
    (13)Mixing is coated using coating agent made of Potato Porous Starch slurries and water soluble chitosan, will be mixed Particle and coating agent are with 6-8:1 weight makes hybrid particles surface be wrapped in one layer of coating agent, the mixing after coating than mixing Particle dries 3~5min in microwave vacuum low-temperature drying machine, water content is less than 10%;
    (14)Non-woven fabrics is selected according to tire core bag inside dimension, doubling sewing margin to seam, while stay mouth, turned welt is into non-woven bag;
    (15)Hybrid particles after coating are put into non-woven bag, then non-woven bag is shakeout on work top, non-woven fabrics Hybrid particles in bag shakeout, it is impossible to and allow hybrid particles to stack, then open-wire line sealing, non-woven bag is finally subjected to netted quilting, Hybrid particles are avoided to walk, corner is sewed with tied rope, turns into hybrid particles tire;
    (16)Finally hybrid particles tire corner is fixed in tire core bag by tied rope, then fetal rhythm bag is placed in quilt cover i.e. Can.
  2. 2. antibacterial anti-mite mulberry silk quilt according to claim 1, it is characterised in that:Described mass percentage concentration is 4% Hydrogen peroxide solution be to be formulated by hydrogen peroxide, sodium metasilicate, sodium EDTA salt and clear water, hydrogen peroxide, sodium metasilicate and The weight ratio of sodium EDTA salt is(2-3):(0.5-0.8):(0.2-0.3).
  3. 3. antibacterial anti-mite mulberry silk quilt according to claim 1, it is characterised in that:Described tire set is pure using high-count and high-density Cotton is made.
  4. 4. antibacterial anti-mite mulberry silk quilt according to claim 1, it is characterised in that:Described spinning net spins for flat board Net, its mesh width are 2-5 millimeters, and the thickness for the net that spins is 1-2 millimeters.
  5. 5. antibacterial anti-mite mulberry silk quilt according to claim 1, it is characterised in that:Described coating agent is to go potato Suitable quantity of water slurrying is added after skin is cooked and is digested, enzymatic hydrolysis condition is:Carbohydrase:α~amylase=2:1, farinaceous size concentration 30%, Enzyme concentration 1.2%, 55 DEG C, reaction time 12h, reaction system pH of reaction temperature are 5~6, prepare Potato Porous Starch;Then Add the water soluble chitosan that molecular weight is 5000~10000 into Potato Porous Starch slurries to stir, potato is more Hole starch is 2 with water soluble chitosan weight content:1, obtain the coating agent solutions of moisture content 40~60%;By coating agent weight It is filled with 5% carbon dioxide so that coating agent solutions carry more bubble.
  6. 6. antibacterial anti-mite mulberry silk quilt according to claim 1, it is characterised in that:Described carboxymethyl cellulose gum sticks agent Formed by carboxymethyl cellulose with appropriate water modulation, wherein carboxymethyl cellulose is in alkalescence by monochloroacetic acid and cellulose Under the conditions of prepared by acting on, quaternization generation alkali cellulose occurs for cellulose and alkali effect, alkali cellulose again with a chlorine vinegar Etherification reaction occurs for acid, obtains carboxymethyl cellulose.
  7. 7. antibacterial anti-mite mulberry silk quilt according to claim 1, it is characterised in that:5 minutes before end is refiningly cooked, add double Oxygen aqueous solution weight 1.5-2% ethylene glycol diglycidylether.
CN201710776404.3A 2017-09-01 2017-09-01 A kind of antibacterial anti-mite mulberry silk quilt Pending CN107595026A (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202234360U (en) * 2011-07-29 2012-05-30 吴江征明纺织有限公司 Bacterium isolation and mite prevention bedding set
CN104117083A (en) * 2014-08-15 2014-10-29 汪建 Chinese herbal medicine preparation
GB2521853A (en) * 2014-01-06 2015-07-08 Fast Engineering Ltd High security blanket
CN106263886A (en) * 2016-08-31 2017-01-04 横县桂华茧丝绸有限责任公司 A kind of preparation method of pure mulberry silk quilt
CN106419443A (en) * 2016-09-22 2017-02-22 广西棕海园林工程有限公司 Antibacterial carpet

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202234360U (en) * 2011-07-29 2012-05-30 吴江征明纺织有限公司 Bacterium isolation and mite prevention bedding set
GB2521853A (en) * 2014-01-06 2015-07-08 Fast Engineering Ltd High security blanket
CN104117083A (en) * 2014-08-15 2014-10-29 汪建 Chinese herbal medicine preparation
CN106263886A (en) * 2016-08-31 2017-01-04 横县桂华茧丝绸有限责任公司 A kind of preparation method of pure mulberry silk quilt
CN106419443A (en) * 2016-09-22 2017-02-22 广西棕海园林工程有限公司 Antibacterial carpet

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Application publication date: 20180119