CN107536351A - A kind of cape jasmine fragrance of a flower mulberry silk quilt - Google Patents

A kind of cape jasmine fragrance of a flower mulberry silk quilt Download PDF

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Publication number
CN107536351A
CN107536351A CN201710775483.6A CN201710775483A CN107536351A CN 107536351 A CN107536351 A CN 107536351A CN 201710775483 A CN201710775483 A CN 201710775483A CN 107536351 A CN107536351 A CN 107536351A
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China
Prior art keywords
hybrid particles
tire
cape jasmine
continuous piece
silk
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CN201710775483.6A
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Inventor
卢受坤
胡勇
黄农审
张同洪
黄娇连
梁晓玲
梁就荣
宋志谊
杨兴
黄小龙
梁有
黄杰容
辛德强
苏小林
甘少秋
麦巧燕
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Guangxi Guihua Silk Co Ltd
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Guangxi Guihua Silk Co Ltd
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Priority to CN201710775483.6A priority Critical patent/CN107536351A/en
Publication of CN107536351A publication Critical patent/CN107536351A/en
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Abstract

A kind of cape jasmine fragrance of a flower mulberry silk quilt, making step are:(1)It is online that matured silkworm is put into spinning;(2)Strip hair silk floss piece;(3)The continuous piece degumming process of hair;(4)Cleaning and dewatering;(5)Continuous piece drying;(6)Continuous piece is weighed;(7)Cut continuous piece;(8)Continuous piece is pulled open one by one and is divided into two parts, respectively by two parts of continuous piece layings;(9)Put anti-race gauze cloth in continuous piece top and bottom;(10)Two parts of continuous one layer of tire sets of piece overcoat, three sides are got ready suture respectively, while staying mouth to turn into tire core bag;(11)Choose gardenia bud;(12)Dry gardenia bud;(13)Prepare hybrid particles;(14)Hybrid particles coating, drying;(15)Prepare non-woven bag;(16)Prepare hybrid particles tire;(17)Finally hybrid particles tire is fixed in tire core bag, then tire core bag is placed in quilt cover.The mulberry silk quilt good product quality, cape jasmine flowery odour can be distributed, and fragrance release is slow, fragrance can be kept for a long time.

Description

A kind of cape jasmine fragrance of a flower mulberry silk quilt
Technical field
The present invention relates to the processing technique field of mulberry silk quilt, specifically a kind of cape jasmine fragrance of a flower mulberry silk quilt and its preparation Method.
Background technology
Silk quilt is a kind of quilt using silk fiber as filler, and its silk fiber is to use silk cocoon or filature byproduct It is process, silk floss manufacturing process is that matured silkworm spinning is cocoond → silk floss → arrangement → baking is washed in cocoon drying → system continuous → practicing continuous → continuous, tradition Processing method can pollute cocoon layer by pupal fat caused by cocoon drying, and obtained silk floss sheet oil-containing is higher;Needed in the process such as system is continuous, white silk silk floss Chemical assistant is added, has a small amount of chemical residual, and causes a certain degree of environmental pollution.In order to obtain more natural environmental-protective Silk silk floss raw material, the present invention research it is a kind of from matured silkworm spinning starts from silk floss, artificially break the normal habit that silkworms spin silk, Change traditional cluster tool condition that silkworm cocooning needs, instead of with plane spinning net, making matured silkworm be formed in online directly spinning flat The silkworm silk floss sheet of planar, instead of matured silkworm spinning and cocoons → continuous traditional silk floss the process of cocoon drying → system, and processing is easier;Pass Processing method of uniting can pollute cocoon layer by pupal fat caused by cocoon drying, and obtained silk floss sheet oil-containing is higher, and directly spins into silk floss by matured silkworm Without rib, it is more excellent without pupal fat, quality.Need to add chemical assistant in the process such as traditional system is continuous, white silk silk floss, have few The chemical residual of amount, and a certain degree of environmental pollution is caused, the preparation method of pure mulberry silk quilt provided by the invention is with matured silkworm The plane silk floss of discharge is as raw material, and employ uniqueness boils continuous method, and the scouring processes of continuous piece need not add chemical assistant, more Natural environmental-protective, while reduce processing cost.
As the improvement of people's living standards, existing silk quilt can not meet the needs of people, therefore, develop A kind of more natural environmental-protective, and the silk quilt that can distribute floral odor is desirability.
The content of the invention
It is an object of the invention to provide a kind of cape jasmine fragrance of a flower mulberry silk quilt, the mulberry silk quilt good product quality, mulberry silk quilt In be placed with gardenia and cape jasmine flower essential oil, cape jasmine flowery odour can be distributed, and fragrance release is slow, fragrance can be kept for a long time.
To achieve these goals, the present invention adopts the technical scheme that:
A kind of cape jasmine fragrance of a flower mulberry silk quilt, is made of following processing step:
(1)The matured silkworm for emptying fecaluria is put into spinning on the net, the density of matured silkworm is 800-900 Tiao/㎡.Described spinning net is flat Plate spinning net, its mesh width is 2-5 millimeters, and spinning net is flat board spinning net, and its thickness is 1-2 millimeters.
(2)After matured silkworm spinning terminates, silk is peeled off from spinning is online, obtains smooth hair silk floss piece.
(3)Practiced with 98-100 DEG C of temperature, the hydrogen peroxide solution that mass percentage concentration is 4% and boil 30-40 minutes, to hair silk floss piece Degumming process is carried out, until content of silk gum is 2.5-3.5%.
(4)The continuous piece after degumming is cleaned up with clear water, then is placed into dewaterer and carries out dewater treatment.
(5)Continuous piece after dehydration is dried after the Shape correction that cleans, and obtains doing continuous piece, standby;Drying temperature is 65-85 degree, regain are controlled below 12%.
(6)Dry continuous piece weight as needed is weighed, pullled after weighing, makes continuous piece fluffy.
(7)Cut according to cotton-wadded quilt size to doing continuous piece.
(8)Dry continuous piece is divided into two parts, does the continuous crisscross laying of piece on platform by two parts respectively, after the completion of laying, Inspection arrangement is carried out to upper and lower surface, goes the removal of impurity and stiff bar.
(9)It will check that two parts put in order dry continuous piece top and bottom respectively place one layer of anti-gauze cloth that runs and get ready and fix respectively It is good, avoid running silk, obtain two silk floss batting cores.
(10)Two silk floss batting cores are overlapped, put cotton tire set, suture is got on three sides ready, makes silk floss batting core and two gauzes Tire core fixes, wherein while staying mouth to turn into tire core bag;Bar tied rope is respectively left in corner in tire core bag.Described tire set is using high branch Highly dense pure cotton cloth is made.
(11)Selected just open gardenia bud, is placed in constant temperature basement, constant temperature basement temperature control is 25 DEG C -30 DEG C, relative humidity 70%-80%.
(12)Gardenia bud is dried into 1~4min with microwave vacuum low-temperature drying machine, water content is less than 10%, with modeling Pocket is sealed standby.Microwave vacuum low-temperature drying machine is bought in Guangzhou Yong Ze microwave energy equipment Co., Ltd, network address: http://www.gz-yongze.com/, address:Guangzhou, Guangdong Baiyun District good farmland town Jin Pan industrial areas 8.
(13)After gardenia bud after drying is broken into powder, add cape jasmine flower essential oil be well mixed, cape jasmine pollen and The weight ratio of cape jasmine flower essential oil is 100:0.1;The glutinous agent of appropriate carboxymethyl cellulose gum is sprayed again and is pressed into grain shape, through screening To the hybrid particles of even particle size.The amount that sprinkling carboxymethyl cellulose gum sticks agent enables cape jasmine pollen to be pressed into particle. Particle is unsuitable excessive, is advisable like cassia seed size.
(14)Hybrid particles are coated using coating agent made of sweet potato porous-starch slurries and water soluble chitosan, By hybrid particles and coating agent with 6-8:1 weight makes hybrid particles surface be wrapped in one layer of coating agent, after coating than mixing Hybrid particles microwave vacuum low-temperature drying machine dry 2~3min, it is 8-10% to make coating water content.
(15)Non-woven fabrics is selected according to tire core bag inside dimension, doubling sewing, while stay mouth, turned welt is into non-woven bag.
(16)Hybrid particles after coating are put into non-woven bag, then non-woven bag is shakeout on work top, nothing The hybrid particles spun in cloth bag shakeout, it is impossible to and allow hybrid particles to stack, then open-wire line sealing, non-woven bag is finally subjected to netted sew with long stitches Seam, avoids hybrid particles from walking, corner is sewed with tied rope, turns into hybrid particles tire.
(17)Finally hybrid particles tire corner is fixed in tire core bag by tied rope, then tire core bag is placed in quilt cover .
After hybrid particles tire does not have fragrance, change hybrid particles tire or remove can obtain after hybrid particles tire it is new Silk wadding quilt.
The hydrogen peroxide solution that described mass percentage concentration is 4% is by hydrogen peroxide, sodium metasilicate, sodium EDTA salt It is formulated with clear water, the weight ratio of hydrogen peroxide, sodium metasilicate and sodium EDTA salt is(2-3):(0.5-0.8):(0.2- 0.3).
Described coating agent is that sweet potato is removed the peel into cooked addition suitable quantity of water slurrying and digested, and enzymatic hydrolysis condition is:Carbohydrase:α ~amylase=2:1, farinaceous size concentration 30%, enzyme concentration 1.5%, 55 DEG C, reaction time 12h, reaction system pH of reaction temperature is 5~6, prepare sweet potato porous-starch;Then the water solubility that molecular weight is 5000~10000 is added into sweet potato porous-starch slurries Chitosan stirs, and sweet potato porous-starch is 2 with water soluble chitosan weight content:1, obtain the bag of moisture content 40~60% Clothing agent solution;5% carbon dioxide is filled with by coating agent weight so that coating agent solutions carry more bubble.
Described carboxymethyl cellulose gum sticks what agent was formed by carboxymethyl cellulose with appropriate water modulation, wherein carboxymethyl Cellulose is prepared by being acted in the basic conditions by monochloroacetic acid and cellulose, and quaternization occurs for cellulose and alkali effect Alkali cellulose is generated, alkali cellulose occurs etherification reaction with monochloroacetic acid again, obtains carboxymethyl cellulose.
In order that silk floss has more preferable intensity and pliability, 5 minutes before end is refiningly cooked to hair silk floss piece, hydrogen peroxide is added Solution weight 1.5-2% ethylene glycol diglycidylether;Ethylene glycol diglycidylether, English name:Glycol Diglycidyl ether, alias:Tetramethyl ammonium chloride tetramethyl ammonium chloride tetramethyl ammonium chloride, No. CAS:2224-15-9, point Minor:C8H14O3
Gardenia, scientific name:Gardenia jasminoides, genus rubia section, originate in China, be mainly distributed on Guizhou, The ground such as Sichuan, Jiangsu, Zhejiang, Anhui, Jiangxi, Guangdong, Yunnan, Fujian, Taiwan, Hunan, Hubei, it is that important garden views and admires plant Thing.Its flower, fruit, leaf and Gen Ke are used as medicine, and have a purging intense heat relieving restlessness, reducing fever and causing diuresis, the effect of removing pattogenic heat from the blood and toxic material from the body.Flower can make the spices of tea, Fruit can anti-inflammatory dispel heat, be excellent fragrant flower.At present, gardenia concrete is produced with gardenia, is widely used in cosmetics perfume Material and food flavor;Gardenia flower oil is used to prepare a variety of floral type perfume, perfumed soap, cosmetic essence etc..In addition, by gardenia flower oil Benzyl acetate and bergamio it is isolated out, as daily make up conventional type-odor or blender, be also commonly used for food perfume Essence.
Beneficial effects of the present invention are:
The silk silk floss that the cape jasmine fragrance of a flower mulberry silk quilt of the present invention uses and preparation method thereof work flow is short, since spinning matured silkworm Make, artificially break the normal habit that silkworms spin silk, change traditional cluster tool condition that silkworm cocooning needs, with plane spinning net generation Replace, matured silkworm is formed plane silkworm silk floss sheet in online directly spinning, instead of matured silkworm spinning cocoon → cocoon drying → system is continuous Traditional silk floss process, processing are easier;Traditional diamond-making technique can pollute cocoon layer, obtained silk floss sheet by pupal fat caused by cocoon drying Oil-containing is higher, and directly spun into by matured silkworm silk floss without rib, it is more excellent without pupal fat, quality.Traditional system is continuous, it is processed to practice silk floss etc. Need to add chemical assistant in journey, have a small amount of chemical residual, and cause a certain degree of environmental pollution, it is provided by the invention The preparation method of pure mulberry silk quilt employs the continuous method of boiling of uniqueness using the plane silk floss that matured silkworm spues as raw material, and continuous piece takes off Glue process need not add chemical assistant, more natural environmental-protective, while reduce processing cost.The application is claimed small using Guangxi locality people The gardenia of yulan is added in mulberry silk quilt, obtains cape jasmine fragrance of a flower silk quilt.The cape jasmine fragrance of a flower silk quilt has unique sweet smell Perfume (or spice) makes people happy, and has certain sedative action.The Industry Promotion of cape jasmine fragrance of a flower silk quilt by be the abundant people thing Matter is lived, and improves the secondary value added of product, is improved utilization rate and the application of Heng County jasmine fresh flower, is being met people's material life demand While, also there is immeasurable impetus to local economic development.Starch from sweet potato is prepared into sweet potato by enzymatic treatment Porous-starch, coating agent is prepared with sweet potato porous-starch and water soluble chitosan, then gardenia and cape jasmine flower essential oil are mixed Particle is coated processing;Starch from sweet potato cost is low, and preparation method is simple;And coating agent can delay gardenia and cape jasmine anthosin The fragrance release of oily hybrid particles, fragrance release is slow, and fragrance can be kept for a long time;If humidity is found using a period of time, only To be put into below sunlight and dry in time, it is impossible to be exposed to the sun, fragrance can be kept more than 2 years.
Embodiment
With reference to embodiment, the technical scheme in invention is clearly and completely described, described embodiment is only Only it is the part of the present invention, rather than whole embodiments.
Embodiment 1
Complete that cape jasmine fragrance of a flower mulberry silk quilt can be made using following steps:
(1)The matured silkworm for emptying fecaluria is put into spinning on the net, the density of matured silkworm is 800-900 Tiao/㎡.Described spinning net is flat Plate spinning net, its mesh width is 2-5 millimeters, and spinning net is flat board spinning net, and its thickness is 1-2 millimeters.
(2)After matured silkworm spinning terminates, silk is peeled off from spinning is online, obtains smooth hair silk floss piece.
(3)Practiced with 98-100 DEG C of temperature, the hydrogen peroxide solution that mass percentage concentration is 4% and boil 30-40 minutes, to hair silk floss piece Degumming process is carried out, until content of silk gum is 2.5-3.5%.
(4)The continuous piece after degumming is cleaned up with clear water, then is placed into dewaterer and carries out dewater treatment.
(5)Continuous piece after dehydration is dried after the Shape correction that cleans, and obtains doing continuous piece, standby;Drying temperature is 65-85 degree, regain are controlled below 12%.
(6)Dry continuous piece weight as needed is weighed, pullled after weighing, makes continuous piece fluffy.
(7)Cut according to cotton-wadded quilt size to doing continuous piece.
(8)Dry continuous piece is divided into two parts, does the continuous crisscross laying of piece on platform by two parts respectively, after the completion of laying, Inspection arrangement is carried out to upper and lower surface, goes the removal of impurity and stiff bar.
(9)It will check that two parts put in order dry continuous piece top and bottom respectively place one layer of anti-gauze cloth that runs and get ready and fix respectively It is good, avoid running silk, obtain two silk floss batting cores.
(10)Two silk floss batting cores are overlapped, put cotton tire set, suture is got on three sides ready, makes silk floss batting core and two gauzes Tire core fixes, wherein while staying mouth to turn into tire core bag;Bar tied rope is respectively left in corner in tire core bag.
(11)Selected just open gardenia bud, is placed in constant temperature basement, constant temperature basement temperature control is 25 DEG C -30 DEG C, relative humidity 70%-80%.
(12)Gardenia bud is dried into 1~4min with microwave vacuum low-temperature drying machine, water content is less than 10%, with modeling Pocket is sealed standby.Microwave vacuum low-temperature drying machine is bought in Guangzhou Yong Ze microwave energy equipment Co., Ltd, network address: http://www.gz-yongze.com/, address:Guangzhou, Guangdong Baiyun District good farmland town Jin Pan industrial areas 8.
(13)After gardenia bud after drying is broken into powder, add cape jasmine flower essential oil be well mixed, cape jasmine pollen and The weight ratio of cape jasmine flower essential oil is 100:0.1;The glutinous agent of appropriate carboxymethyl cellulose gum is sprayed again and is pressed into grain shape, through screening To the hybrid particles of even particle size.The amount that sprinkling carboxymethyl cellulose gum sticks agent enables cape jasmine pollen to be pressed into particle. Particle is unsuitable excessive, is advisable like cassia seed size.
(14)Hybrid particles are coated using coating agent made of sweet potato porous-starch slurries and water soluble chitosan, By hybrid particles and coating agent with 6-8:1 weight makes hybrid particles surface be wrapped in one layer of coating agent, after coating than mixing Hybrid particles microwave vacuum low-temperature drying machine dry 2~3min, it is 8-10% to make coating water content.
(15)Non-woven fabrics is selected according to tire core bag inside dimension, doubling sewing, while stay mouth, turned welt is into non-woven bag.
(16)Hybrid particles after coating are put into non-woven bag, then non-woven bag is shakeout on work top, nothing The hybrid particles spun in cloth bag shakeout, it is impossible to and allow hybrid particles to stack, then open-wire line sealing, non-woven bag is finally subjected to netted sew with long stitches Seam, avoids hybrid particles from walking, corner is sewed with tied rope, turns into hybrid particles tire.
(17)Finally hybrid particles tire corner is fixed in tire core bag by tied rope, then tire core bag is placed in quilt cover .
After hybrid particles tire does not have fragrance, change hybrid particles tire or remove can obtain after hybrid particles tire it is new Silk wadding quilt.
The hydrogen peroxide solution that described mass percentage concentration is 4% is by hydrogen peroxide, sodium metasilicate, sodium EDTA salt It is formulated with clear water, the weight ratio of hydrogen peroxide, sodium metasilicate and sodium EDTA salt is(2-3):(0.5-0.8):(0.2- 0.3).
Described coating agent is that sweet potato is removed the peel into cooked addition suitable quantity of water slurrying and digested, and enzymatic hydrolysis condition is:Carbohydrase:α ~amylase=2:1, farinaceous size concentration 30%, enzyme concentration 1.5%, 55 DEG C, reaction time 12h, reaction system pH of reaction temperature is 5~6, prepare sweet potato porous-starch;Then the water solubility that molecular weight is 5000~10000 is added into sweet potato porous-starch slurries Chitosan stirs, and sweet potato porous-starch is 2 with water soluble chitosan weight content:1, obtain the bag of moisture content 40~60% Clothing agent solution;5% carbon dioxide is filled with by coating agent weight so that coating agent solutions carry more bubble.
Described carboxymethyl cellulose gum sticks what agent was formed by carboxymethyl cellulose with appropriate water modulation, wherein carboxymethyl Cellulose is prepared by being acted in the basic conditions by monochloroacetic acid and cellulose, and quaternization occurs for cellulose and alkali effect Alkali cellulose is generated, alkali cellulose occurs etherification reaction with monochloroacetic acid again, obtains carboxymethyl cellulose.
Embodiment 2
Complete that cape jasmine fragrance of a flower mulberry silk quilt can be made using following steps:
(1)The matured silkworm for emptying fecaluria is put into spinning on the net, the density of matured silkworm is 800-900 Tiao/㎡.Described spinning net is flat Plate spinning net, its mesh width is 2-5 millimeters, and spinning net is flat board spinning net, and its thickness is 1-2 millimeters.
(2)After matured silkworm spinning terminates, silk is peeled off from spinning is online, obtains smooth hair silk floss piece.
(3)Practiced with 98-100 DEG C of temperature, the hydrogen peroxide solution that mass percentage concentration is 4% and boil 30-40 minutes, to hair silk floss piece Degumming process is carried out, until content of silk gum is 2.5-3.5%;Refiningly cook before terminating 5 minutes, add hydrogen peroxide solution weight 1.5-2% Ethylene glycol diglycidylether.
(4)The continuous piece after degumming is cleaned up with clear water, then is placed into dewaterer and carries out dewater treatment.
(5)Continuous piece after dehydration is dried after the Shape correction that cleans, and obtains doing continuous piece, standby;Drying temperature is 65-85 degree, regain are controlled below 12%.
(6)Dry continuous piece weight as needed is weighed, pullled after weighing, makes continuous piece fluffy.
(7)Cut according to cotton-wadded quilt size to doing continuous piece.
(8)Dry continuous piece is divided into two parts, does the continuous crisscross laying of piece on platform by two parts respectively, after the completion of laying, Inspection arrangement is carried out to upper and lower surface, goes the removal of impurity and stiff bar.
(9)It will check that two parts put in order dry continuous piece top and bottom respectively place one layer of anti-gauze cloth that runs and get ready and fix respectively It is good, avoid running silk, obtain two silk floss batting cores.
(10)Two silk floss batting cores are overlapped, put cotton tire set, suture is got on three sides ready, makes silk floss batting core and two gauzes Tire core fixes, wherein while staying mouth to turn into tire core bag;Bar tied rope is respectively left in corner in tire core bag.
(11)Selected just open gardenia bud, is placed in constant temperature basement, constant temperature basement temperature control is 25 DEG C -30 DEG C, relative humidity 70%-80%.
(12)Gardenia bud is dried into 1~4min with microwave vacuum low-temperature drying machine, water content is less than 10%, with modeling Pocket is sealed standby.Microwave vacuum low-temperature drying machine is bought in Guangzhou Yong Ze microwave energy equipment Co., Ltd, network address: http://www.gz-yongze.com/, address:Guangzhou, Guangdong Baiyun District good farmland town Jin Pan industrial areas 8.
(13)After gardenia bud after drying is broken into powder, add cape jasmine flower essential oil be well mixed, cape jasmine pollen and The weight ratio of cape jasmine flower essential oil is 100:0.1;The glutinous agent of appropriate carboxymethyl cellulose gum is sprayed again and is pressed into grain shape, through screening To the hybrid particles of even particle size.The amount that sprinkling carboxymethyl cellulose gum sticks agent enables cape jasmine pollen to be pressed into particle. Particle is unsuitable excessive, is advisable like cassia seed size.
(14)Hybrid particles are coated using coating agent made of sweet potato porous-starch slurries and water soluble chitosan, By hybrid particles and coating agent with 6-8:1 weight makes hybrid particles surface be wrapped in one layer of coating agent, after coating than mixing Hybrid particles microwave vacuum low-temperature drying machine dry 2~3min, it is 8-10% to make coating water content.
(15)Non-woven fabrics is selected according to tire core bag inside dimension, doubling sewing, while stay mouth, turned welt is into non-woven bag.
(16)Hybrid particles after coating are put into non-woven bag, then non-woven bag is shakeout on work top, nothing The hybrid particles spun in cloth bag shakeout, it is impossible to and allow hybrid particles to stack, then open-wire line sealing, non-woven bag is finally subjected to netted sew with long stitches Seam, avoids hybrid particles from walking, corner is sewed with tied rope, turns into hybrid particles tire.
(17)Finally hybrid particles tire corner is fixed in tire core bag by tied rope, then tire core bag is placed in quilt cover .
After hybrid particles tire does not have fragrance, change hybrid particles tire or remove can obtain after hybrid particles tire it is new Silk wadding quilt.
The hydrogen peroxide solution that described mass percentage concentration is 4% is by hydrogen peroxide, sodium metasilicate, sodium EDTA salt It is formulated with clear water, the weight ratio of hydrogen peroxide, sodium metasilicate and sodium EDTA salt is(2-3):(0.5-0.8):(0.2- 0.3).
Described coating agent is that sweet potato is removed the peel into cooked addition suitable quantity of water slurrying and digested, and enzymatic hydrolysis condition is:Carbohydrase:α ~amylase=2:1, farinaceous size concentration 30%, enzyme concentration 1.5%, 55 DEG C, reaction time 12h, reaction system pH of reaction temperature is 5~6, prepare sweet potato porous-starch;Then the water solubility that molecular weight is 5000~10000 is added into sweet potato porous-starch slurries Chitosan stirs, and sweet potato porous-starch is 2 with water soluble chitosan weight content:1, obtain the bag of moisture content 40~60% Clothing agent solution;5% carbon dioxide is filled with by coating agent weight so that coating agent solutions carry more bubble.
Described carboxymethyl cellulose gum sticks what agent was formed by carboxymethyl cellulose with appropriate water modulation, wherein carboxymethyl Cellulose is prepared by being acted in the basic conditions by monochloroacetic acid and cellulose, and quaternization occurs for cellulose and alkali effect Alkali cellulose is generated, alkali cellulose occurs etherification reaction with monochloroacetic acid again, obtains carboxymethyl cellulose.
Application Example
1st, Hengxian County's silk company, the said firm make the cape jasmine fragrance of a flower mulberry silk quilt of the present invention to 15 volunteer's experience With the quilt has light cape jasmine flowery odour, and 15 volunteers unanimously think the cape jasmine fragrance of a flower mulberry silk quilt of the present invention than tradition Mulberry silk quilt use it is more comfortable.
Described above is not limitation of the present invention, and the present invention is also not limited to examples detailed above, the art it is general Logical technical staff, in the essential scope of the present invention, the variations, modifications, additions or substitutions made, it should all belong to the guarantor of the present invention Protect scope.

Claims (7)

  1. A kind of 1. cape jasmine fragrance of a flower mulberry silk quilt, it is characterised in that:It is made of following processing step:
    (1)The matured silkworm for emptying fecaluria is put into spinning on the net, the density of matured silkworm is 800-900 Tiao/㎡;
    (2)After matured silkworm spinning terminates, silk is peeled off from spinning is online, obtains smooth hair silk floss piece;
    (3)Practiced with 98-100 DEG C of temperature, the hydrogen peroxide solution that mass percentage concentration is 4% and boil 30-40 minutes, hair silk floss piece is carried out Degumming process, until content of silk gum is 2.5-3.5%;
    (4)The continuous piece after degumming is cleaned up with clear water, then is placed into dewaterer and carries out dewater treatment;
    (5)Continuous piece after dehydration is dried after the Shape correction that cleans, and obtains doing continuous piece, standby;Drying temperature is 65-85 Degree, regain are controlled below 12%;
    (6)Dry continuous piece weight as needed is weighed, pullled after weighing, makes continuous piece fluffy;
    (7)Cut according to cotton-wadded quilt size to doing continuous piece;
    (8)Dry continuous piece is divided into two parts, the continuous crisscross laying of piece is done on platform by two parts respectively, after the completion of laying, to upper Lower two sides carries out inspection arrangement, goes the removal of impurity and stiff bar;
    (9)It will check that two parts put in order dry continuous piece top and bottom respectively place one layer of anti-gauze cloth that runs and get ready and fix respectively, keep away Exempt to run silk, obtain two silk floss batting cores;
    (10)Two silk floss batting cores are overlapped, put cotton tire set, suture is got on three sides ready, makes silk floss batting core and two gauze tire cores Fix, wherein while staying mouth to turn into tire core bag;Bar tied rope is respectively left in corner in tire core bag;
    (11)Selected just open gardenia bud, is placed in constant temperature basement, constant temperature basement temperature control is at 25 DEG C -30 DEG C, relative humidity 70%-80%;
    (12)Gardenia bud is dried into 1~4min with microwave vacuum low-temperature drying machine, water content is less than 10%, uses polybag It is sealed standby;
    (13)After gardenia bud after drying is broken into powder, adds cape jasmine flower essential oil and be well mixed, cape jasmine pollen and cape jasmine The weight ratio of flower essential oil is 100:0.1;Appropriate carboxymethyl cellulose gum is sprayed again stick agent and be pressed into grain shape, obtained through screening Grain hybrid particles of uniform size;
    (14)Hybrid particles are coated using coating agent made of sweet potato porous-starch slurries and water soluble chitosan, will be mixed Particle and coating agent are closed with 6-8:1 weight makes hybrid particles surface be wrapped in one layer of coating agent, mixed after coating than mixing Close particle and dry 2~3min in microwave vacuum low-temperature drying machine, it is 8-10% to make coating water content;
    (15)Non-woven fabrics is selected according to tire core bag inside dimension, doubling sewing, while stay mouth, turned welt is into non-woven bag;
    (16)Hybrid particles after coating are put into non-woven bag, then non-woven bag is shakeout on work top, non-woven fabrics Hybrid particles in bag shakeout, it is impossible to and allow hybrid particles to stack, then open-wire line sealing, non-woven bag is finally subjected to netted quilting, Hybrid particles are avoided to walk, corner is sewed with tied rope, turns into hybrid particles tire;
    (17)Finally hybrid particles tire corner is fixed in tire core bag by tied rope, then tire core bag is placed in quilt cover i.e. Can.
  2. 2. cape jasmine fragrance of a flower mulberry silk quilt according to claim 1, it is characterised in that:Described mass percentage concentration is 4% Hydrogen peroxide solution be to be formulated by hydrogen peroxide, sodium metasilicate, sodium EDTA salt and clear water, hydrogen peroxide, sodium metasilicate and The weight ratio of sodium EDTA salt is(2-3):(0.5-0.8):(0.2-0.3).
  3. 3. cape jasmine fragrance of a flower mulberry silk quilt according to claim 1, it is characterised in that:Described tire set is pure using high-count and high-density Cotton is made.
  4. 4. cape jasmine fragrance of a flower mulberry silk quilt according to claim 1, it is characterised in that:Described spinning net spins for flat board Net, its mesh width are 2-5 millimeters, and spinning net is flat board spinning net, and its thickness is 1-2 millimeters.
  5. 5. cape jasmine fragrance of a flower mulberry silk quilt according to claim 1, it is characterised in that:Described coating agent is to remove the peel sweet potato Cooked to add suitable quantity of water slurrying and digest, enzymatic hydrolysis condition is:Carbohydrase:α~amylase=2:1, farinaceous size concentration 30% is enzyme-added Amount 1.5%, 55 DEG C, reaction time 12h, reaction system pH of reaction temperature are 5~6, prepare sweet potato porous-starch;Then to sweet potato Add the water soluble chitosan that molecular weight is 5000~10000 in porous-starch slurries to stir, sweet potato porous-starch and water Soluble chitosan weight content is 2:1, obtain the coating agent solutions of moisture content 40~60%;The two of 5% are filled with by coating agent weight Carbon oxide gas so that coating agent solutions carry more bubble.
  6. 6. cape jasmine fragrance of a flower mulberry silk quilt according to claim 1, it is characterised in that:Described carboxymethyl cellulose gum sticks agent Formed by carboxymethyl cellulose with appropriate water modulation, wherein carboxymethyl cellulose is in alkalescence by monochloroacetic acid and cellulose Under the conditions of prepared by acting on, quaternization generation alkali cellulose occurs for cellulose and alkali effect, alkali cellulose again with a chlorine vinegar Etherification reaction occurs for acid, obtains carboxymethyl cellulose.
  7. 7. cape jasmine fragrance of a flower mulberry silk quilt according to claim 1, it is characterised in that:Refiningly cook before terminating 5 minutes, add dioxygen Aqueous solution weight 1.5-2% ethylene glycol diglycidylether.
CN201710775483.6A 2017-08-31 2017-08-31 A kind of cape jasmine fragrance of a flower mulberry silk quilt Pending CN107536351A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109610014A (en) * 2018-12-03 2019-04-12 河南民兴生物科技股份有限公司 Silk quilt machining production line

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN203506216U (en) * 2013-10-24 2014-04-02 李健军 Cotton quilt
CN104117083A (en) * 2014-08-15 2014-10-29 汪建 Chinese herbal medicine preparation
GB2521853A (en) * 2014-01-06 2015-07-08 Fast Engineering Ltd High security blanket
CN105286396A (en) * 2014-06-25 2016-02-03 蓝汉才 Healthcare silk quilt
CN106361073A (en) * 2016-08-31 2017-02-01 横县桂华茧丝绸有限责任公司 Preparation method of pure mulberry silk quilt with aglaia odorata lour fragrance

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN203506216U (en) * 2013-10-24 2014-04-02 李健军 Cotton quilt
GB2521853A (en) * 2014-01-06 2015-07-08 Fast Engineering Ltd High security blanket
CN105286396A (en) * 2014-06-25 2016-02-03 蓝汉才 Healthcare silk quilt
CN104117083A (en) * 2014-08-15 2014-10-29 汪建 Chinese herbal medicine preparation
CN106361073A (en) * 2016-08-31 2017-02-01 横县桂华茧丝绸有限责任公司 Preparation method of pure mulberry silk quilt with aglaia odorata lour fragrance

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109610014A (en) * 2018-12-03 2019-04-12 河南民兴生物科技股份有限公司 Silk quilt machining production line

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