CN107582429A - A kind of tearable nail polish glue of one-step shaping and preparation method thereof - Google Patents

A kind of tearable nail polish glue of one-step shaping and preparation method thereof Download PDF

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Publication number
CN107582429A
CN107582429A CN201710819632.4A CN201710819632A CN107582429A CN 107582429 A CN107582429 A CN 107582429A CN 201710819632 A CN201710819632 A CN 201710819632A CN 107582429 A CN107582429 A CN 107582429A
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CN
China
Prior art keywords
parts
resin
nail polish
tearable
polish glue
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Pending
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CN201710819632.4A
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Chinese (zh)
Inventor
刘彬
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Shanghai Spectrum Intelligent Technology Co Ltd
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Shanghai Spectrum Intelligent Technology Co Ltd
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Priority to CN201710819632.4A priority Critical patent/CN107582429A/en
Publication of CN107582429A publication Critical patent/CN107582429A/en
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Abstract

The invention discloses tearable nail polish glue of a kind of one-step shaping and preparation method thereof, including raw material:18 22 parts of Resin A, 28 43 parts of resin B, 28 parts of resin C, 20 26 parts of diluent, 37 parts of initiator, trigger 15 parts of accelerator, 56 parts of colouring agent, 0.2 part of levelling agent.There is no penetrating odor by the nail polish glue prepared to the science addition proportioning of each raw material, nail is not injured, health environment-friendly;Secondly, to the strong adaptability of UV LED light sources, rapid curing can be realized under the ultraviolet of different wave length by being embodied in;Compared with nail polish glue product on the market, there is the advantage of one-step shaping, it is not necessary to bottom, dyed layer and sealing are smeared repeatedly, can full wafer is peeled off without tearing up at any time situation moreover, with high toughness;In addition, the adhesive force of the nail polish glue reaches a kind of poised state, can persistently be kept for one week or so in the case where not influenceing to peel off.

Description

A kind of tearable nail polish glue of one-step shaping and preparation method thereof
Technical field
The present invention relates to nail polish technical field, specially a kind of tearable nail polish glue of one-step shaping and preparation method thereof.
Background technology
Nail polish belongs to a major class product of color make-up, and the woman to like to be beautiful always prefers to use bright-coloured red nail polish and is coated in long nail On, to show the glamour of fine and slim hands.
With the improvement of living standards, the quickening of rhythm of life.The youth women that likes to be beautiful likes mood dressing according to oneself To change the nail colour of oneself.At present, most products on the market, drying is slower, and unloading difficulty is, it is necessary to specifically unload first Wrap to unload.And the main component for unloading first bag is acetone, excitant is very strong, exists to human body and injures.
With the quickening pace of modern life, the concept of time of people also increasingly strengthens.Traditional nail polish glue must first priming operation warm Color layer is applied afterwards finally one layer of sealing.Complex steps, take considerable time.Moreover, nail polish has strong impulse Smell, and this penetrating odor does not meet Modern consumer idea.
The content of the invention
It is an object of the invention to provide a kind of nonpoisonous and tasteless tearable nail polish glue of healthy one-step shaping and preparation method thereof, Possess brightness height, persistently long, tearable the advantages that shelling one-step shaping, to solve the problems mentioned in the above background technology.
To achieve the above object, the present invention provides following technical scheme:A kind of tearable nail polish glue of one-step shaping, including it is following The raw material of parts by weight proportioning:Resin A 18-22 parts, resin B 28-43 parts, resin C 2-8 parts, diluent 20-26 parts, trigger Agent 3-7 parts, trigger accelerator 1-5 parts, colouring agent 5-6 parts, 0.2 part of levelling agent.
Preferably, including raw material:20 parts of Resin A, 30 parts of resin B, 5 parts of resin C, 31 parts of diluent, 5 parts of initiator, Trigger 4 parts of accelerator, 5 parts of colouring agent, 0.2 part of levelling agent.
Preferably, including raw material:20 parts of Resin A, 40 parts of resin B, 3 parts of resin C, 25 parts of diluent, 5 parts of initiator, Trigger 4 parts of accelerator, 3 parts of colouring agent, 0.2 part of levelling agent.
Preferably, the Resin A is aliphatic urethane acrylate, and resin B is polyether urethane, resin C is amino acrylic resin.
Preferably, the Resin A is the 996 of the production of Sartomer Chemical Co., Ltd., and resin B is to wear Maas ultraviolet glue The 582I10 of equipment Co., Ltd production, resin C are the 9051 of Sartomer Chemical Co., Ltd. production.
Preferably, the initiator is 2,4,6- trimethylbenzoy-dipheny phosphine oxides.
Preferably, the initiator is the TPO of German BASF production.
Preferably, the initiation accelerator is polyhydroxy mercaptan.
Preferably, it is described to trigger accelerator as one or more mixtures in four to eight hydroxy thiols.
Preferably, it is characterised in that the colouring agent is the mill base of Penn color mill bases company of U.S. production.
Preferably, the colouring agent be specially CI 77891, CI 77491, CI 77492, CI 19140, CI 15850, One or more mixtures in CI 42090, CI 45410.
Preferably, the UV for the model 2200 that the levelling agent produces for Ying Chuan Specialty Chemicals Co., Ltd is resin moderated helps Agent.
The present invention provides another technical solution:A kind of preparation method of the tearable nail polish glue of one-step shaping, including it is following Step:
S1:The initiator is added in the diluent, is heated to 90 degrees Celsius, stirs 10-20 minutes, until the initiation Agent is dissolved completely in the diluent;
S2:The Resin A, resin B, resin C are heated to 60 degrees Celsius respectively, successively by Resin A, resin B, resin C press than Example is added in S1 resulting solutions, and is stirred 20 minutes with 2000r/min rotating speed in dispersion machine, until solution dissolves each other completely;
S3:By the initiator, trigger accelerator, levelling agent to be proportionally added into S2 resulting solutions, in dispersion machine with 2000r/min rotating speed stirs 10 minutes, until stirring;
S4:The colouring agent is proportionally added into above-mentioned S3 resulting solutions, stirred in dispersion machine with 3000r/min rotating speed After mixing 10 minutes, mixed solution is obtained;
S5:The mixed solution obtained by S4 is ground using three-roller, described one-step shaping is can obtain after the completion of grinding Tearable nail polish glue.
Compared with prior art, the beneficial effects of the invention are as follows:
1. tearable nail polish glue of an one-step shaping and preparation method thereof, without penetrating odor, nail is not injured, healthy ring Protect.
2. tearable nail polish glue of an one-step shaping and preparation method thereof, to the strong adaptability of UV-LED light sources, is embodied in Rapid curing can be realized under the ultraviolet of different wave length.
3. tearable nail polish glue of an one-step shaping and preparation method thereof, compared with nail polish glue product on the market, have a step into The advantage of type, it is not necessary to smear bottom, dyed layer and sealing repeatedly.
4. tearable nail polish glue of an one-step shaping and preparation method thereof, after smearing one layer of solidification, it has high toughness, can Situation about being peeled off with full wafer at any time without tearing up.
5. tearable nail polish glue of an one-step shaping and preparation method thereof, its adhesive force reaches a kind of poised state, can be not Influence persistently to be kept for one week or so in the case of peeling off.
Embodiment
The embodiment of the present invention is will be detailed below, however, the embodiment of the present invention is not limited thereto.Based in the present invention Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made, Belong to the scope of protection of the invention.
In the embodiment of the present invention:A kind of tearable nail polish glue of one-step shaping, include the raw material of following parts by weight proportioning:Resin A 18-22 parts, resin B 28-43 parts, resin C 2-8 parts, diluent 20-26 parts, initiator 3-7 parts, trigger accelerator 1-5 Part, colouring agent 5-6 parts, 0.2 part of levelling agent;Wherein, Resin A is aliphatic urethane acrylate, and resin B is polyether-polyurethane Acrylate, resin C are amino acrylic resin, and specific Resin A is the 996 of the production of Sartomer Chemical Co., Ltd., resin B To wear the 582I10 of Maas UV glue wetting system Co., Ltd production, resin C is the production of Sartomer Chemical Co., Ltd. 9051;Initiator is 2,4,6- trimethylbenzoy-dipheny phosphine oxides, specially the TPO for the production of German BASF;Draw Hair accelerator is polyhydroxy mercaptan, specific to trigger accelerator as one or more mixtures in four to eight hydroxy thiols; The mill base that colouring agent produces for Penn color mill bases company of the U.S., specially CI 77891, CI 77491, CI 77492, CI 19140th, one or more mixtures in CI 15850, CI 42090, CI 45410;Levelling agent is limited to win wound Specialty Chemical The resin moderated auxiliary agents of UV of the model 2200 of company's production.
Embodiment one:
Take raw material:20 parts of Resin A, 30 parts of resin B, 5 parts of resin C, 31 parts of diluent, 5 parts of initiator, trigger accelerator 4 Part, 5 parts of colouring agent, 0.2 part of levelling agent.
Matched based on above-mentioned raw materials, there is provided a kind of preparation method of the tearable nail polish glue of one-step shaping, comprise the following steps:
The first step:According to formula, 5 parts of initiators are added in 31 parts of diluent, be heated to 90 degrees Celsius, 10-20 points of stirring Clock, until initiator is dissolved completely in diluent;
Second step:20 parts of Resin As, 30 parts of resin Bs, 5 parts of resin C are heated to 60 degrees Celsius respectively, successively by the tree after heating Fat A, resin B, resin C are added in above-mentioned steps resulting solution, are stirred 20 minutes with 2000r/min rotating speed in dispersion machine, Until solution dissolves each other completely;
3rd step:Trigger accelerator, 0.2 part of levelling agent to be proportionally added into above-mentioned resulting solution by 4 parts, in dispersion machine with 2000r/min rotating speed stirs 10 minutes, until stirring;
4th step:5 parts of colouring agents are proportionally added into above-mentioned steps resulting solution, with 3000r/min in dispersion machine Rotating speed stir 10 minutes after, obtain mixed solution;
5th step:The mixed solution obtained by step 4 is ground using three-roller, can obtain after the completion of grinding described The tearable nail polish glue of one-step shaping.
Embodiment two:
Compared with embodiment one, using identical raw material and preparation method, it the difference is that only the composition of raw material and contain Amount is as follows:20 parts of Resin A, 40 parts of resin B, 3 parts of resin C, 25 parts of diluent, 5 parts of initiator, trigger 4 parts of accelerator, 3 parts of toner, 0.2 part of levelling agent.
Matched based on above-mentioned raw materials, there is provided a kind of preparation method of the tearable nail polish glue of one-step shaping, comprise the following steps:
The first step:According to formula, 5 parts of initiators are added in 25 parts of diluents, are heated to 90 degrees Celsius, stir 10-20 minutes, Until initiator is dissolved completely in diluent;
Second step:20 parts of Resin As, 40 parts of resin Bs, 3 parts of resin C are heated to 60 degrees Celsius respectively, resin after heating successively A, resin B, resin C are added in above-mentioned steps resulting solution, stir 20 minutes in dispersion machine with 2000r/min rotating speed, directly Dissolved each other completely to solution;
3rd step:Trigger accelerator, 0.2 part of levelling agent to be proportionally added into above-mentioned resulting solution by 4 parts, in dispersion machine with 2000r/min rotating speed stirs 10 minutes, until stirring;
4th step:3 parts of colouring agents are proportionally added into above-mentioned steps resulting solution, turned in dispersion machine with 3000r/min After speed stirring 10 minutes, mixed solution is obtained;
5th step:The mixed solution obtained by step 4 is ground using three-roller, can obtain after the completion of grinding described The tearable nail polish glue of one-step shaping.
The tearable nail polish glue of one-step shaping that the present embodiment one and two obtains, after being applied to testing crew finger, through UV-LED After irradiating the 60-80 seconds, nail polish adhesive curing is complete, and surface drying is good, smooth glossy;In persistence test is carried out, pass through simulation Normal living scene, measure duration and maintain one week.
In summary:Tearable nail polish glue of this one-step shaping and preparation method thereof, without penetrating odor, nail is not hindered Evil, health environment-friendly;Secondly, to the strong adaptability of UV-LED light sources, being embodied in can be real under the ultraviolet of different wave length Existing rapid curing;Compared with nail polish glue product on the market, there is the advantage of one-step shaping, it is not necessary to smear bottom, coloring repeatedly Layer and sealing, can full wafer is peeled off without tearing up at any time situation moreover, with high toughness;In addition, the first The adhesive force of factice reaches a kind of poised state, can persistently be kept for one week or so in the case where not influenceing to peel off.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with A variety of changes, modification can be carried out to these embodiments, replace without departing from the principles and spirit of the present invention by understanding And modification, the scope of the present invention is defined by the appended.

Claims (9)

1. a kind of tearable nail polish glue of one-step shaping, it is characterised in that include the raw material of following parts by weight proportioning:Resin A 18- 22 parts, resin B 28-43 parts, resin C 2-8 parts, diluent 20-26 parts, initiator 3-7 parts, trigger accelerator 1-5 parts, coloring Agent 5-6 parts, 0.2 part of levelling agent.
2. the tearable nail polish glue of a kind of one-step shaping according to claim 1, it is characterised in that including raw material:Resin A 20 Part, 30 parts of resin B, 5 parts of resin C, 31 parts of diluent, 5 parts of initiator, trigger 4 parts of accelerator, 5 parts of colouring agent, levelling agent 0.2 part.
3. the tearable nail polish glue of a kind of one-step shaping according to claim 1, it is characterised in that including raw material:Resin A 20 Part, 40 parts of resin B, 3 parts of resin C, 25 parts of diluent, 5 parts of initiator, trigger 4 parts of accelerator, 3 parts of colouring agent, levelling agent 0.2 part.
A kind of 4. tearable nail polish glue of one-step shaping according to claim 1-3 any one, it is characterised in that the resin A is aliphatic urethane acrylate, and resin B is polyether urethane, and resin C is amino acrylic resin, wherein, Resin A is the 996 of Sartomer Chemical Co., Ltd. production, and resin B is to wear Maas UV glue wetting system Co., Ltd to produce 582I10, resin C are the 9051 of Sartomer Chemical Co., Ltd. production.
A kind of 5. tearable nail polish glue of one-step shaping according to claim 1-3 any one, it is characterised in that the initiation The TPO that agent produces for German BASF, specially 2,4,6- trimethylbenzoy-dipheny phosphine oxides.
A kind of 6. tearable nail polish glue of one-step shaping according to claim 1-3 any one, it is characterised in that the initiation Accelerator is polyhydroxy mercaptan, one or more mixtures in specially four to eight hydroxy thiols.
A kind of 7. tearable nail polish glue of one-step shaping according to claim 1-3 any one, it is characterised in that the coloring The mill base that agent produces for Penn color mill bases company of the U.S., specially CI 77891, CI 77491, CI 77492, CI 19140th, one or more mixtures in CI 15850, CI 42090, CI 45410.
A kind of 8. tearable nail polish glue of one-step shaping according to claim 1-3 any one, it is characterised in that the levelling Agent is the resin moderated auxiliary agents of UV of the model 2200 of Ying Chuan Specialty Chemicals Co., Ltd production.
9. a kind of preparation method of the tearable nail polish glue of one-step shaping according to claim 1, it is characterised in that including following Step:
S1:The initiator is added in the diluent, is heated to 90 degrees Celsius, stirs 10-20 minutes, until the initiation Agent is dissolved completely in the diluent;
S2:The Resin A, resin B, resin C are heated to 60 degrees Celsius respectively, successively by Resin A, resin B, resin C press than Example is added in S1 resulting solutions, and is stirred 20 minutes with 2000r/min rotating speed in dispersion machine, until solution dissolves each other completely;
S3:By the initiator, trigger accelerator, levelling agent to be proportionally added into S2 resulting solutions, in dispersion machine with 2000r/min rotating speed stirs 10 minutes, until stirring;
S4:The colouring agent is proportionally added into above-mentioned S3 resulting solutions, stirred in dispersion machine with 3000r/min rotating speed After mixing 10 minutes, mixed solution is obtained;
S5:The mixed solution obtained by S4 is ground using three-roller, described one-step shaping is can obtain after the completion of grinding Tearable nail polish glue.
CN201710819632.4A 2017-09-13 2017-09-13 A kind of tearable nail polish glue of one-step shaping and preparation method thereof Pending CN107582429A (en)

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Application Number Priority Date Filing Date Title
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108852866A (en) * 2018-07-20 2018-11-23 广州市精合致新材料科技有限公司 One kind is from ordor removing nail polish glue and preparation method thereof
CN111110588A (en) * 2020-01-16 2020-05-08 佛山市蓝狐生物科技有限公司 Peelable base glue and preparation method thereof
CN113576144A (en) * 2021-08-03 2021-11-02 上海慧姿化妆品有限公司 Composition for nail sticker and preparation method thereof
CN115991948A (en) * 2022-12-09 2023-04-21 南雄市沃太化工有限公司 UV-LED cured additive base adhesive and preparation method thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1997000664A1 (en) * 1995-06-20 1997-01-09 Eastman Chemical Company Aqueous nail polish compositions containing acrylic resins crosslinked with acrylated urethane oligomers
CN102766399A (en) * 2012-07-31 2012-11-07 上海零玖科技有限公司 Gel polish, LED gel polish and LED nail polish
CN105213221A (en) * 2015-10-08 2016-01-06 上海应用技术学院 A kind of quick-drying nail polish glue and preparation method thereof
CN105534741A (en) * 2016-01-20 2016-05-04 上海应用技术学院 Strippable nail polish gel and synthesis method thereof
CN105686972A (en) * 2016-02-23 2016-06-22 上海应用技术学院 Soak-off gel and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1997000664A1 (en) * 1995-06-20 1997-01-09 Eastman Chemical Company Aqueous nail polish compositions containing acrylic resins crosslinked with acrylated urethane oligomers
CN102766399A (en) * 2012-07-31 2012-11-07 上海零玖科技有限公司 Gel polish, LED gel polish and LED nail polish
CN105213221A (en) * 2015-10-08 2016-01-06 上海应用技术学院 A kind of quick-drying nail polish glue and preparation method thereof
CN105534741A (en) * 2016-01-20 2016-05-04 上海应用技术学院 Strippable nail polish gel and synthesis method thereof
CN105686972A (en) * 2016-02-23 2016-06-22 上海应用技术学院 Soak-off gel and preparation method thereof

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108852866A (en) * 2018-07-20 2018-11-23 广州市精合致新材料科技有限公司 One kind is from ordor removing nail polish glue and preparation method thereof
CN111110588A (en) * 2020-01-16 2020-05-08 佛山市蓝狐生物科技有限公司 Peelable base glue and preparation method thereof
CN113576144A (en) * 2021-08-03 2021-11-02 上海慧姿化妆品有限公司 Composition for nail sticker and preparation method thereof
CN115991948A (en) * 2022-12-09 2023-04-21 南雄市沃太化工有限公司 UV-LED cured additive base adhesive and preparation method thereof
CN115991948B (en) * 2022-12-09 2024-03-08 南雄市沃太化工有限公司 UV-LED cured additive base adhesive and preparation method thereof

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Application publication date: 20180116