CN108852866A - One kind is from ordor removing nail polish glue and preparation method thereof - Google Patents
One kind is from ordor removing nail polish glue and preparation method thereof Download PDFInfo
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- CN108852866A CN108852866A CN201810806291.1A CN201810806291A CN108852866A CN 108852866 A CN108852866 A CN 108852866A CN 201810806291 A CN201810806291 A CN 201810806291A CN 108852866 A CN108852866 A CN 108852866A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/87—Polyurethanes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q3/00—Manicure or pedicure preparations
- A61Q3/02—Nail coatings
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- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
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Abstract
The present invention provides a kind of preparation method from ordor removing nail polish glue, includes the following steps：S1：30-40 parts of urethane acrylates, 10-20 parts of modified epoxy acrylic esters and 30-40 parts of hydroxyethyl methacrylates are put into reaction vessel by formula；It is stirred 15-30 minutes with 1000-1500 revs/min of revolving speed；S2：Add 5-15 parts of Tourmaline powders and 5-10 parts of group of the lanthanides light rare earths；With 2000-3000 revs/min high-speed stirred 30-60 minutes；S3：Add bis- (2,4,6- trimethylbenzoyl) phosphine oxides of 2-4 parts of 1- hydroxycyclohexyl phenyl ketones, 2-10 parts of phenyl, 1-2 parts of fumed silicas, 0.5-1 parts of defoaming agents and 0-1 parts of levelling agents；It is stirred with 1000-1500 revs/min of revolving speed, S4：Average grain diameter is ground to no more than 5 microns using three-roll grinder.Coating of the invention only passes through UV/LED light and irradiates, can rapid curing, fine and close, bright-colored, the excellent flexibility of coating, environmentally protective, good ply adhesion, auto purification smell and with negative ion-releasing function.
Description
Technical field
The invention belongs to cosmetic fields, especially a kind of from ordor removing nail polish glue and preparation method thereof.
Background technique
From ordor removing nail polish glue as-kind substitution nail polish novel environment friendly cosmetics, developed certainly due to its operation letter
Single, persistence is good, glossiness and bright in luster, and smell is low, and small to human body irritation, the timeliness in operating process is shorter, and not
It is perishable, it saves more convenient so being more widely applied, and dosage increases year by year, becomes feminine charm of liking to be beautiful mostly
The essential product of first.
Due to being to carry out under UV/LED lamp from ordor removing nail polish adhesive curing, so usually from ordor removing nail polish glue by acrylate
Oligomer, methacrylic oligomer or epoxy oligomer are constituted with the subsequently cross-linked monomer reacted of composition and additive.When with
When nail, these compositions are made into laminated coating structure from ordor removing nail polish glue.The multicoat mainly includes basic
Three-layer coating, such as priming coat, coloured coating (or polychromatic finish) and surface covering.Tradition has following lack from ordor removing nail polish glue
Point：It is formed after laminated coating structure, remaining small molecule is blocked by surface covering after solidifying, and causes small molecule natural
Volatilization, it is harmful to nail and human body.It is therefore desirable to be further improved the self-purification capacity from ordor removing nail polish glue coloured coating.
Summary of the invention
In order to solve prior art problem, the present invention provides a kind of coating from ordor removing nail polish glue, only passes through UV/LED light
Irradiation, can rapid curing, fine and close, bright-colored, the excellent flexibility of coating, environmentally protective, good ply adhesion, oneself
It purifies smell and there is negative ion-releasing function.
To achieve the above object, technical solution provided by the present invention is：One kind is from ordor removing nail polish glue, which is characterized in that
It is made of the raw material below according to parts by weight, and specific formula is：
The present invention also provides a kind of above-mentioned preparation methods from ordor removing nail polish glue, which is characterized in that includes the following steps：
S1：By formula by 30-40 parts of urethane acrylates, 10-20 parts of modified epoxy acrylic esters and 30-40 parts of methyl
Hydroxy-ethyl acrylate is put into reaction vessel；It is stirred 15-30 minutes with 1000-1500 revs/min of revolving speed；
S2：Add 5-15 parts of Tourmaline powders and 5-10 parts of group of the lanthanides light rare earths；With 2000-3000 revs/min of high-speed stirred
30-60 minutes；
S3：It is bis- (2,4,6- trimethylbenzoyl) to add 2-4 parts of 1- hydroxycyclohexyl phenyl ketones, 2-10 parts of phenyl
Phosphine oxide, 1-2 part fumed silica, 0.1-1 parts of defoaming agents and 0.1-1 parts of levelling agents；With 1000-1500 revs/min turn
Speed stirring；
S4：Average grain diameter is ground to no more than 5 microns using three-roll grinder；
S5：0-5 parts of mill bases are added in ground coating, with 1000-1500 revs/min stirring 15-30 minutes.
Preferably, the defoaming agent is tego920 defoaming agent, and the levelling agent is tego450 levelling agent, the gas phase two
Silica is the R974 of Degussa.
Preferably, the group of the lanthanides light rare earth is group of the lanthanides cerium group rare-earth.
Preferably, the particle size of the Tourmaline powder is nanoscale.
Preferably, the blender used in the step S1 and S2 is that Dongguan benefit is risen the production of intelligent Equipment Limited
FS30 twin shaft frequency-control blender.
Preferably, the grinder used in the step S4 for Changzhou rely on oneself chemical machinery Co., Ltd production S260 high
Imitate three-roller.
Preferably, mill base used is red or yellow or blue or black or gold or silver color in the step S5.
Preferably, in the step S5 mill base used be Merck chemical industry nano red mill base 8020.
The mechanism of action of the invention：
The mechanism of coating generation anion：
Anionic additive with natural minerals Tourmaline powder (tourmaline powder) be main raw material(s), while in proportion addition can
The group of the lanthanides cerium group rare-earth for increasing releasing effect mixes, and is added to from ordor removing nail polish glue to make it have permanently to discharge and bear
The function of ion, release anion reach 1500-50000/cm3.Product is discharged to from ordor removing nail polish glue priming coat and finish coat
The toxic, pernicious gas such as formaldehyde, ammonia, benzene, TVOC there is effect of dispelling, for the elimination factor of PARA FORMALDEHYDE PRILLS(91,95) greater than 90%, degerming rate is big
In 90%, thus assign from ordor removing nail polish glue self-purification function.Coating is gently dilute by addition Tourmaline powder and group of the lanthanides in formula
As filler material, Tourmaline powder and group of the lanthanides light rare earth are blended in ink coating soil after solidification, light using Tourmaline powder and group of the lanthanides
Rare earth cooperates long-acting efficient to discharge anion.
The present invention has the advantages that：
It is of the invention from ordor removing nail polish glue environment-friendly high-efficiency, do not influence color, flash of light, coloured coating can be divided；A wide selection of colours and designs；It produces
Raw anion is 1500-50000/cm through professional anionic textiles instrument KEC900 measurement anion average measurement value3；It reduces
Harmful substance, dispelling abnormal flavor, potent sterilizing, product to from ordor removing self-cleaning taste nail polish glue priming coat and finish coat release formaldehyde,
Ammonia, benzene, TVOC etc. be toxic, pernicious gas has and dispels effect, the test through Guangzhou Institute of Analysis, the elimination factor of PARA FORMALDEHYDE PRILLS(91,95)
Greater than 90%, degerming rate is greater than 90%.
Specific embodiment
Combined with specific embodiments below, the invention will be further described：
Embodiment 1：
A kind of preparation method from ordor removing nail polish glue, includes the following steps：
S1：By formula by 30 parts of urethane acrylates, 10 parts of modified epoxy acrylic esters and 30 parts of hydroxyethyl methacrylates
Ethyl ester is put into reaction vessel；It is risen the production FS30 twin shaft frequency control stirring of intelligent Equipment Limited using Dongguan benefit
Machine is stirred 15-30 minutes with 1000-1500 revs/min of revolving speed；
S2：Add 5 parts of nanoscale Tourmaline powders and 5 parts of group of the lanthanides cerium group rare-earths；It is risen intelligent equipment using Dongguan benefit
Co., Ltd produce FS30 twin shaft frequency-control blender, with 2000-3000 revs/min high-speed stirred 30-60 minutes；
S3：Add 2 parts of 1- hydroxycyclohexyl phenyl ketones, 2 parts of phenyl bis- (2,4,6- trimethylbenzoyls) oxidation
R974 fumed silica, 0.1 part of tego920 defoaming agent and the 0.1 part of tego450 levelling agent of phosphine, 1 part of Degussa；With 1000-
1500 revs/min of revolving speed stirring；
S4：Using Changzhou rely on oneself chemical machinery Co., Ltd production the efficient three-roller of S260 ground, be ground to flat
Equal partial size is not more than 5 microns；
Above method obtain from ordor removing nail polish glue first with hairbrush brushing on first piece surface；Solidified again using UV/LED lamp,
Solidification energy is 80mj/cm2, using from ordor removing nail polish glue and using common nail polish glue, each index compares test, as a result such as
Shown in following table：
Table 1：
Embodiment 2：
A kind of preparation method from ordor removing nail polish glue, includes the following steps：
S1：By formula by 40 parts of urethane acrylates, 20 parts of modified epoxy acrylic esters and 40 parts of hydroxyethyl methacrylates
Ethyl ester is put into reaction vessel；It is risen the production FS30 twin shaft frequency control stirring of intelligent Equipment Limited using Dongguan benefit
Machine is stirred 15-30 minutes with 1000-1500 revs/min of revolving speed；
S2：Add 15 parts of nanoscale Tourmaline powders and 10 parts of group of the lanthanides cerium group rare-earths；It is risen intelligent dress using Dongguan benefit
Standby Co., Ltd produces FS30 twin shaft frequency-control blender, with 2000-3000 revs/min high-speed stirred 30-60 minutes；
S3：Add 4 parts of 1- hydroxycyclohexyl phenyl ketones, 10 parts of phenyl bis- (2,4,6- trimethylbenzoyls) oxidation
R974 fumed silica, 1 part of tego920 defoaming agent and the 1 part of tego450 levelling agent of phosphine, 2 parts of Degussas；With 1000-1500
Rev/min revolving speed stirring；
S4：Using Changzhou rely on oneself chemical machinery Co., Ltd production the efficient three-roller of S260 ground, be ground to flat
Equal partial size is not more than 5 microns；
S5：Ground coating is added to the red nano mill base 8020 of 5 parts of Merck chemical industry, with 1000-1500 revs/min
Stirring 15-30 minutes.
Above method obtain from ordor removing nail polish glue first with hairbrush brushing on first piece surface；Solidified again using UV/LED lamp,
Solidification energy is 80mj/cm2, using from ordor removing nail polish glue and using common nail polish glue, each index compares test, as a result such as
Shown in following table：
Table 2：
Embodiment 3：
A kind of preparation method from ordor removing nail polish glue, includes the following steps：
S1：By formula by 35 parts of urethane acrylates, 15 parts of modified epoxy acrylic esters and 35 parts of hydroxyethyl methacrylates
Ethyl ester is put into reaction vessel；It is risen the production FS30 twin shaft frequency control stirring of intelligent Equipment Limited using Dongguan benefit
Machine is stirred 15-30 minutes with 1000-1500 revs/min of revolving speed；
S2：Add 10 parts of nanoscale Tourmaline powders and 8 parts of group of the lanthanides cerium group rare-earths；It is risen intelligent equipment using Dongguan benefit
Co., Ltd produce FS30 twin shaft frequency-control blender, with 2000-3000 revs/min high-speed stirred 30-60 minutes；
S3：Add 3 parts of 1- hydroxycyclohexyl phenyl ketones, 6 parts of phenyl bis- (2,4,6- trimethylbenzoyls) oxidation
R974 fumed silica, 0.5 part of tego920 defoaming agent and the 0.5 part of tego450 levelling agent of phosphine, 1.5 parts of Degussas；With
1000-1500 revs/min of revolving speed stirring；
S4：Using Changzhou rely on oneself chemical machinery Co., Ltd production the efficient three-roller of S260 ground, be ground to flat
Equal partial size is not more than 5 microns；
S5：3 parts of yellow mill bases are added in ground coating, with 1000-1500 revs/min stirring 15-30 minutes.
Above method obtain from ordor removing nail polish glue first with hairbrush brushing on first piece surface；Solidified again using UV/LED lamp,
Solidification energy is 80mj/cm2, and using from ordor removing nail polish glue and using common nail polish glue, each index compares test, as a result such as
Shown in following table：
Table 3：
Embodiment 4：
A kind of preparation method from ordor removing nail polish glue, includes the following steps：
S1：By formula by 30 parts of urethane acrylates, 10 parts of modified epoxy acrylic esters and 30 parts of hydroxyethyl methacrylates
Ethyl ester is put into reaction vessel；It is risen the production FS30 twin shaft frequency control stirring of intelligent Equipment Limited using Dongguan benefit
Machine is stirred 15-30 minutes with 1000-1500 revs/min of revolving speed；
S2：Add 4 parts of nanoscale Tourmaline powders and 5 parts of group of the lanthanides cerium group rare-earths；It is risen intelligent equipment using Dongguan benefit
Co., Ltd produce FS30 twin shaft frequency-control blender, with 2000-3000 revs/min high-speed stirred 30-60 minutes；
S3：Add 2 parts of 1- hydroxycyclohexyl phenyl ketones, 2 parts of phenyl bis- (2,4,6- trimethylbenzoyls) oxidation
R974 fumed silica, 0.1 part of tego920 defoaming agent and the 0.1 part of tego450 levelling agent of phosphine, 1 part of Degussa；With 1000-
1500 revs/min of revolving speed stirring；
S4：Using Changzhou rely on oneself chemical machinery Co., Ltd production the efficient three-roller of S260 ground, be ground to flat
Equal partial size is not more than 5 microns.
Above method obtain from ordor removing nail polish glue first with hairbrush brushing on first piece surface；Solidified again using UV/LED lamp,
Solidification energy is 80mj/cm2, and using from ordor removing nail polish glue and using common nail polish glue, each index compares test, as a result such as
Shown in following table：
Table 4：
Embodiment 5：
A kind of preparation method from ordor removing nail polish glue, includes the following steps：
S1：By formula by 30 parts of urethane acrylates, 10 parts of modified epoxy acrylic esters and 30 parts of hydroxyethyl methacrylates
Ethyl ester is put into reaction vessel；It is risen the production FS30 twin shaft frequency control stirring of intelligent Equipment Limited using Dongguan benefit
Machine is stirred 15-30 minutes with 1000-1500 revs/min of revolving speed；
S2：Add 20 parts of nanoscale Tourmaline powders and 5 parts of group of the lanthanides cerium group rare-earths；It is risen intelligent equipment using Dongguan benefit
Co., Ltd produce FS30 twin shaft frequency-control blender, with 2000-3000 revs/min high-speed stirred 30-60 minutes；
S3：Add 2 parts of 1- hydroxycyclohexyl phenyl ketones, 2 parts of phenyl bis- (2,4,6- trimethylbenzoyls) oxidation
R974 fumed silica, 0.1 part of tego920 defoaming agent and the 0.1 part of tego450 levelling agent of phosphine, 1 part of Degussa；With 1000-
1500 revs/min of revolving speed stirring；
S4：Using Changzhou rely on oneself chemical machinery Co., Ltd production the efficient three-roller of S260 ground, be ground to flat
Equal partial size is not more than 5 microns；
Above method obtain from ordor removing nail polish glue first with hairbrush brushing on first piece surface；Solidified again using UV/LED lamp,
Solidification energy is 80mj/cm2, and using from ordor removing nail polish glue and using common nail polish glue, each index compares test, as a result such as
Shown in following table：
Table 5：
By obtaining from table 4 and the data of table 5, when the parts by weight of Tourmaline powder are lower than 5 parts, various performances are substantially
Decline, and when the parts by weight of Tourmaline powder are higher than 15 parts, each performance does not change much yet, increase waste on foot, therefore, support
The parts by weight of Ma beautiful jade powder are 5-15 parts.
Embodiment 6：
A kind of preparation method from ordor removing nail polish glue, includes the following steps：
S1：By formula by 30 parts of urethane acrylates, 10 parts of modified epoxy acrylic esters and 30 parts of hydroxyethyl methacrylates
Ethyl ester is put into reaction vessel；It is risen the production FS30 twin shaft frequency control stirring of intelligent Equipment Limited using Dongguan benefit
Machine is stirred 15-30 minutes with 1000-1500 revs/min of revolving speed；
S2：Add 5 parts of nanoscale Tourmaline powders and 4 parts of group of the lanthanides cerium group rare-earths；It is risen intelligent equipment using Dongguan benefit
Co., Ltd produce FS30 twin shaft frequency-control blender, with 2000-3000 revs/min high-speed stirred 30-60 minutes；
S3：Add 2 parts of 1- hydroxycyclohexyl phenyl ketones, 2 parts of phenyl bis- (2,4,6- trimethylbenzoyls) oxidation
R974 fumed silica, 0.1 part of tego920 defoaming agent and the 0.1 part of tego450 levelling agent of phosphine, 1 part of Degussa；With 1000-
1500 revs/min of revolving speed stirring；
S4：Using Changzhou rely on oneself chemical machinery Co., Ltd production the efficient three-roller of S260 ground, be ground to flat
Equal partial size is not more than 5 microns.
Above method obtain from ordor removing nail polish glue first with hairbrush brushing on first piece surface；Solidified again using UV/LED lamp,
Solidification energy is 80mj/cm2, and using from ordor removing nail polish glue and using common nail polish glue, each index compares test, as a result such as
Shown in following table：
Table 6：
Embodiment 7:
A kind of preparation method from ordor removing nail polish glue, includes the following steps：
S1：By formula by 30 parts of urethane acrylates, 10 parts of modified epoxy acrylic esters and 30 parts of hydroxyethyl methacrylates
Ethyl ester is put into reaction vessel；It is risen the production FS30 twin shaft frequency control stirring of intelligent Equipment Limited using Dongguan benefit
Machine is stirred 15-30 minutes with 1000-1500 revs/min of revolving speed；
S2：Add 5 parts of nanoscale Tourmaline powders and 20 parts of group of the lanthanides cerium group rare-earths；It is risen intelligent equipment using Dongguan benefit
Co., Ltd produce FS30 twin shaft frequency-control blender, with 2000-3000 revs/min high-speed stirred 30-60 minutes；
S3：Add 2 parts of 1- hydroxycyclohexyl phenyl ketones, 2 parts of phenyl bis- (2,4,6- trimethylbenzoyls) oxidation
R974 fumed silica, 0.1 part of tego920 defoaming agent and the 0.1 part of tego450 levelling agent of phosphine, 1 part of Degussa；With 1000-
1500 revs/min of revolving speed stirring；
S4：Using Changzhou rely on oneself chemical machinery Co., Ltd production the efficient three-roller of S260 ground, be ground to flat
Equal partial size is not more than 5 microns；
Above method obtain from ordor removing nail polish glue first with hairbrush brushing on first piece surface；Solidified again using UV/LED lamp,
Solidification energy is 80mj/cm2, and using from ordor removing nail polish glue and using common nail polish glue, each index compares test, as a result such as
Shown in following table：
Table 7：
It is obtained from table 6 and the data of table 7, when the parts by weight of group of the lanthanides cerium group rare-earth are lower than 5 parts, various performances are substantially
Decline, and when the parts by weight of group of the lanthanides cerium group rare-earth are higher than 15 parts, each performance does not change much yet, increase waste on foot, because
This, the parts by weight of Tourmaline powder are 5-10 parts.
In the seven above embodiments, the color selection of mill base is limited, and the color of mill base can use red or yellow or indigo plant
Color or black or gold or silver color.
The examples of implementation of the above are only the preferred embodiments of the invention, and implementation model of the invention is not limited with this
It encloses, therefore all shapes according to the present invention, changes made by principle, should all be included within the scope of protection of the present invention.
Claims (9)
1. a kind of from ordor removing nail polish glue, which is characterized in that it is made of the raw material below according to parts by weight, and specific formula is：
2. one kind is as described in the appended claim 1 from the preparation method of ordor removing nail polish glue, which is characterized in that include the following steps：
S1：By formula by 30-40 parts of urethane acrylates, 10-20 parts of modified epoxy acrylic esters and 30-40 parts of metering systems
Sour hydroxyl ethyl ester is put into reaction vessel；It is stirred 15-30 minutes with 1000-1500 revs/min of revolving speed；
S2：Add 5-15 parts of Tourmaline powders and 5-10 parts of group of the lanthanides light rare earths；With 2000-3000 revs/min of high-speed stirred 30-60
Minute；
S3：Add 2-4 parts of 1- hydroxycyclohexyl phenyl ketones, 2-10 parts of phenyl bis- (2,4,6- trimethylbenzoyls) oxidation
Phosphine, 1-2 part fumed silica, 0.1-1 parts of defoaming agents and 0.1-1 parts of levelling agents；It is stirred with 1000-1500 revs/min of revolving speed
It mixes；
S4：Average grain diameter is ground to no more than 5 microns using three-roll grinder；
S5：0-5 parts of mill bases are added in ground coating, with 1000-1500 revs/min stirring 15-30 minutes.
3. a kind of preparation method from ordor removing nail polish glue according to claim 2, it is characterised in that：The defoaming agent is
Tego920 defoaming agent, the levelling agent are tego450 levelling agent, and the fumed silica is the R974 of Degussa.
4. a kind of preparation method from ordor removing nail polish glue according to claim 2, it is characterised in that：The group of the lanthanides light rare earth
For group of the lanthanides cerium group rare-earth.
5. a kind of preparation method from ordor removing nail polish glue according to claim 2, it is characterised in that：The Tourmaline powder
Particle size is nanoscale.
6. a kind of preparation method from ordor removing nail polish glue according to claim 2, it is characterised in that：The step S1 and S2
The blender of middle use is that Dongguan benefit is risen the FS30 twin shaft frequency-control blender of intelligent Equipment Limited production.
7. a kind of preparation method from ordor removing nail polish glue according to claim 2, it is characterised in that：It is adopted in the step S4
Grinder be Changzhou rely on oneself chemical machinery Co., Ltd production the efficient three-roller of S260.
8. a kind of preparation method from ordor removing nail polish glue according to claim 2, it is characterised in that：The mill base is red
Or yellow or blue or black or gold or silver color.
9. a kind of preparation method from ordor removing nail polish glue according to claim 2, it is characterised in that：The mill base is Merck
The nano red mill base 8020 of chemical industry.
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| CN201810806291.1A CN108852866A (en) | 2018-07-20 | 2018-07-20 | One kind is from ordor removing nail polish glue and preparation method thereof |
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| CN201810806291.1A CN108852866A (en) | 2018-07-20 | 2018-07-20 | One kind is from ordor removing nail polish glue and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111875755A (en) * | 2020-07-21 | 2020-11-03 | 珠海展辰新材料股份有限公司 | Primer resin, preparation method thereof and nail polish primer |
| CN114903816A (en) * | 2022-06-06 | 2022-08-16 | 东莞市百拓实业有限公司 | Nail polish gel and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105496814A (en) * | 2015-12-02 | 2016-04-20 | 杭州莱凡网络科技有限公司 | 4D nail polish gel and application method thereof |
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| CN105496814A (en) * | 2015-12-02 | 2016-04-20 | 杭州莱凡网络科技有限公司 | 4D nail polish gel and application method thereof |
| CN105902413A (en) * | 2016-05-12 | 2016-08-31 | 天津市莱思雅化妆品有限公司 | One-step strippable nail polish gel |
| CN106634556A (en) * | 2017-01-17 | 2017-05-10 | 中山市鑫峰光固化材料有限公司 | Novel ultraviolet-curable coating and preparation and use methods thereof |
| CN107582429A (en) * | 2017-09-13 | 2018-01-16 | 上海指谱智能科技有限公司 | A kind of tearable nail polish glue of one-step shaping and preparation method thereof |
| CN107868543A (en) * | 2017-12-11 | 2018-04-03 | 浙江爱丽莎环保科技股份有限公司 | A kind of acrylic acid aqueous medium of releasable negative oxygen ion and preparation method thereof |
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| CN111875755A (en) * | 2020-07-21 | 2020-11-03 | 珠海展辰新材料股份有限公司 | Primer resin, preparation method thereof and nail polish primer |
| CN111875755B (en) * | 2020-07-21 | 2023-03-31 | 珠海展辰新材料股份有限公司 | Primer resin, preparation method thereof and nail polish primer |
| CN114903816A (en) * | 2022-06-06 | 2022-08-16 | 东莞市百拓实业有限公司 | Nail polish gel and preparation method thereof |
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