CN111110588A - Peelable base glue and preparation method thereof - Google Patents
Peelable base glue and preparation method thereof Download PDFInfo
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- CN111110588A CN111110588A CN202010047399.4A CN202010047399A CN111110588A CN 111110588 A CN111110588 A CN 111110588A CN 202010047399 A CN202010047399 A CN 202010047399A CN 111110588 A CN111110588 A CN 111110588A
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- initiator
- primer
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- peelable
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q3/00—Manicure or pedicure preparations
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Abstract
The invention relates to the technical field of primer preparation and application, and discloses a peelable primer and a preparation method thereof, wherein the peelable primer comprises the following steps: 1) 2), 3) and 4). The peelable primer and the preparation method thereof are characterized in that 184 initiator, TOP initiator, HP6220 resin, HEMA monomer solvent and BYK333 flatting agent are selected and prepared according to the preparation processes of the steps 1) to 4) by heating, stirring, placing, filtering and other methods, the peelable primer is obtained after the preparation is finished, meanwhile, the peelable primer has no obvious peculiar smell, the drying time is 30-60 seconds, and the peelable primer can be directly peeled by hand, so that the effects of environmental protection, convenience for quick drying and peeling by hand are achieved, the problem that the primer often has pungent tastes such as peculiar smell and the like in the using process is solved, the peeling is troublesome after the use, and the drying time is relatively general when the peelable primer is used is solved.
Description
Technical Field
The invention relates to the technical field of primer preparation and application, in particular to a peelable primer and a preparation method thereof.
Background
The nail polish is a cosmetic for decorating and improving the beauty of nails, and can form a layer of friction-resistant film on the surface of the nails to play a role in protecting and beautifying the nails, the components of the common nail polish generally comprise two types, one type is solid components, mainly pigments, glittering substances and the like, the other type is liquid solvent components, mainly acetone, ethyl acetate, phthalate, formaldehyde and the like are used, the pigments are various, including natural and artificial ones, the most widely used artificial pigments are artificial pigments, but many artificial pigments are toxic, and therefore the artificial pigments are possibly harmful to human bodies.
The application of nail polish is quite wide at present, a layer of primer can be coated on a nail before the nail polish is coated, so that the nail polish is convenient to clean and cannot directly contact the nail, and the nail polish can be protected.
Disclosure of Invention
Technical problem to be solved
Aiming at the defects of the prior art, the invention provides the peelable primer and the preparation method thereof, which have the advantages of environmental protection, convenience for quick drying, capability of being peeled by hand and the like, and solve the problems that the primer often has pungent taste such as peculiar smell and the like in the use process, the primer needs to be peeled off after use, and the drying time is relatively common in use.
(II) technical scheme
In order to realize the purposes of environmental protection, convenient quick drying and hand peeling, the invention provides the following technical scheme: a peelable primer comprises the following raw materials: the initiator comprises a first initiator, a second initiator, resin, a monomer solvent and a flatting agent.
A preparation method of a peelable primer comprises the following steps:
1) taking out the first initiator, the second initiator, the resin, the monomer solvent and the flatting agent for later use, wherein the storage temperature is indoor temperature, and the temperature interval is 20-25 ℃;
2) preparing a reaction container, placing a first initiator, a second initiator and a monomer solvent in the reaction container, heating and stirring after the placing is finished, wherein the temperature interval is 25-35 ℃, the initial speed of the rotating stirring is 80rpm, the highest rotating speed is 400rpm, the duration of the rotating is 30min, the rotating speed is adjusted from slow to fast at a constant speed in the rotating process, a primer mixture A is obtained after the heating and stirring are finished, and the primer mixture A is taken out and placed for later use;
3) placing the primer mixture A and resin into a reaction container at the same time, heating and stirring after the primer mixture A and the resin are placed into the reaction container, wherein the temperature interval is 28-32 ℃, the initial speed of rotating stirring is 80rpm, the highest rotating speed is 600rpm, the duration of rotating is 30min, the rotating speed is adjusted from slow to fast at a constant speed in the rotating process, and after the heating and stirring are finished, a primer mixture B is obtained, and the primer mixture A is taken out and placed for later use;
4) and simultaneously placing the primer mixture B and the leveling agent in a reaction container, heating and stirring after the placing is finished, wherein the temperature range is 25-35 ℃, the rotating stirring speed is 100-600 rpm, the rotating duration time is 10min, heating and stirring are finished to obtain a primer mixture C, at the moment, the primer mixture C is taken out and placed in a room temperature environment, the temperature range is 20-25 ℃, and meanwhile, the primer mixture C is the required strippable primer.
Preferably, the raw materials in the step 1) are sequentially as follows: the first initiator is 184 initiator, the second initiator is TOP initiator, the resin is HP6220 resin, the monomer solvent is HEMA monomer solvent, and the leveling agent is BYK333 leveling agent.
Preferably, the first initiator, the second initiator and the monomer solvent in the step 2) are respectively in the following ratio: 4% of a first initiator, 8% of a second initiator and 30% of a monomer solvent.
Preferably, the proportion content of the resin in the step 3) is 58%, and the proportion content of the leveling agent in the step 4) is 0.3%.
Preferably, the reaction vessel in the step 2), the step 3) and the step 4) is a stirring vessel with a cylindrical shape, and the vessel is provided with a temperature raising structure and a stirring structure.
(III) advantageous effects
Compared with the prior art, the invention provides a peelable base glue and a preparation method thereof, and the peelable base glue has the following beneficial effects:
1. the peelable primer and the preparation method thereof are characterized in that 184 initiator, TOP initiator, HP6220 resin, HEMA monomer solvent and BYK333 flatting agent are selected and prepared by heating, stirring, placing, filtering and other methods according to the preparation processes in the steps 1) to 4), the peelable primer is obtained after the preparation is finished, meanwhile, the peelable primer has no obvious peculiar smell, the drying time is 30-60 seconds, and the peelable primer can be directly peeled by hand, so that the effects of environmental protection, convenience for quick drying and peeling by hand are achieved, the peelable primer is simplified in material, the preparation process is simple, the devices used in preparation are reaction containers and filtering devices, and the peelable primer and the preparation method thereof are convenient to realize and have good practicability.
2. The peelable base glue and the preparation method thereof can be stored at the normal temperature of 20-25 ℃, the heating temperature and the stirring speed required in the preparation process are very common, therefore, only common equipment on the market is needed to be selected, the conditions that the preparation environment is complicated and the cost of the obtained peelable primer is high due to the troublesome preparation process and the need of expensive preparation equipment in the peelable primer and the preparation method thereof can be effectively avoided, the peelable bottom glue can increase the firmness of the adhesive when in use, and the duration time can be kept for one month, thereby effectively enhancing the practicability of the peelable bottom glue, thereby effectually solved the primer can often have irritative taste such as peculiar smell in the use, and it is very troublesome when need peeling off after finishing using simultaneously, and drying time is also comparatively general problem during the use.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
A peelable primer comprises the following raw materials: the initiator comprises a first initiator, a second initiator, resin, a monomer solvent and a flatting agent.
A preparation method of a peelable primer comprises the following steps:
1) taking out the first initiator, the second initiator, the resin, the monomer solvent and the flatting agent for later use, wherein the storage temperature is indoor temperature, the temperature interval is 20-25 ℃, and the steps of 1) sequentially comprise the following raw materials: the first initiator is 184 initiator, the second initiator is TOP initiator, the resin is HP6220 resin, the monomer solvent is HEMA monomer solvent, and the leveling agent is BYK333 leveling agent;
2) preparing a reaction container, placing a first initiator, a second initiator and a monomer solvent in the reaction container, heating and stirring after the placing is finished, wherein the temperature interval is 25-35 ℃, the initial speed of the rotating stirring is 80rpm, the highest rotating speed is 400rpm, the duration of the rotating is 30min, the rotating speed is adjusted from slow to fast at a constant speed in the rotating process, a primer mixture A is obtained after the heating and stirring are finished, the primer mixture A is taken out and placed for standby, and the proportion content of the first initiator, the second initiator and the monomer solvent in the step 2) is respectively as follows: 4% of a first initiator, 8% of a second initiator and 30% of a monomer solvent;
3) simultaneously placing the primer mixture A and resin into a reaction container, heating and stirring after the primer mixture A and the resin are placed into the reaction container, wherein the temperature range is 28-32 ℃, the initial speed of the rotating stirring is 80rpm, the highest rotating speed is 600rpm, the duration of the rotating is 30min, the rotating speed is adjusted from slow to fast at a constant speed in the rotating process, the primer mixture B is obtained after the heating and stirring are completed, the primer mixture A is taken out and placed for later use, and meanwhile, the proportion content of the resin in the step 3) is 58%;
4) simultaneously placing the base glue mixture B and the leveling agent into a reaction container, heating and stirring after the placing, wherein the temperature range is 25-35 ℃, the rotating stirring speed is 100-600 rpm, the rotating duration time is 10min, taking out the base glue mixture after the heating and stirring are finished, placing the base glue mixture into a filtering device for filtering, obtaining a base glue mixture C after the filtering is finished, taking out the base glue mixture C and placing the base glue mixture C in a room temperature environment, wherein the temperature range is 20-25 ℃, simultaneously, the base glue mixture C is the required strippable base glue, simultaneously, the proportioning content of the leveling agent in the step 4) is 0.3%, the reaction container in the steps 2), 3) and 4) is a stirring container with a cylindrical shape, the container is provided with a heating structure and a stirring structure, and the color of the strippable base glue obtained in the steps is more suitable for fingernails, is not easy to fall off and is very effective in peeling.
The primer is more adhesive to the nail and is not easy to fall off, and the primer is firstly smeared when the nail is beautiful, and the seal layer is used on the uppermost surface, so that the nail is bright as new, and the nail is more wear-resistant.
The invention has the beneficial effects that: the peelable primer and the preparation method thereof are characterized in that the peelable primer is prepared by selecting 184 initiator, TOP initiator, HP6220 resin, HEMA monomer solvent and BYK333 flatting agent and heating, stirring, placing, filtering and the like according to the preparation processes in the steps 1) to 4), the peelable primer is obtained after the preparation is finished, meanwhile, the peelable primer has no obvious peculiar smell, the drying time is 30-60 seconds, and the peelable primer can be directly peeled by hand, so that the effects of environmental protection, convenience for quick drying and peeling by hand are achieved, the peelable primer is simplified in material consumption, the preparation process is simple, the devices used in the preparation are reaction containers and filtering devices, the peelable primer and the preparation method thereof are convenient to realize and have good practicability, and the peelable primer and the preparation method thereof are prepared by storing the peelable primer at the normal temperature of 20-25 ℃, the required temperature rise and stirring speed in the preparation process are very common, so that the conditions that the preparation environment is complex and the cost of the obtained peelable primer is high due to the fact that the preparation process is very troublesome and expensive preparation equipment is needed can be effectively avoided, the situation that the peelable primer and the preparation method thereof are complex in preparation environment and expensive in manufacturing cost due to the fact that the preparation process is very troublesome and the preparation equipment is needed, the firmness of the adhesive can be improved when the peelable primer is used, the lasting time of the peelable primer can be kept for a long time, the practicability of the peelable primer can be effectively enhanced, and the problems that the primer can often have pungent tastes such as peculiar smell and the like in the use process, the primer is very troublesome to peel after being used and the drying time is relatively common in use are solved effectively.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (6)
1. The peelable base glue is characterized by comprising the following raw materials: the initiator comprises a first initiator, a second initiator, resin, a monomer solvent and a flatting agent.
2. The preparation method of the peelable primer is characterized by comprising the following steps:
1) taking out the first initiator, the second initiator, the resin, the monomer solvent and the flatting agent for later use, wherein the storage temperature is indoor temperature, and the temperature interval is 20-25 ℃;
2) preparing a reaction container, placing a first initiator, a second initiator and a monomer solvent in the reaction container, heating and stirring after the placing is finished, wherein the temperature interval is 25-35 ℃, the initial speed of the rotating stirring is 80rpm, the highest rotating speed is 400rpm, the duration of the rotating is 30min, the rotating speed is adjusted from slow to fast at a constant speed in the rotating process, a primer mixture A is obtained after the heating and stirring are finished, and the primer mixture A is taken out and placed for later use;
3) placing the primer mixture A and resin into a reaction container at the same time, heating and stirring after the primer mixture A and the resin are placed into the reaction container, wherein the temperature interval is 28-32 ℃, the initial speed of rotating stirring is 80rpm, the highest rotating speed is 600rpm, the duration of rotating is 30min, the rotating speed is adjusted from slow to fast at a constant speed in the rotating process, and after the heating and stirring are finished, a primer mixture B is obtained, and the primer mixture A is taken out and placed for later use;
4) and simultaneously placing the primer mixture B and the leveling agent in a reaction container, heating and stirring after the placing, wherein the temperature range is 25-35 ℃, the rotating stirring speed is 100-600 rpm, the rotating duration time is 10min, taking out the primer mixture B after the heating and stirring are finished, placing the primer mixture B in a filtering device for filtering, obtaining a primer mixture C after the filtering is finished, taking out the primer mixture C and placing the primer mixture C in a room-temperature environment, wherein the temperature range is 20-25 ℃, and meanwhile, the primer mixture C is the required strippable primer.
3. The method for preparing a peelable primer according to claim 2, wherein: the raw materials in the step 1) are sequentially as follows: the first initiator is 184 initiator, the second initiator is TOP initiator, the resin is HP6220 resin, the monomer solvent is HEMA monomer solvent, and the leveling agent is BYK333 leveling agent.
4. The method for preparing a peelable primer according to claim 2, wherein: the proportioning contents of the first initiator, the second initiator and the monomer solvent in the step 2) are respectively as follows: 4% of a first initiator, 8% of a second initiator and 30% of a monomer solvent.
5. The method for preparing a peelable primer according to claim 2, wherein: the proportion content of the resin in the step 3) is 58%, and the proportion content of the flatting agent in the step 4) is 0.3%.
6. The method for preparing a peelable primer according to claim 2, wherein: the reaction container in the step 2), the step 3) and the step 4) is a stirring container with a cylindrical shape, and the container is provided with a heating structure and a stirring structure.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010047399.4A CN111110588A (en) | 2020-01-16 | 2020-01-16 | Peelable base glue and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010047399.4A CN111110588A (en) | 2020-01-16 | 2020-01-16 | Peelable base glue and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN111110588A true CN111110588A (en) | 2020-05-08 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202010047399.4A Pending CN111110588A (en) | 2020-01-16 | 2020-01-16 | Peelable base glue and preparation method thereof |
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| CN (1) | CN111110588A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105434189A (en) * | 2016-01-20 | 2016-03-30 | 上海应用技术学院 | Strippable nail polish gel and preparation method thereof |
| CN105902413A (en) * | 2016-05-12 | 2016-08-31 | 天津市莱思雅化妆品有限公司 | One-step strippable nail polish gel |
| CN107582429A (en) * | 2017-09-13 | 2018-01-16 | 上海指谱智能科技有限公司 | A kind of tearable nail polish glue of one-step shaping and preparation method thereof |
| US20180125774A1 (en) * | 2016-11-07 | 2018-05-10 | Lijuan Zhen | Method and Composition for Visible Light Dryable Nail Coatings |
-
2020
- 2020-01-16 CN CN202010047399.4A patent/CN111110588A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105434189A (en) * | 2016-01-20 | 2016-03-30 | 上海应用技术学院 | Strippable nail polish gel and preparation method thereof |
| CN105902413A (en) * | 2016-05-12 | 2016-08-31 | 天津市莱思雅化妆品有限公司 | One-step strippable nail polish gel |
| US20180125774A1 (en) * | 2016-11-07 | 2018-05-10 | Lijuan Zhen | Method and Composition for Visible Light Dryable Nail Coatings |
| CN107582429A (en) * | 2017-09-13 | 2018-01-16 | 上海指谱智能科技有限公司 | A kind of tearable nail polish glue of one-step shaping and preparation method thereof |
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Application publication date: 20200508 |